DE2401904C3 - Polyäthergemische - Google Patents
PolyäthergemischeInfo
- Publication number
- DE2401904C3 DE2401904C3 DE2401904A DE2401904A DE2401904C3 DE 2401904 C3 DE2401904 C3 DE 2401904C3 DE 2401904 A DE2401904 A DE 2401904A DE 2401904 A DE2401904 A DE 2401904A DE 2401904 C3 DE2401904 C3 DE 2401904C3
- Authority
- DE
- Germany
- Prior art keywords
- mdg
- polyether mixtures
- polyether
- mixtures
- total
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000000203 mixture Substances 0.000 title claims description 8
- 239000004721 Polyphenylene oxide Substances 0.000 title claims 2
- 229920000570 polyether Polymers 0.000 title claims 2
- 150000001875 compounds Chemical class 0.000 claims 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- 239000007795 chemical reaction product Substances 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- AFCARXCZXQIEQB-UHFFFAOYSA-N N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CCNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 AFCARXCZXQIEQB-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M3/00—Liquid compositions essentially based on lubricating components other than mineral lubricating oils or fatty oils and their use as lubricants; Use as lubricants of single liquid substances
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
- C08G65/2606—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups
- C08G65/2609—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups containing aliphatic hydroxyl groups
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
- C10M2209/107—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of two or more specified different alkylene oxides covered by groups C10M2209/104 - C10M2209/106
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/08—Hydraulic fluids, e.g. brake-fluids
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polyethers (AREA)
- Lubricants (AREA)
Description
Tabelle 2 | 2 | Einsätze (l/h) | 24 | Tabelle 3 | öl) | 01 904 | 360 | DE-AS | 1231835 | MG | MG AG | 3 | 360 | 4 | 360 | 3,1 | 10 | 360 | 6 | 350 | 0,66 | 7 | 340 | t | |
Kennzahlen der Mischoxalkylate von | 3 | Äther frisch (vgl. Zeile 1) | 990 | Oxalkylierungskomp. M | M | 990 | 990 | 990 | 990 | 0,52 | 990 | j - |
|||||||||||||
Zeile | 4 | Äther Kreislauf | 145 | Zusammensetzung des Oxidgemisches |
1 | 1,5 1,5 | 125 | 100 | 5,1 | 75 | 115 | 2,7 | 150 | > | |||||||||||
9' | 5 | E im Gemisch | Beispiel 1 bis | 7 | 80 | I (kg) 1 | 1 | 0,76 | 1,14 1,14 | 100 | 125 | 5 | 150 | 150 | 4,7 | 150 | I | ||||||||
a | 6 | E im Seitenstrom | Beispiel 1 2 |
225 | I (kMol) 0,76 | 0,76 | 4,4 | 4,0 4,0 | 225 | 225 | 225 | 265 | 23,8 | 300 | |||||||||||
b | E gesamt | 225 | (E+ P) ,..„ ~ . , | 4,4 | 225 | 225 | 225 | 175 | 130 | \ | |||||||||||||||
C | 7 | P im Gemisch | 360 | 1800 | Oxalk. Komp. | 5,4 | 5,0 5,0 | 1800 | 1800 | 1800 | 1790 | 252 | 1780 | ||||||||||||
d | 8 | Gesamteinsatz | 990 | MDG | Gesamtoxidgehalt | 4,4 | MDG | MDG | MDG MDG | 301 | MDG | ||||||||||||||
e | 225 | (E + P) /.,,-K,„n , 4 | ! | ||||||||||||||||||||||
f | 9 | - | 1 | Alkohol | 1 | 1 | 1 | 12,8 | 0,44 | ||||||||||||||||
g | 10 | 225 | 0,76 | 0,76 | 0,76 | 0,76 | 890 | 0,33 | |||||||||||||||||
1 | 225 | 2,7 | 2,7 | 2,7 | 2,7 | 2,7 | |||||||||||||||||||
1800 | 4,7 | 4,7 | 4,7 | 4,7 | 4,7 | ||||||||||||||||||||
In das System eingespeiste Oxalky- lierungskomponente (vgl. Zeile a) |
MDG | 30,4 | 30,4 | 30,4 | 30,4 | 18,0 | |||||||||||||||||||
Zusammensetzung des Oxidgemisches | EDG MDG | ||||||||||||||||||||||||
p | 1 | 255 | 255 | 255 | 255 | 249 | |||||||||||||||||||
ζ (kMol) E |
0,76 | 303 | 301 | 302 | 302 | 1,5 1,86 | 303 | S % |
|||||||||||||||||
(E + P) ,...,., | 2,7 | 1,14 1,41 | \ | ||||||||||||||||||||||
Oxalk. Komp. (kMol) | 4,7 | 13,0 | 12,9 | 12,8 | 12,6 | 3,15 3,08 | 13,3 |
h
t I |
|||||||||||||||||
(E -I- P) | 30,4 | 962 | 932 | 905 | 870 | 950 | ! | ||||||||||||||||||
Alkohol | 5,15 5,08 | 1 | |||||||||||||||||||||||
Gew.-% P im Endprodukt (bez. auf Ges. Oxid) |
255 | Kennzahlen der Mischoxalkylate verschiedener Anmelder | 1 | ||||||||||||||||||||||
Kennzahlen des Endproduktes | 301 | Zeile | DE-OS 1593178 |
DE-OS | 21 37 970 | I | |||||||||||||||||||
Mittl. Molgewicht | 1 | ATG | MDG | MDG | MDG |
J
1 |
|||||||||||||||||||
Siedepunkt (X/ASTM) | 13,1 | 1 | |||||||||||||||||||||||
Viskosität | 970 | 2 | nur P . „, eingesetzt ' |
1,86 | 1,86 |
1
f: a 1 |
|||||||||||||||||||
CSt20O | 3 | nur P eingesetzt' |
1,41 | 1,41 | it ϊ ι |
||||||||||||||||||||
cst_40o | 4 | nur P 0,6 |
3,26 | 3,12 |
S
ι |
||||||||||||||||||||
ι
ι |
|||||||||||||||||||||||||
5 | 3,6 | 5,26 | 5,12 |
S
'ί ϊ! 1 |
|||||||||||||||||||||
\ | |||||||||||||||||||||||||
ί | |||||||||||||||||||||||||
ί | |||||||||||||||||||||||||
11 12
Fortsetzung
Zeile DE-AS 1231835 DE-OS DE-OS 2137970
1593178
6 Gew.-% P im Endprodukt 39,7 41,7 41,7 49,5 49,5 20,7 40,8 43,4 38,9 42,2 42,3
(bez. auf Gesamtoxid)
Kennzahlen des Endproduktes
7 Mittleres Molgewicht 202 252 296 282 296 213 276 287 282 281 283
8 Siedepunkt(°C/ASTM) 244 256 272 256 271 262 300 305 300 297 · 298
Viskosität
9 cst20o 12,1 16,8 ~17 16,5 16,8 10,5 nicht aufgeführt
10 CSL40O 930 1569 fest 1563 1663 620 1640
Claims (1)
1. Verfahren zur Herstellung von Polyäthergemischen, hauptsächlich bestehend aus Verbindungen
der allgemeinen Formel
RO · (CH2CH2O)x
CH2 · CHOJ3,(CH2CH2O)Z - H
(D
10
Priority Applications (11)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE2401904A DE2401904C3 (de) | 1974-01-16 | 1974-01-16 | Polyäthergemische |
ZA00750005A ZA755B (en) | 1974-01-16 | 1975-01-02 | Polyether mixtures |
NL7500313A NL7500313A (nl) | 1974-01-16 | 1975-01-10 | Polyethermengsels. |
GB1339/75A GB1480432A (en) | 1974-01-16 | 1975-01-13 | Polyethers and their use as brake fluids |
IT19263/75A IT1028363B (it) | 1974-01-16 | 1975-01-14 | Miscele di polieteri |
AT22075A ATA22075A (de) | 1974-01-16 | 1975-01-14 | Bremsflussigkeit |
JP50006001A JPS50101308A (de) | 1974-01-16 | 1975-01-14 | |
SE7500423A SE7500423L (de) | 1974-01-16 | 1975-01-15 | |
BR281/75A BR7500281A (pt) | 1974-01-16 | 1975-01-15 | Misturas de polieter e processo para sua preparacao continua |
FR7501250A FR2257675B1 (de) | 1974-01-16 | 1975-01-16 | |
BE152430A BE824445A (fr) | 1974-01-16 | 1975-01-16 | Melanges de polyethers utilisables dans des systemes hydrauliques et leur preparation |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE2401904A DE2401904C3 (de) | 1974-01-16 | 1974-01-16 | Polyäthergemische |
Publications (3)
Publication Number | Publication Date |
---|---|
DE2401904A1 DE2401904A1 (de) | 1975-11-27 |
DE2401904B2 DE2401904B2 (de) | 1979-07-19 |
DE2401904C3 true DE2401904C3 (de) | 1980-03-06 |
Family
ID=5904903
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE2401904A Expired DE2401904C3 (de) | 1974-01-16 | 1974-01-16 | Polyäthergemische |
Country Status (11)
Country | Link |
---|---|
JP (1) | JPS50101308A (de) |
AT (1) | ATA22075A (de) |
BE (1) | BE824445A (de) |
BR (1) | BR7500281A (de) |
DE (1) | DE2401904C3 (de) |
FR (1) | FR2257675B1 (de) |
GB (1) | GB1480432A (de) |
IT (1) | IT1028363B (de) |
NL (1) | NL7500313A (de) |
SE (1) | SE7500423L (de) |
ZA (1) | ZA755B (de) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5212685A (en) * | 1975-07-22 | 1977-01-31 | Sanyo Chem Ind Ltd | High boiling brake fluid |
DE3207612C2 (de) * | 1982-03-03 | 1986-04-03 | Akzo Gmbh, 5600 Wuppertal | Polyätherderivate und deren Verwendung als Emulgatoren |
DE3249740C2 (de) * | 1982-03-03 | 1986-07-17 | Akzo Gmbh, 5600 Wuppertal | Emulsionen mit Polyätherderivaten als Emulgator |
DE3829839A1 (de) * | 1988-09-02 | 1990-03-08 | Akzo Gmbh | Verdickungsmittel fuer waessrige systeme |
SE467254B (sv) * | 1990-07-02 | 1992-06-22 | Perstorp Ab | Foerfarande foer framstaellning av etoxylerat polyolpropoxylat |
US5543557A (en) * | 1990-07-02 | 1996-08-06 | Perstorp Ab | Acrylate monomer having a reduced primary irritation index and a method of making same |
-
1974
- 1974-01-16 DE DE2401904A patent/DE2401904C3/de not_active Expired
-
1975
- 1975-01-02 ZA ZA00750005A patent/ZA755B/xx unknown
- 1975-01-10 NL NL7500313A patent/NL7500313A/xx not_active Application Discontinuation
- 1975-01-13 GB GB1339/75A patent/GB1480432A/en not_active Expired
- 1975-01-14 JP JP50006001A patent/JPS50101308A/ja active Pending
- 1975-01-14 AT AT22075A patent/ATA22075A/de not_active IP Right Cessation
- 1975-01-14 IT IT19263/75A patent/IT1028363B/it active
- 1975-01-15 SE SE7500423A patent/SE7500423L/xx unknown
- 1975-01-15 BR BR281/75A patent/BR7500281A/pt unknown
- 1975-01-16 BE BE152430A patent/BE824445A/xx unknown
- 1975-01-16 FR FR7501250A patent/FR2257675B1/fr not_active Expired
Also Published As
Publication number | Publication date |
---|---|
FR2257675B1 (de) | 1978-07-13 |
ZA755B (en) | 1976-01-28 |
BR7500281A (pt) | 1975-11-04 |
DE2401904B2 (de) | 1979-07-19 |
NL7500313A (nl) | 1975-07-18 |
BE824445A (fr) | 1975-07-16 |
SE7500423L (de) | 1975-07-17 |
FR2257675A1 (de) | 1975-08-08 |
GB1480432A (en) | 1977-07-20 |
IT1028363B (it) | 1979-01-30 |
ATA22075A (de) | 1978-04-15 |
DE2401904A1 (de) | 1975-11-27 |
JPS50101308A (de) | 1975-08-11 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
C3 | Grant after two publication steps (3rd publication) | ||
8339 | Ceased/non-payment of the annual fee |