TWI746733B - 不良氣味抑制劑 - Google Patents
不良氣味抑制劑 Download PDFInfo
- Publication number
- TWI746733B TWI746733B TW106143983A TW106143983A TWI746733B TW I746733 B TWI746733 B TW I746733B TW 106143983 A TW106143983 A TW 106143983A TW 106143983 A TW106143983 A TW 106143983A TW I746733 B TWI746733 B TW I746733B
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- Taiwan
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- mass
- protein
- oils
- odor
- oxidized
- Prior art date
Links
- 239000003112 inhibitor Substances 0.000 title claims abstract description 28
- 235000021243 milk fat Nutrition 0.000 claims abstract description 58
- 235000013305 food Nutrition 0.000 claims abstract description 49
- 238000000034 method Methods 0.000 claims abstract description 18
- 150000002978 peroxides Chemical class 0.000 claims abstract description 15
- 239000004480 active ingredient Substances 0.000 claims abstract description 6
- 239000003925 fat Substances 0.000 claims description 107
- 239000003921 oil Substances 0.000 claims description 106
- 239000000203 mixture Substances 0.000 claims description 50
- 108090000623 proteins and genes Proteins 0.000 claims description 47
- 102000004169 proteins and genes Human genes 0.000 claims description 47
- 235000010627 Phaseolus vulgaris Nutrition 0.000 claims description 31
- 244000046052 Phaseolus vulgaris Species 0.000 claims description 31
- 240000004808 Saccharomyces cerevisiae Species 0.000 claims description 19
- 235000014647 Lens culinaris subsp culinaris Nutrition 0.000 claims description 17
- 235000010523 Cicer arietinum Nutrition 0.000 claims description 16
- 244000045195 Cicer arietinum Species 0.000 claims description 16
- 235000010469 Glycine max Nutrition 0.000 claims description 15
- 244000068988 Glycine max Species 0.000 claims description 14
- 235000010582 Pisum sativum Nutrition 0.000 claims description 13
- 240000004713 Pisum sativum Species 0.000 claims description 13
- 235000021374 legumes Nutrition 0.000 claims description 8
- 244000043158 Lens esculenta Species 0.000 claims 3
- 235000019197 fats Nutrition 0.000 description 97
- 235000019198 oils Nutrition 0.000 description 95
- 235000019645 odor Nutrition 0.000 description 79
- 108010073771 Soybean Proteins Proteins 0.000 description 39
- 235000018102 proteins Nutrition 0.000 description 39
- 238000002360 preparation method Methods 0.000 description 26
- 230000000694 effects Effects 0.000 description 25
- 235000015220 hamburgers Nutrition 0.000 description 25
- 235000019484 Rapeseed oil Nutrition 0.000 description 22
- 229940001941 soy protein Drugs 0.000 description 22
- 235000019710 soybean protein Nutrition 0.000 description 17
- 241000251468 Actinopterygii Species 0.000 description 16
- 241000234282 Allium Species 0.000 description 16
- 235000002732 Allium cepa var. cepa Nutrition 0.000 description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 16
- 230000035943 smell Effects 0.000 description 15
- 240000004322 Lens culinaris Species 0.000 description 14
- 238000004519 manufacturing process Methods 0.000 description 14
- 235000010724 Wisteria floribunda Nutrition 0.000 description 10
- 239000000463 material Substances 0.000 description 10
- 240000008415 Lactuca sativa Species 0.000 description 9
- 235000012045 salad Nutrition 0.000 description 9
- 239000003549 soybean oil Substances 0.000 description 9
- 235000012424 soybean oil Nutrition 0.000 description 9
- 241001465754 Metazoa Species 0.000 description 8
- 235000014347 soups Nutrition 0.000 description 8
- 230000001629 suppression Effects 0.000 description 8
- 239000000654 additive Substances 0.000 description 7
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 7
- 235000014113 dietary fatty acids Nutrition 0.000 description 7
- 238000011156 evaluation Methods 0.000 description 7
- 229930195729 fatty acid Natural products 0.000 description 7
- 239000000194 fatty acid Substances 0.000 description 7
- 239000001301 oxygen Substances 0.000 description 7
- 229910052760 oxygen Inorganic materials 0.000 description 7
- 239000000843 powder Substances 0.000 description 7
- 239000002994 raw material Substances 0.000 description 7
- 238000003756 stirring Methods 0.000 description 7
- 235000019482 Palm oil Nutrition 0.000 description 6
- 230000000996 additive effect Effects 0.000 description 6
- 239000004615 ingredient Substances 0.000 description 6
- 238000002156 mixing Methods 0.000 description 6
- 230000003647 oxidation Effects 0.000 description 6
- 238000007254 oxidation reaction Methods 0.000 description 6
- 239000002540 palm oil Substances 0.000 description 6
- 239000006071 cream Substances 0.000 description 5
- 235000011194 food seasoning agent Nutrition 0.000 description 5
- 229910001220 stainless steel Inorganic materials 0.000 description 5
- 239000010935 stainless steel Substances 0.000 description 5
- 240000008042 Zea mays Species 0.000 description 4
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 4
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 4
- 235000005822 corn Nutrition 0.000 description 4
- 239000003995 emulsifying agent Substances 0.000 description 4
- 239000004519 grease Substances 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 229910052751 metal Inorganic materials 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- 239000012778 molding material Substances 0.000 description 4
- 238000000465 moulding Methods 0.000 description 4
- 239000006188 syrup Substances 0.000 description 4
- 235000020357 syrup Nutrition 0.000 description 4
- 239000012138 yeast extract Substances 0.000 description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 3
- 108010084695 Pea Proteins Proteins 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 239000002671 adjuvant Substances 0.000 description 3
- 239000005018 casein Substances 0.000 description 3
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 description 3
- 235000021240 caseins Nutrition 0.000 description 3
- 235000005687 corn oil Nutrition 0.000 description 3
- 239000002285 corn oil Substances 0.000 description 3
- 235000020247 cow milk Nutrition 0.000 description 3
- ZPWVASYFFYYZEW-UHFFFAOYSA-L dipotassium hydrogen phosphate Chemical compound [K+].[K+].OP([O-])([O-])=O ZPWVASYFFYYZEW-UHFFFAOYSA-L 0.000 description 3
- 229910000396 dipotassium phosphate Inorganic materials 0.000 description 3
- 235000019797 dipotassium phosphate Nutrition 0.000 description 3
- 239000000796 flavoring agent Substances 0.000 description 3
- 235000019634 flavors Nutrition 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 235000013372 meat Nutrition 0.000 description 3
- 235000013336 milk Nutrition 0.000 description 3
- 239000008267 milk Substances 0.000 description 3
- 210000004080 milk Anatomy 0.000 description 3
- 239000003002 pH adjusting agent Substances 0.000 description 3
- 235000019702 pea protein Nutrition 0.000 description 3
- 235000015067 sauces Nutrition 0.000 description 3
- 239000001509 sodium citrate Substances 0.000 description 3
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 description 3
- KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 description 3
- 229910001948 sodium oxide Inorganic materials 0.000 description 3
- -1 sorbitan fatty acid ester Chemical class 0.000 description 3
- 235000013322 soy milk Nutrition 0.000 description 3
- 239000007921 spray Substances 0.000 description 3
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 3
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 3
- FYELSNVLZVIGTI-UHFFFAOYSA-N 2-[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]-5-ethylpyrazol-1-yl]-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethanone Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C=1C=NN(C=1CC)CC(=O)N1CC2=C(CC1)NN=N2 FYELSNVLZVIGTI-UHFFFAOYSA-N 0.000 description 2
- 239000004278 EU approved seasoning Substances 0.000 description 2
- 241000269851 Sarda sarda Species 0.000 description 2
- JAZBEHYOTPTENJ-JLNKQSITSA-N all-cis-5,8,11,14,17-icosapentaenoic acid Chemical compound CC\C=C/C\C=C/C\C=C/C\C=C/C\C=C/CCCC(O)=O JAZBEHYOTPTENJ-JLNKQSITSA-N 0.000 description 2
- 229940041514 candida albicans extract Drugs 0.000 description 2
- 239000008157 edible vegetable oil Substances 0.000 description 2
- 235000020673 eicosapentaenoic acid Nutrition 0.000 description 2
- 229960005135 eicosapentaenoic acid Drugs 0.000 description 2
- JAZBEHYOTPTENJ-UHFFFAOYSA-N eicosapentaenoic acid Natural products CCC=CCC=CCC=CCC=CCC=CCCCC(O)=O JAZBEHYOTPTENJ-UHFFFAOYSA-N 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- 235000014593 oils and fats Nutrition 0.000 description 2
- 230000001590 oxidative effect Effects 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- DVSZKTAMJJTWFG-SKCDLICFSA-N (2e,4e,6e,8e,10e,12e)-docosa-2,4,6,8,10,12-hexaenoic acid Chemical compound CCCCCCCCC\C=C\C=C\C=C\C=C\C=C\C=C\C(O)=O DVSZKTAMJJTWFG-SKCDLICFSA-N 0.000 description 1
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 description 1
- LPZOCVVDSHQFST-UHFFFAOYSA-N 2-[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]-3-ethylpyrazol-1-yl]-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethanone Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C=1C(=NN(C=1)CC(=O)N1CC2=C(CC1)NN=N2)CC LPZOCVVDSHQFST-UHFFFAOYSA-N 0.000 description 1
- YJLUBHOZZTYQIP-UHFFFAOYSA-N 2-[5-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]-1,3,4-oxadiazol-2-yl]-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethanone Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C1=NN=C(O1)CC(=O)N1CC2=C(CC1)NN=N2 YJLUBHOZZTYQIP-UHFFFAOYSA-N 0.000 description 1
- GZJLLYHBALOKEX-UHFFFAOYSA-N 6-Ketone, O18-Me-Ussuriedine Natural products CC=CCC=CCC=CCC=CCC=CCC=CCCCC(O)=O GZJLLYHBALOKEX-UHFFFAOYSA-N 0.000 description 1
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 1
- 235000017491 Bambusa tulda Nutrition 0.000 description 1
- 241000238366 Cephalopoda Species 0.000 description 1
- 235000007688 Lycopersicon esculentum Nutrition 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 244000082204 Phyllostachys viridis Species 0.000 description 1
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 1
- 235000019485 Safflower oil Nutrition 0.000 description 1
- 240000003768 Solanum lycopersicum Species 0.000 description 1
- 235000019486 Sunflower oil Nutrition 0.000 description 1
- 244000273928 Zingiber officinale Species 0.000 description 1
- 235000006886 Zingiber officinale Nutrition 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 239000011425 bamboo Substances 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 235000008429 bread Nutrition 0.000 description 1
- 239000000828 canola oil Substances 0.000 description 1
- 235000019519 canola oil Nutrition 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 235000019868 cocoa butter Nutrition 0.000 description 1
- 229940110456 cocoa butter Drugs 0.000 description 1
- 239000003240 coconut oil Substances 0.000 description 1
- 235000019864 coconut oil Nutrition 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 235000012343 cottonseed oil Nutrition 0.000 description 1
- 239000002385 cottonseed oil Substances 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 235000020669 docosahexaenoic acid Nutrition 0.000 description 1
- KAUVQQXNCKESLC-UHFFFAOYSA-N docosahexaenoic acid (DHA) Natural products COC(=O)C(C)NOCC1=CC=CC=C1 KAUVQQXNCKESLC-UHFFFAOYSA-N 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 239000010685 fatty oil Substances 0.000 description 1
- 238000004108 freeze drying Methods 0.000 description 1
- 235000008397 ginger Nutrition 0.000 description 1
- 239000010649 ginger oil Substances 0.000 description 1
- 125000005456 glyceride group Chemical group 0.000 description 1
- 235000020993 ground meat Nutrition 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 239000000543 intermediate Substances 0.000 description 1
- 239000000787 lecithin Substances 0.000 description 1
- 229940067606 lecithin Drugs 0.000 description 1
- 235000010445 lecithin Nutrition 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 235000015167 meat floss Nutrition 0.000 description 1
- 150000004667 medium chain fatty acids Chemical class 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 235000021096 natural sweeteners Nutrition 0.000 description 1
- 239000003346 palm kernel oil Substances 0.000 description 1
- 235000019865 palm kernel oil Nutrition 0.000 description 1
- 239000000546 pharmaceutical excipient Substances 0.000 description 1
- 230000001766 physiological effect Effects 0.000 description 1
- 235000012029 potato salad Nutrition 0.000 description 1
- 235000004252 protein component Nutrition 0.000 description 1
- 235000020185 raw untreated milk Nutrition 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 235000005713 safflower oil Nutrition 0.000 description 1
- 239000003813 safflower oil Substances 0.000 description 1
- 235000013580 sausages Nutrition 0.000 description 1
- 235000015170 shellfish Nutrition 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 239000002600 sunflower oil Substances 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 235000010436 thaumatin Nutrition 0.000 description 1
- 239000000892 thaumatin Substances 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS OR COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings or cooking oils
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J3/00—Working-up of proteins for foodstuffs
- A23J3/14—Vegetable proteins
- A23J3/16—Vegetable proteins from soybean
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L35/00—Foods or foodstuffs not provided for in groups A23L5/00 - A23L33/00; Preparation or treatment thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Biochemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Seeds, Soups, And Other Foods (AREA)
- Beans For Foods Or Fodder (AREA)
- Edible Oils And Fats (AREA)
- Meat, Egg Or Seafood Products (AREA)
- Seasonings (AREA)
- Dairy Products (AREA)
- General Preparation And Processing Of Foods (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2016253873 | 2016-12-27 | ||
JP2016-253873 | 2016-12-27 |
Publications (2)
Publication Number | Publication Date |
---|---|
TW201828825A TW201828825A (zh) | 2018-08-16 |
TWI746733B true TWI746733B (zh) | 2021-11-21 |
Family
ID=62707505
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
TW106143983A TWI746733B (zh) | 2016-12-27 | 2017-12-14 | 不良氣味抑制劑 |
Country Status (4)
Country | Link |
---|---|
JP (1) | JP7051713B2 (ja) |
CN (1) | CN110072400A (ja) |
TW (1) | TWI746733B (ja) |
WO (1) | WO2018123596A1 (ja) |
Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2019073811A1 (ja) * | 2017-10-13 | 2019-04-18 | 株式会社J-オイルミルズ | 食品用油脂感増強剤、及びそれを含有する食品 |
CN111109549A (zh) * | 2020-02-11 | 2020-05-08 | 荣成泰祥食品股份有限公司 | 一种油炸鱼肉馅料即食食品的制作方法 |
JPWO2023053972A1 (ja) * | 2021-09-29 | 2023-04-06 | ||
WO2023176455A1 (ja) * | 2022-03-15 | 2023-09-21 | 株式会社J-オイルミルズ | 植物性タンパク臭抑制剤、植物性タンパク臭抑制用油脂組成物、及びこれらの利用 |
WO2023176454A1 (ja) * | 2022-03-15 | 2023-09-21 | 株式会社J-オイルミルズ | 植物性タンパク臭抑制剤、植物性タンパク臭抑制用油脂組成物、及びこれらの利用 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2008182934A (ja) * | 2007-01-29 | 2008-08-14 | Mitsui Norin Co Ltd | 飲食品組成物 |
TW201247105A (en) * | 2011-05-23 | 2012-12-01 | J Oil Mills Inc | Oil and fat composition |
TW201713218A (zh) * | 2015-10-02 | 2017-04-16 | J 制油股份有限公司 | 油脂組成物及其製造方法 |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2005328754A (ja) * | 2004-05-20 | 2005-12-02 | Minoru Hishinuma | インスタント加工米食品及びその製造法 |
SG11201502724PA (en) * | 2012-11-14 | 2015-05-28 | J Oil Mills Inc | Sweetness and/or milk flavor enhancer |
JP6357741B2 (ja) | 2013-09-11 | 2018-07-18 | 株式会社カネカ | 乳風味呈味材 |
WO2016084788A1 (ja) * | 2014-11-26 | 2016-06-02 | 不二製油グループ本社株式会社 | 塩味増強油脂の製造方法 |
-
2017
- 2017-12-13 JP JP2018559020A patent/JP7051713B2/ja active Active
- 2017-12-13 WO PCT/JP2017/044750 patent/WO2018123596A1/ja active Application Filing
- 2017-12-13 CN CN201780077303.5A patent/CN110072400A/zh active Pending
- 2017-12-14 TW TW106143983A patent/TWI746733B/zh not_active IP Right Cessation
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2008182934A (ja) * | 2007-01-29 | 2008-08-14 | Mitsui Norin Co Ltd | 飲食品組成物 |
TW201247105A (en) * | 2011-05-23 | 2012-12-01 | J Oil Mills Inc | Oil and fat composition |
TW201713218A (zh) * | 2015-10-02 | 2017-04-16 | J 制油股份有限公司 | 油脂組成物及其製造方法 |
Also Published As
Publication number | Publication date |
---|---|
CN110072400A (zh) | 2019-07-30 |
JP7051713B2 (ja) | 2022-04-11 |
JPWO2018123596A1 (ja) | 2019-10-31 |
WO2018123596A1 (ja) | 2018-07-05 |
TW201828825A (zh) | 2018-08-16 |
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Legal Events
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MM4A | Annulment or lapse of patent due to non-payment of fees |