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SU508495A1 - The method of obtaining a mixture of alkyladman-tans - Google Patents

The method of obtaining a mixture of alkyladman-tans

Info

Publication number
SU508495A1
SU508495A1 SU1998263A SU1998263A SU508495A1 SU 508495 A1 SU508495 A1 SU 508495A1 SU 1998263 A SU1998263 A SU 1998263A SU 1998263 A SU1998263 A SU 1998263A SU 508495 A1 SU508495 A1 SU 508495A1
Authority
SU
USSR - Soviet Union
Prior art keywords
mixture
alkyladman
tans
obtaining
catalyst
Prior art date
Application number
SU1998263A
Other languages
Russian (ru)
Inventor
Борис Григорьевич Гаврилов
Вадим Евгеньевич Ковязин
Вячеслав Васильевич Тахистов
Виктор Григорьевич Лукша
Original Assignee
Ленинградский Ордена Ленина Иордена Трудового Красного Знаменигосударственный Университетим.А.А.Жданова
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ленинградский Ордена Ленина Иордена Трудового Красного Знаменигосударственный Университетим.А.А.Жданова filed Critical Ленинградский Ордена Ленина Иордена Трудового Красного Знаменигосударственный Университетим.А.А.Жданова
Priority to SU1998263A priority Critical patent/SU508495A1/en
Application granted granted Critical
Publication of SU508495A1 publication Critical patent/SU508495A1/en

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Description

II фракци  - целевой продукт с т. кип. 195-250°С составл ет 18 вес. %.Fraction II - target product with m. Bale. 195-250 ° C is 18 wt. %

Пример 2. Оиыт ировод т по примеру 1. Врем  реакции 20 час.Example 2. Washed in accordance with Example 1. The reaction time is 20 hours.

Выход целевого продукта составл ет 28,4 вес. %, выход фракции с т. кип. 40- 195° С-23,5 вес. %.The yield of the target product is 28.4 wt. %, the output fraction with t. Kip. 40- 195 ° C-23.5 weight. %

Пример 3. Опыт провод т по примеру 1, исход  из 45 г фракции с т. кип. 40-195°С примеров 1 и 2 и катализаторного комллекса в количестве 45 г по примеру 2.Example 3. The experiment was carried out as in Example 1, starting from a 45 g fraction with m.p. 40-195 ° C of examples 1 and 2 and the catalyst complex in the amount of 45 g in example 2.

Температура процесса 150±5°С; врем  реакции 20 час.Process temperature 150 ± 5 ° С; reaction time 20 hours.

Выход целевого цродукта с т. кип. 195-250°С составл ет 31,1 вес. %, The yield of the desired product with t. Kip. 195-250 ° C is 31.1 wt. %

выход фракции с т. кип. 40-195°С-29,9 вес. %.yield fraction with m. Kip. 40-195 ° C-29.9 weight. %

Claims (2)

1.Способ получени  смеси алкиладамантанов нагреванием циклогексана в присутствии катализатора, отличающийс  тем, что, с целью интенсификации процесса, в качестве катализатора используют смесь га.югеиида алюмини  с галогепводородом.1. A method of producing a mixture of alkyladamantanes by heating cyclohexane in the presence of a catalyst, characterized in that, in order to intensify the process, a mixture of gaugüyide aluminum with hydrogen halide is used as a catalyst. 2.Способ по п. 1, о т л и ч а ю щ и и с   тем, что процесс осуществл ют при весовом соотношении циклогексана и катализатора 1 : : 0,5-2 и нагревание ведут до 140-180°С.2. The method according to claim 1, wherein the process is carried out at a weight ratio of cyclohexane and catalyst 1: 0.5-2 and is heated to 140-180 ° C.
SU1998263A 1974-02-22 1974-02-22 The method of obtaining a mixture of alkyladman-tans SU508495A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
SU1998263A SU508495A1 (en) 1974-02-22 1974-02-22 The method of obtaining a mixture of alkyladman-tans

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SU1998263A SU508495A1 (en) 1974-02-22 1974-02-22 The method of obtaining a mixture of alkyladman-tans

Publications (1)

Publication Number Publication Date
SU508495A1 true SU508495A1 (en) 1976-03-30

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
SU1998263A SU508495A1 (en) 1974-02-22 1974-02-22 The method of obtaining a mixture of alkyladman-tans

Country Status (1)

Country Link
SU (1) SU508495A1 (en)

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