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FR3095813B1 - Procédé de production de film de zéolite - Google Patents

Procédé de production de film de zéolite Download PDF

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Publication number
FR3095813B1
FR3095813B1 FR2004212A FR2004212A FR3095813B1 FR 3095813 B1 FR3095813 B1 FR 3095813B1 FR 2004212 A FR2004212 A FR 2004212A FR 2004212 A FR2004212 A FR 2004212A FR 3095813 B1 FR3095813 B1 FR 3095813B1
Authority
FR
France
Prior art keywords
reactor
constant temperature
hydrothermal synthesis
zeolite
support
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR2004212A
Other languages
English (en)
Other versions
FR3095813A1 (fr
Inventor
Kazuya Maekawa
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsui E&s Co Ltd Jp
Original Assignee
Mitsui E&S Machinery Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsui E&S Machinery Co Ltd filed Critical Mitsui E&S Machinery Co Ltd
Publication of FR3095813A1 publication Critical patent/FR3095813A1/fr
Application granted granted Critical
Publication of FR3095813B1 publication Critical patent/FR3095813B1/fr
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14—Ultrafiltration; Microfiltration
    • B01D61/147—Microfiltration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0039—Inorganic membrane manufacture
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0039—Inorganic membrane manufacture
    • B01D67/0051—Inorganic membrane manufacture by controlled crystallisation, e,.g. hydrothermal growth
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/10—Supported membranes; Membrane supports
    • B01D69/105—Support pretreatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/12—Composite membranes; Ultra-thin membranes
    • B01D69/1213—Laminated layers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
    • B01D71/02—Inorganic material
    • B01D71/028—Molecular sieves
    • B01D71/0281—Zeolites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/0013—Controlling the temperature of the process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/30—Loose or shaped packing elements, e.g. Raschig rings or Berl saddles, for pouring into the apparatus for mass or heat transfer
    • B01J19/305—Supporting elements therefor, e.g. grids, perforated plates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/023—Preparation of physical mixtures or intergrowth products of zeolites chosen from group C01B39/04 or two or more of groups C01B39/14 - C01B39/48
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2323/00—Details relating to membrane preparation
    • B01D2323/08—Specific temperatures applied
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2323/00—Details relating to membrane preparation
    • B01D2323/08—Specific temperatures applied
    • B01D2323/081—Heating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2323/00—Details relating to membrane preparation
    • B01D2323/10—Specific pressure applied
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2323/00—Details relating to membrane preparation
    • B01D2323/50—Control of the membrane preparation process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00162—Controlling or regulating processes controlling the pressure

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Water Supply & Treatment (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Chemical Vapour Deposition (AREA)

Abstract

On propose un procédé de production d’un film de zéolite en continu et efficacement. De la zéolite est formée sur une surface d’un support à l’aide d’un procédé incluant : une première étape consistant à fixer des cristaux fins de zéolite à une surface d’un support ; une deuxième étape consistant à préparer du gel synthétique pour la croissance des cristaux fins ; une troisième étape consistant à placer le support et le gel synthétique dans un réacteur et à réaliser une synthèse hydrothermique ; et une quatrième étape consistant à nettoyer le support soumis à la synthèse hydrothermique, dans lequel dans la troisième étape, des contenants multiples agencés pour pouvoir se déplacer dans un appareil à température constante sont chacun utilisés comme réacteur, la température et la pression pour la synthèse hydrothermique sont ajustées par la température et la pression dans l’appareil à température constante, et le temps de réaction de la synthèse hydrothermique est ajusté en réglant le temps allant du moment où le réacteur entre dans l’appareil à température constante au moment où le réacteur sort de l’appareil à température constante. Figure pour l'abrégé : Figure 1
FR2004212A 2019-05-09 2020-04-28 Procédé de production de film de zéolite Active FR3095813B1 (fr)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2019-089194 2019-05-09
JP2019089194A JP6611295B1 (ja) 2019-05-09 2019-05-09 ゼオライト膜の製造方法
PCT/JP2019/029592 WO2020225932A1 (fr) 2019-05-09 2019-07-29 Procédé de fabrication de membrane de zéolite

Publications (2)

Publication Number Publication Date
FR3095813A1 FR3095813A1 (fr) 2020-11-13
FR3095813B1 true FR3095813B1 (fr) 2022-10-28

Family

ID=68692030

Family Applications (1)

Application Number Title Priority Date Filing Date
FR2004212A Active FR3095813B1 (fr) 2019-05-09 2020-04-28 Procédé de production de film de zéolite

Country Status (9)

Country Link
US (1) US11034587B2 (fr)
JP (1) JP6611295B1 (fr)
KR (1) KR102432100B1 (fr)
CN (1) CN111249911A (fr)
DE (1) DE102020204901B4 (fr)
FR (1) FR3095813B1 (fr)
MY (1) MY190742A (fr)
TW (1) TWI704957B (fr)
WO (1) WO2020225932A1 (fr)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102668540B1 (ko) 2021-11-02 2024-05-22 주식회사 케이티앤지 헤파 필터를 포함하는 부류연 제거 장치

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20010048971A1 (en) * 1997-09-17 2001-12-06 Sridhar Komarneni Method of producing a porous ceramic with a zeolite coating
CN1112231C (zh) * 2000-02-24 2003-06-25 中国石油化工集团公司 制备x型分子筛膜的方法
JP2004076087A (ja) 2002-08-15 2004-03-11 Univ Waseda 気相合成法による酸化珪素系セラミック膜の製造方法及び製造装置
JP2004099338A (ja) 2002-09-05 2004-04-02 Mitsui Eng & Shipbuild Co Ltd ゼオライト膜の合成方法及び合成装置
JP4923487B2 (ja) * 2005-09-01 2012-04-25 三菱化学株式会社 ゼオライト分離膜及びその製造方法
JP5231748B2 (ja) * 2007-04-03 2013-07-10 信越化学工業株式会社 ゼオライト微粒子の製造方法、安定化されたゼオライト及びその利用方法
JP5125221B2 (ja) * 2007-05-18 2013-01-23 日立造船株式会社 ゼオライト膜の水熱合成装置
CN201127733Y (zh) * 2007-12-11 2008-10-08 山东新华医疗器械股份有限公司 连续式灭菌器
JP5121605B2 (ja) 2008-07-08 2013-01-16 日立造船株式会社 ゼオライト分離膜の製造方法
JP2010058015A (ja) * 2008-09-02 2010-03-18 Hitachi Zosen Corp ゼオライト膜の形成法
JP2010158665A (ja) * 2008-12-10 2010-07-22 Ngk Insulators Ltd Ｄｄｒ型ゼオライト膜配設体の製造方法
CN102791366B (zh) * 2010-02-25 2015-05-06 日本碍子株式会社 沸石膜以及沸石膜的制造方法
JP5087644B2 (ja) 2010-03-05 2012-12-05 三井造船株式会社 Ｚｓｍ−５型ゼオライト膜の製造方法
JP6167482B2 (ja) 2012-03-06 2017-07-26 三菱ケミカル株式会社 多孔質支持体−ゼオライト膜複合体の製造方法

Also Published As

Publication number Publication date
JP6611295B1 (ja) 2019-11-27
WO2020225932A1 (fr) 2020-11-12
TW202041273A (zh) 2020-11-16
FR3095813A1 (fr) 2020-11-13
KR102432100B1 (ko) 2022-08-17
DE102020204901B4 (de) 2022-04-28
US20200392007A1 (en) 2020-12-17
US11034587B2 (en) 2021-06-15
DE102020204901A1 (de) 2020-11-12
MY190742A (en) 2022-05-12
JP2020182919A (ja) 2020-11-12
TWI704957B (zh) 2020-09-21
KR20210148382A (ko) 2021-12-07
CN111249911A (zh) 2020-06-09

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