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DE69320467D1 - Verfahren zur herstellung von cyclischen estern aus hydroxysäuren und deren derivaten - Google Patents

Verfahren zur herstellung von cyclischen estern aus hydroxysäuren und deren derivaten

Info

Publication number
DE69320467D1
DE69320467D1 DE69320467T DE69320467T DE69320467D1 DE 69320467 D1 DE69320467 D1 DE 69320467D1 DE 69320467 T DE69320467 T DE 69320467T DE 69320467 T DE69320467 T DE 69320467T DE 69320467 D1 DE69320467 D1 DE 69320467D1
Authority
DE
Germany
Prior art keywords
cyclic esters
derivatives
disclosed
acids
hydroxysic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69320467T
Other languages
English (en)
Other versions
DE69320467T2 (de
Inventor
Herman Benecke
Alex Cheung
George Cremeans
Melville Hillman
Edward Lipinsky
Richard Markle
Richard Sinclair
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Biopak Technology Ltd
Original Assignee
Biopak Technology Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Biopak Technology Ltd filed Critical Biopak Technology Ltd
Application granted granted Critical
Publication of DE69320467D1 publication Critical patent/DE69320467D1/de
Publication of DE69320467T2 publication Critical patent/DE69320467T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C08J5/18—Manufacture of films or sheets
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D319/00—Heterocyclic compounds containing six-membered rings having two oxygen atoms as the only ring hetero atoms
    • C07D319/10—1,4-Dioxanes; Hydrogenated 1,4-dioxanes
    • C07D319/12—1,4-Dioxanes; Hydrogenated 1,4-dioxanes not condensed with other rings
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L67/00—Compositions of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Compositions of derivatives of such polymers
    • C08L67/04—Polyesters derived from hydroxycarboxylic acids, e.g. lactones
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D167/00—Coating compositions based on polyesters obtained by reactions forming a carboxylic ester link in the main chain; Coating compositions based on derivatives of such polymers
    • C09D167/04—Polyesters derived from hydroxycarboxylic acids, e.g. lactones
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/19—Details relating to the geometry of the reactor
    • B01J2219/194—Details relating to the geometry of the reactor round
    • B01J2219/1941—Details relating to the geometry of the reactor round circular or disk-shaped
    • B01J2219/1942—Details relating to the geometry of the reactor round circular or disk-shaped spherical
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2367/00—Characterised by the use of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Derivatives of such polymers
    • C08J2367/04—Polyesters derived from hydroxy carboxylic acids, e.g. lactones

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Manufacturing & Machinery (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)
  • Polyesters Or Polycarbonates (AREA)
DE69320467T 1992-03-19 1993-03-17 Verfahren zur herstellung von cyclischen estern aus hydroxysäuren und deren derivaten Expired - Fee Related DE69320467T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US07/854,559 US5319107A (en) 1990-09-18 1992-03-19 Method to produce cyclic esters
PCT/US1993/002483 WO1993019058A2 (en) 1992-03-19 1993-03-17 Process for the production of cyclic esters from hydroxy acids and derivatives thereof

Publications (2)

Publication Number Publication Date
DE69320467D1 true DE69320467D1 (de) 1998-09-24
DE69320467T2 DE69320467T2 (de) 1999-04-22

Family

ID=25319033

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69320467T Expired - Fee Related DE69320467T2 (de) 1992-03-19 1993-03-17 Verfahren zur herstellung von cyclischen estern aus hydroxysäuren und deren derivaten

Country Status (16)

Country Link
US (1) US5319107A (de)
EP (1) EP0632807B1 (de)
JP (1) JP2922303B2 (de)
KR (1) KR950700898A (de)
CN (1) CN1080921A (de)
AT (1) ATE169913T1 (de)
AU (1) AU677183B2 (de)
BR (1) BR9306101A (de)
DE (1) DE69320467T2 (de)
FI (1) FI115459B (de)
IL (1) IL104765A0 (de)
MY (1) MY116462A (de)
NO (1) NO943464L (de)
NZ (1) NZ251210A (de)
TW (1) TW321645B (de)
WO (1) WO1993019058A2 (de)

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US6469133B2 (en) 1999-12-13 2002-10-22 Board Of Trustees Of Michigan State University Process for the preparation of polymers of dimeric cyclic esters
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CN101925591B (zh) * 2007-12-26 2013-12-04 克坦顿有限公司 用于生产α-羟酸的环二酯的方法
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JP5459974B2 (ja) * 2008-04-11 2014-04-02 株式会社日立製作所 精製乳酸環状二量体の製造方法及び製造装置、並びに、ポリ乳酸の製造方法及び製造装置
BE1018247A3 (fr) * 2008-08-14 2010-07-06 Futerro Sa Procede d'obtention de lactide.
EP2321294B1 (de) * 2008-08-29 2015-09-30 Uhde Inventa-Fischer GmbH Verfahren zur herstellung eines gemisches von lactid-derivaten
KR101154029B1 (ko) 2009-05-20 2012-06-07 한국화학연구원 젖산에스테르로부터 락타이드의 직접 전환용 촉매 및 이를 이용한 락타이드의 제조방법
WO2012000921A1 (en) 2010-06-29 2012-01-05 Solvay Sa Process for the manufacture of lactide
EP2407463A1 (de) 2010-07-14 2012-01-18 Solvay SA Verfahren zur Herstellung eines cyclischen Diesters einer alpha-Hydroxysäure
BR112013004935A2 (pt) * 2010-09-07 2016-08-02 Myriant Corp "desitratação catalítica de ácido láctico e ésteres de ácido láctico".
KR101616171B1 (ko) 2010-10-28 2016-04-28 토탈 마케팅 서비스 유기산 제조에서의 모나스쿠스의 용도
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KR101326521B1 (ko) * 2011-05-26 2013-11-07 현대자동차주식회사 유산으로부터 락타이드의 제조 방법
CN102351838B (zh) * 2011-07-21 2013-07-24 凯莱英医药集团（天津）股份有限公司 一种1,4-二氧六环-2,5-二醇的合成方法
KR101459819B1 (ko) * 2012-04-04 2014-11-07 현대자동차주식회사 유산염으로부터 락타이드의 제조방법
WO2013160485A1 (de) 2012-04-28 2013-10-31 Uhde Inventa-Fischer Gmbh Verfahren zur kontinuierlichen herstellung von lactid direkt aus konzentrierter milchsäure
EP3056490A1 (de) * 2015-02-13 2016-08-17 PURAC Biochem BV Verfahren zur Herstellung von Lactid
CN105801555A (zh) * 2016-03-31 2016-07-27 东华大学 一种聚合级丙交酯的制备方法
JP2019519609A (ja) * 2016-06-20 2019-07-11 トタル リサーチ アンド テクノロジー フエリユイ オリゴマーおよび触媒の加水分解を回収し水で行う単一工程によるラクチドの製造方法
JP2019519608A (ja) * 2016-06-20 2019-07-11 トタル リサーチ アンド テクノロジー フエリユイ 溶剤を別に供給する単一工程によるラクチドの製造方法
JP2019521186A (ja) * 2016-06-20 2019-07-25 トタル リサーチ アンド テクノロジー フエリユイ 熱回収を行なうラクチドの一段階製造方法
CN109563068A (zh) * 2016-06-20 2019-04-02 道达尔研究技术弗吕公司 通过滗析回收水的单步骤丙交酯生产工艺
GB201621549D0 (en) 2016-12-19 2017-02-01 Univ Leuven Kath Catalytic process
EP3891135A1 (de) * 2018-12-06 2021-10-13 Haldor Topsøe A/S Verfahren zur herstellung von glykolid
CN113387921B (zh) * 2021-06-18 2022-08-19 华东理工大学 一种合成乙交酯的方法
EP4134365A1 (de) * 2021-08-12 2023-02-15 Sulzer Management AG Anlage und effizientes verfahren zur herstellung von lactid aus milchsäure
CN113861159A (zh) * 2021-10-28 2021-12-31 北京工商大学 一种直接缩聚制备丙交酯的方法
CN113842657B (zh) * 2021-10-28 2023-10-03 北京工商大学 一种循环制备丙交酯的设备
CN114163414A (zh) * 2021-11-26 2022-03-11 上海中化科技有限公司 乙交酯的制备方法和制备装置
CN114195755B (zh) * 2021-11-26 2023-09-19 上海浦景化工技术股份有限公司 一种乙交酯的制备方法
CN114621179B (zh) * 2022-03-17 2024-03-26 中国神华煤制油化工有限公司 乙交酯的合成方法
CN114805285A (zh) * 2022-06-07 2022-07-29 南昌大学 一种从l-乳酸制备丙交酯的方法

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Also Published As

Publication number Publication date
DE69320467T2 (de) 1999-04-22
JPH07504916A (ja) 1995-06-01
EP0632807A1 (de) 1995-01-11
AU3813093A (en) 1993-10-21
WO1993019058A3 (en) 1993-11-11
MY116462A (en) 2004-02-28
EP0632807A4 (de) 1995-05-03
JP2922303B2 (ja) 1999-07-19
US5319107A (en) 1994-06-07
FI944275A0 (fi) 1994-09-15
NO943464D0 (no) 1994-09-16
KR950700898A (ko) 1995-02-20
AU677183B2 (en) 1997-04-17
ATE169913T1 (de) 1998-09-15
WO1993019058A2 (en) 1993-09-30
IL104765A0 (en) 1993-06-10
NO943464L (no) 1994-11-15
CN1080921A (zh) 1994-01-19
NZ251210A (en) 1996-10-28
FI115459B (fi) 2005-05-13
TW321645B (de) 1997-12-01
BR9306101A (pt) 1995-09-12
EP0632807B1 (de) 1998-08-19
FI944275L (fi) 1994-11-16

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