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CN1525942A - 一种超细的改性氢氧化铝及其制备方法 - Google Patents

一种超细的改性氢氧化铝及其制备方法 Download PDF

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Publication number
CN1525942A
CN1525942A CNA018198430A CN01819843A CN1525942A CN 1525942 A CN1525942 A CN 1525942A CN A018198430 A CNA018198430 A CN A018198430A CN 01819843 A CN01819843 A CN 01819843A CN 1525942 A CN1525942 A CN 1525942A
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aluminum hydroxide
aluminium hydroxide
modified
present
particle size
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CN1232443C (zh
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½
陈建峰
郭奋
梁磊
沈志刚
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Beijing University of Chemical Technology
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Beijing University of Chemical Technology
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    • C—CHEMISTRY; METALLURGY
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    • C01F7/00—Compounds of aluminium
    • C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
    • C01F7/04—Preparation of alkali metal aluminates; Aluminium oxide or hydroxide therefrom
    • C01F7/14—Aluminium oxide or hydroxide from alkali metal aluminates
    • C01F7/141—Aluminium oxide or hydroxide from alkali metal aluminates from aqueous aluminate solutions by neutralisation with an acidic agent
    • C01F7/142—Aluminium oxide or hydroxide from alkali metal aluminates from aqueous aluminate solutions by neutralisation with an acidic agent with carbon dioxide
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    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
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    • C—CHEMISTRY; METALLURGY
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    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/74—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by peak-intensities or a ratio thereof only
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  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)

Abstract

本发明为一种超细改性氢氧化铝的制备方法。由在旋转床超重力条件下的碳分分解和改性处理两道步骤组成，本发明的碳分分解反应在旋转床的多孔填料层中进行，极大地强化了反应的传质及微观混合过程，随后的改性处理过程使得到的氢氧化铝凝胶(沉淀或/和干粉)进一步转化。可实现对氢氧化铝改性晶粒大小的控制、粒度分布均匀、反应时间短，尤其是改性处理过程大大提高了其失重温度，失重率，极大地扩大了氢氧化铝作为阻燃剂等的使用范围。得到的改性氢氧化铝颗粒平均粒径可在50nm到几个微米间变化并可控，粒径分布均匀，颗粒纳米化，可提高聚合物的力学性能。本发明的方法易于工业化，可大幅度地提高生产效率及产品品位。

Description

PCT国内申请，说明书已公开。

Claims (1)

  1. PCT国内申请，权利要求书已公开。
CNB018198430A 2001-05-18 2001-05-18 一种超细的改性氢氧化铝及其制备方法 Expired - Fee Related CN1232443C (zh)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/CN2001/000810 WO2002094715A1 (fr) 2001-05-18 2001-05-18 Hydroxyde d'aluminium modifie ultrafin et sa preparation

Publications (2)

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CN1525942A true CN1525942A (zh) 2004-09-01
CN1232443C CN1232443C (zh) 2005-12-21

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US (1) US20050167641A1 (zh)
CN (1) CN1232443C (zh)
WO (1) WO2002094715A1 (zh)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100348490C (zh) * 2005-01-06 2007-11-14 北京化工大学 一种超细针须状改性氢氧化铝及其制备方法
CN100460481C (zh) * 2005-10-12 2009-02-11 中国矿业大学（北京校区） 一种磷酸锌包覆氢氧化铝型复合无机阻燃剂的制备方法
CN107814400A (zh) * 2017-12-04 2018-03-20 中国恩菲工程技术有限公司 氢氧化铝的分级处理工艺
CN112662088A (zh) * 2020-12-10 2021-04-16 界首市鑫豪塑胶有限公司 一种阻燃型pvc/nbr橡塑地板材料及其加工方法

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CN1313378C (zh) * 2002-09-24 2007-05-02 北京化工大学 制备钛酸锶粉体的方法
US7790088B2 (en) * 2005-06-23 2010-09-07 The Boeing Company Fire resistance for optically transparent thermoplastics
CN100395185C (zh) * 2005-11-22 2008-06-18 华东理工大学 超细氢氧化铝的制备方法
CN100462304C (zh) * 2005-12-28 2009-02-18 财团法人工业技术研究院 特定晶型的氢氧化铝晶粒的制备方法
CN101837999B (zh) * 2010-06-10 2012-08-01 中国铝业股份有限公司 一种β型氢氧化铝的制备方法
CN103801242B (zh) * 2012-11-03 2015-12-02 中国石油化工股份有限公司 反应器和利用这种反应器的烷基化反应方法
CN104591243B (zh) * 2015-02-03 2017-05-31 青岛农业大学 一种制备氢氧化铝微粉联产碳酸钾的方法
CN105400267A (zh) * 2015-12-17 2016-03-16 江苏省常熟环通实业有限公司 一种复合型氧化铁防锈颜料及其制备方法
CN108484150A (zh) * 2018-03-30 2018-09-04 胡果青 一种致密型高导热陶瓷基板的制备方法
CN108905895B (zh) * 2018-06-06 2021-01-12 浙江海洋大学 一种快速水热合成装置及方法
CN109279876A (zh) * 2018-09-21 2019-01-29 佛山皖和新能源科技有限公司 一种导热型陶瓷基板的制备方法
CN110655095B (zh) * 2019-10-16 2021-11-30 淄博鹏丰新材料科技有限公司 一种低吸油值氢氧化铝微粉阻燃剂的制备方法
CN112830508A (zh) * 2021-01-29 2021-05-25 郑州大学 一种利用铝灰脱氮固氟熟料制备氢氧化铝的方法
CN115818681B (zh) * 2022-12-12 2024-01-23 洛阳中超新材料股份有限公司 一段法制备单晶大颗粒氢氧化铝的方法

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100348490C (zh) * 2005-01-06 2007-11-14 北京化工大学 一种超细针须状改性氢氧化铝及其制备方法
CN100460481C (zh) * 2005-10-12 2009-02-11 中国矿业大学（北京校区） 一种磷酸锌包覆氢氧化铝型复合无机阻燃剂的制备方法
CN107814400A (zh) * 2017-12-04 2018-03-20 中国恩菲工程技术有限公司 氢氧化铝的分级处理工艺
CN112662088A (zh) * 2020-12-10 2021-04-16 界首市鑫豪塑胶有限公司 一种阻燃型pvc/nbr橡塑地板材料及其加工方法
CN112662088B (zh) * 2020-12-10 2023-03-31 安吉天则塑业有限公司 一种阻燃型pvc/nbr橡塑地板材料及其加工方法

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US20050167641A1 (en) 2005-08-04
WO2002094715A1 (fr) 2002-11-28
CN1232443C (zh) 2005-12-21

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