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CN107747236A - 一种改善猪鬃柔软性用染色剂 - Google Patents

一种改善猪鬃柔软性用染色剂 Download PDF

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CN107747236A
CN107747236A CN201710850499.9A CN201710850499A CN107747236A CN 107747236 A CN107747236 A CN 107747236A CN 201710850499 A CN201710850499 A CN 201710850499A CN 107747236 A CN107747236 A CN 107747236A
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parts
bristles
flexibility
coloring agent
improve
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宣永昌
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Yongchang Wuwei County Anhui Province Bristle Brush Manufacturing Co Ltd
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Yongchang Wuwei County Anhui Province Bristle Brush Manufacturing Co Ltd
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Abstract

本发明公开了一种改善猪鬃柔软性用染色剂，其原料包括：天然染料、喹啉黄、稀土、纳米二氧化硅、硫酸铝铵、硫酸钠、氢氧化钠、山梨酸钾、壳聚糖、渗透剂JFC、聚乙烯醇、丙二醇、烷基糖苷、山梨醇酐三油酸酯、二萘基甲烷二磺酸钠、分散剂WA、胆矾、癸二酸二丁酯、环氧大豆油、环氧糠油酸丁酯、苯甲酸乙酯、软化剂YS、软化剂ES、去离子水。本发明提出的一种改善猪鬃柔软性用染色剂，污染小，染色效率高，上色深且均匀，染色后猪鬃具有良好的耐光性和耐候性，不易褪色，色牢度好，同时提高猪鬃弹性和柔软性，有效提高猪鬃制品的性能，延长猪鬃制品的使用寿命。

Description

一种改善猪鬃柔软性用染色剂
技术领域
本发明涉及染色剂技术领域，尤其涉及一种改善猪鬃柔软性用染色剂。
背景技术
猪鬃是指猪颈部和背部生长的5厘米以上的刚毛，常被用于制备日用刷、油漆刷、机器刷等。猪鬃的颜色主要有黑色、白色、黄色和花色。天然黄色猪鬃产量少，无法满足实际生产需要，而目前猪鬃所用染色剂存在污染大，染色效率低，上色浅且不均匀，染色后猪鬃耐光性和耐候性差，易褪色，且不能有效提高猪鬃弹性和柔软性，影响猪鬃制品的性能，降低猪鬃制品的使用寿命。
发明内容
基于背景技术存在的技术问题，本发明提出了一种改善猪鬃柔软性用染色剂，污染小，染色效率高，上色深且均匀，染色后猪鬃具有良好的耐光性和耐候性，不易褪色，色牢度好，同时提高猪鬃弹性和柔软性，有效提高猪鬃制品的性能，延长猪鬃制品的使用寿命。
本发明提出的一种改善猪鬃柔软性用染色剂，其原料按重量份包括：天然染料10-25份、喹啉黄1-3份、稀土0.4-1份、纳米二氧化硅0.1-0.4份、硫酸铝铵0.3-0.8份、硫酸钠0.2-0.5份、氢氧化钠0.4-0.7份、山梨酸钾0.2-0.5份、壳聚糖0.5-2份、渗透剂JFC 0.5-1份、聚乙烯醇2-5份、丙二醇2-4份、烷基糖苷0.8-1.5份、山梨醇酐三油酸酯0.2-0.6份、二萘基甲烷二磺酸钠0.2-0.6份、分散剂WA 0.3-0.7份、胆矾0.2-0.8份、癸二酸二丁酯0.1-0.4份、环氧大豆油0.8-1.5份、环氧糠油酸丁酯0.4-0.8份、苯甲酸乙酯0.2-0.6份、软化剂YS0.15-0.4份、软化剂ES 0.2-0.5份、去离子水70-120份。
具体实施方式中，天然染料的重量份还可以为12、14、16、18、20、23份，喹啉黄的重量份还可以为1.4、1.8、2、2.2、2.5、2.8份，稀土的重量份还可以为0.5、0.6、0.7、0.8、0.9份，纳米二氧化硅的重量份还可以为0.15、0.2、0.25、0.3、0.35份，硫酸铝铵的重量份还可以为0.4、0.5、0.55、0.6、0.7份，硫酸钠的重量份还可以为0.25、0.3、0.35、0.4、0.45份，氢氧化钠的重量份还可以为0.45、0.5、0.55、0.6、0.65份，山梨酸钾的重量份还可以为0.25、0.3、0.35、0.4、0.45份，壳聚糖的重量份还可以为0.8、1、1.2、1.4、1.6、1.8份，渗透剂JFC的重量份还可以为0.6、0.65、0.7、0.8、0.9份，聚乙烯醇的重量份还可以为2.5、3、3.5、4、4.5份，丙二醇的重量份还可以为2.4、2.8、3、3.2、3.5、3.8份，烷基糖苷的重量份还可以为1、1.1、1.2、1.3、1.4份，山梨醇酐三油酸酯的重量份还可以为0.3、0.35、0.4、0.45、0.5份，二萘基甲烷二磺酸钠的重量份还可以为0.25、0.3、0.4、0.45、0.5份，分散剂WA的重量份还可以为0.35、0.4、0.45、0.5、0.6份，胆矾的重量份还可以为0.3、0.4、0.5、0.6、0.7份，癸二酸二丁酯的重量份还可以为0.15、0.2、0.25、0.3、0.35份，环氧大豆油的重量份还可以为0.9、1、1.1、1.2、1.3、1.4份，环氧糠油酸丁酯的重量份还可以为0.45、0.5、0.55、0.6、0.7份，苯甲酸乙酯的重量份还可以为0.25、0.3、0.35、0.4、0.5份，软化剂YS的重量份还可以为0.2、0.25、0.3、0.35份，软化剂ES的重量份还可以为0.25、0.3、0.35、0.4、0.45份，去离子水的重量份还可以为75、80、85、90、95、100、110份。
优选地，天然染料按以下工艺进行制备：
S1、将香蕉皮、芒果皮和黄栀子粉碎，混合，加入溶剂A提取2-4次，合并提取液，浓缩，得到物料B；
S2、将大黄、荩草和玉米清洗，晒干，粉碎，然后加入溶剂C提取2-4次，合并提取液，浓缩，得到物料D；
S3、将物料B、物料D和姜黄素混合，得到天然染料。
优选地，S1中，采用微波提取法进行提取，其中，微波功率为300-350W，微波时间为10-15min。
优选地，S1中，溶剂A为体积分数为72-80％的乙醇水溶液。
优选地，S1中，提取时料液比为1:25-35。
优选地，S1中，提取时料液比为1:25-35为每次提取时的料液比。
优选地，S2中，采用回流提取法进行提取，且提取温度为82-90℃，提取时间为30-40min。
优选地，S2中，提取时料液比为1:22-25。
优选地，S2中，提取时料液比为1:22-25为每次提取时的料液比。
优选地，S2中，溶剂C为体积分数为55-65％的乙醇水溶液。
优选地，S3中，物料B、物料D和姜黄素之间的重量比为2-5:5-10:1-1.5。
本发明制品采用常规制备工艺制得。
本发明中提出的一种改善猪鬃柔软性用染色剂中，天然染料通过优化制备工艺，有效提取香蕉皮、芒果皮、黄栀子和大黄、荩草、玉米中的色素，与姜黄素混合，得到的天然染料绿色环保，生物降解性好，具有良好的抗菌、防紫外线等功能，加入本发明制品中，染色效果明显，色彩鲜艳，与喹啉黄、稀土、纳米二氧化硅、硫酸铝铵、硫酸钠、氢氧化钠、山梨酸钾、壳聚糖、渗透剂JFC、聚乙烯醇、丙二醇、烷基糖苷、山梨醇酐三油酸酯、二萘基甲烷二磺酸钠、分散剂WA、胆矾、癸二酸二丁酯、环氧大豆油、环氧糠油酸丁酯、苯甲酸乙酯、软化剂YS、软化剂ES、去离子水配合，污染小，各物料相容性好，分散均匀，且具有良好的协同作用，同时综合了天然染料与人工合成染料喹啉黄的优点，对猪鬃具有良好的润湿及疏通毛孔等作用，有效改善猪鬃表面活性，着色效果好，渗透效果明显，染色深，固色率高且上色均匀，色牢度好，不易褪色，同时有效还改善猪鬃耐磨性、耐光性、耐候性、耐腐蚀性和顺滑性，且有效提高猪鬃柔软性、弹性等性能，综合提高了猪鬃质量，有效延长猪鬃制品的使用寿命。
具体实施方式
下面，通过具体实施例对本发明的技术方案进行详细说明。
实施例1
本发明提出的一种改善猪鬃柔软性用染色剂，其原料按重量份包括：天然染料10份、喹啉黄3份、稀土0.4份、纳米二氧化硅0.4份、硫酸铝铵0.3份、硫酸钠0.5份、氢氧化钠0.4份、山梨酸钾0.5份、壳聚糖0.5份、渗透剂JFC1份、聚乙烯醇2份、丙二醇4份、烷基糖苷0.8份、山梨醇酐三油酸酯0.6份、二萘基甲烷二磺酸钠0.2份、分散剂WA 0.7份、胆矾0.2份、癸二酸二丁酯0.4份、环氧大豆油0.8份、环氧糠油酸丁酯0.8份、苯甲酸乙酯0.2份、软化剂YS 0.4份、软化剂ES 0.2份、去离子水70份。
实施例2
本发明提出的一种改善猪鬃柔软性用染色剂，其原料按重量份包括：天然染料25份、喹啉黄1份、稀土1份、纳米二氧化硅0.1份、硫酸铝铵0.8份、硫酸钠0.2份、氢氧化钠0.7份、山梨酸钾0.2份、壳聚糖2份、渗透剂JFC 0.5份、聚乙烯醇5份、丙二醇2份、烷基糖苷1.5份、山梨醇酐三油酸酯0.2份、二萘基甲烷二磺酸钠0.6份、分散剂WA 0.3份、胆矾0.8份、癸二酸二丁酯0.1份、环氧大豆油1.5份、环氧糠油酸丁酯0.4份、苯甲酸乙酯0.6份、软化剂YS0.15份、软化剂ES 0.5份、去离子水70份。
其中，天然染料按以下工艺进行制备：
S1、将香蕉皮、芒果皮和黄栀子粉碎，混合，加入溶剂A提取2次，合并提取液，浓缩，得到物料B；
S2、将大黄、荩草和玉米清洗，晒干，粉碎，然后加入溶剂C提取4次，合并提取液，浓缩，得到物料D；
S3、将物料B、物料D和姜黄素混合，得到天然染料。
实施例3
本发明提出的一种改善猪鬃柔软性用染色剂，其原料按重量份包括：天然染料18份、喹啉黄2份、稀土0.65份、纳米二氧化硅0.25份、硫酸铝铵0.52份、硫酸钠0.35份、氢氧化钠0.55份、山梨酸钾0.35份、壳聚糖1.2份、渗透剂JFC 0.8份、聚乙烯醇3.5份、丙二醇3份、烷基糖苷1.1份、山梨醇酐三油酸酯0.4份、二萘基甲烷二磺酸钠0.4份、分散剂WA 0.5份、胆矾0.45份、癸二酸二丁酯0.2份、环氧大豆油1.1份、环氧糠油酸丁酯0.6份、苯甲酸乙酯0.4份、软化剂YS 0.22份、软化剂ES 0.35份、去离子水90份。
其中，天然染料按以下工艺进行制备：
S1、将香蕉皮、芒果皮和黄栀子粉碎，混合，加入体积分数为78％的乙醇水溶液，采用微波提取法提取3次，合并提取液，浓缩，得到物料B；其中，微波提取过程汇总，微波功率为320W，微波时间为12min；提取时料液比为1:30；
S2、将大黄、荩草和玉米清洗，晒干，粉碎，然后加入体积分数为60％的乙醇水溶液，回流提取法提取3次，合并提取液，浓缩，得到物料D；其中，提取时料液比为1:24；
S3、将物料B、物料D和姜黄素以重量比为3:8:1.2进行混合，得到天然染料。
实施例4
本发明提出的一种改善猪鬃柔软性用染色剂，其原料按重量份包括：天然染料14份、喹啉黄1.5份、稀土0.5份、纳米二氧化硅0.25份、硫酸铝铵0.45份、硫酸钠0.35份、氢氧化钠0.5份、山梨酸钾0.25份、壳聚糖0.8份、渗透剂JFC 0.65份、聚乙烯醇2.5份、丙二醇2.5份、烷基糖苷1份、山梨醇酐三油酸酯0.3份、二萘基甲烷二磺酸钠0.3份、分散剂WA 0.35份、胆矾0.3份、癸二酸二丁酯0.2份、环氧大豆油1份、环氧糠油酸丁酯0.55份、苯甲酸乙酯0.25份、软化剂YS 0.2份、软化剂ES 0.25份、去离子水85份。
其中，天然染料按以下工艺进行制备：
S1、将香蕉皮、芒果皮和黄栀子粉碎，混合，加入体积分数为72％的乙醇水溶液，采用微波提取法提取4次，合并提取液，浓缩，得到物料B；其中，微波提取过程汇总，微波功率为300W，微波时间为15min；提取时料液比为1:25；
S2、将大黄、荩草和玉米清洗，晒干，粉碎，然后加入体积分数为55％的乙醇水溶液，回流提取法提取2次，合并提取液，浓缩，得到物料D；其中，提取时料液比为1:22；
S3、将物料B、物料D和姜黄素以重量比为2:5:1进行混合，得到天然染料。
实施例5
本发明提出的一种改善猪鬃柔软性用染色剂，其原料按重量份包括：天然染料22.5份、喹啉黄2.5份、稀土0.85份、纳米二氧化硅0.35份、硫酸铝铵0.7份、硫酸钠0.4份、氢氧化钠0.55份、山梨酸钾0.4份、壳聚糖1.6份、渗透剂JFC 0.8份、聚乙烯醇4.2份、丙二醇3.5份、烷基糖苷1.2份、山梨醇酐三油酸酯0.5份、二萘基甲烷二磺酸钠0.5份、分散剂WA0.6份、胆矾0.7份、癸二酸二丁酯0.3份、环氧大豆油1.25份、环氧糠油酸丁酯0.65份、苯甲酸乙酯0.5份、软化剂YS 0.3份、软化剂ES 0.45份、去离子水110份。
其中，天然染料按以下工艺进行制备：
S1、将香蕉皮、芒果皮和黄栀子粉碎，混合，加入体积分数为80％的乙醇水溶液，采用微波提取法提取3次，合并提取液，浓缩，得到物料B；其中，微波提取过程汇总，微波功率为350W，微波时间为10min；提取时料液比为1:35；
S2、将大黄、荩草和玉米清洗，晒干，粉碎，然后加入体积分数为65％的乙醇水溶液，回流提取法提取2次，合并提取液，浓缩，得到物料D；其中，提取时料液比为1:25；
S3、将物料B、物料D和姜黄素以重量比为5:10:1.5进行混合，得到天然染料。
以上所述，仅为本发明较佳的具体实施方式，但本发明的保护范围并不局限于此，任何熟悉本技术领域的技术人员在本发明揭露的技术范围内，根据本发明的技术方案及其发明构思加以等同替换或改变，都应涵盖在本发明的保护范围之内。

Claims (9)

1.一种改善猪鬃柔软性用染色剂，其特征在于，其原料按重量份包括：天然染料10-25份、喹啉黄1-3份、稀土0.4-1份、纳米二氧化硅0.1-0.4份、硫酸铝铵0.3-0.8份、硫酸钠0.2-0.5份、氢氧化钠0.4-0.7份、山梨酸钾0.2-0.5份、壳聚糖0.5-2份、渗透剂JFC 0.5-1份、聚乙烯醇2-5份、丙二醇2-4份、烷基糖苷0.8-1.5份、山梨醇酐三油酸酯0.2-0.6份、二萘基甲烷二磺酸钠0.2-0.6份、分散剂WA 0.3-0.7份、胆矾0.2-0.8份、癸二酸二丁酯0.1-0.4份、环氧大豆油0.8-1.5份、环氧糠油酸丁酯0.4-0.8份、苯甲酸乙酯0.2-0.6份、软化剂YS 0.15-0.4份、软化剂ES 0.2-0.5份、去离子水70-120份。
2.根据权利要求1所述改善猪鬃柔软性用染色剂，其特征在于，天然染料按以下工艺进行制备：
S1、将香蕉皮、芒果皮和黄栀子粉碎，混合，加入溶剂A提取2-4次，合并提取液，浓缩，得到物料B；
S2、将大黄、荩草和玉米清洗，晒干，粉碎，然后加入溶剂C提取2-4次，合并提取液，浓缩，得到物料D；
S3、将物料B、物料D和姜黄素混合，得到天然染料。
3.根据权利要求2所述改善猪鬃柔软性用染色剂，其特征在于，S1中，采用微波提取法进行提取，其中，微波功率为300-350W，微波时间为10-15min。
4.根据权利要求2所述改善猪鬃柔软性用染色剂，其特征在于，S1中，溶剂A为体积分数为72-80％的乙醇水溶液。
5.根据权利要求2所述改善猪鬃柔软性用染色剂，其特征在于，S1中，提取时料液比为1:25-35。
6.根据权利要求2所述改善猪鬃柔软性用染色剂，其特征在于，S2中，采用回流提取法进行提取，且提取温度为82-90℃，提取时间为30-40min。
7.根据权利要求2所述改善猪鬃柔软性用染色剂，其特征在于，S2中，提取时料液比为1:22-25。
8.根据权利要求2所述改善猪鬃柔软性用染色剂，其特征在于，S2中，溶剂C为体积分数为55-65％的乙醇水溶液。
9.根据权利要求2所述改善猪鬃柔软性用染色剂，其特征在于，S3中，物料B、物料D和姜黄素之间的重量比为2-5:5-10:1-1.5。
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