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DE60135525D1 - Polymerisationsreaktion und -Vorrichtung - Google Patents

Polymerisationsreaktion und -Vorrichtung

Info

Publication number
DE60135525D1
DE60135525D1 DE60135525T DE60135525T DE60135525D1 DE 60135525 D1 DE60135525 D1 DE 60135525D1 DE 60135525 T DE60135525 T DE 60135525T DE 60135525 T DE60135525 T DE 60135525T DE 60135525 D1 DE60135525 D1 DE 60135525D1
Authority
DE
Germany
Prior art keywords
reaction mixture
predetermined
viscosity
inlet
inlet means
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE60135525T
Other languages
English (en)
Inventor
Jean Marc Gilson
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dow Silicones Belgium SPRL
Original Assignee
Dow Corning Europe SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Corning Europe SA filed Critical Dow Corning Europe SA
Application granted granted Critical
Publication of DE60135525D1 publication Critical patent/DE60135525D1/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00Processes of polymerisation
    • C08F2/01Processes of polymerisation characterised by special features of the polymerisation apparatus used
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/0033Optimalisation processes, i.e. processes with adaptive control systems
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J14/00Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04Polysiloxanes
    • C08G77/06Preparatory processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002Chemical plants
    • B01J2219/00027Process aspects
    • B01J2219/00033Continuous processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094Jackets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00162Controlling or regulating processes controlling the pressure
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00164Controlling or regulating processes controlling the flow
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00168Controlling or regulating processes controlling the viscosity

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
  • Automation & Control Theory (AREA)
  • Silicon Polymers (AREA)
  • Other Resins Obtained By Reactions Not Involving Carbon-To-Carbon Unsaturated Bonds (AREA)
  • Polymerisation Methods In General (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
DE60135525T 2000-07-26 2001-07-02 Polymerisationsreaktion und -Vorrichtung Expired - Lifetime DE60135525D1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GBGB0018162.8A GB0018162D0 (en) 2000-07-26 2000-07-26 Polymerisation reactor and process

Publications (1)

Publication Number Publication Date
DE60135525D1 true DE60135525D1 (de) 2008-10-09

Family

ID=9896259

Family Applications (1)

Application Number Title Priority Date Filing Date
DE60135525T Expired - Lifetime DE60135525D1 (de) 2000-07-26 2001-07-02 Polymerisationsreaktion und -Vorrichtung

Country Status (9)

Country Link
US (1) US6964753B2 (de)
EP (1) EP1175937B1 (de)
JP (1) JP4780868B2 (de)
KR (2) KR100835125B1 (de)
CN (1) CN1261459C (de)
AT (1) ATE406207T1 (de)
DE (1) DE60135525D1 (de)
ES (1) ES2309038T3 (de)
GB (1) GB0018162D0 (de)

Families Citing this family (14)

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GB0018162D0 (en) * 2000-07-26 2000-09-13 Dow Corning Sa Polymerisation reactor and process
CA2456482A1 (en) * 2004-02-03 2005-08-03 Bayer Inc. Method and apparatus for controlling a polymerization reaction
DE102004023911A1 (de) * 2004-05-13 2005-12-01 Wacker-Chemie Gmbh Verfahren zur diskontinuierlichen Herstellung von Silicon-Emulsionen
US20070293650A1 (en) * 2006-06-14 2007-12-20 Vere Orland Archibald Polymerization process
DE102006028300A1 (de) * 2006-06-20 2007-12-27 Wacker Chemie Ag Verfahren zur Herstellung von hochmolekularen Organopolysiloxanen
DE102007020568A1 (de) * 2007-05-02 2008-11-06 Wacker Chemie Ag Verfahren zur kontinuierlichen Herstellung von Aminoalkylgruppen aufweisenden Organopolysiloxanen
JP5959253B2 (ja) 2012-03-22 2016-08-02 住友化学株式会社 連続重合装置および重合体組成物の製造方法
EP3038748A4 (de) * 2013-08-30 2017-01-25 Momentive Performance Materials Inc. Katalysator zur synthese von siloxanen
CN104497186B (zh) * 2014-12-03 2017-05-17 浙江大学 一种制备顺丁橡胶的催化剂预混方法与装置
US11136436B2 (en) 2018-08-24 2021-10-05 Dow Silicones Corporation Method for condensation polymerization of hydroxyl-terminated polydiorganosiloxanes
KR20210047823A (ko) 2018-08-24 2021-04-30 다우 글로벌 테크놀로지스 엘엘씨 하이드록실-말단화된 폴리디오르가노실록산의 축합 중합 방법
CN110128579B (zh) * 2019-04-13 2021-08-20 复旦大学 高通量聚合物库的自动合成装置与方法
CN115521461B (zh) * 2022-09-09 2023-11-24 湖北兴瑞硅材料有限公司 一种低粘度乙烯基硅油连续化生产工艺
CN115738983A (zh) * 2022-11-18 2023-03-07 唐山三友硅业有限责任公司 α,ω-二羟基聚二甲基硅氧烷的生产系统及生产方法

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US3160601A (en) * 1959-07-13 1964-12-08 Dow Corning Amine salts of phosphoric acid and amine salts of carboxylic acid as silanol condensation catalysts
US3094497A (en) 1960-07-28 1963-06-18 Dow Corning Condensation catalysts
GB1174219A (en) 1967-05-09 1969-12-17 Werner & Pfleiderer Method of and Apparatus for the Production of Silicone Products
US3649842A (en) * 1969-04-30 1972-03-14 William J Thornhill Signal generation
US4175169A (en) * 1971-03-19 1979-11-20 Exxon Research & Engineering Co. Production of polyethylene
DE2212962C2 (de) * 1972-03-17 1985-01-24 Basf Ag, 6700 Ludwigshafen Verfahren zur Polymerisation von Vinylchlorid in wäßriger Suspension
CA993596A (en) 1972-05-03 1976-07-20 Polysar Limited Control of emulsion polymerization process
DE2229514C3 (de) * 1972-06-16 1979-01-04 Wacker-Chemie Gmbh, 8000 Muenchen Verfahren zur Förderung von Kondensations- und/oder Äquilibrierungsreaktionen von Organosiliciumverbindungen
US4027085A (en) * 1972-10-20 1977-05-31 Dart Industries Inc. Apparatus for controlling operational parameters in polymerization equipment and related method
US3903202A (en) * 1973-09-19 1975-09-02 Monsanto Co Continuous mass polymerization process for polyblends
FR2373385A1 (fr) * 1976-12-09 1978-07-07 Rhone Poulenc Ind Procede d'extrusion pour la fabrication de corps creux
US4220518A (en) * 1977-09-28 1980-09-02 Hitachi, Ltd. Method for preventing coking in fluidized bed reactor for cracking heavy hydrocarbon oil
CA1075309A (en) * 1977-10-12 1980-04-08 Her Majesty The Queen, In Right Of Canada, As Represented By The Minister Of National Defence Zinc electrode for low temperatures
AU5900880A (en) * 1979-06-18 1981-01-08 General Electric Company Continuous manufacture of siloxane polymers
DE3428581A1 (de) * 1984-08-02 1986-02-13 Wacker-Chemie GmbH, 8000 München Verfahren zum stabilisieren von organopolysiloxanen
WO1987001614A1 (en) * 1985-09-16 1987-03-26 J.C. Schumacher Company Vacuum vapor transport control
DE3533028A1 (de) * 1985-09-16 1987-03-19 Wacker Chemie Gmbh Verfahren zum stabilisieren von organopolysiloxanen
GB8902935D0 (en) 1989-02-09 1989-03-30 Dow Corning Process for producing organosilicon products
US4952345A (en) * 1989-02-10 1990-08-28 E. I. Du Pont De Nemours And Company Method for controlling polymer viscosity
DE3914912A1 (de) * 1989-05-05 1990-11-08 Wacker Chemie Gmbh Verfahren zur kontinuierlichen herstellung von hochmolekularen organosiliciumverbindungen
JPH04175169A (ja) * 1990-11-09 1992-06-23 Marktec Corp 放電印字装置
GB9103666D0 (en) 1991-02-21 1991-04-10 Dow Corning Sa Method of making organopolysiloxanes
GB9115170D0 (en) * 1991-07-12 1991-08-28 Dow Corning Sa Process and apparatus for the production of organosilicon compounds
JP3323211B2 (ja) * 1991-08-09 2002-09-09 ジーイー東芝シリコーン株式会社 シロキサンポリマーの連続的製造法
JPH05222178A (ja) * 1992-02-14 1993-08-31 Fuji Photo Film Co Ltd 反応制御方法
JP3309502B2 (ja) * 1993-07-12 2002-07-29 大日本インキ化学工業株式会社 生分解性ポリエステル系ポリマーの連続製造法
GB9325342D0 (en) * 1993-12-10 1994-02-16 Dow Corning Sa Process for polymerisation
NO178790C (no) * 1993-12-13 1996-06-05 Borealis Holding As Fremgangsmåte ved fremstilling av olefinpolymerer i en autoklavrektor
US5504150A (en) * 1995-04-05 1996-04-02 Dow Corning Corporation Method of making polysiloxane emulsions
GB9703554D0 (en) 1997-02-20 1997-04-09 Dow Corning Polymerisation of cyclosiloxanes
US5980790A (en) * 1997-03-04 1999-11-09 Mitsubishi Gas Chemical Company, Inc. Process for producing a copolymer
GB2334958B (en) * 1998-02-25 2001-11-07 Porpoise Viscometers Ltd Melt flow index determination in polymer process control
JP4108819B2 (ja) * 1998-03-27 2008-06-25 新日鐵化学株式会社 重合液組成物の脱揮処理方法
US6306658B1 (en) * 1998-08-13 2001-10-23 Symyx Technologies Parallel reactor with internal sensing
US6864092B1 (en) * 1998-08-13 2005-03-08 Symyx Technologies, Inc. Parallel reactor with internal sensing and method of using same
GB9818539D0 (en) 1998-08-26 1998-10-21 Dow Corning Process for producing a silicone polymer
GB0018162D0 (en) * 2000-07-26 2000-09-13 Dow Corning Sa Polymerisation reactor and process
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US6692708B2 (en) * 2001-04-05 2004-02-17 Symyx Technologies, Inc. Parallel reactor for sampling and conducting in situ flow-through reactions and a method of using same

Also Published As

Publication number Publication date
GB0018162D0 (en) 2000-09-13
EP1175937A2 (de) 2002-01-30
CN1334274A (zh) 2002-02-06
EP1175937B1 (de) 2008-08-27
US20020035230A1 (en) 2002-03-21
ES2309038T3 (es) 2008-12-16
KR20020009487A (ko) 2002-02-01
JP2002121287A (ja) 2002-04-23
JP4780868B2 (ja) 2011-09-28
EP1175937A3 (de) 2003-03-26
KR100835125B1 (ko) 2008-06-05
US6964753B2 (en) 2005-11-15
KR100861894B1 (ko) 2008-11-06
KR20080095831A (ko) 2008-10-29
CN1261459C (zh) 2006-06-28
ATE406207T1 (de) 2008-09-15

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Legal Events

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