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CN102038716A - Traditional Chinese medicine extraction method and special device - Google Patents

Traditional Chinese medicine extraction method and special device Download PDF

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Publication number
CN102038716A
CN102038716A CN2009101536848A CN200910153684A CN102038716A CN 102038716 A CN102038716 A CN 102038716A CN 2009101536848 A CN2009101536848 A CN 2009101536848A CN 200910153684 A CN200910153684 A CN 200910153684A CN 102038716 A CN102038716 A CN 102038716A
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chinese medicine
liquid
collection chamber
traditional chinese
chamber
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CN102038716B (en
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吴江平
周脱牛
秦云飞
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Abstract

The invention provides a novel traditional Chinese medicine extraction method and a special device. The method comprises the following steps of: (1) placing moisturized traditional Chinese medicines in a closed container, heating the closed container by using an external fire source till the traditional Chinese medicines are charred, and condensing and recovering the exhausted gas to obtain a coarse liquid of the traditional Chinese medicines; and (2) precipitating the coarse liquid obtained in the step (1), taking the supernatant liquid for distilling, taking the distillation liquid of 98-103 DEG C fractions, absorbing by activated carbon, filtering by filter paper, and taking the filter liquid to obtain the traditional Chinese medicine extraction liquid. The invention has the main advantages that a completely new traditional Chinese medicine extraction method is provided by the invention, the traditional Chinese medicine extraction liquid obtained by using the method of the invention has long storage time, fewer toxic and side effects, good taste and greatly improved curative effects on diseases, a basic platform for further improving curative effects of traditional Chinese medicinal herbs, normalizing formulations and overcoming difficult miscellaneous diseases of human is provided, and the foundation is laid for applying the traditional Chinese medicine by all nations around the world, increasing the international status of the traditional Chinese medicine and exploring the traditional Chinese medicine.

Description

A kind of Chinese medicine extraction method and special equipment
(1) technical field
The present invention relates to a kind of Chinese medicine extraction method and reach the special equipment that extracts Chinese medicine with this method.
(2) background technology
Chinese medicine is the rarity of China's traditional national culture, special culture, history, national background are arranged, cause traditional Chinese medical science school many, be a disciple of different, yet numerous just academic school to benefiting our pursuits in the Chinese medicine and pharmacy theory and practice, the medicine in the Chinese medicine and pharmacy more need grind deeply debates disease opinion and controls, dedicate itself to innovation, the side's of choosing medication silk silk people button should be followed traditional prescription and application of principle, pays attention to again drawing visiting and grinds new achievement in research.The tcm theory organic conception is looked artificial an organic whole, with the heart, liver, spleen, lung, kidney five big systems notion, and with closely related naturally, completely becomes integral body.By negative and positive, QI and blood internal organs, systems such as meridians, the physiology of human body, pathology, inside and outside, up and down, device matter, function, spirit material body environment etc. are unified as a whole, adopted process of preparing Chinese medicine prescription decocting Chinese medicine that the vital organs of the human body of human body are unclogged and readjusted and transferred the doctor, yet medicine often is tending towards flat to the disease effect in the human body, dose is big, mouthfeel is poor, be difficult to swallow, difficulty can be seen special effect, directly wipes out the crux of difficult miscellaneous diseases, adding decocting side's soup with tradition like this often is difficult to prove effective, execute that to add opinion in the process of controlling again different, lack standard, at same disease, executing in the process of controlling prescription often of living in executes to control to disease opinion is respectively arranged, vary with each individual, the doctor of institute drug effect is had nothing in common with each other, but " natural green " in the Chinese medicine is again a referential valuable part, natural resources of Chinese medicinal materials spreads all over all over the world in addition, have find to utilize with undiscovered application.It is most complete that China find to use in this field, has a whole set of Chinese medicine culture to be worth our succession and develops.Simultaneously, it is perfect that Chinese medicine needs new extracting method, and substantial Chinese medical culture is also very urgent.
At present, yet there are no with the book on Chinese herbal medicine in the Chinese medicine, ore deposit, mountain stone, water, animal drugs and carry out carbonization, collect the condensation of gas extracting liq to prolong its holding time, to improve the report of its drug effect.
(3) summary of the invention
The object of the invention provides a kind of new Chinese medicine extraction method and uses the special equipment that this method is extracted Chinese medicine, and is long with the Chinese medicine extraction liquid resting period that this method obtains, toxic and side effects is few, mouthfeel good, the treatment curative effect of disease is good.
The technical solution used in the present invention is:
A kind of Chinese medicine extraction method comprises:
(1) Chinese medicine (comprising animals and plants, ore deposit, mountain stone, water class medicine) through soaking into is placed hermetic container, with outside burning things which may cause a fire disaster hermetic container being burnt is heated to the Chinese medicine carbonization, and expellant gas reclaims through condensation and obtains the thick liquid of Chinese medicine; The thick liquid great majority of described Chinese medicine are water white transparency, the smoked smell of burning is arranged, usually after irradiate light, become light yellow, but do not influence result of use, the thick liquid of Chinese medicine includes a certain amount of organic acid, alcohol, phenol, amine etc., as adding mine stone medicine, the liquid composition also contains metallic chemical elements such as a certain amount of copper, ferrum;
(2) the thick liquid of step (1) gained Chinese medicine staticly settles, gets the supernatant distillation; get the distillate of 98~103 ℃ of fractions; through activated carbon adsorption (needing more than 2 hours usually), filter paper filtering; get filtrate; promptly get Chinese medicine extraction liquid; usually the addition of active carbon is 10~50% of a distillate quality, also can be excessive.
Concrete, the coprecipitation mode of described step (2) comprises two kinds, by first kind of intermediate processing, (20 is as follows: the thick liquid of step (1) gained Chinese medicine leaves standstill half an hour~3 day (not producing acid in this process) to step, get the supernatant distillation, get the distillate of 98~103 ℃ of fractions, through activated carbon adsorption, filter paper filtering, get filtrate, promptly get Chinese medicine extraction liquid.
Plant intermediate processing by (2), described step (2) is as follows: the thick liquid of step (1) gained Chinese medicine places hermetic container to leave standstill 3 months~5 and produces acid (must leave standstill more than 3 months and just may produce acid) per year, get the supernatant distillation, get the distillate of 98~103 ℃ of fractions, through activated carbon adsorption, filter paper filtering, get filtrate, promptly get Chinese medicine extraction liquid.
Described Chinese medicine can be fresh collection, without the former medicine of concocting of Chinese medicine, or, also can be the prepared slices of Chinese crude drugs of concocting according to official method without the dry crude drug of concocting.Record now in that " all available the inventive method of all single medicinal materials in the Chinese pharmacopoeia is extracted, and extracting mode of the present invention also is applicable to and carries the Chinese prescription that certain proportioning is formed.
Gained Chinese medicine extraction liquid liquid water white transparency has smoke flavour, becomes light yellowly to rice-pudding yellow after irradiate light, tastes acid, puckery, includes organic acid, alcohol, phenol, amine etc., and Chinese medicine contains metallic chemical elements such as a certain amount of copper, ferrum if any ore deposit, mountain stone medicine.The present invention adopts outside burning things which may cause a fire disaster that Chinese medicine is carried out carbonization, and is different with the Chinese medicine extracting method, and it is many to obtain effective ingredient, the extraction efficiency height, disappearance is few, and gained Chinese medicine extraction liquid molecular structure diminishes, be more conducive to absorption of human body, thereby promote the treatment disease to promote the effect of medicine.
According to the Chinese medicine extraction liquid that the inventive method obtains, the resting period is long, and toxic and side effects is few, and mouthfeel is good, and the treatment curative effect of disease improves greatly, can add other pharmaceutic adjuvant, makes each section's treatment that unguentum, tablet, liquor, spray and pill are used for human diseases.
The invention still further relates to the special equipment that the thick liquid of preceding method Chinese medicine extracts, described equipment comprises: the airtight carbonization chamber of calcining Chinese medicine, and the collection chamber of the flue gas that collection Chinese medicine forms when carbonization, described carbonization chamber below is provided with the combustion furnace; The inner chamber of described carbonization chamber communicates with described collection chamber inner chamber by airway, described airway can be provided with a plurality of, be evenly arranged in the described collection chamber inner chamber, common described airway extend into collection chamber height 1/3 place, to prevent that liquid from pouring in down a chimney to carbonization chamber, described collection chamber top is provided with and the airtight lid that is connected of described collection chamber, described lid is the cooling back installation that is provided with cooling water inlet A and coolant outlet A, it is the cooling pan of liquid that the periphery of described collection chamber is provided with the flue gas condensing in the described collection chamber, described cooling pan is provided with cooling water inlet B and coolant outlet B, described collection chamber is arranged in the cooling pan, the bottom of described collection chamber is provided with the sharp mouth shape liquid outlet that the thick liquid of Chinese medicine is discharged, and the bottom that described liquid outlet passes cooling pan communicates with atmosphere.Around the collection chamber of the present invention and top is provided with cooling device, more helps the condensation of flue gas, and it is divided into two parts, can be convenient to dismounting, clean.Liquid outlet of the present invention is sharp mouth shape, and certain length is arranged, mainly be to guarantee that the thick liquid of Chinese medicine of flue gas condensing one-tenth can form the liquid sealing of certain altitude at sharp mouth shape liquid outlet place, can guarantee collection chamber and atmospheric sealing so on the one hand, can make on the other hand to condense into the thick liquid of Chinese medicine and flow out fast.
Recommend described collection chamber to be annular, described liquid outlet can be provided with a plurality of, be evenly arranged in described annular gas-collecting chamber bottom, the bottom center arch of described collection chamber is bell jar shape projection to increase the heat exchange area of described collection chamber and cooling water, accelerates the condensation rate of flue gas.
The gap is left in described bell jar shape rising height and described lid bottom.
Further, the part that described lid and described collection chamber interlock is down the pot type, the bell jar shape rising height of described collection chamber is concordant with the height of the coolant outlet B of cooling pan, can make the contact area of collection chamber and cooling pan and condensing unit bigger like this, can allow flue gas condensing form the thick liquid of Chinese medicine fast.
Described cooling water inlet A is arranged on described lid bottom, and described coolant outlet A is arranged on described lid top, and described cooling water inlet B is arranged on described cooling pan bottom, and described coolant outlet B is arranged on described cooling pan top.This is the structure of most chillers, and the present invention does not get rid of the arrangement mode of other chiller yet, as long as can allow cooling pan and chiller performance condensation efficiency.
Described carbonization chamber comprises staving and bung, described bung and described staving are tightly connected, because of incendiary temperature higher, the mode of existing employing sealing gasket can't satisfy the present invention, therefore the present invention does not adopt the seal with elastometic washer mode, need to adopt the rigidity fit system, can be provided with the hold-down mechanism that described bung is compressed to described staving on the described bung, cover because of chamber pot as far as possible in addition and the smooth slit of not staying of contact surface of staving.It is the cross bar that both ends are provided with snap ring that the present invention recommends described hold-down mechanism, but described cross bar is provided with the clamp nut of up-down adjustment, and described staving is provided with the shelves part that cooperates with described snap ring.When being used for bung and staving and compressing, the snap ring of hold-down mechanism is cooperated with a shelves part, and the height by adjusting nut applies a big downward pressure, makes staving and bung seal, a plurality of nuts can be arranged on the described cross bar, the compactness of bung and staving can be strengthened like this; Hold-down mechanism also can be established two cross bars, be arranged to the cross type, corresponding snap ring all has two pairs with the shelves part, is evenly arranging height-adjustable nut on the cross bar of cross type, the compactness of bung and staving is strengthened, thoroughly reached the purpose of sealing.
During concrete operations, to put into carbonization chamber through the Chinese medicine that soaks into earlier, arrange airway, make it to stretch into staving and collection chamber, the snap ring of hold-down mechanism is cooperated with the shelves part, the height of adjusting nut compresses bung and staving, and cooperates lid and collection chamber are airtight, open the cooling water of cooling pan and chiller, light the combustion furnace, the Chinese medicine in the staving carbonization chamber is fired to carbonization, the flue gas that carbonization is produced imports in the collection chamber, under the effect of chiller, flue gas in the collection chamber formation medicinal liquid that is condensed is discharged by liquid outlet, the convenient collection.
Chinese medicine extraction method major advantage of the present invention is as follows:
1, Chinese medicine extraction method of the present invention has thoroughly changed traditional Chinese medicine extraction mode, the dissolubility of pharmaceutically active ingredient during this extracting mode can improve, promote the change of molecular structure, strengthen the activity of medicine, weaken zest, improve inhibitory effect, played conclusive effect for reducing antibiotic use, also be that the Chinese medicine processing method has been carried out revolutionary change, for the Chinese medicine processing extracting method has been opened brand-new approach.
2, Chinese medicine extraction method of the present invention prolongs greatly to holding time of Chinese medicine, removed the worry that medicinal cupping is everyday boiled medicine from, stablized the property of medicine, standard prescription, for future Chinese patent medicine go abroad and provide the foundation.
3, Chinese medicine extraction method of the present invention has been carried out hydrolysis to some drug toxicities, in the toxic and side effects that has alleviated the property of medicine in varying degrees greatly, makes Chinese medicine really become " the green treasure-house " of world's human diseases medicinal application.
4, Chinese medicine extraction method of the present invention has improved its curative effect greatly, and to difficult miscellaneous diseases in the world, platform base has been established on the road that the exploration of incurable disease is captured.
5, Chinese medicine extraction method of the present invention is strengthened national medicine inspection department to the management in Chinese medicine market decompression for standard, and effect is played in the Chinese medicine quality inspection standard bar position of halting.
6, Chinese medicine extraction method of the present invention has a prevention effect at market is at random.To scale, Chinese patent medicine is produced in intensification leading effect, for future Chinese people to people of the world's diseases prevention, cure the disease, reduce drug contamination and contribute.
Beneficial effect of the present invention is mainly reflected in: the invention provides a kind of brand-new Chinese medicine extraction method, Chinese medicine extraction liquid according to the inventive method acquisition, resting period is long, toxic and side effects is few, mouthfeel is good, and the treatment curative effect of disease improves greatly, for Chinese herbal medicine further improves curative effect, standard prescription and capture among the mankind difficult miscellaneous diseases platform that provides the foundation has been explored the new approaches of Chinese medicine in preparation process.Chinese medicine goes to the world and is used by various countries, improves status and the Chinese medicine exploration of Chinese medicine in the world and lays a good foundation.
(4) description of drawings
Fig. 1 is the cutaway view of present device.
(5) specific embodiment
The present invention is described further below in conjunction with specific embodiment, but protection scope of the present invention is not limited in this:
The thick liquid extraction element of Chinese medicine is referring to accompanying drawing 1 among the embodiment:
Described equipment comprises: the airtight carbonization chamber 1 of calcining Chinese medicine, and the collection chamber 2 of the flue gas that collection Chinese medicine forms when carbonization, described carbonization chamber below is provided with the combustion furnace; The inner chamber of described carbonization chamber communicates with described collection chamber inner chamber by airway 3, described airway is provided with 6, be evenly arranged in the described collection chamber inner chamber, described airway extend into 1/3rd places of collection chamber height, described collection chamber top is provided with and the airtight lid that is connected of described collection chamber, described lid is the cooling back installation 41 that is provided with cooling water inlet 51 and coolant outlet 61, it is the cooling pan 42 of liquid that the periphery of described collection chamber is provided with the flue gas condensing in the described collection chamber, described cooling pan is provided with cooling water inlet 52 and coolant outlet 62, and described collection chamber is arranged in the cooling pan.Described collection chamber is an annular, and the bottom center arch of described collection chamber is bell jar shape projection to increase the heat exchange area of described collection chamber and cooling water, accelerates the condensation rate of flue gas.The bottom of described collection chamber is provided with the sharp mouth shape liquid outlet 21 that the thick liquid of Chinese medicine is discharged, and sharp mouth shape liquid outlet is provided with 4, is evenly distributed on annular collection chamber bottom, and described liquid outlet communicates with atmosphere.
The gap is left in described bell jar shape rising height and described lid bottom.
The part that described lid and collection chamber interlock is down the pot type, and described pot type the bottom of a pan part 411 forms the top cover of described collection chamber 2, and the sidewall 22 of described lid and described collection chamber 2 is tightly connected.Contacted of lid and collection chamber are smooth, use the screw bolt tight on every side, the bell jar shape rising height of described collection chamber is concordant with the height of the coolant outlet 62 of cooling pan, can make flue gas and cooling water in the collection chamber that bigger contact area is arranged like this, makes the flue gas rapid condensation become the thick liquid of Chinese medicine.
Described cooling water inlet 51 is arranged on described lid bottom, described coolant outlet 52 is arranged on described lid top, described cooling water inlet 61 is arranged on described cooling pan bottom, and described coolant outlet 62 is arranged on described cooling pan top.
Described carbonization chamber 1 comprises staving 11 and bung 12, and described bung 12 is tightly connected with described staving 11, and described bung 12 tops are provided with the hold-down mechanism that described bung 12 is compressed to described staving 11.
The described hold-down mechanism of described hold-down mechanism is the cross bar 71 that both ends are provided with snap ring 73, but described cross bar is provided with the clamp nut 72 of up-down adjustment, and described staving is provided with the shelves part 74 that cooperates with described snap ring.When being used for bung and staving and compressing, the snap ring of hold-down mechanism is cooperated with a shelves part, and the height by adjusting nut applies a big downward pressure, makes staving and bung seal, evenly arrange a plurality of nuts on the described cross bar, can strengthen the compactness of bung and staving like this.
The thick liquid extracting method of Chinese medicine: during concrete operations, to put into carbonization chamber 1 through the Chinese medicine that soaks into earlier, arrange airway, make it to stretch into staving (carbonization chamber) and collection chamber 2, the snap ring of hold-down mechanism is cooperated with the shelves part, the height of adjusting nut compresses bung and staving, and cooperates lid and collection chamber are airtight, open the cooling water of cooling pan and chiller, light the combustion furnace, the Chinese medicine in the staving carbonization chamber is fired to carbonization, the flue gas that carbonization is produced imports in the collection chamber, under the effect of chiller, flue gas in the collection chamber formation medicinal liquid that is condensed is discharged by liquid outlet, the convenient collection.
Embodiment 1:
1, prescription (single card dosage): Herba Ephedrae 12g, Ramulus Cinnamomi 20g, Semen Armeniacae Amarum 20g, Radix Glycyrrhizae 50g;
2, the effect of medicine: relieving the exterior syndrome by diaphoresis, no perspiration but asthma, the headache body is painful;
3, method:
1. decocting instructions about how to take medicine:
By above-mentioned prescription 10 patch amounts, get the prepared slices of Chinese crude drugs and add the 750g decocting and boiled 2 hours, decocting liquid; 300~400cc once swallows clothes, pharynx every day clothes 3 times, and swallow the liquid total amount of taking medicine every day is 900~1200cc;
2. extraction method of the present invention:
By above-mentioned prescription 10 patch amounts, the prepared slices of Chinese crude drugs are placed on water infiltration in the carbonization chamber of extraction equipment shown in Figure 1, open the combustion furnace, be fired to the Chinese medicine carbonization, collect by liquid outlet and obtain thick liquid; After thick liquid places hermetic container to leave standstill 3 months, get the supernatant distillation, get the distillate of 98~103 ℃ of fractions,, get filtrate, promptly get Chinese medicine extraction liquid through activated carbon adsorption (6 hours), filter paper filtering.4, purpose: the 1. curative effect of first and second liang of group control drug, 2. mouthfeel, the 3. amount agent, the time of 4. depositing of pharynx clothes;
Ma, 27 years old, regular flu, the past decocting soup side drink more, ordinary circumstance is used the above-mentioned prescription usefulness that is decocted in water for oral dose, cold symptoms could disappear more than seven days, the decoction dose is more than 200cc, the mouthfeel suffering is swallowed, and need boil medicine everyday; The back adopts same prescription to extract medicinal liquid pharynx clothes with the inventive method, cold symptoms just can disappear on the 3rd day as a result, and each dose reduces, only drink 50cc, mouthfeel is also with a kind of fragrant, the Chinese medicine that new extraction method is extracted is because have resting period advantage of a specified duration, do not have mycete, rotten over a year yet,, removed the worry of everyday boiling medicine from getting with drinking.
Embodiment 2:
Usually, after bright ginseng is received, boil to dry and be processed into Radix Ginseng Rubra, bright ginseng is dried and is called Radix Ginseng.Need when eating ginseng the Radix Ginseng section to be stewed the ginseng sheet for a long time with slow fire water again, special expend energy on.Join farming and receiving the ginseng time, usually rot because of reasons such as weather are gone mouldy fresh Radix Ginseng and sent out, the ginseng farming is impaired and anxious because of economy.Radix Ginseng also is an a difficult problem even if the Radix Ginseng that processes concerning pharmaceuticals, is deposited keeping, damages by worms, and humidity can make the Radix Ginseng mycete grow thickly.
If adopt extracting method of the present invention, can not allow ginseng farming worry for the processing and the Changes in weather of Radix Ginseng, can allow pharmaceuticals and ginseng merchants remove worry from again, can also allow and eat ginseng person and shorten the stewed ginseng time.The ginseng liquid that extracts according to embodiment 1 method has concentrated property, the nourishing curative effect increases greatly, and 19 people that every year eat the ginseng strengthening body have same reaction, and they say: the liquid that this method is extracted saves time and is convenient, main is that tonic usefulness increases, and has no side effect.
Embodiment 3:
1, prescription (single card dosage): Radix Achyranthis Bidentatae 30g, Haematitum 15g, Os Draconis 30g, Concha Ostreae 15g, give birth to Carapax Et Plastrum Testudinis 30g, Radix Scrophulariae 20g, Radix Asparagi 20g, Radix Ophiopogonis 15g, Fructus Toosendan 15g, Fructus Hordei Germinatus 30g, Herba Artemisiae Scopariae 15g, Radix Glycyrrhizae 30g
2, the curative effect of medicine: hypertension, hypertensive renal disease, apoplexy
3, method:
1. carbonization condensation method of the present invention:
By above-mentioned prescription 10 patch amounts, be placed on the Chinese medicine dry product in the carbonization chamber of extraction equipment shown in Figure 1 with water infiltration, open the combustion furnace, be fired to the Chinese medicine carbonization, obtain thick liquid by the liquid outlet collection, thick liquid leaves standstill half an hour, gets the supernatant distillation, get the distillate of 98~103 ℃ of fractions, through activated carbon adsorption (4 hours), filter paper filtering, get filtrate, promptly get Chinese medicine extraction liquid.
2. traditional decocting decoction:
By above-mentioned prescription 10 patch amounts, get the Chinese medicine dry product and add the 1000g decocting and boiled 2 hours, decocting liquid; Each 300~400cc medicinal liquid, every day 3 times;
Hu, 65 years old, symptom was a hypertension, apoplexy often adopts the decocting decoction in two years, does not have too big curative effect at me, extraction method of the present invention is adopted in the back, former side does not have under the situation about becoming, and the curative effect effect improves greatly, drinks every 50cc of extracting solution, blood pressure has just been fallen, and see that the sensation that medicine is just vomitted has not had yet, and one month dosage, two day time just can finish.New extraction method has become Chinese medicine fully with Western medicine and has made things convenient for equally, and curative effect and function do not have change yet, and curative effect has increased.
Embodiment 4:
1, prescription (single card dosage): Calculus Bovis 3g, Radix Curcumae 15g, Cornu Bubali 20g, Rhizoma Coptidis 20g, Radix Scutellariae 25g, mountain mast 30g, Cinnabaris 8g, Realgar 6g, Borneolum Syntheticum 2g, Margarita 10g
2, method:
1. first group: by above-mentioned prescription 10 patch amounts, the Chinese medicine dry product is placed on water infiltration in the carbonization chamber of extraction equipment shown in Figure 1, opens the combustion furnace, be fired to the Chinese medicine carbonization, collect by liquid outlet and obtain thick liquid; Thick liquid in hermetic container, leave standstill 5 years, get the supernatant distillation, get the distillate of 98~103 ℃ of fractions, through activated carbon adsorption (5 hours), filter paper filtering, get filtrate, promptly get Chinese medicine extraction liquid; 2. second group tradition decoction decocting method: by above-mentioned prescription 10 patch amounts, get the Chinese medicine dry product and add the 750g decocting and boiled 4 hours, decocting liquid; Each 100~200cc medicinal liquid, every day 3 times;
3, purpose: under conditions such as the same environment that configures, temperature, first and second liang of group liquid are put the comparison resting period in the glass container.
The prescription that deal is identical is classified and is poured in first and second glass containers of same specification with above-mentioned two kinds of method gained medicinal liquids, rests in the same cabinet, and observe once every day.After 4 days as a result, traditional decoction has taken place to go mouldy, and the medicinal liquid no change that extraction method of the present invention obtains.Observe traditional decoction after 7 days and send out mashed, stench, casing wall goes mouldy, and the medicinal liquid that extraction method of the present invention obtains is no change also.After 1 year, observe the still acomia change of mildewing of medicinal liquid that extraction method of the present invention obtains again, stench, corrosion phenomenon.
Embodiment 5:
Public certain, woman, 41 years old, self-employed entrepreneur.City, the seashore prunier of having dinner of going out returned the guard station after one day, inappetence, and dizziness, myasthenia of limbs, left limb, thigh, root be subcutaneous to go out little clot point; With fever.After the People's Hospital, city is diagnosed as anaphylactoid purpura, with Chinese medicine decocting soup side, the bitter and difficult pharynx of mouthfeel, hearing medicine has the vomiting sense, and the January of taking medicine is surplus, no positive effect.After use Chinese medicine extraction method of the present invention pharynx clothes instead, the first quarter moon of taking medicine is surplus, sees it, disease is slowed down to some extent, does not have the fever sense, the medicine dosing also obtains reducing, and twice of every day needs 100cc, self-induction is good, evident in efficacy by the Chinese medicine mouthfeel of extraction method of the present invention.The whole cancellations of disease after continuous one week of clothes, with normal person's indistinction, back tracing observation does not have recurrence.
Chinese prescription (single card dosage): Rhizoma Paridis 10g, Flos Lonicerae 100g, Herba Artemisiae Scopariae 20g, Herba Agrimoniae 20g, Herba Scutellariae Barbatae 20g, Radix Et Rhizoma Rhei 20g, Radix Scutellariae 20g, Cortex Phellodendri 12g, Radix Rehmanniae 50g, Radix Glycyrrhizae 50g;
The decocting method: by above-mentioned prescription 10 patch amounts, get the Chinese medicine dry product and add the 750g decocting and boiled 3 hours, decocting liquid; Each 100~200cc medicinal liquid, every day 3 times;
The inventive method: by above-mentioned prescription 10 patch amounts, the Chinese medicine dry product is placed on water infiltration in the carbonization chamber of extraction equipment shown in Figure 1, opens the combustion furnace, be fired to the Chinese medicine carbonization, collect by liquid outlet and obtain thick liquid; Thick liquid left standstill in hermetic container 6 months, got the supernatant distillation, got the distillate of 98~103 ℃ of fractions, through activated carbon adsorption (4 hours), filter paper filtering, got filtrate, promptly got Chinese medicine extraction liquid.
Embodiment 6:
In certain, the man, 39 years old, upfitter (carpenter) had a liking for cigarette as life, every winter-spring season, cough with asthma repeatedly, morbidity dry cough without phlegm in period, wait some antitussive classes with the cough with asthma spirit, surplus January with Tri-Biocin, all there is not too obvious curative effects, bad during the symptom fashion, the cough with asthma history reaches 10 years, meets with it when checking decoration quality in the back, seeing that its cough with asthma does not have to have a rest reaches three minutes, cyanosis on the face and lips, and misery is very much, after asking clearly situation, writing a prescription for its cube takes with decocting, does not have positive effect behind the first quarter moon.The back adopts extraction method of the present invention to soak into medical herbs burning carbonate cooling absorption, extracts medicinal liquid, and every only needs 50CC, two drug delivery on an empty stomach sooner or later, and other adjuvant of period in a medicine, just received effect the same day, cough with asthma obviously alleviates, and the expectorant in the larynx that can spue.The seven days symptoms of taking medicine are eliminated, and after it's 2 years is past thing, ask its symptom, and the main suit does not have recurrence.Observed result shows that new extraction method can increase curative effect, reduces antibiotic dependence.
Chinese prescription (single card dosage): 3 pieces of Fructus Momordicaes, Flos Farfarae 10g, Radix Asteris 10g, Bulbus Fritillariae Cirrhosae 10g, Semen Trichosanthis 20g, orange 15g, Radix Glycyrrhizae 80g;
The decocting method: by above-mentioned prescription 10 patch amounts, get the Chinese medicine dry product and add the 750g decocting and boiled 2 hours, decocting liquid; Each 100~200cc medicinal liquid, every day 3 times;
The inventive method: by above-mentioned prescription 10 patch amounts, the Chinese medicine dry product is placed on water infiltration in the carbonization chamber of extraction equipment shown in Figure 1, opens the combustion furnace, be fired to the Chinese medicine carbonization, collect by liquid outlet and obtain thick liquid; Thick liquid left standstill in hermetic container 3 months, got the supernatant distillation, got the distillate of 98~103 ℃ of fractions, through activated carbon adsorption (4 hours), filter paper filtering, got filtrate, promptly got Chinese medicine extraction liquid.
Embodiment 7:
Car, man, 45 years old, government functionary.Head, back cervical region, two femoribus internus furuncle and phyma, after the affected part was good, other skin part reappeared again and grows, and often with fever, reached 17 years so repeatedly.The how tame hospital of going to a doctor, the Chinese and western legal medical expert has no result to the greatest extent eventually.Mention herbal treatment, he shakes the head at once: do not want to drink, Chinese medicine is too bitter, once eating soup medicine stomach pain unbearably, and busy again in addition boiling medicine.The back makes Chinese medicine with new extraction method and sends to, after he sees not letter be Chinese medicine, advise and drink 80CC its every day on an empty stomach, oral two, after spending ten days, he specially tells: this Chinese medicine is excellent, and is convenient, and pharynx clothes mouthfeel is good, fragrant is arranged, and stomach is also non-stimulated, allows and extracts 20 days dose once more.After January, see that his disease is fully good, work energy is also abundant than before.
Chinese prescription (single card dosage): spend SHECAO 20g in vain, Rhizoma Curcumae 15g, Herba Portulacae 20g, Fructus Cnidii 15g, leaf of Lignum cinnamomi camphorae 30g, Herba Artemisiae Scopariae 50g, Radix Rehmanniae 50g;
Medicinal liquid extracting method: by above-mentioned prescription 10 patch amounts, the Chinese medicine dry product is placed on water infiltration in the carbonization chamber of extraction equipment shown in Figure 1, opens the combustion furnace, be fired to the Chinese medicine carbonization, collect by liquid outlet and obtain thick liquid; Thick liquid left standstill in hermetic container 3 months, got the supernatant distillation, got the distillate of 98~103 ℃ of fractions, through activated carbon adsorption (4 hours), filter paper filtering, got filtrate, promptly got Chinese medicine extraction liquid.
Embodiment 8:
White horse with a black mane, the man, 72 years old, traffic accident caused that many places such as arm, foot, the back of the body are hemorrhage, blood stasis, cause redness in various degree after livid purple, and pyogenic infection is arranged.The hospitalize first quarter moon is had a surplus, and leaves hospital not have to be clearly better, and looks for me to seek medical advice.Adopt the Pinus koraiensis extracting solution to clean a wound and injury with blood-stasis place multipass, with sterilization towel hot compress 20 minutes, the reuse spray is bottled went into Chinese medicine extraction liquid such as Flos Carthami, Radix Notoginseng, evenly is sprayed at and suffers from three times, allows extracting solution infiltrate deep skin.Redness disappears after adopting above method first quarter moon, wound healing, and the decrustation place skin pinkiness and the peripheral colour of skin are inconsistent, what bruise pain cancellation, pink skin and peripheral skin basically identical after January.
The preparation of Pinus koraiensis extracting solution: the Pinus koraiensis tree root is placed on water infiltration in the carbonization chamber of extraction equipment shown in Figure 1, opens the combustion furnace, be fired to carbonization, condensed gas obtains thick liquid by the liquid outlet collection; After thicker liquid sealing being left standstill 3 months, remove upper strata grease and lower sediment, get middle level liquid, 98 ℃~103 ℃ fraction liquid are got in distillation, and activated carbon adsorption, filter paper filtering get the Pinus koraiensis extracting solution;
Chinese prescription (single card dosage): Flos Carthami 30g: Radix Notoginseng 30g; Paederus densipennis Bernh.: 30g: yellow wine 1000g;
The medicinal liquid extracting method: by above-mentioned prescription 10 patch amounts, the Chinese medicine beverage is placed on water infiltration in the carbonization chamber of extraction equipment shown in Figure 1, opens the combustion furnace, be fired to the Chinese medicine carbonization, condensed gas obtains thick liquid by the liquid outlet collection; After thicker liquid being left standstill half an hour, get supernatant, 98 ℃~103 ℃ fraction liquid are got in distillation, pack in the spray bottle, are sprayed on the affected part.
Embodiment 9:
Chen, man, 28 years old, fever, after flu heals, nasal obstruction, the nasal mucus Huang is dense, is sinusitis through hospital diagnosis, because nasal obstruction is obstructed, feel dizzy, very painful, injection of antibiotic, the oral first quarter moon of antibiotic medicine do not have to take a turn for the better, and I am it with drop bottle with Chinese medicine extraction drop numbers such as Fel Sus domestica, Herba Pogostemoniss droplet in nasal cavity for the back, used four days every day for several times, and above symptom condition all disappears.
Chinese prescription (single card dosage): Fel Sus domestica crystal 10gization water, Herba Pogostemonis 1000g, Herba Menthae 500g, water 200g;
Medicinal liquid extracting method: by above-mentioned prescription 10 patch amounts, the Chinese medicine dry product is placed on water infiltration in the carbonization chamber of extraction equipment shown in Figure 1, opens the combustion furnace, be fired to the Chinese medicine carbonization, collect gas, obtain thick liquid by the liquid outlet collection, thicker liquid after static two hours, is got the supernatant distillation, get 98 ℃~103 ℃ fraction liquid, activated carbon adsorption, filter paper filtering are packed in the drop bottle that disinfects, and with weeping pipe medicinal liquid are sent into nasal cavity.
Embodiment 10:
Zhao, Wang, 13 of Lee etc., beriberi patient, very itch unbearably between the toe slit, be white in color between toe, and decortication, sole has the needle-like blister, meets cold and hot outbreak, and it is incomparable very to itch, scratch to separate very with hand rubbing and to itch, medical history for many years, after find here, execute the method for controlling with Chinese medicine synthetic fluids such as Herba Houttuyniae, implement to spray affected part treatment, spray the back and very itch half an hour and to stop with spray bottle, affected part skin exfoliation after three days, the needle-like blister disappears, and skin is tending towards normal condition between toe.
Chinese prescription (single card dosage): Herba Houttuyniae 80g, Herba Violae 80g, Spica Prunellae 80g, Herba Portulacae 80g, water 100g;
Medicinal liquid extracting method: by above-mentioned prescription 10 patch amounts, the herbarium recentium of gathering is washed in the carbonization chamber that is statically placed in extraction equipment shown in Figure 1, open the combustion furnace, be fired to the Chinese medicine carbonization, collect gas, obtain thick liquid by the liquid outlet collection, again thick liquid after airtight 1 year, is got the supernatant distillation and got 98 ℃~103 ℃ fraction liquid, activated carbon adsorption, filter paper filtering, pack in the spray bottle, the time spent takes out and sprays the affected part.
Embodiment 11:
Wu, the Qin, certain 30 multidigit women such as grade of week, symptom shows as pudendum very itches, and how down leucorrhea cleans pudendum with JIEERYIN usually, still recurrence later, disease can't be removed root.I adopt the back Chinese medicine such as Fructus Cnidii to add the synthetic extracting solution of Chinese liquor to clean and sprayed many days, and disease is eliminated, and does not have recurrence so far.
Chinese prescription (single card dosage): Fructus Cnidii 150g, spend SHECAO 150g in vain, Herba Violae 150g, high spirit 1500g;
The medicinal liquid extracting method, by above-mentioned prescription 10 patch amounts, bright Chinese herbal medicine is cleaned, added high spirit and put into the carbonization chamber that liquid equipment is got in extraction shown in Figure 1, open the combustion furnace and be fired to the Chinese medicine carbonization, obtain thick liquid by the liquid outlet collection, again that thick liquid is airtight static more than three months, get the supernatant distillate, get 98 ℃~103 ℃ fraction liquid, activated carbon adsorption, filter paper filtering, standby in the bottle of packing into.
More than new extraction method to the example application of infectious disease, parasitic disease, internal disease, surgical diseases, pediatric disease, gynaecopathia, otorhinolaryngology disease, just emphasized the superior functionality of new extraction method, but used prescription is just enumerated, and is not limited thereto.

Claims (11)

1. Chinese medicine extraction method comprises:
(1) Chinese medicine through soaking into is placed hermetic container, with outside burning things which may cause a fire disaster hermetic container is heated to the Chinese medicine carbonization, expellant gas reclaims through condensation and obtains the thick liquid of Chinese medicine;
(2) the thick liquid of step (1) gained Chinese medicine staticly settles, gets the supernatant distillation, gets the distillate of 98~103 ℃ of fractions, through activated carbon adsorption, filter paper filtering, gets filtrate, promptly gets Chinese medicine extraction liquid.
2. the method for claim 1 is characterized in that described being precipitated as of described step (2): the thick liquid of step (1) gained leaves standstill half an hour~3 day.
3. the method for claim 1, it is characterized in that described being precipitated as of described step (2): the thick liquid of step (1) gained left standstill in hermetic container 3 months~5 years.
4. as the described method of one of claim 1~3, it is characterized in that described Chinese medicine is the former medicine of Chinese medicine or the prepared slices of Chinese crude drugs.
5. special equipment of Chinese medicine extraction method according to claim 1, described equipment comprises: the airtight carbonization chamber of calcining Chinese medicine, collect Chinese medicine forms flue gas when carbonization collection chamber, be provided with the combustion furnace below the described carbonization chamber; The inner chamber of described carbonization chamber communicates with described collection chamber inner chamber by airway, described collection chamber top is provided with and the airtight lid that is connected of described collection chamber, described lid is the cooling back installation that is provided with cooling water inlet A and coolant outlet A, it is the cooling pan of the thick liquid of Chinese medicine that the periphery of described collection chamber is provided with the flue gas condensing in the described collection chamber, described cooling pan is provided with cooling water inlet B and coolant outlet B, described collection chamber is arranged in the cooling pan, the bottom of described collection chamber is provided with the sharp mouth shape liquid outlet that the thick liquid of Chinese medicine is discharged, and described liquid outlet communicates with atmosphere.
6. special equipment as claimed in claim 5 is characterized in that: described collection chamber is annular, and the bottom center arch of described collection chamber is bell jar shape projection.
7. special equipment as claimed in claim 6 is characterized in that leaving the gap bottom described bell jar shape rising height and the described lid.
8. special equipment as claimed in claim 7 is characterized in that the part that described lid and described collection chamber interlock is down the pot type, and the bell jar shape rising height of described collection chamber is concordant with the height of the coolant outlet B of cooling pan.
9. special equipment as claimed in claim 4, it is characterized in that: described cooling water inlet A is arranged on described lid bottom, described coolant outlet A is arranged on described lid top, described cooling water inlet B is arranged on described cooling pan bottom, and described coolant outlet B is arranged on described cooling pan top.
10. special equipment as claimed in claim 4 is characterized in that: described carbonization chamber comprises staving and bung, and described bung and described staving are tightly connected, and described bung top is provided with the hold-down mechanism that described bung and described staving are compressed.
11. special equipment as claimed in claim 4 is characterized in that: described hold-down mechanism is the cross bar that both ends are provided with snap ring, but described cross bar is provided with the clamp nut of up-down adjustment, and described staving is provided with the shelves part that cooperates with described snap ring.
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* Cited by examiner, † Cited by third party
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CN102641450A (en) * 2012-05-16 2012-08-22 周国生 Traditional Chinese medicine for treating hypertension
CN104587696A (en) * 2015-02-02 2015-05-06 银川多贝科技有限公司 Square gas cooling tank
CN104644695A (en) * 2014-06-12 2015-05-27 唐泽光 Extraction method of Chinese herbal medicine
CN106929158A (en) * 2017-05-02 2017-07-07 刘建兰 A kind of equipment that plant essence is extracted by burning plant
CN112206343A (en) * 2020-09-22 2021-01-12 浙江省立同德医院 Anti-inflammatory hemostatic dressing and preparation method thereof, PICC (peripherally inserted central catheter) catheter and CVC catheter
CN115191626A (en) * 2022-07-27 2022-10-18 宁波长荣酿造设备有限公司 Roasting machine
CN116650589A (en) * 2023-07-13 2023-08-29 海南京都堂药业有限公司 Preparation method of rhizoma pinellinae praeparata loquat leaf extract

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Publication number Priority date Publication date Assignee Title
CN102641450A (en) * 2012-05-16 2012-08-22 周国生 Traditional Chinese medicine for treating hypertension
CN104644695A (en) * 2014-06-12 2015-05-27 唐泽光 Extraction method of Chinese herbal medicine
CN104587696A (en) * 2015-02-02 2015-05-06 银川多贝科技有限公司 Square gas cooling tank
CN106929158A (en) * 2017-05-02 2017-07-07 刘建兰 A kind of equipment that plant essence is extracted by burning plant
CN112206343A (en) * 2020-09-22 2021-01-12 浙江省立同德医院 Anti-inflammatory hemostatic dressing and preparation method thereof, PICC (peripherally inserted central catheter) catheter and CVC catheter
CN115191626A (en) * 2022-07-27 2022-10-18 宁波长荣酿造设备有限公司 Roasting machine
CN115191626B (en) * 2022-07-27 2024-04-05 宁波长荣酿造设备有限公司 Roasting machine
CN116650589A (en) * 2023-07-13 2023-08-29 海南京都堂药业有限公司 Preparation method of rhizoma pinellinae praeparata loquat leaf extract

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