CN115737456B - Skin cleansing scrub and preparation method thereof - Google Patents
Skin cleansing scrub and preparation method thereof Download PDFInfo
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- CN115737456B CN115737456B CN202211473753.5A CN202211473753A CN115737456B CN 115737456 B CN115737456 B CN 115737456B CN 202211473753 A CN202211473753 A CN 202211473753A CN 115737456 B CN115737456 B CN 115737456B
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Landscapes
- Cosmetics (AREA)
Abstract
The invention discloses a skin cleansing scrub and a preparation method thereof. The skin cleaning scrub cream has synergistic effect of cleaning agent, softening agent and scrub agent, and can improve sharpness of scrub agent, and softening agent has softening effect on scrub particles, and can remove dead skin without damaging skin; on the other hand, the addition of the cleaning agent and the interaction of the cleaning agent play a role in buffering, so that the excessive cleaning effect in the bathing process can be effectively relieved, and the effect of cleaning and non-degreasing can be achieved; the skin cleaning scrub has the effects of cleaning the skin surface layer of the bath lotion, removing sweat, dust and dirt, deeply cleaning the skin, removing chicken skin dead skin of body cream, brightening skin color and tightening skin; the skin cleaning scrub has the effects of bath lotion, scrub and body lotion, and is used for moistening skin, keeping fresh and non-greasy, and light and well absorbed after use, and the skin is moist and has light fragrance to help sleep.
Description
Technical Field
The invention relates to the technical field of daily chemicals, in particular to a mild multi-component composite skin cleansing scrub and a preparation method thereof.
Background
The scrub cream is a skin cleaning product, contains the emulsion shape of uniform and fine particles, and can effectively clear the effects of dirt, grease, cutin and the like on the surface of the skin. At present, various types of scrub cream in the market are various, but the particle and formula structural design is unreasonable, the scrub pain is felt when the scrub cream is used, the skin is not required to be used, and the scrub cream has the problems of dryness, high irritation, easy damage to skin, greasy texture, difficult cleaning, fake slip and the like, so that the use is further influenced.
The invention discloses a scrub cream and a preparation method thereof, belongs to the field of daily chemicals, and provides a scrub cream, which comprises the following components in parts by weight: the cream has small skin irritation, and can remove deep dirt and metabolites of skin, and simultaneously (the components are obviously not consistent with the provided data) make the nutritional ingredients in the cream fully absorbed by skin, remove dead skin and nourish the skin. However, the scrub is difficult to make skin absorb nutrient components effectively, has poor cleaning performance and has single function. The invention discloses a skin cleansing scrub and a preparation method thereof.
Disclosure of Invention
In order to achieve the above purpose, the invention provides a skin cleansing scrub and a preparation method thereof.
A skin cleansing cream comprising: cleaning agents, abrasive agents and emollients; the cleaning agent is an anionic surfactant, a zwitterionic surfactant or a nonionic surfactant; the softening agent is grease or silicone oil; the abrasive is silica.
Further, the skin cleansing scrub comprises 1.2-10.3 parts by weight of cleaning agent, 1-7 parts by weight of scrub agent and 1.2-10 parts by weight of softening agent.
Further the silica is hydrated silica.
The silica is modified silica, and is formed by compounding and modifying hydrated silica and peach shell.
The silica is further modified silica, and is formed by adopting hydrated silica and walnut shells and/or sweet almond shells to be compositely modified.
The cleaning agent is one or more than two of sodium methyl cocoyl taurate, potassium cocoyl glycinate and xylitol-based glucoside.
The softening agent is one or more than two of isononyl isononanoate, polydimethylsiloxane, octyl dodecanol pivalate and phytosterol/octyl dodecanol lauroyl glutamate.
The skin cleansing scrub comprises a phase A, a phase B, a phase C and a phase D; wherein:
the phase A comprises the following raw materials: a humectant, a thickener, and a solvent;
the phase B comprises the following raw materials: a cleaning agent;
the phase C comprises the following raw materials: a emollient and an emulsifier;
The phase D comprises the following raw materials: antioxidants, preservatives, fragrances, pH adjusters, colorants, skin conditioning agents, and abrasive agents.
The invention also discloses modified silica and a preparation method thereof.
A modified silica is prepared by compounding and modifying hydrated silica and peach shell, wherein the peach shell is walnut shell and/or sweet almond shell.
Further, a skin cleansing cream: comprises phase A, phase B, phase C and phase D.
The phase A consists of the following raw materials: a humectant, a thickener, and a solvent;
The humectant is one or more of glycerol, dehydrated xylitol, pseudomonas fermentation product extract, glucose, fructose, octanol, tocopherol, erythritol, and BAIHUA seed oil.
Further preferably, the humectant is composed of the following raw materials in parts by weight: 1-5 parts by weight of glycerol, 1-4 parts by weight of dehydrated xylitol, 1-3 parts by weight of xylitol, 1-10 parts by weight of pseudomonas fermentation product extract, 0.5-3 parts by weight of glucose, 0.5-3 parts by weight of fructose, 0.5-2 parts by weight of octaethylene glycol, 0.5-3 parts by weight of tocopherol, 0.5-3 parts by weight of erythritol and 1-4 parts by weight of white pond flower seed oil.
The thickener is one or more than two of acrylamide dimethyl taurate/VP copolymer and carbomer. Further preferably, the thickener is composed of the following raw materials in parts by weight: 1-5 parts by weight of an ammonium acryloyldimethyl taurate/VP copolymer and 1-2 parts by weight of carbomer.
The solvent is water; preferably, the solvent is 5-20 parts by weight of water.
The phase B consists of the following raw materials: a cleaning agent;
The cleaning agent is one or two of potassium cocoyl glycinate and sodium methyl cocoyl taurate; further preferably, the cleaning agent is composed of the following raw materials in parts by weight: 0.6-6 parts by weight of potassium cocoyl glycinate and 0.6-4.3 parts by weight of sodium methyl cocoyl taurate.
The phase C consists of the following raw materials: a emollient and an emulsifier;
The softening agent is one or more than two of isononyl isononanoate, polydimethylsiloxane, octyl dodecanol pivalate and phytosterol/octyl dodecanol lauroyl glutamate; further preferably, the softener is composed of the following raw materials in parts by weight: 0.5-3 parts by weight of isononyl isononanoate, 0.1-2 parts by weight of polydimethylsiloxane, 0.5-2 parts by weight of octyl dodecanol pivalate and 0.1-3 parts by weight of phytosterol/octyl dodecanol lauroyl glutamate.
The emulsifier is one or more than two of cetostearyl oleate, PEG-100 stearate, cetostearyl alcohol, sorbitan olive oleate, ammonium acryloyldimethyl taurate/behenate polyether-25 methacrylate crosslinked polymer; further preferably, the emulsifier is composed of the following raw materials in parts by weight: 0.1 to 1 part by weight of cetostearyl oleate, 0.1 to 2 parts by weight of PEG-100 stearate, 0.1 to 1 part by weight of cetostearyl alcohol, 0.1 to 2 parts by weight of sorbitan olive oleate, 0.1 to 3 parts by weight of ammonium acryloyldimethyl taurate/behenate-25 methacrylate cross-linked polymer.
The phase D consists of the following raw materials: antioxidants, preservatives, fragrances, pH adjusters, colorants, skin conditioning agents, and abrasive agents;
the antioxidant is inulin; further preferably, the antioxidant is inulin in an amount of 0.1 to 1 part by weight.
The preservative is p-hydroxyacetophenone; further preferably, the preservative is 0.1 to 0.5 parts by weight of p-hydroxyacetophenone.
The aromatic is one or two of essence and plant extract; the plant extract is one or two of flos Rosae Rugosae (ROSA RUGOSA) flower extract and Hibiscus sabdariffa (HIBISCUS SABDARIFFA) extract; further preferably, the flavoring agent is 0.01-0.05 weight parts of (daily) essence, 0.1-1 weight parts of flos Rosae Rugosae (ROSA RUGOSA) flower extract, and 0.1-1 weight parts of Hibiscus sabdariffa (HIBISCUS SABDARIFFA) extract.
The pH regulator is arginine; further preferably, the pH regulator is 0.01-0.2 parts by weight of arginine.
The colorant is one or two of caramel color and CI 14700; further preferably, the colorant is composed of the following raw materials in parts by weight: 0.01 to 0.1 weight part of caramel color and 0.01 to 0.1 weight part of CI 14700.
The skin conditioner and functional component are one or more than two of acetyl heptapeptide-4, tetradecylamino Ding Xianxie amino amidobutyric acid urea trifluoroacetate, undaria pinnatifida (UNDARIA PINNATIFIDA) extract, soluble collagen and palmitoyl tripeptide-5. Further preferably, the skin conditioning agent is composed of the following raw materials in parts by weight: 0.1 to 5 parts by weight of extract of rhododendron alpina (RHODODENDRON FERRUGINEUM), 0.1 to 3 parts by weight of acetyl heptapeptide-4, 0.01 to 0.5 part by weight of tetradecylamino Ding Xianxie amino amidobutyric acid urea trifluoroacetate, 0.1 to 3 parts by weight of extract of undaria pinnatifida (UNDARIA PINNATIFIDA), 0.1 to 5 parts by weight of soluble collagen and 0.1 to 2 parts by weight of palmitoyl tripeptide-5.
The abrasive is hydrated silica. Further preferably, the abrasive agent is 1 to 7 parts by weight of hydrated silica.
Further preferably, the mass ratio of the cleaning agent, the frosting agent and the softening agent is (1.2-10.3): (1-7) and (1.2-10).
According to the invention, the hydrated silica is compounded with natural plant walnut shell particles, so that the skin is massaged, old cutin on the surface of the skin and impurities in pores are removed, the growth of new skin cells is promoted, and the phenomena of rough skin, water shortage and the like are improved; however, the general silica raw material has irregular shape, small specific surface area, high hardness and sharp edges and corners, and causes damage to skin in the using process, and the spherical hydrated silica is better than the similar abrasive agent, so that the using body feeling of cleaning care is brought.
It is further preferred to use modified silica instead of hydrated silica.
The preparation method of the modified silica comprises the following steps:
S1, uniformly mixing 5-10 parts by weight of hydrated silica and 1-2 parts by weight of sodium hydroxide to obtain a mixture;
S2, adding 5-10 parts by weight of the mixture prepared in the step S1 into 60-100 parts by weight of glycerol aqueous solution, uniformly mixing, then placing into a hydrothermal kettle, heating to 120-160 ℃ for reacting for 12-24 hours, centrifuging to obtain precipitate, washing, drying, and crushing to 80-100 meshes to obtain pretreated silica powder; the preparation method of the glycerol aqueous solution comprises the steps of mixing glycerol and water according to the mass ratio of (1-3);
S3, adding 3-5 parts by weight of pretreated silica powder, 1-3 parts by weight of sodium tripolyphosphate and 0.5-2 parts by weight of modifier into 50-80 parts by weight of water, uniformly mixing, then carrying out crosslinking reaction at room temperature for 10-40min, centrifuging after the reaction is finished, taking precipitate, washing and drying to obtain the modified silica.
The modifier is one or more than two of ceramide and fibroin peptide; further preferably, the modifier is prepared from ceramide and fibroin peptide according to the mass ratio of (1-3): (1-3) and mixing.
The invention adopts the hydrated silica to massage the skin, removes the old cutin and impurities in pores on the surface of the skin, promotes the growth of new skin cells, and improves the phenomena of rough skin, water deficiency and the like; but the raw hydrated silica has small specific surface area, high hardness and sharp edges and corners, and causes damage to skin in the use process. And thus do not provide good sanding and cleaning in the scrub. Based on the above, the present inventors treated the hydrated silica with sodium hydroxide, and recovered the silicon hydroxyl groups on the surface of the hydrated silica during the calcination procedure, thereby increasing the specific surface area of the hydrated silica and further improving the cleaning performance. The hydrated silica has high hardness and sharp edges and corners, and is harmful to skin in the using process, the inventor further adopts sodium tripolyphosphate, ceramide and fibroin peptide to modify the hydrated silica, on one hand, the ceramide and the fibroin peptide are wrapped on the surface of the silica, so that the soft feeling of walnut shell particles is improved, the sharp edges and corners are prevented from scratching the skin, meanwhile, the ceramide and the fibroin peptide have the effects of moisturizing and moistening the skin, and have good repairing and protecting effects on the skin, and the hydrated silica is adopted to adsorb dirt, cutin and cosmetic residues on the surface of the skin, so that sebaceous gland and sweat gland channel blockage is improved, the skin is cleaned, and the skin is not degreased, and normal skin barrier function can be maintained; on the other hand, the hydrated silica is uniformly dispersed in the scrub and does not precipitate. And the hydrated silica gradually releases grease and nutrient substances in the sanding process, so as to promote the separation of aged cutin and skin.
Squalane (Squalene)
Except squalane, squalane from plant sources is rich in phytosterol and triterpenes, is a natural component of skin, has better antioxidant and immunity stimulating effects, can be quickly dissolved with moisture and grease in skin to form a natural skin protection barrier, has excellent stability, can not generate oxidation with air, ultraviolet rays and the like, can effectively protect the skin from being damaged by external substances, has excellent penetrability and high oxygen carrying performance, can regulate the water-oil balance of the skin, avoid rough and dull skin and restore the original tender touch of the skin. Is especially suitable for use in cold season, is lubricating oil for skin, and can supplement natural sebum for skin.
Thickening agent
The acrylamide dimethyl taurate/VP copolymer is used for preparing oil-in-water emulsion and cream, has good dispersibility, quick absorption and no sticky feel, and has the main functions of thickening agent and emulsifying agent in cosmetics and skin care products.
Humectant type
Xylitol has good moisturizing effect, can improve the fine grain dryness of skin, has a certain stabilizing effect on pigment, and has cleaning effect; widely applied to cosmetics and skin care products, has no irritation to health and is very mild.
Pseudomonas fermentation product extract
The Pseudomonas fermentation product extract, which is named PSEUDOALTEROMONAS FERMENT EXTRACT, is an extracellular polymer obtained in marine unicellular genus through biotechnology, can effectively reduce redundant oil and sebum, shrink pores, reduce spots and the like, and is mainly used as a humectant and an astringent in cosmetics and skin care products.
Xylitol-based glucoside
Xylitol-based glucoside is a cleanser and a humectant, has small and safe skin irritation, obvious thickening, tackifying and detergency, and simultaneously has good moisturizing effect, and can be used for conditioning the moisture content of skin and being applied to skin care products and cosmetics.
Isononyl isononanoate
Isononyl isononanoate is an excellent skin-friendly grease, and a protective film is formed on the skin, so that the skin is softer and has glossiness while moisturizing the skin. At the same time, the cosmetic can also prevent damage to the skin caused by external matters, and has a moisturizing effect in cosmetics.
Polydimethylsiloxane
The polydimethylsiloxane has good lubricating property, can form a uniform protective film with water resistance after being coated on the skin, but does not have any sticky or greasy feeling, has good glossiness and good ultraviolet radiation resistance, and can not cause oxidative deterioration under ultraviolet rays to cause skin irritation. Meanwhile, the skin static electricity after being smeared with the polysiloxane-containing skin cream is completely eliminated, the dust-proof effect is obvious, the air permeability is good, and the sweat discharge is not affected even if a siloxane film is formed on the skin. The product has slow release and fragrance fixing effects on essence and spice, so that the product has long fragrance retention period, high stability, chemical inertness, no adverse effect on other components of cosmetics, especially active ingredients, and good matching property.
Softening agent
Octyl dodecanol pivalate is an excellent silicone compatibility agent, i.e. compatible with both silicon-containing compounds and hydrocarbons, and is commonly used as a emollient in skin care products.
The phytosterol/octyl dodecanol lauroyl glutamate is an emollient derived from glutamic acid and phytosterol of natural fatty acid, has the property of being easy to form a liquid crystal film like ceramide, is natural, mild and environment-friendly, and has good skin softening effect.
The glyceryl stearate citrate is a nonionic surfactant-ester, and the stearate group has strong degreasing and fat dissolving capabilities, can promote the skin to secrete fat in a short period, and can weaken the resistance of the skin after being excessively used for a long period, so that acne is caused; and the emulsion is widely applied to the field of personal care products, and has the main functions of emulsifying agent and lubricant in cosmetics and skin care products, and has good emulsifying, dispersing and wetting properties.
Cetyl stearyl olive oleate is a natural source emulsifier and is widely applied to cosmetics and skin care products.
The sorbitan olive oleate is a chemical substance, belongs to a nonionic lipophilic emulsifier, and can make emulsion products glossy, creamy, light, thin, easy to absorb and smooth when applied to cosmetics.
PEG-100 stearate has good emulsifying property, and has main function as emulsifying agent in cosmetics and skin care products.
The glyceryl stearate is generally in a solid, semi-solid or thick oil state, has high heat resistance, stability and viscosity, and can be used as an emulsifier and a lubricant to achieve a soft lubricating effect.
Cetostearyl alcohol
Cetyl stearyl alcohol is a fatty alcohol, and appears as white solid crystals, granules or wax blocks, and has a fragrance. The cetyl stearyl alcohol has the advantages of filling the gaps of skin cuticle fragments, smoothing skin texture, softening skin, moisturizing skin, high safety, no toxicity and no harm to skin. The cream is often used as a softener, a thickener, a humectant and an emulsifier, is suitable for various cosmetics, is used as a matrix, and is particularly suitable for cream and emulsion.
Tetradecylamino Ding Xianxie amino amido butyric acid urea trifluoroacetate
Tetradecylamino Ding Xianxie amino acid carbamide trifluoroacetate, abbreviated TAUT, is a tripeptide with smaller molecular weight, which can stimulate the synthesis of collagen up to 300% in vivo, and can improve the quality of collagen fibers, such as decorin (decorin) and zymosan (lumican), by adding some structural skin elements (so-called proteoglycans). By both mechanisms, an effect of counteracting skin laxity and compacting the skin contour is achieved.
The invention adopts active substances such as tannins, reducing substances, cardiac glycoside, flavonoid, neutral resin, acid resin, grease, volatile oil and the like contained in the extract of the rhododendron (RHODODENDRON FERRUGINEUM) of the alpine rose to inhibit and kill various bacteria on the skin, regulate the balance of the pH value of the skin, remove deep dirt and toxin of the skin and have anti-keratinization effect on normal skin and skin infected by acne; the rose extract is distilled from the rose, has the effects of relieving and conditioning skin, effectively improves the vitality of the skin, can effectively nourish the skin, moisten and whiten the skin, improves the vitality of the skin, relieves the listlessness and revitalizes the skin again. The roselle (HIBISCUS SABDARIFFA) extract has good inhibition on tyrosinase and strong antioxidant property, can be used as a whitening agent of cosmetics, has prevention and treatment effects on skin pigmentation, and has the moisturizing effect; the undaria pinnatifida (UNDARIA PINNATIFIDA) extract has an inhibitory effect on the activity of human leukocyte elastase, which indicates that the undaria pinnatifida has an anti-inflammatory function; the soluble collagen can effectively supplement collagen of skin, delay skin aging, recover and keep skin moisture and elasticity, and promote skin smoothness and tenderness. Palmitoyl tripeptide-5 is a small molecular peptide for beautifying and protecting skin, has the characteristic of promoting synthesis of collagen and elastin in dermis, is a skin conditioner, promotes growth of skin cells, inhibits oxygen free radicals and hydroxyl free radicals, and is likely to promote conversion of elastin, hyaluronic acid, glycosaminoglycan and fibronectin; the pseudoalteromonas fermentation product extract is an extracellular polymer obtained in marine unicellular fungus genus through biotechnology, and can effectively reduce redundant oil light and sebum, shrink pores, reduce spots and the like; the white pool flower (LIMNANTHES ALBA) seed oil is one of a plurality of vegetable oils, the white pool flower seed oil contains 98% of long-chain fatty acid and has good oxidation resistance, and the contained desquamation hormone has the effects of preventing water loss and regenerating skin and is a skin metabolism activator. Acetyl heptapeptide-4 is a heptapeptide for strengthening fragile skin by promoting balance and diversity of microbial communities and increasing beneficial bacteria (characteristics of healthy skin in close contact with nature), and acetyl heptapeptide-4 can increase skin beneficial bacteria, improve skin immune response and strengthen integrity of physical barrier, so that the defending system of skin itself can be improved. The microbial community can make the microbial community of urban skin healthier, make the microbial community approach to the microbial community of human ancestor closely contacted with the nature, and can also observe that the cell adhesion is enhanced and the protective effect of the barrier is also enhanced.
Meanwhile, the cleaning agent, the softening agent and the abrasive agent have synergistic effect, so that on one hand, the sharpness of the abrasive agent is improved, the softening agent has soft effect on abrasive particles, the sharpness of the abrasive particles is reduced, and meanwhile, the effects of removing dead skin and preventing skin from being hurt are achieved, and the effect of protecting skin is very good; on the other hand, the addition of the cleaning agent and the interaction of the cleaning agent play a role in buffering, so that the excessive cleaning effect in the bathing process can be effectively relieved, and the effect of cleaning and non-degreasing is achieved.
The rose extract, the roselle extract and the undaria pinnatifida extract natural substances are added in the invention, the plant extracts have the functions of moisturizing and locking water, the plant extracts have the effects of moisturizing and locking water on dry skin, and the plant extracts contain abundant microelements, so that the skin is tender, and can interact with other skin conditioning agents, cleaning agents, softening agents, frosting agents and interactions, and the skin is clear and smooth and mild in touch feeling, and moisturizes the skin when the skin is used.
The skin cleansing cream prepared by the invention has the effects of cleaning the skin surface layer of the bath cream and removing sweat, dust and dirt, also has the effects of deeply cleaning the skin by the cream, such as removing cutin, dead skin and the like and deeply removing dirt, also has the effects and efficacies of body cream, and supplements moisture for the skin, moistens and moisturizes the skin, so that the skin is fine and tender; the skin cleansing scrub prepared by the invention has the effects of three in one of bath cream, scrub and body cream, and has the advantages of clear, smooth and mild touch feeling like water, moisturizing and moisturizing skin, and fresh and non-greasy skin; the product is easy to clean, light and easy to absorb after use, and has the advantages of no stickiness and greasiness, reduced skin fatigue, and light fragrance, and is helpful for sleeping.
The invention also discloses a preparation method of the skin cleansing scrub.
A process for preparing a skin cleansing cream, comprising the steps of:
Step 1, uniformly stirring the phase A substance according to a formula, and heating to 80-85 ℃; adding phase B, mixing uniformly, keeping the temperature of 80-85 ℃ for continuous reaction, adding phase C, mixing uniformly, keeping the temperature of 80-85 ℃ for continuous reaction for 1-10min, vacuumizing, homogenizing for 1-10min with stirring 10000-20000r/min, cooling to 60-65 ℃, finally adding phase D, vacuumizing, mixing uniformly, keeping the temperature of 60-65 ℃ for continuous reaction for 1-10min, cooling to 50-55 ℃, and degassing;
Step 2, discharging: discharging the emulsion after the emulsion is qualified by inspection;
and 3, filling: filling and sealing according to the specified weight after the microorganism is checked to be qualified;
Step 4, inner packaging: spraying codes on the filled packaging bags;
step 5, external packing: packaging the product;
Step 6, warehouse entry: and (5) checking the finished product, and warehousing to obtain the skin cleansing cream.
The invention has the beneficial effects that:
1. According to the invention, the cleaning agent, the softening agent and the abrasive agent act synergistically, so that on one hand, the sharpness of the abrasive agent is improved, the softening agent plays a role in softening abrasive particles, the sharpness of the abrasive agent particles is reduced, and meanwhile, the effects of removing dead skin and preventing skin from being hurt are achieved, and a good skin protection effect is achieved; on the other hand, the addition of the cleaning agent and the interaction of the cleaning agent play a role in buffering, so that the excessive cleaning effect of the shower gel can be effectively relieved, and the effect of cleaning and non-degreasing can be achieved.
2. The skin cleansing cream prepared by the invention has the effects of cleaning the skin surface layer of the bath cream and removing sweat, dust and dirt, also has the effects of deeply cleaning the skin by the cream, such as removing cutin, dead skin and the like and deeply removing dirt, also has the effects and efficacies of body cream, and supplements moisture for the skin, moistens and moisturizes the skin, so that the skin is fine and tender; the skin cleansing scrub prepared by the invention has the effects of three in one of bath cream, scrub and body cream, and has the advantages of clear, smooth and mild touch feeling like water when in use, moistening and moisturizing skin, refreshing and non-greasy skin, light and good absorption after use, non-sticky dressing, and reduced skin fatigue with light fragrance, thereby being beneficial to sleeping.
3. The skin cleansing cream prepared by the invention has the advantages of unique formula, synergistic interaction among various substances, moisturizing, whitening and the like, good cleaning performance, no degreasing, mild removal of horny layer, no stimulation to skin, strong usability, good safety and wide application prospect.
Detailed Description
Sources of the respective substances in the examples:
White pond flower seed oil, goods number: 069 purchased from Jishui county Huayuan perfume oil plants in Jiangxi province.
Ammonium acryloyldimethyl taurate/VP copolymer, pH (1% aqueous solution): 4.0-6.0, viscosity (1% aqueous solution): 48000-80000Mpas, the manufacturer is U.S. Coloranthracene.
Dehydrated xylitol, brand: sanlong original, content/extraction ratio: 10:1, mesh number: 60 mesh purchased from Guangdong Kagao Royal trade Co.
Polydimethyl siloxane, model: FZ-3196, purchased from the company Ji Peng silicon fluorine materials Co., shenzhen City.
PEG-100 stearate, cosmetic grade, purchased from the sea Ann petrochemical plant, jiangsu province.
Cetostearyl alcohol, cosmetic grade, CAS 246159-33-1, purchased from Nanjing Baimuda Biotechnology Inc.
Phytosterol/octyldodecanol lauroyl glutamate, ELDEW PS-203, purchased from Zhenyue (Guangdong) technologies research and development limited.
The silica hydrate is used to hydrate the silica,250PC, particle size: 180-480 μm, cosmetic grade, purchased from Shenzhen New chemical materials, inc.
Caramel color, purchased from shanxi Zhongnuo biotechnology limited.
Acetyl heptapeptide-4, purchased from Nanjing Seiko Biotechnology Co.
CI 14700 is also known as carmine SX, carmine, purchased from Sigma Aldrich trade Inc.
Rose extract, cat No.: ZKD0417, purchased from the western security ida biotechnology limited.
Roselle extract, cat No.: YM-BL369 is purchased from plant technology Co.Ltd.
Undaria pinnatifida extract, product number: 352 purchased from western amp, he bio-technology limited.
Soluble collagen, cat No.: BIO-MARINE COLLAGEN6, purchased from Guangzhou Aibi trade Co.
Palmitoyl tripeptide-5, model: 5433 purchased from Shaanxi Saen Biotech Co.
Fibroin peptide, which is a polypeptide substance formed by degrading silk fibroin protein into water-soluble one, with molecular weight of 100-5000D, purchased from Jinan Meiweida Biotechnology Co.
Example 1
A skin cleansing cream: consists of A phase, B phase, C phase and D phase.
The phase A consists of the following raw materials in parts by weight: 20 parts by weight of water, 3 parts by weight of glycerol, 4 parts by weight of white pool flower (LIMNANTHES ALBA) seed oil, 1 part by weight of dehydrated xylitol, 2 parts by weight of an ammonium acryloyldimethyl taurate/VP copolymer, 1 part by weight of xylitol, 4 parts by weight of a fermentation product extract of pseudoalteromonas, 0.8 part by weight of glucose, 1 part by weight of carbomer, 1 part by weight of fructose, 1 part by weight of octaethylene glycol, 2 parts by weight of tocopherol, 1 part by weight of erythritol;
the phase B consists of the following raw materials: a cleaning agent;
the cleaning agent comprises the following raw materials in parts by weight: 3.3 parts by weight of potassium cocoyl glycinate and 2.5 parts by weight of sodium methyl cocoyl taurate.
The phase C consists of the following raw materials in parts by weight: 0.5 parts by weight isononyl isononanoate, 0.3 parts by weight polydimethylsiloxane, 0.5 parts by weight octyldodecanol pivalate, 0.2 parts by weight cetostearyl alcohol olivetoate, 0.5 parts by weight PEG-100 stearate, 0.1 parts by weight cetostearyl alcohol, 0.3 parts by weight sorbitan olivetoate, 0.1 parts by weight phytosterol/octyldodecanol lauroyl glutamate, 0.1 parts by weight ammonium acryloyldimethyl taurate/behenate polyether-25 methacrylate cross-linked polymer;
The phase D consists of the following raw materials in parts by weight: 0.5 part by weight of inulin, 0.5 part by weight of hydrated silica, 0.2 part by weight of p-hydroxyacetophenone, 0.03 part by weight of (daily) essence, 0.05 part by weight of arginine, 0.08 part by weight of caramel color, 2 parts by weight of rhododendron alpensum (RHODODENDRON FERRUGINEUM) extract, 1 part by weight of acetyl heptapeptide-4, 0.05 part by weight of CI 14700, 0.05 part by weight of tetradecylamino Ding Xianxie amino butyric acid urea trifluoroacetate, 0.5 part by weight of rose (ROSA RUGOSA) flower extract, 1 part by weight of roselle (HIBISCUS SABDARIFFA) extract, 2 parts by weight of Undaria pinnatifida (UNDARIA PINNATIFIDA) extract, 1 part by weight of soluble collagen, and 1 part by weight of palmitoyl tripeptide-5.
The preparation process of the skin cleansing scrub comprises the following steps:
Step 1, uniformly stirring the phase A substance according to a formula, and heating to 85 ℃; adding phase B, mixing uniformly, keeping 85 ℃ for continuous reaction, adding phase C, mixing uniformly, keeping 85 ℃ for continuous reaction for 5min, vacuumizing, stirring and homogenizing for 5min at 10000r/min, cooling to 65 ℃, finally adding phase D, vacuumizing, mixing uniformly, keeping 65 ℃ for continuous reaction for 5min, cooling to 50 ℃, and degassing;
Step 2, discharging: discharging the emulsion after the emulsion is qualified by inspection;
and 3, filling: filling and sealing according to the specified weight after the microorganism is checked to be qualified;
Step 4, inner packaging: spraying codes on the filled packaging bags;
step 5, external packing: packaging the product;
Step 6, warehouse entry: and (5) checking the finished product, and warehousing to obtain the skin cleansing cream.
Example 2
A skin cleansing cream: consists of A phase, B phase, C phase and D phase.
The phase A consists of the following raw materials in parts by weight: 20 parts by weight of water, 3 parts by weight of glycerol, 4 parts by weight of white pool flower (LIMNANTHES ALBA) seed oil, 1 part by weight of dehydrated xylitol, 2 parts by weight of an ammonium acryloyldimethyl taurate/VP copolymer, 1 part by weight of xylitol, 4 parts by weight of a fermentation product extract of pseudoalteromonas, 0.8 part by weight of glucose, 1 part by weight of carbomer, 1 part by weight of fructose, 1 part by weight of octaethylene glycol, 2 parts by weight of tocopherol (vitamin E), 1 part by weight of erythritol;
the phase B consists of the following raw materials: a cleaning agent;
the cleaning agent comprises the following raw materials in parts by weight: 3.3 parts by weight of potassium cocoyl glycinate and 2.5 parts by weight of sodium methyl cocoyl taurate.
The phase C consists of the following raw materials in parts by weight: 0.5 parts by weight isononyl isononanoate, 0.3 parts by weight polydimethylsiloxane, 0.5 parts by weight octyldodecanol pivalate, 0.2 parts by weight cetostearyl alcohol olivetoate, 0.5 parts by weight PEG-100 stearate, 0.1 parts by weight cetostearyl alcohol, 0.3 parts by weight sorbitan olivetoate, 0.1 parts by weight phytosterol/octyldodecanol lauroyl glutamate, 0.1 parts by weight ammonium acryloyldimethyl taurate/behenate polyether-25 methacrylate cross-linked polymer;
The phase D consists of the following raw materials in parts by weight: 0.5 part by weight of inulin, 0.5 part by weight of modified silica, 0.2 part by weight of p-hydroxyacetophenone, 0.03 part by weight of (daily) essence, 0.05 part by weight of arginine, 0.08 part by weight of caramel color, 2 parts by weight of rhododendron alpensum (RHODODENDRON FERRUGINEUM) extract, 1 part by weight of acetyl heptapeptide-4, 0.05 part by weight of CI 14700, 0.05 part by weight of tetradecylamino Ding Xianxie amino butyric acid urea trifluoroacetate, 0.5 part by weight of rose (ROSA RUGOSA) flower extract, 1 part by weight of roselle (HIBISCUS SABDARIFFA) extract, 2 parts by weight of Undaria pinnatifida (UNDARIA PINNATIFIDA) extract, 1 part by weight of soluble collagen, and 1 part by weight of palmitoyl tripeptide-5.
The preparation method of the modified silica comprises the following steps:
s1, uniformly mixing 10 parts by weight of hydrated silica and 2 parts by weight of sodium hydroxide to obtain a mixture;
S2, adding 10 parts by weight of the mixture prepared in the step S1 into 60 parts by weight of glycerol aqueous solution, uniformly mixing, then placing into a hydrothermal kettle, heating to 160 ℃ for reaction for 12 hours, centrifuging to obtain precipitate, washing, drying, and crushing and sieving with 80 meshes to obtain modified silica; the preparation method of the glycerol aqueous solution comprises the step of mixing glycerol and water according to a mass ratio of 3:1.
The preparation process of the skin cleansing scrub comprises the following steps:
Step 1, uniformly stirring the phase A substance according to a formula, and heating to 85 ℃; adding phase B, mixing uniformly, keeping 85 ℃ for continuous reaction, adding phase C, mixing uniformly, keeping 85 ℃ for continuous reaction for 5min, vacuumizing, stirring and homogenizing for 5min at 10000r/min, cooling to 65 ℃, finally adding phase D, vacuumizing, mixing uniformly, keeping 65 ℃ for continuous reaction for 5min, cooling to 50 ℃, and degassing;
Step 2, discharging: discharging the emulsion after the emulsion is qualified by inspection;
and 3, filling: filling and sealing according to the specified weight after the microorganism is checked to be qualified;
Step 4, inner packaging: spraying codes on the filled packaging bags;
step 5, external packing: packaging the product;
Step 6, warehouse entry: and (5) checking the finished product, and warehousing to obtain the skin cleansing cream.
Example 3
A skin cleansing cream: consists of A phase, B phase, C phase and D phase.
The phase A consists of the following raw materials in parts by weight: 20 parts by weight of water, 3 parts by weight of glycerol, 4 parts by weight of white pool flower (LIMNANTHES ALBA) seed oil, 1 part by weight of dehydrated xylitol, 2 parts by weight of an ammonium acryloyldimethyl taurate/VP copolymer, 1 part by weight of xylitol, 4 parts by weight of a fermentation product extract of pseudoalteromonas, 0.8 part by weight of glucose, 1 part by weight of carbomer, 1 part by weight of fructose, 1 part by weight of octaethylene glycol, 2 parts by weight of tocopherol (vitamin E), 1 part by weight of erythritol;
the phase B consists of the following raw materials: a cleaning agent;
the cleaning agent comprises the following raw materials in parts by weight: 3.3 parts by weight of potassium cocoyl glycinate and 2.5 parts by weight of sodium methyl cocoyl taurate.
The phase C consists of the following raw materials in parts by weight: 0.5 parts by weight isononyl isononanoate, 0.3 parts by weight polydimethylsiloxane, 0.5 parts by weight octyldodecanol pivalate, 0.2 parts by weight cetostearyl alcohol olivetoate, 0.5 parts by weight PEG-100 stearate, 0.1 parts by weight cetostearyl alcohol, 0.3 parts by weight sorbitan olivetoate, 0.1 parts by weight phytosterol/octyldodecanol lauroyl glutamate, 0.1 parts by weight ammonium acryloyldimethyl taurate/behenate polyether-25 methacrylate cross-linked polymer;
The phase D consists of the following raw materials in parts by weight: 0.5 part by weight of inulin, 0.5 part by weight of modified silica, 0.2 part by weight of p-hydroxyacetophenone, 0.03 part by weight of (daily) essence, 0.05 part by weight of arginine, 0.08 part by weight of caramel color, 2 parts by weight of rhododendron alpensum (RHODODENDRON FERRUGINEUM) extract, 1 part by weight of acetyl heptapeptide-4, 0.05 part by weight of CI 14700, 0.05 part by weight of tetradecylamino Ding Xianxie amino butyric acid urea trifluoroacetate, 0.5 part by weight of rose (ROSA RUGOSA) flower extract, 1 part by weight of roselle (HIBISCUS SABDARIFFA) extract, 2 parts by weight of Undaria pinnatifida (UNDARIA PINNATIFIDA) extract, 1 part by weight of soluble collagen, and 1 part by weight of palmitoyl tripeptide-5.
The preparation method of the modified silica comprises the following steps:
s1, uniformly mixing 10 parts by weight of hydrated silica and 2 parts by weight of sodium hydroxide to obtain a mixture;
S2, adding 10 parts by weight of the mixture prepared in the step S1 into 60 parts by weight of glycerol aqueous solution, uniformly mixing, then placing in a hydrothermal kettle, heating to 160 ℃ for reaction for 12 hours, centrifuging to obtain precipitate, washing, drying, and crushing and sieving with 80 meshes to obtain pretreated silica powder; the preparation method of the glycerol aqueous solution comprises the steps of mixing glycerol and water according to a mass ratio of 1:1;
S3, adding 5 parts by weight of pretreated silica powder, 3 parts by weight of sodium tripolyphosphate and 2 parts by weight of modifier into 50 parts by weight of water, uniformly mixing, then carrying out crosslinking reaction at room temperature for 30min, centrifuging after the reaction is finished, taking precipitate, washing and drying to obtain modified silica.
The modifier is prepared from ceramide and fibroin peptide according to a mass ratio of 1:1, and mixing.
The preparation process of the skin cleansing scrub comprises the following steps:
Step 1, uniformly stirring the phase A substance according to a formula, and heating to 85 ℃; adding phase B, mixing uniformly, keeping 85 ℃ for continuous reaction, adding phase C, mixing uniformly, keeping 85 ℃ for continuous reaction for 5min, vacuumizing, stirring and homogenizing for 5min at 10000r/min, cooling to 65 ℃, finally adding phase D, vacuumizing, mixing uniformly, keeping 65 ℃ for continuous reaction for 5min, cooling to 50 ℃, and degassing;
Step 2, discharging: discharging the emulsion after the emulsion is qualified by inspection;
and 3, filling: filling and sealing according to the specified weight after the microorganism is checked to be qualified;
Step 4, inner packaging: spraying codes on the filled packaging bags;
step 5, external packing: packaging the product;
Step 6, warehouse entry: and (5) checking the finished product, and warehousing to obtain the skin cleansing cream.
Example 4
A skin cleansing cream: consists of A phase, B phase, C phase and D phase.
The phase A consists of the following raw materials in parts by weight: 20 parts by weight of water, 3 parts by weight of glycerol, 4 parts by weight of white pool flower (LIMNANTHES ALBA) seed oil, 1 part by weight of dehydrated xylitol, 2 parts by weight of an ammonium acryloyldimethyl taurate/VP copolymer, 1 part by weight of xylitol, 4 parts by weight of a fermentation product extract of pseudoalteromonas, 0.8 part by weight of glucose, 1 part by weight of carbomer, 1 part by weight of fructose, 1 part by weight of octaethylene glycol, 2 parts by weight of tocopherol (vitamin E), 1 part by weight of erythritol;
the phase B consists of the following raw materials: a cleaning agent;
the cleaning agent comprises the following raw materials in parts by weight: 3.3 parts by weight of potassium cocoyl glycinate and 2.5 parts by weight of sodium methyl cocoyl taurate.
The phase C consists of the following raw materials in parts by weight: 0.5 parts by weight isononyl isononanoate, 0.3 parts by weight polydimethylsiloxane, 0.5 parts by weight octyldodecanol pivalate, 0.2 parts by weight cetostearyl alcohol olivetoate, 0.5 parts by weight PEG-100 stearate, 0.1 parts by weight cetostearyl alcohol, 0.3 parts by weight sorbitan olivetoate, 0.1 parts by weight phytosterol/octyldodecanol lauroyl glutamate, 0.1 parts by weight ammonium acryloyldimethyl taurate/behenate polyether-25 methacrylate cross-linked polymer;
The phase D consists of the following raw materials in parts by weight: 0.5 part by weight of inulin, 0.5 part by weight of modified silica, 0.2 part by weight of p-hydroxyacetophenone, 0.03 part by weight of (daily) essence, 0.05 part by weight of arginine, 0.08 part by weight of caramel color, 2 parts by weight of rhododendron alpensum (RHODODENDRON FERRUGINEUM) extract, 1 part by weight of acetyl heptapeptide-4, 0.05 part by weight of CI 14700, 0.05 part by weight of tetradecylamino Ding Xianxie amino butyric acid urea trifluoroacetate, 0.5 part by weight of rose (ROSA RUGOSA) flower extract, 1 part by weight of roselle (HIBISCUS SABDARIFFA) extract, 2 parts by weight of Undaria pinnatifida (UNDARIA PINNATIFIDA) extract, 1 part by weight of soluble collagen, and 1 part by weight of palmitoyl tripeptide-5.
The preparation method of the modified silica comprises the following steps:
s1, uniformly mixing 10 parts by weight of hydrated silica and 2 parts by weight of sodium hydroxide to obtain a mixture;
S2, adding 10 parts by weight of the mixture prepared in the step S1 into 60 parts by weight of glycerol aqueous solution, uniformly mixing, then placing in a hydrothermal kettle, heating to 160 ℃ for reaction for 12 hours, centrifuging to obtain precipitate, washing, drying, and crushing and sieving with 80 meshes to obtain pretreated silica powder; the preparation method of the glycerol aqueous solution comprises the steps of mixing glycerol and water according to a mass ratio of 1:1;
S3, adding 5 parts by weight of pretreated silica powder, 3 parts by weight of sodium tripolyphosphate and 2 parts by weight of modifier into 50 parts by weight of water, uniformly mixing, then carrying out crosslinking reaction at room temperature for 30min, centrifuging after the reaction is finished, taking precipitate, washing and drying to obtain modified silica.
The modifier is ceramide.
The preparation process of the skin cleansing scrub comprises the following steps:
Step 1, uniformly stirring the phase A substance according to a formula, and heating to 85 ℃; adding phase B, mixing uniformly, keeping 85 ℃ for continuous reaction, adding phase C, mixing uniformly, keeping 85 ℃ for continuous reaction for 5min, vacuumizing, stirring and homogenizing for 5min at 10000r/min, cooling to 65 ℃, finally adding phase D, vacuumizing, mixing uniformly, keeping 65 ℃ for continuous reaction for 5min, cooling to 50 ℃, and degassing;
Step 2, discharging: discharging the emulsion after the emulsion is qualified by inspection;
and 3, filling: filling and sealing according to the specified weight after the microorganism is checked to be qualified;
Step 4, inner packaging: spraying codes on the filled packaging bags;
step 5, external packing: packaging the product;
Step 6, warehouse entry: and (5) checking the finished product, and warehousing to obtain the skin cleansing cream.
Example 5
A skin cleansing cream: consists of A phase, B phase, C phase and D phase.
The phase A consists of the following raw materials in parts by weight: 20 parts by weight of water, 3 parts by weight of glycerol, 4 parts by weight of white pool flower (LIMNANTHES ALBA) seed oil, 1 part by weight of dehydrated xylitol, 2 parts by weight of an ammonium acryloyldimethyl taurate/VP copolymer, 1 part by weight of xylitol, 4 parts by weight of a fermentation product extract of pseudoalteromonas, 0.8 part by weight of glucose, 1 part by weight of carbomer, 1 part by weight of fructose, 1 part by weight of octaethylene glycol, 2 parts by weight of tocopherol (vitamin E), 1 part by weight of erythritol;
the phase B consists of the following raw materials: a cleaning agent;
the cleaning agent comprises the following raw materials in parts by weight: 3.3 parts by weight of potassium cocoyl glycinate and 2.5 parts by weight of sodium methyl cocoyl taurate.
The phase C consists of the following raw materials in parts by weight: 0.5 parts by weight isononyl isononanoate, 0.3 parts by weight polydimethylsiloxane, 0.5 parts by weight octyldodecanol pivalate, 0.2 parts by weight cetostearyl alcohol olivetoate, 0.5 parts by weight PEG-100 stearate, 0.1 parts by weight cetostearyl alcohol, 0.3 parts by weight sorbitan olivetoate, 0.1 parts by weight phytosterol/octyldodecanol lauroyl glutamate, 0.1 parts by weight ammonium acryloyldimethyl taurate/behenate polyether-25 methacrylate cross-linked polymer;
The phase D consists of the following raw materials in parts by weight: 0.5 part by weight of inulin, 0.5 part by weight of modified silica, 0.2 part by weight of p-hydroxyacetophenone, 0.03 part by weight of (daily) essence, 0.05 part by weight of arginine, 0.08 part by weight of caramel color, 2 parts by weight of rhododendron alpensum (RHODODENDRON FERRUGINEUM) extract, 1 part by weight of acetyl heptapeptide-4, 0.05 part by weight of CI 14700, 0.05 part by weight of tetradecylamino Ding Xianxie amino butyric acid urea trifluoroacetate, 0.5 part by weight of rose (ROSA RUGOSA) flower extract, 1 part by weight of roselle (HIBISCUS SABDARIFFA) extract, 2 parts by weight of Undaria pinnatifida (UNDARIA PINNATIFIDA) extract, 1 part by weight of soluble collagen, and 1 part by weight of palmitoyl tripeptide-5.
The preparation method of the modified silica comprises the following steps:
s1, uniformly mixing 10 parts by weight of hydrated silica and 2 parts by weight of sodium hydroxide to obtain a mixture;
S2, adding 10 parts by weight of the mixture prepared in the step S1 into 60 parts by weight of glycerol aqueous solution, uniformly mixing, then placing in a hydrothermal kettle, heating to 160 ℃ for reaction for 12 hours, centrifuging to obtain precipitate, washing, drying, and crushing and sieving with 80 meshes to obtain pretreated silica powder; the preparation method of the glycerol aqueous solution comprises the steps of mixing glycerol and water according to a mass ratio of 1:1;
S3, adding 5 parts by weight of pretreated silica powder, 3 parts by weight of sodium tripolyphosphate and 2 parts by weight of modifier into 50 parts by weight of water, uniformly mixing, then carrying out crosslinking reaction at room temperature for 30min, centrifuging after the reaction is finished, taking precipitate, washing and drying to obtain modified silica.
The modifier is fibroin peptide.
The preparation process of the skin cleansing scrub comprises the following steps:
Step 1, uniformly stirring the phase A substance according to a formula, and heating to 85 ℃; adding phase B, mixing uniformly, keeping 85 ℃ for continuous reaction, adding phase C, mixing uniformly, keeping 85 ℃ for continuous reaction for 5min, vacuumizing, stirring and homogenizing for 5min at 10000r/min, cooling to 65 ℃, finally adding phase D, vacuumizing, mixing uniformly, keeping 65 ℃ for continuous reaction for 5min, cooling to 50 ℃, and degassing;
Step 2, discharging: discharging the emulsion after the emulsion is qualified by inspection;
and 3, filling: filling and sealing according to the specified weight after the microorganism is checked to be qualified;
Step 4, inner packaging: spraying codes on the filled packaging bags;
step 5, external packing: packaging the product;
Step 6, warehouse entry: and (5) checking the finished product, and warehousing to obtain the skin cleansing cream.
Test example 1
Cleaning performance test: a layer of 1cm 3 color cosmetics is coated on a 3M breathable adhesive tape with the thickness of 1cm x 3cm, the weight is weighed, the skin cleansing cream with the weight of 1cm 3 is taken to carry out friction for 2min, the adhesive tape is washed by clean water and then dried, the weight is weighed, and the residual amount of the color cosmetics is calculated. The net weight of the 3M breathable tape was 0.8g, 1cm by 3 cm.
Skin cleansing scrub cleanliness= (weight of adhesive tape before use-weight of adhesive tape after use)/(weight of adhesive tape before use-net weight of adhesive tape)
Table 1 results of cleaning performance test of skin cleansing cream
As is clear from Table 1, the cleaning performance of example 2 is significantly better than that of example 1, probably because the silica is treated with sodium hydroxide, so that part of the silicon hydroxyl groups on the surface of the silica are recovered in the calcination procedure, the specific surface area of the silica is increased, the adsorption of the silica to dirt and cutin is improved, and the cleaning performance is further improved.
The cleaning performance of example 3 is significantly better than that of example 2, probably because the inventors treated silica with sodium hydroxide restored part of the silica surface silicon hydroxyl groups during the firing protocol, increased the specific surface area of the silica, and further improved the cleaning performance. The silica hardness is high, edges and corners are sharp, skin is damaged in the using process, the inventor further adopts sodium tripolyphosphate, ceramide and fibroin peptide to modify the silica, on one hand, the ceramide and the fibroin peptide are wrapped on the surface of the silica, so that the soft feeling of walnut shell particles is improved, the sharp edges and corners are prevented from scratching the skin, meanwhile, the ceramide and the fibroin peptide have the effects of moisturizing and moistening the skin, and have good repairing and protecting effects on the skin, and the silica is adopted to adsorb dirt, cutin and cosmetic residues on the surface of the skin, so that sebaceous gland and sweat gland channel blockage is improved, the skin is clean, degreasing is avoided, and the normal skin barrier function is maintained; on the other hand, the silica is uniformly dispersed in the scrub and does not precipitate. And the silica gradually releases grease and nutrient substances in the sanding process, so that the aged cutin is promoted to be separated from the skin.
The cleaning performance of the embodiment 3 is obviously superior to that of the embodiments 4-5, and the possible reasons are that the synergistic effect of the ceramide and the fibroin peptide is wrapped on the surface of silica, so that the tenderness of walnut shell particles is improved, sharp edges and corners are avoided to scratch skin, meanwhile, the ceramide and the fibroin peptide have the effects of moisturizing and moistening skin, have good repairing and protecting effects on the skin, adsorb dirt, cutin and cosmetic residues on the surface of the skin by adopting silica, improve sebaceous gland and sweat gland channel blockage, ensure that the skin is clean and is not degreased, and can maintain normal skin barrier function; on the other hand, the silica is uniformly dispersed in the scrub and does not precipitate. And the silica gradually releases grease and nutrient substances in the sanding process, so that the aged cutin is promoted to be separated from the skin.
Test example 2
Sensory evaluation: the skin cleansing cream prepared in each example was distributed to 150 testers for use, 30 testers per group (randomly distributed), and the testers used the skin cleansing cream in the same manner for 4 weeks and 2 times a week. The tester scores according to his own feeling.
The scoring criteria used 10 points, 1 point being the worst, 10 points being the best, the higher the score the better.
Table 2 sensory evaluation test results of skin cleansing cream
As shown in Table 2, the skin cleansing cream prepared by the invention has good cleaning performance, the skin cleansing cream prepared by the invention takes the rhododendron (RHODODENDRON FERRUGINEUM) extract, the undaria pinnatifida (UNDARIA PINNATIFIDA) extract, the soluble collagen, the palmitoyl tripeptide-5, the acetyl heptapeptide-4, the white pond flower (LIMNANTHES ALBA) seed oil, the squalane and the pseudoalteromonas fermentation product extract as main active components, and the substances are mutually cooperated, so that the skin cleansing cream has good effects of resisting bacteria, diminishing inflammation, relieving itching, cleaning skin and the like, has the effects of moisturizing, whitening and the like, and is mild in horny layer removal, free of irritation to skin, strong in usability and good in safety.
Claims (4)
1. A skin cleansing cream comprising: cleaning agents, abrasive agents and emollients; the cleaning agent is an anionic surfactant, a zwitterionic surfactant or a nonionic surfactant; the softening agent is grease or silicone oil; comprises 1.2 to 10.3 weight parts of cleaning agent, 1 to 7 weight parts of frosting agent and 1.2 to 10 weight parts of softening agent; the abrasive agent is modified silica;
The preparation method of the modified silica comprises the following steps:
S1, uniformly mixing 5-10 parts by weight of hydrated silica and 1-2 parts by weight of sodium hydroxide to obtain a mixture;
S2, adding 5-10 parts by weight of the mixture prepared in the step S1 into 60-100 parts by weight of glycerol aqueous solution, uniformly mixing, then placing into a hydrothermal kettle, heating to 120-160 ℃ for reacting for 12-24 hours, centrifuging to obtain precipitate, washing, drying, and crushing to 80-100 meshes to obtain pretreated silica powder; the preparation method of the glycerol aqueous solution comprises the steps of mixing glycerol and water according to the mass ratio of (1-3);
S3, adding 3-5 parts by weight of pretreated silica powder, 1-3 parts by weight of sodium tripolyphosphate and 0.5-2 parts by weight of modifier into 50-80 parts by weight of water, uniformly mixing, then carrying out crosslinking reaction at room temperature for 10-40min, centrifuging after the reaction is finished, taking precipitate, washing and drying to obtain modified silica;
the modifier is one or more than two of ceramide and fibroin peptide.
2. The skin cleansing cream of claim 1, wherein: the cleaning agent is one or more than two of sodium methyl cocoyl taurate, potassium cocoyl glycinate and xylitol-based glucoside.
3. The skin cleansing cream of claim 1, wherein: the softening agent is one or more than two of isononyl isononanoate, polydimethylsiloxane, octyl dodecanol pivalate and phytosterol/octyl dodecanol lauroyl glutamate.
4. The skin cleansing cream of claim 1, wherein: comprises a phase A, a phase B, a phase C and a phase D; wherein:
the phase A comprises the following raw materials: a humectant, a thickener, and a solvent;
the phase B comprises the following raw materials: a cleaning agent;
the phase C comprises the following raw materials: a emollient and an emulsifier;
The phase D comprises the following raw materials: antioxidants, preservatives, fragrances, pH adjusters, colorants, skin conditioning agents, and abrasive agents.
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