RU2008118478A - Способ получения полиизоциануратного полиуретанового материала - Google Patents
Способ получения полиизоциануратного полиуретанового материала Download PDFInfo
- Publication number
- RU2008118478A RU2008118478A RU2008118478/04A RU2008118478A RU2008118478A RU 2008118478 A RU2008118478 A RU 2008118478A RU 2008118478/04 A RU2008118478/04 A RU 2008118478/04A RU 2008118478 A RU2008118478 A RU 2008118478A RU 2008118478 A RU2008118478 A RU 2008118478A
- Authority
- RU
- Russia
- Prior art keywords
- polyisocyanate
- isocyanate
- weight
- amount
- polyol
- Prior art date
Links
- 239000000463 material Substances 0.000 title claims abstract 7
- 229920000582 polyisocyanurate Polymers 0.000 title claims abstract 3
- 239000011495 polyisocyanurate Substances 0.000 title claims abstract 3
- 239000004814 polyurethane Substances 0.000 title claims abstract 3
- 229920002635 polyurethane Polymers 0.000 title claims abstract 3
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 229920001228 polyisocyanate Polymers 0.000 claims abstract 18
- 239000005056 polyisocyanate Substances 0.000 claims abstract 18
- 238000000034 method Methods 0.000 claims abstract 8
- 150000001875 compounds Chemical class 0.000 claims abstract 7
- 229920005862 polyol Polymers 0.000 claims abstract 7
- 150000003077 polyols Chemical class 0.000 claims abstract 7
- UPMLOUAZCHDJJD-UHFFFAOYSA-N 4,4'-Diphenylmethane Diisocyanate Chemical compound C1=CC(N=C=O)=CC=C1CC1=CC=C(N=C=O)C=C1 UPMLOUAZCHDJJD-UHFFFAOYSA-N 0.000 claims abstract 6
- 125000006353 oxyethylene group Chemical group 0.000 claims abstract 3
- 239000004721 Polyphenylene oxide Substances 0.000 claims abstract 2
- 239000003054 catalyst Substances 0.000 claims abstract 2
- 238000006243 chemical reaction Methods 0.000 claims abstract 2
- 239000012948 isocyanate Substances 0.000 claims abstract 2
- 150000002513 isocyanates Chemical class 0.000 claims abstract 2
- 239000007788 liquid Substances 0.000 claims abstract 2
- 229920000570 polyether Polymers 0.000 claims abstract 2
- 238000005829 trimerization reaction Methods 0.000 claims abstract 2
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/09—Processes comprising oligomerisation of isocyanates or isothiocyanates involving reaction of a part of the isocyanate or isothiocyanate groups with each other in the reaction mixture
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/09—Processes comprising oligomerisation of isocyanates or isothiocyanates involving reaction of a part of the isocyanate or isothiocyanate groups with each other in the reaction mixture
- C08G18/092—Processes comprising oligomerisation of isocyanates or isothiocyanates involving reaction of a part of the isocyanate or isothiocyanate groups with each other in the reaction mixture oligomerisation to isocyanurate groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/16—Catalysts
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/48—Polyethers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/48—Polyethers
- C08G18/4833—Polyethers containing oxyethylene units
- C08G18/4837—Polyethers containing oxyethylene units and other oxyalkylene units
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
- C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
- C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
- C08G18/7657—Polyisocyanates or polyisothiocyanates cyclic aromatic containing two or more aromatic rings
- C08G18/7664—Polyisocyanates or polyisothiocyanates cyclic aromatic containing two or more aromatic rings containing alkylene polyphenyl groups
- C08G18/7671—Polyisocyanates or polyisothiocyanates cyclic aromatic containing two or more aromatic rings containing alkylene polyphenyl groups containing only one alkylene bisphenyl group
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyurethanes Or Polyureas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
1. Способ получения полиизоциануратного полиуретанового материала, включающий взаимодействие полиизоцианата и реакционно-способной по отношению к изоцианату композиции, где взаимодействие проводят при изоцианатном индексе от 1600 до 100000 и в присутствии катализатора тримеризации, где полиизоцианат содержит а) 75-100 мас.% дифенилметандиизоцианата, содержащего по меньшей мере 40 мас.%, 4,4'-дифенилметандиизоцианата и/или варианта указанного дифенилметандиизоцианата, каковой вариант является жидким при 25оС и имеет величину NCO по меньшей мере 20 мас.% (полиизоцианат а), и b) 25-0 мас.% другого полиизоцианата (полиизоцианат b), причем количество полиизоцианата а) и полиизоцианата b) рассчитано на суммарное количество этого полиизоцианата а) и полиизоцианата b), и где реакционно-способная по отношению к изоцианату композиция содержит а) 80-100 мас.% полиэфирполиола, имеющего среднюю номинальную функциональность 2-6, среднюю эквивалентную массу 1100-5000 и содержание оксиэтилена (ЕО) 65-100 мас.%, и b) 20-0 мас.% одного или нескольких других реакционно-способных по отношению к изоцианату соединений, где количество полиола а) и соединения b) рассчитано на суммарное количество этого полиола а) и соединения b) и где содержание жестких блоков составляет по меньшей мере 50%. ! 2. Способ по п.1, где эквивалентный вес составляет 1100-4000 и индекс составляет 1700-50000. ! 3. Способ по п.1 или 2, где содержание оксиэтилена составляет 65-90 мас.%, количество полиола а) составляет 90-100% и количество соединения b) составляет 0-10 мас.%. ! 4. Способ по п.1 или 2, в котором материал имеет плотность более 100 кг/м3. ! 5. Способ по п.3, в котором материал имеет плотность более 100 кг/м3. ! 6. Материал, изг�
Claims (7)
1. Способ получения полиизоциануратного полиуретанового материала, включающий взаимодействие полиизоцианата и реакционно-способной по отношению к изоцианату композиции, где взаимодействие проводят при изоцианатном индексе от 1600 до 100000 и в присутствии катализатора тримеризации, где полиизоцианат содержит а) 75-100 мас.% дифенилметандиизоцианата, содержащего по меньшей мере 40 мас.%, 4,4'-дифенилметандиизоцианата и/или варианта указанного дифенилметандиизоцианата, каковой вариант является жидким при 25оС и имеет величину NCO по меньшей мере 20 мас.% (полиизоцианат а), и b) 25-0 мас.% другого полиизоцианата (полиизоцианат b), причем количество полиизоцианата а) и полиизоцианата b) рассчитано на суммарное количество этого полиизоцианата а) и полиизоцианата b), и где реакционно-способная по отношению к изоцианату композиция содержит а) 80-100 мас.% полиэфирполиола, имеющего среднюю номинальную функциональность 2-6, среднюю эквивалентную массу 1100-5000 и содержание оксиэтилена (ЕО) 65-100 мас.%, и b) 20-0 мас.% одного или нескольких других реакционно-способных по отношению к изоцианату соединений, где количество полиола а) и соединения b) рассчитано на суммарное количество этого полиола а) и соединения b) и где содержание жестких блоков составляет по меньшей мере 50%.
2. Способ по п.1, где эквивалентный вес составляет 1100-4000 и индекс составляет 1700-50000.
3. Способ по п.1 или 2, где содержание оксиэтилена составляет 65-90 мас.%, количество полиола а) составляет 90-100% и количество соединения b) составляет 0-10 мас.%.
4. Способ по п.1 или 2, в котором материал имеет плотность более 100 кг/м3.
5. Способ по п.3, в котором материал имеет плотность более 100 кг/м3.
6. Материал, изготовленный согласно способу по пп.1-5.
7. Материал, получаемый согласно способу по пп.1-5.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP05109530 | 2005-10-13 | ||
| EP05109530.5 | 2005-10-13 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RU2008118478A true RU2008118478A (ru) | 2009-11-20 |
| RU2415877C2 RU2415877C2 (ru) | 2011-04-10 |
Family
ID=35788185
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2008118478/04A RU2415877C2 (ru) | 2005-10-13 | 2006-09-29 | Способ получения полиизоциануратного полиуретанового материала |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US8785570B2 (ru) |
| EP (1) | EP1940899B1 (ru) |
| JP (1) | JP5044561B2 (ru) |
| KR (1) | KR20080057271A (ru) |
| CN (1) | CN101283012B (ru) |
| AT (1) | ATE438669T1 (ru) |
| AU (1) | AU2006301367B2 (ru) |
| BR (1) | BRPI0616662B1 (ru) |
| CA (1) | CA2625689C (ru) |
| DE (1) | DE602006008337D1 (ru) |
| ES (1) | ES2327569T3 (ru) |
| RU (1) | RU2415877C2 (ru) |
| WO (1) | WO2007042411A1 (ru) |
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|---|---|---|---|---|
| AU2004247421B2 (en) * | 2003-06-12 | 2008-03-13 | Huntsman International Llc | Process for preparing a polyisocyanurate polyurethane material |
| RU2415877C2 (ru) | 2005-10-13 | 2011-04-10 | Хантсмэн Интернэшнл Ллс | Способ получения полиизоциануратного полиуретанового материала |
| CA2636621C (en) * | 2006-02-21 | 2013-06-25 | Huntsman International Llc | Process for making a polyisocyanurate composite |
| CN101466517B (zh) | 2006-06-14 | 2012-02-22 | 亨茨曼国际有限公司 | 复合面板 |
| CA2712054C (en) * | 2008-02-14 | 2015-02-03 | Huntsman International Llc | Elastomeric materials having a high hardblock content and process for preparing them |
| CN101959921B (zh) | 2008-03-07 | 2013-03-27 | 亨茨曼国际有限公司 | 包含高硬嵌段含量基质的泡沫材料及其制备方法 |
| EP2182017A1 (en) * | 2008-07-10 | 2010-05-05 | Huntsman International Llc | A polyisocyanurate-based syntactic coating for offshore applications |
| PL2342252T3 (pl) | 2008-08-28 | 2017-09-29 | Huntsman International Llc | Mieszanina uzyskana przez przereagowanie poliolu i bezwodnika oraz jej zastosowanie w poliizocyjanianach do tworzenia poliizocyjanuratów |
| BRPI1011009B1 (pt) * | 2009-06-09 | 2020-01-28 | Huntsman Int Llc | material, e, processo para preparar um material |
| EP2591029A1 (en) | 2010-07-08 | 2013-05-15 | Huntsman International LLC | Polyisocyanate-based anti-corrosion coating |
| WO2012062801A1 (en) | 2010-11-09 | 2012-05-18 | Rockwool International A/S | Mineral fibre product having reduced thermal conductivity |
| WO2012062796A1 (en) | 2010-11-09 | 2012-05-18 | Rockwool International A/S | Method for manufacturing an aerogel-containing composite and composite produced by said method |
| KR20140127856A (ko) | 2012-02-08 | 2014-11-04 | 바이엘 인텔렉쳐 프로퍼티 게엠베하 | 경질 폴리우레탄-폴리이소시아누레이트 발포체의 제조 방법 |
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| EP2743284A1 (de) | 2012-12-13 | 2014-06-18 | Basf Se | Hydrolysestabiles Polyurethan zur Beschichtung von Elementen in maritimen Anwendungen |
| EP2743285A1 (de) | 2012-12-13 | 2014-06-18 | Basf Se | Hydrolysestabiles Polyurethan zur Anwendung im off-shore Bereich |
| US10442885B2 (en) | 2012-12-13 | 2019-10-15 | Basf Se | Hydrolysis-stable polyurethane for coating elements in maritime applications |
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| BR9915380A (pt) | 1998-11-16 | 2001-07-31 | Huntsman Ici Chem Llc | Sistema de poliisocianurato, processo de extrusão por tração para a preparação de um compósito polimérico reforçado por fibra de poliisocianurato curado, e, produto de poliisocianurato |
| DE19918726C2 (de) | 1999-04-24 | 2002-04-11 | Bayer Ag | Offenzellige Polyurethanhartschaumstoffe |
| US6509392B1 (en) | 2000-01-25 | 2003-01-21 | H.A. International Llc | Foundry binder and process |
| EP1167414A1 (en) | 2000-06-29 | 2002-01-02 | Huntsman International Llc | Process for making rigid polyurethane foams having high adhesion |
| EP1172387A1 (en) | 2000-07-14 | 2002-01-16 | Huntsman International Llc | Process for preparing an elastomer |
| EP1178063A1 (en) | 2000-08-01 | 2002-02-06 | Huntsman International Llc | Process for preparing a polyurethane material |
| FR2812653A1 (fr) | 2000-08-03 | 2002-02-08 | Michelin Soc Tech | Colle pour compositions de caoutchouc, son procede de preparation et articles comportant cette colle |
| JP4472856B2 (ja) * | 2000-09-19 | 2010-06-02 | 有限会社サン・イースト・リサーチ | 親水性連続微細気泡ポリイソシアヌレートフォームの製造方法並びに親水性連続微細気泡ポリイソシアヌレートフォーム |
| IT1319215B1 (it) | 2000-10-16 | 2003-09-26 | Industrialesud Spa | Prodotto multistrato, suo uso per la realizzazione di articolileggeri, fonoassorbenti, autoportanti e articoli ottenibili con detto |
| DE10145458B4 (de) | 2001-09-14 | 2014-03-20 | Basf Se | Verfahren zur Herstellung von Urethan- und überwiegend Isocyanuratgruppen aufweisenden Polyurethanhartschaumstoffen |
| US6773756B2 (en) | 2002-03-20 | 2004-08-10 | Bayer Polymers Llc | Process to manufacture three dimensionally shaped substrate for sound abatement |
| US6729045B2 (en) * | 2002-10-02 | 2004-05-04 | Dale F. Isackson | Tap device for clogging shoes |
| US20040069971A1 (en) | 2002-10-15 | 2004-04-15 | Witteveen Martijn M. | Polyol compositions and rigid polyisocyanurate foams prepared therefrom |
| DE10257633A1 (de) | 2002-12-09 | 2004-06-24 | Basf Ag | Verbundelemente, insbesondere gedämmte Rohre |
| US20040249078A1 (en) | 2003-06-04 | 2004-12-09 | Honeywell International, Inc. | Foam catalyst systems |
| AU2004247421B2 (en) | 2003-06-12 | 2008-03-13 | Huntsman International Llc | Process for preparing a polyisocyanurate polyurethane material |
| DE10359024A1 (de) | 2003-12-15 | 2005-07-21 | Basf Ag | Zinnfreie Polyurethanschaumstoffe |
| US7763341B2 (en) | 2004-01-23 | 2010-07-27 | Century-Board Usa, Llc | Filled polymer composite and synthetic building material compositions |
| ITRM20040375A1 (it) | 2004-07-23 | 2004-10-23 | Tekno Garden S R L | Materiali compositi a base di resine leganti, procedimenti per la loro preparazione e usi. |
| RU2415877C2 (ru) | 2005-10-13 | 2011-04-10 | Хантсмэн Интернэшнл Ллс | Способ получения полиизоциануратного полиуретанового материала |
| RU2428436C2 (ru) | 2005-10-13 | 2011-09-10 | Хантсмэн Интернэшнл Ллс | Способ получения полиизоциануратного полиуретанового материала |
| CA2636621C (en) | 2006-02-21 | 2013-06-25 | Huntsman International Llc | Process for making a polyisocyanurate composite |
-
2006
- 2006-09-29 RU RU2008118478/04A patent/RU2415877C2/ru active
- 2006-09-29 BR BRPI0616662-8A patent/BRPI0616662B1/pt not_active IP Right Cessation
- 2006-09-29 JP JP2008534979A patent/JP5044561B2/ja not_active Expired - Fee Related
- 2006-09-29 US US12/089,831 patent/US8785570B2/en active Active
- 2006-09-29 WO PCT/EP2006/066889 patent/WO2007042411A1/en active Application Filing
- 2006-09-29 AT AT06793910T patent/ATE438669T1/de not_active IP Right Cessation
- 2006-09-29 CN CN2006800377177A patent/CN101283012B/zh active Active
- 2006-09-29 ES ES06793910T patent/ES2327569T3/es active Active
- 2006-09-29 AU AU2006301367A patent/AU2006301367B2/en not_active Ceased
- 2006-09-29 KR KR1020087008753A patent/KR20080057271A/ko not_active Application Discontinuation
- 2006-09-29 CA CA2625689A patent/CA2625689C/en active Active
- 2006-09-29 DE DE602006008337T patent/DE602006008337D1/de active Active
- 2006-09-29 EP EP06793910A patent/EP1940899B1/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| EP1940899B1 (en) | 2009-08-05 |
| EP1940899A1 (en) | 2008-07-09 |
| CN101283012A (zh) | 2008-10-08 |
| DE602006008337D1 (de) | 2009-09-17 |
| US8785570B2 (en) | 2014-07-22 |
| BRPI0616662A2 (pt) | 2012-12-25 |
| CN101283012B (zh) | 2011-07-06 |
| CA2625689C (en) | 2013-07-09 |
| BRPI0616662B1 (pt) | 2017-06-13 |
| US20080262168A1 (en) | 2008-10-23 |
| JP5044561B2 (ja) | 2012-10-10 |
| WO2007042411A1 (en) | 2007-04-19 |
| AU2006301367B2 (en) | 2012-02-02 |
| JP2009511685A (ja) | 2009-03-19 |
| RU2415877C2 (ru) | 2011-04-10 |
| AU2006301367A1 (en) | 2007-04-19 |
| ATE438669T1 (de) | 2009-08-15 |
| CA2625689A1 (en) | 2007-04-19 |
| ES2327569T3 (es) | 2009-10-30 |
| KR20080057271A (ko) | 2008-06-24 |
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