CN206321315U - The density calibration system of mass flowmenter - Google Patents
The density calibration system of mass flowmenter Download PDFInfo
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Abstract
本实用新型提供一种质量流量计的密度标定系统,该系统包括:标定溶液装置,其用于提供多种密度不同的标定溶液;溶液泵,其用于提供动力将标定溶液以一定压力流动于标定管道内;标准表与多个待测的质量流量计沿所述溶液泵输出端均匀安装于所述标定管道上;所述标准表用于为标定管道内标定溶液的密度;计算机,其分别连接多个待测的质量流量计、标准表和开关;其用于控制所述开关切换不同介质的标定溶液标定所述质量流量计的密度,按照密度标定数学模型将计算的密度标定系数写入对应的质量流量计。采用计算机在不同介质的标定溶液,多次测量质量流量计的密度,通过密度标定数学模型计算待测质量流量计的密度,提高了标定的效率与精度。
The utility model provides a density calibration system for a mass flowmeter, which comprises: a calibration solution device, which is used to provide a variety of calibration solutions with different densities; a solution pump, which is used to provide power to flow the calibration solution at a certain pressure In the calibration pipeline; a standard gauge and a plurality of mass flowmeters to be tested are evenly installed on the calibration pipeline along the output end of the solution pump; the standard gauge is used to calibrate the density of the solution in the calibration pipeline; the computer, respectively Connect a plurality of mass flowmeters to be tested, standard meters and switches; it is used to control the switches to switch the calibration solution of different media to calibrate the density of the mass flowmeter, and write the calculated density calibration coefficient according to the density calibration mathematical model Corresponding mass flow meter. Using computer calibration solutions in different media, the density of mass flowmeters is measured multiple times, and the density of mass flowmeters to be tested is calculated through the density calibration mathematical model, which improves the efficiency and accuracy of calibration.
Description
技术领域technical field
本实用新型属于仪表校正技术领域,特别是涉及一种质量流量计的密度标定系统。The utility model belongs to the technical field of instrument correction, in particular to a density calibration system of a mass flow meter.
背景技术Background technique
质量流量计,即科里奥利力质量流量计,它是利用流体力学原理来研发设计的一款流量计量仪器仪表。其主要用于测量气体、液体的质量流量和密度,以及质量流量和密度衍生出来的体积流量、总质量、总体积等工程所需的参数。质量流量计可测的流体范围比较广泛,包括高粘度液的各种液体,含有固形物的浆液,含有少量均匀分布气体的液体,有足够密度的气体,如高压的气体。总而,它能够测量液体,悬浮液,乳浊液和气体的质量流量、密度和温度。Mass flowmeter, that is, Coriolis force mass flowmeter, is a flow measurement instrument developed and designed using the principle of fluid mechanics. It is mainly used to measure the mass flow and density of gas and liquid, as well as the volume flow, total mass and total volume derived from mass flow and density, etc. Mass flowmeters can measure a wide range of fluids, including various liquids with high viscosity liquids, slurries containing solids, liquids containing a small amount of uniformly distributed gas, and gases with sufficient density, such as high-pressure gases. Overall, it is capable of measuring mass flow, density and temperature of liquids, suspensions, emulsions and gases.
对于质量流量计的质量流量数学模型的建立与实现,以及在生产中实现标定的流程,在国内外的很多论文、期刊和专利上都有大量的阐述,可供参数方法数不胜数,但是在密度方面的数学模型和标定方法及相关的标定设备上可参考的文献资料并不多。对于质量流量计来讲,第一参数为质量流量,与它相关且对应正比例输出的参数就是传感器测量管两侧检测输出正弦信号的相位差;第二参数为密度,它与传感器自身固有的机械频率相关,只有第二参数密度的存在,才会有由质量流量和密度衍生出来的体积流量和总体积等工程参数。所以在石油、石化、造纸、食品、制药等众多领域中用于计量各种常规流体、非常规流体、浆液、液化气体和压缩天然气的质量流量、密度、体积流量等参数时就会用到质量流量计。因此,对于质量流量计的生厂商来说,提高改善质量流量计传感器的设计、生产加工工艺,以及质量流量标定装置、密度标定装置至关重要。For the establishment and realization of the mass flow mathematical model of the mass flowmeter, as well as the calibration process in production, there are a lot of explanations in many papers, journals and patents at home and abroad, and there are countless parameter methods available, but in terms of density There are not many literatures that can be referred to on the mathematical model, calibration method and related calibration equipment. For mass flowmeters, the first parameter is mass flow, and the parameter related to it and corresponding to the proportional output is the phase difference of the output sinusoidal signal detected on both sides of the sensor measuring tube; the second parameter is density, which is related to the inherent mechanical properties of the sensor itself. Frequency dependent, only the existence of the second parameter density, there will be engineering parameters such as volume flow and total volume derived from mass flow and density. Therefore, in many fields such as petroleum, petrochemical, papermaking, food, pharmaceuticals, etc., mass flow rate, density, volume flow rate and other parameters of various conventional fluids, unconventional fluids, slurry, liquefied gas and compressed natural gas will be used. flow meter. Therefore, for mass flowmeter manufacturers, it is very important to improve the design, production and processing technology of mass flowmeter sensors, as well as mass flow calibration devices and density calibration devices.
如图1所示,为现有的科里奥利力质量流量计密度标定系统的结构示意图,其中,低气压缸,其用于存放小于5个大气压强的低压干燥空气;气阀,其用于控制低气压缸内的低压气体进入标定管道的开关;标定溶液器皿,其用于盛放密度标定的介质溶液,通常标定溶液在该器皿中配比;溶液进口端,其为密度标定溶液的起始端,设计为漏斗式,便于标定溶液经过此端口流入传感器测量管道而无侧漏的现象;标定管道,其用于标定介质溶液流经的通道;质量流量计,其为待密度标定的质量流量计;固定基架,其为水泥桩,用于固定装夹待密度标定的质量流量计;溶液出口端,其为密度标定管道的终端,设计为漏斗式,便于标定溶液经过此端口流入计量体积的容具中;开关,其用于控制密度标定溶液流入体积容具的量;体积容具,其用于盛放密度标定的介质溶液,同时计量密度标定溶液的体积;电子称,其用于计量体积容具内密度标定溶液的质量。As shown in Figure 1, it is a schematic structural diagram of an existing Coriolis force mass flowmeter density calibration system, wherein, the low-pressure cylinder is used to store low-pressure dry air less than 5 atmospheres; the air valve is used for The switch used to control the low-pressure gas in the low-pressure cylinder entering the calibration pipeline; the calibration solution container, which is used to hold the medium solution for density calibration, and the calibration solution is usually proportioned in the container; the solution inlet port, which is the density calibration solution. The starting end is designed as a funnel, which is convenient for the calibration solution to flow into the sensor measurement pipeline through this port without side leakage; the calibration pipeline is used to calibrate the channel through which the medium solution flows; the mass flowmeter is the mass to be calibrated for density Flowmeter; fixed base frame, which is a cement pile, used to fix and clamp the mass flowmeter to be calibrated; the solution outlet port, which is the terminal of the density calibration pipe, is designed as a funnel, which is convenient for the calibration solution to flow into the meter through this port In the container of volume; switch, which is used to control the amount of density calibration solution flowing into the volume container; volume container, which is used to hold the medium solution for density calibration, and simultaneously measure the volume of density calibration solution; electronic scale, which is used The mass of the density calibration solution in the metered volume.
图1中的质量流量计的密度标定系统的标定方法流程,详述如下:The flow chart of the calibration method of the density calibration system of the mass flowmeter in Fig. 1 is described in detail as follows:
步骤1,将质量流量计密度标定系统置于25℃的恒温密室中,同时,使得气阀和标定管道终端的开关均处于关闭状态;Step 1, put the mass flowmeter density calibration system in a constant temperature closed room at 25°C, and at the same time, make the gas valve and the switch at the end of the calibration pipeline in the closed state;
步骤2,将待测的质量流量计,如图1所示的方式进行安装于标定管道上,且保证标定管道与质量流量计安装法兰处于密封状态,即无泄漏现象,同时,保证质量流量计壳体与地面垂直;Step 2, install the mass flowmeter to be tested on the calibration pipeline as shown in Figure 1, and ensure that the calibration pipeline and the mounting flange of the mass flowmeter are in a sealed state, that is, there is no leakage, and at the same time, the mass flow rate is guaranteed The meter housing is perpendicular to the ground;
步骤3,将待密度标定的质量流量计进行上电工作,同时将5种以上不同密度的标定溶液(介质溶液1,介质溶液2,介质溶液3……)也放置于用于密度标定的密室中,保持该状态下工作180分钟左右,其目的是使质量流量计密度标定的整套系统和密度标定溶液的温度均与密室温度相同或无限接近;Step 3, power on the mass flowmeter to be calibrated for density, and place more than 5 calibration solutions of different densities (medium solution 1, medium solution 2, medium solution 3...) in the secret room for density calibration In the middle, keep working in this state for about 180 minutes, the purpose is to make the temperature of the entire system of mass flowmeter density calibration and the temperature of the density calibration solution be the same as or infinitely close to the temperature of the closed room;
步骤4,采集当前25℃的恒温密室中当前标定管道上待密度标定质量流量计转换器上输出传感器的空管频率;Step 4, collect the empty pipe frequency of the output sensor on the mass flowmeter converter to be calibrated on the currently calibrated pipeline in the current 25°C constant temperature closed chamber;
步骤5,打开溶液进口端上面的密封盖,将密度标定介质溶液1通过标定溶液器皿装置缓慢的倒入溶液进口端,观测溶液出口端的液面变化,当液面接近溶液出口端的顶端时,停止溶液进口端继续倒入密度标定介质溶液1;Step 5, open the sealing cover above the solution inlet, slowly pour the density calibration medium solution 1 into the solution inlet through the calibration solution container device, observe the change of the liquid level at the solution outlet, when the liquid level is close to the top of the solution outlet, stop Continue to pour density calibration medium solution 1 into the solution inlet;
步骤6,延时2分钟,直到密度标定介质溶液1在标定管道装置内处于平稳状态时,采集当前质量流量计转换器上输出传感器的频率值;Step 6, delaying for 2 minutes, until the density calibration medium solution 1 is in a stable state in the calibration pipeline device, collect the frequency value of the output sensor on the current mass flowmeter converter;
步骤7,缓慢调节标定管道终端的开关,将管道内的密度标定介质溶液1排放至电子称上端的容具中,使密度标定介质溶液1的排出量达到容具1000ml刻度的位置;Step 7, slowly adjust the switch at the end of the calibration pipeline, discharge the density calibration medium solution 1 in the pipeline into the container at the upper end of the electronic scale, so that the discharge volume of the density calibration medium solution 1 reaches the position of the 1000ml scale of the container;
步骤8,获取电子称上计量1000ml密度标定介质溶液1的质量示数,且将密度标定介质溶液1倒回原溶液装置中,并换取相同容量的干燥的容具放置电子称上面;Step 8, obtain the mass indication of 1000ml of density calibration medium solution 1 measured on the electronic scale, and pour the density calibration medium solution 1 back into the original solution device, and replace it with a dry container of the same capacity and place it on the electronic scale;
步骤9,将溶液进口端上方的密封盖压紧溶液进口端,缓慢调节气阀,直到将标定管道内的密度标定介质溶液1驱除标定管道外,关闭气阀;Step 9, press the sealing cap above the solution inlet end tightly to the solution inlet end, slowly adjust the air valve until the density calibration medium solution 1 in the calibration pipeline is driven out of the calibration pipeline, and then close the air valve;
步骤10,重复步骤5~9,完成其它密度标定介质溶液(介质溶液2,介质溶液3……)的标定流程;Step 10, repeat steps 5 to 9 to complete the calibration process of other density calibration medium solutions (medium solution 2, medium solution 3...);
步骤11,依据密度标定记录数据,计算待密度标定质量流量计的密度系数,并将系数通过按键操作的方式写入至质量流量计转换器的EEPROM中;Step 11, calculate the density coefficient of the mass flowmeter to be density calibrated according to the density calibration record data, and write the coefficient into the EEPROM of the mass flowmeter converter through key operation;
步骤12,进行质量流量计的密度精度检测与重复性检测;Step 12, performing density accuracy detection and repeatability detection of the mass flowmeter;
步骤13,打开溶液进口端上面的密封盖和标定管道终端的开关,将密度标定介质溶液1 通过标定溶液器皿装置缓慢的倒入溶液进口端,观察容具内液面的变化,当液面刻度接近为1000ml时,关闭标定管道终端的开关,继续向溶液进口端倒入适量的密度标定介质溶液1;Step 13, open the sealing cover above the solution inlet and the switch at the end of the calibration pipe, slowly pour the density calibration medium solution 1 through the calibration solution vessel device into the solution inlet, observe the change of the liquid level in the container, when the liquid level scale When it is close to 1000ml, turn off the switch at the end of the calibration pipeline, and continue to pour an appropriate amount of density calibration medium solution 1 into the solution inlet;
步骤14,微调标定管道终端的开关的开度,直到密度标定介质溶液1滴落值容具内达到1000ml刻度位置位置,采集当前质量流量计转换器输出密度值和电子称计量密度标定介质溶液1的总质量;Step 14, fine-tune the opening of the switch at the end of the calibration pipeline until the drop value of the density calibration medium solution 1 reaches the 1000ml scale position in the container, collect the current output density value of the mass flowmeter converter and the electronic scale to measure the density calibration medium solution 1 the total mass of
步骤15,将溶液进口端上方的密封盖压紧溶液进口端,微调气阀,直到将标定管道内的密度标定介质溶液1驱除标定管道外,关闭气阀;Step 15, press the sealing cap above the solution inlet end tightly to the solution inlet end, fine-tune the air valve until the density calibration medium solution 1 in the calibration pipeline is driven out of the calibration pipeline, and then close the air valve;
步骤16,重复步骤13~15,完成其它选取密度标定介质溶液的密度检定流程;Step 16, repeating steps 13 to 15 to complete the density verification process of other selected density calibration medium solutions;
步骤17,计算质量流量计的密度输出精度及重复性。Step 17, calculating the density output accuracy and repeatability of the mass flow meter.
现有的科里奥利力质量流量计密度标定系统中,最多仅能容纳3台质量流量计的密度标定与检测,极大地降低了质量流量计的标定效率;同时,在整个标定与检测的流程中,需要要人工参与,且标定溶液的密度均是以小容具为计量体积,电子秤计量标定溶液的质量,通过计算确定标定溶液的密度标准值。然而,这些因素会带来一定程度的计量标定误差,降低了整个质量流量计密度标定系统的精度。In the existing Coriolis force mass flowmeter density calibration system, it can only accommodate the density calibration and detection of 3 mass flowmeters at most, which greatly reduces the calibration efficiency of mass flowmeters; at the same time, in the whole calibration and detection In the process, manual participation is required, and the density of the calibration solution is measured with a small container as the volume. The electronic scale measures the quality of the calibration solution, and the standard value of the density of the calibration solution is determined by calculation. However, these factors will bring a certain degree of measurement calibration error, which reduces the accuracy of the entire mass flowmeter density calibration system.
实用新型内容Utility model content
鉴于以上所述现有技术的缺点,本实用新型的目的在于提供一种质量流量计的密度标定系统,用于解决现有技术中质量流量计在密度标定时,需要人工操作导致整个质量流量计密度标定的效率低与精度低问题。In view of the above-mentioned shortcomings of the prior art, the purpose of this utility model is to provide a density calibration system for mass flowmeters, which is used to solve the problem of manual operation of mass flowmeters in the prior art during density calibration, which causes the entire mass flowmeter to Low efficiency and low precision of density calibration.
为实现上述目的及其他相关目的,本实用新型提供一种质量流量计的密度标定系统,包括:In order to achieve the above purpose and other related purposes, the utility model provides a density calibration system for a mass flow meter, including:
标定溶液装置,其用于提供多种密度不同的标定溶液;溶液泵,其用于提供动力将标定溶液以一定压力流动于标定管道内;标准表与多个待测的质量流量计沿所述溶液泵输出端均匀安装于所述标定管道上;所述标准表用于为标定管道内标定溶液的密度;计算机,其分别连接多个待测的质量流量计、标准表和开关;其用于控制所述开关切换不同介质的标定溶液标定所述质量流量计的密度,按照密度标定数学模型将计算的密度标定系数写入对应的质量流量计。Calibration solution device, which is used to provide a variety of calibration solutions with different densities; solution pump, which is used to provide power to flow the calibration solution in the calibration pipeline at a certain pressure; The output end of the solution pump is evenly installed on the calibration pipeline; the standard meter is used to calibrate the density of the solution in the calibration pipeline; the computer is connected to a plurality of mass flow meters, standard meters and switches to be measured respectively; it is used for Control the switch to switch the calibration solutions of different media to calibrate the density of the mass flowmeter, and write the calculated density calibration coefficient into the corresponding mass flowmeter according to the density calibration mathematical model.
如上所述,本实用新型的质量流量计的密度标定系统,具有以下有益效果:As mentioned above, the density calibration system of the mass flowmeter of the present invention has the following beneficial effects:
通过将原有人工操作的密度标定系统替换为计算机自动控制的密度标定系统,相对于原有密度标定系统每次标定数量由三台变成了十台,提高了产品的标定的效率;采用计算机控制开关切换在不同介质的标定溶液,在每种标定溶液下多次测量质量流量计的密度,标定过程中完全无需人为参与,通过密度标定数学模型计算待测质量流量计的密度,不仅杜绝了传统质量体积方式的标定误差,还大幅度提高了质量流量计密度标定的精度;同时,在密度标定系统中引入了恒压恒流罐,消除了因溶液泵在工作时所产的标定溶液涓流与空气气泡的问题,从本质上提高了质量流量计的标定精度。By replacing the original manually operated density calibration system with a computer-controlled density calibration system, compared with the original density calibration system, the number of each calibration is changed from three to ten, which improves the efficiency of product calibration; adopts computer The control switch switches the calibration solutions in different media, and the density of the mass flowmeter is measured multiple times under each calibration solution. There is no need for human participation in the calibration process. The density of the mass flowmeter to be tested is calculated through the density calibration mathematical model, which not only eliminates the The calibration error of the traditional mass volume method also greatly improves the accuracy of the density calibration of the mass flowmeter; at the same time, a constant pressure and constant flow tank is introduced into the density calibration system, which eliminates the calibration solution produced by the solution pump when it is working. The problem of flow and air bubbles essentially improves the calibration accuracy of the mass flow meter.
附图说明Description of drawings
图1显示为本实用新型提供的现有的科里奥利力质量流量计标定系统的结构示意图;Fig. 1 shows the structural representation of the existing Coriolis force mass flowmeter calibration system provided for the utility model;
图2显示为本实用新型提供的一种质量流量计的密度标定系统结构图;Fig. 2 shows the structural diagram of a density calibration system of a mass flowmeter provided by the utility model;
图3显示为本实用新型提供的一种质量流量计的密度标定系统的实施例结构图。Fig. 3 shows a structure diagram of an embodiment of a mass flow meter density calibration system provided by the utility model.
具体实施方式detailed description
以下由特定的具体实施例说明本实用新型的实施方式,熟悉此技术的人士可由本说明书所揭露的内容轻易地了解本实用新型的其他优点及功效。The implementation of the present utility model is illustrated by specific specific examples below, and those skilled in the art can easily understand other advantages and effects of the present utility model from the content disclosed in this specification.
请参阅图2至图3。须知,本说明书所附图式所绘示的结构、比例、大小等,均仅用以配合说明书所揭示的内容,以供熟悉此技术的人士了解与阅读,并非用以限定本实用新型可实施的限定条件,故不具技术上的实质意义,任何结构的修饰、比例关系的改变或大小的调整,在不影响本实用新型所能产生的功效及所能达成的目的下,均应仍落在本实用新型所揭示的技术内容得能涵盖的范围内。同时,本说明书中所引用的如“上”、“下”、“左”、“右”、“中间”及“一”等的用语,亦仅为便于叙述的明了,而非用以限定本实用新型可实施的范围,其相对关系的改变或调整,在无实质变更技术内容下,当亦视为本实用新型可实施的范畴。Please refer to Figure 2 to Figure 3. It should be noted that the structures, proportions, sizes, etc. shown in the drawings attached to this specification are only used to match the content disclosed in the specification, for those who are familiar with this technology to understand and read, and are not used to limit the implementation of the utility model Therefore, it has no technical substantive meaning. Any modification of structure, change of proportional relationship or adjustment of size shall still fall within the scope of The technical content disclosed by the utility model must be within the scope covered. At the same time, terms such as "upper", "lower", "left", "right", "middle" and "one" quoted in this specification are only for the convenience of description and are not used to limit this specification. The practicable range of the utility model, and the change or adjustment of its relative relationship, without any substantial change in the technical content, shall also be regarded as the practicable scope of the utility model.
请参阅图2,本实用新型提供一种质量流量计的密度标定系统结构图,包括:Please refer to Figure 2, the utility model provides a structural diagram of a density calibration system for a mass flowmeter, including:
标定溶液装置1,其用于提供多种密度不同的标定溶液;溶液泵3,其用于提供动力将标定溶液以一定压力流动于标定管道内;标准表4与多个待测的质量流量计5沿所述溶液泵3输出端均匀安装于所述标定管道上;所述标准表4用于为标定管道内标定溶液的密度;计算机6,其分别连接多个待测的质量流量计5、标准表4和开关3;其用于控制所述开关3切换不同介质的标定溶液标定所述质量流量计5的密度,按照密度标定数学模型将计算的密度标定系数写入对应的质量流量计5。Calibration solution device 1, which is used to provide a variety of calibration solutions with different densities; solution pump 3, which is used to provide power to flow the calibration solution in the calibration pipeline at a certain pressure; standard meter 4 and a plurality of mass flowmeters to be tested 5 is evenly installed on the calibration pipeline along the output end of the solution pump 3; the standard meter 4 is used to calibrate the density of the solution in the calibration pipeline; a computer 6 is connected to a plurality of mass flowmeters to be measured 5, Standard table 4 and switch 3; it is used to control the switch 3 to switch the calibration solution of different media to calibrate the density of the mass flowmeter 5, and write the calculated density calibration coefficient into the corresponding mass flowmeter 5 according to the density calibration mathematical model .
其中,所述计算机6可替换为工控机或终端,标定溶液装置1可为多个,每个标定溶液装置1盛有介质密度相同的标定溶液;而标定溶液装置1、溶液泵3、标准表4、质量流量计5之间均使用标定管道相互连接;且每个标定溶液装置1的输出端与溶液泵3之间的标定管道上均设置一个开关2,每个标定溶液装置1的输入端连接的标定管道上均设置一个开关2,在此处所述开关2保证每次只有一种介质标定溶液在密度标定系统内标定管道流动。Wherein, the computer 6 can be replaced by an industrial computer or a terminal, and the calibration solution device 1 can be multiple, and each calibration solution device 1 is filled with a calibration solution with the same medium density; and the calibration solution device 1, the solution pump 3, the standard gauge 4. The mass flowmeters 5 are connected to each other using calibration pipes; and a switch 2 is set on the calibration pipe between the output end of each calibration solution device 1 and the solution pump 3, and the input end of each calibration solution device 1 A switch 2 is arranged on the connected calibration pipelines, and the switch 2 here ensures that only one medium calibration solution flows in the calibration pipeline in the density calibration system at a time.
所述溶液泵3和标准表4之间设置有用于控制标定溶液流动的开关,而在此处设置对应的关开2可保证溶液泵3通过其自身动力将标定溶液流动于标准表4,同时,在开关闭合时,溶液泵不停地运转可排挤标定管道内存有的空气气泡,其中,所述开关2为阀门、闸门与电磁阀,优选为电磁阀,可直接受计算机6控制,通过计算机6远程控制切换在不同介质的标定溶液,在每种标定溶液下多次测量质量流量计5的密度,标定过程中完全无需人为参与,通过密度标定数学模型计算待测质量流量计5的密度,不仅杜绝了传统质量体积方式的标定误差,还大幅度提高了质量流量计5密度标定的精度。A switch for controlling the flow of the calibration solution is arranged between the solution pump 3 and the standard meter 4, and a corresponding switch 2 is set here to ensure that the solution pump 3 flows the calibration solution to the standard meter 4 through its own power, and at the same time , when the switch is closed, the solution pump keeps running to displace the air bubbles in the calibration pipeline, wherein the switch 2 is a valve, a gate and a solenoid valve, preferably a solenoid valve, which can be directly controlled by the computer 6, through the computer 6 Remotely control and switch the calibration solutions in different media, and measure the density of the mass flowmeter 5 multiple times under each calibration solution, without human participation in the calibration process, and calculate the density of the mass flowmeter 5 to be tested through the density calibration mathematical model, Not only eliminates the calibration error of the traditional mass volume method, but also greatly improves the accuracy of the density calibration of the mass flow meter 5 .
如果对密度标定系统中标定溶液的压力与流速有要求,可在所述溶液泵3和靠近标准表4的开关2之间设有用于稳流稳压的恒压恒流罐,通过打开恒压恒流罐装置上的排气开关,直到溶液泵3供给的标定溶液最大限度的充满恒压恒流罐,则关闭排气开关,其目的是消除标定溶液中存在空气气泡和标定溶液非恒压恒流的状态,在此处如果要设置恒压恒流罐,其必定控制总线连接计算机,以实现自动化控制的目的。If there is a requirement for the pressure and flow rate of the calibration solution in the density calibration system, a constant pressure and constant flow tank for steady flow and pressure can be provided between the solution pump 3 and the switch 2 close to the standard meter 4. By opening the constant pressure The exhaust switch on the constant flow tank device, until the calibration solution supplied by the solution pump 3 fills the constant pressure constant flow tank to the maximum, then close the exhaust switch, the purpose is to eliminate the air bubbles in the calibration solution and the non-constant pressure of the calibration solution In the state of constant current, if a constant pressure and constant current tank is to be installed here, it must be connected to a computer by the control bus to achieve the purpose of automatic control.
在本申请中,所述计算机6与待测的多个质量流量计5、标准表4和开关2均采用控制总线通讯,通过计算机发送指令控制开关2的开启与关闭,采集标准表4与质量流量计5的数据,按照密度标定数学模型计算各个待测质量流量计5密度值与精度。其中,待测的质量流量计5的数目最多为十台,相比原来的最多只能同时标定三台,提高了标定的效率。In the present application, the computer 6 communicates with the multiple mass flowmeters 5 to be tested, the standard meter 4 and the switch 2 through the control bus, and the computer sends instructions to control the opening and closing of the switch 2, and collects the standard meter 4 and the mass flowmeter. For the data of the flowmeter 5, the density value and accuracy of each mass flowmeter 5 to be tested are calculated according to the density calibration mathematical model. Among them, the number of mass flow meters 5 to be tested is at most ten, compared with the original method that can only calibrate at most three at the same time, which improves the efficiency of calibration.
本申请中,密度标定数学模型如下:In this application, the density calibration mathematical model is as follows:
式(1)中,ρ:质量流量计标定计量介质溶液的密度,单位kg/M3;Kd:标定计算输出的密度系数,无量纲;Fe(25):质量流量计传感器在恒温25℃温度下测量管的谐振频率,单位Hz;Fkt:质量流量计传感器整机材质、结构与温度相关的修正系数,通常为每升高或是降低1℃,传感器测量管谐振频率的变化量;T:质量流量计传感器温度;Fr:质量流量计传感器测量管道充满计量介质溶液时的实际输出频率,单位Hz;在计算出Kd的情况下,根据读取的Fr计算出质量流量计标定的介质溶液的密度。In formula (1), ρ: the density of the mass flowmeter calibration measurement medium solution, unit kg/M 3 ; K d : the density coefficient output by the calibration calculation, dimensionless; F e (25): the mass flowmeter sensor at a constant temperature of 25 The resonant frequency of the measuring tube at ℃ temperature, unit Hz; F kt : the correction coefficient related to the material, structure and temperature of the mass flowmeter sensor, usually the change of the resonant frequency of the sensor measuring tube for every increase or decrease of 1°C ; T: mass flowmeter sensor temperature; F r : the actual output frequency of the mass flowmeter sensor when the measuring pipe is filled with the measurement medium solution, unit Hz; in the case of calculating K d , calculate the mass flow rate according to the read F r The density of the medium solution calibrated by the meter.
还包括固定机架,其设置于所述质量流量计5与标准表4的两侧用于支撑其工作,该固定机架优选为水泥支架,其不但可以消除管道的振动对待密度标定质量流量计仪表的影响,也可以消除因质量流量计5传感器自身机械振动对密度标定的影响。同时,该固定机架也是为在线待密度标定整机质量流量计5之间起到隔离的作用,防止待密度标定的质量流量计5之间的相互影响。It also includes a fixed frame, which is arranged on both sides of the mass flowmeter 5 and the standard meter 4 to support its work. The fixed frame is preferably a cement support, which can not only eliminate the vibration of the pipeline, but also eliminate the mass flowmeter to be calibrated for density. The influence of the instrument can also eliminate the influence of the mass flowmeter 5 sensor itself on the density calibration due to the mechanical vibration. At the same time, the fixed frame is also used to isolate the mass flowmeters 5 of the whole machine to be calibrated online, and to prevent the mutual influence between the mass flowmeters 5 to be calibrated.
如图3所示,为本实用新型提供的一种质量流量计的密度标定系统的实施例结构图;包括:As shown in Figure 3, it is a structural diagram of an embodiment of a density calibration system for a mass flowmeter provided by the utility model; including:
在本实施例中,所述待密度标定的质量流量计5的数目为十台,标准表4与十台质量流量计5沿着溶液泵3输出方向从左至右的顺序分别安装于标定管道上,所述质量流量计5与标准表4的两侧用于支撑其工作的固定机架。介质溶液装置1分为五个分别盛有不同介质的标定溶液,其中,第一至第五介质溶液装置1的输出端的标定管道上分别对应安装第一至第五电磁阀,第一至第五介质溶液装置1的输入端的标定管道上分别对应安装第六至第十电磁阀,编号为第十的质量流量计5(即最右边的质量流量计5)输出的标定管道分别连接至各个介质溶液装置1的输入端,以使得每种介质的标定溶液均能在标定管道内循环后重新回到介质溶液装置1,第十一电磁阀安装于溶液泵3与标准表4之间的标定管道上。In this embodiment, the number of mass flowmeters 5 to be calibrated is ten, and the standard meter 4 and ten mass flowmeters 5 are respectively installed in the calibration pipeline along the output direction of the solution pump 3 from left to right. Above, both sides of the mass flow meter 5 and the standard meter 4 are used to support the fixed frame for its work. The medium solution device 1 is divided into five calibration solutions filled with different media, wherein the first to fifth solenoid valves are respectively installed on the calibration pipelines at the output ends of the first to fifth medium solution devices 1, and the first to fifth solenoid valves are respectively installed. The sixth to tenth solenoid valves are respectively installed on the calibration pipelines at the input end of the medium solution device 1, and the calibration pipelines output by the tenth mass flowmeter 5 (that is, the rightmost mass flowmeter 5) are respectively connected to each medium solution The input end of the device 1, so that the calibration solution of each medium can return to the medium solution device 1 after circulating in the calibration pipeline, and the eleventh solenoid valve is installed on the calibration pipeline between the solution pump 3 and the standard gauge 4 .
所述计算机6通过控制总线方式分别连接标准表4、多个质量流量计5与多个电磁阀,通过控制电磁阀开关切换每种介质的标定溶液,例如,在第十一电磁阀打开时,需要盛有某种介质的标定溶液的介质溶液装置1打开其电磁阀,关闭其它电磁阀,使得该种介质的标定溶液流动到整个密度标定系统,当该种介质的标定溶液在标定管道无气泡且处于静止状态时,依次读取待测的质量流量计的输出频率;通过密度标定数学模型计算各个待测的质量流量计的密度系数,然后,重复上述步骤,即可得到一种或多种介质溶液情况下,各个待测的质量流量计5的密度,根据待测的质量流量计5的密度计算对应的质量流量计的精度。The computer 6 is respectively connected to the standard meter 4, a plurality of mass flowmeters 5 and a plurality of electromagnetic valves through a control bus, and switches the calibration solution of each medium by controlling the electromagnetic valve switch. For example, when the eleventh electromagnetic valve is opened, The medium solution device 1 that needs to contain the calibration solution of a certain medium opens its solenoid valve and closes other solenoid valves so that the calibration solution of this medium flows to the entire density calibration system. When the calibration solution of this medium has no bubbles in the calibration pipeline And in a static state, read the output frequency of the mass flowmeter to be tested in sequence; calculate the density coefficient of each mass flowmeter to be tested through the density calibration mathematical model, and then repeat the above steps to obtain one or more In the case of the medium solution, the density of each mass flowmeter 5 to be tested is calculated according to the density of the mass flowmeter 5 to be tested, and the accuracy of the corresponding mass flowmeter is calculated.
在本实施例中,按照上述的质量流量计的密度标定方法,包括:In this embodiment, according to the above-mentioned density calibration method of the mass flow meter, including:
步骤1,初始化密度标定系统,确保待测的质量流量计趋于平稳状态;Step 1, initialize the density calibration system to ensure that the mass flowmeter to be tested tends to a stable state;
具体地,密度标定系统在初始化过程中,计算机控制所有开关均处于关闭状态,将待测的质量流量计安装于标定管道中,确保质量流量计处于密封状态,即无泄漏;标准表与质量流量计均上电,计算机通过总线控制连接准表、质量流量计与电磁阀;例如,一般采用延时几分钟,使得待密度标定的质量流量计在标定管道的空管状态或趋于平稳的工作状态。Specifically, during the initialization process of the density calibration system, the computer controls all switches to be closed, and the mass flowmeter to be tested is installed in the calibration pipeline to ensure that the mass flowmeter is in a sealed state, that is, there is no leakage; the standard meter and mass flow The meters are all powered on, and the computer is connected to the calibration meter, mass flowmeter and solenoid valve through the bus control; state.
步骤2,在质量流量计处于空管状态下,依次读取待测的质量流量计输出的频率值;Step 2, when the mass flowmeter is in an empty pipe state, sequentially read the output frequency value of the mass flowmeter to be tested;
步骤3,开启某种介质标定溶液装置的开关以及靠近标准表的开关,使得该种介质的标定溶液在标定管道循环流动,直到流动于待测的质量流量计中的标定溶液无气泡为止;Step 3, turn on the switch of a certain medium calibration solution device and the switch close to the standard meter, so that the calibration solution of this medium circulates in the calibration pipeline until the calibration solution flowing in the mass flowmeter to be tested has no bubbles;
步骤4,关闭该标定溶液装置的开关以及靠近标准表的开关,直到标定管道内标定溶液处于静止状态为止;Step 4, turn off the switch of the calibration solution device and the switch close to the standard meter until the calibration solution in the calibration pipeline is in a static state;
步骤5,读取标准表当前的密度值,且依次读取待测的质量流量计输出的频率值;Step 5, read the current density value of the standard meter, and sequentially read the output frequency value of the mass flowmeter to be tested;
步骤6,在不同介质的标定溶液下,重复步骤3至5,获取标准表的密度值与待测的质量流量计输出的频率值;Step 6, under the calibration solution of different media, repeat steps 3 to 5 to obtain the density value of the standard meter and the frequency value output by the mass flowmeter to be tested;
步骤7,调用密度标定数学模型依次计算每个待测质量流量计的密度系数,将其写入至对应待测质量流量计内;Step 7, call the density calibration mathematical model to calculate the density coefficient of each mass flowmeter to be tested in turn, and write it into the corresponding mass flowmeter to be tested;
步骤8,在每种介质标定溶液下,多次重复步骤3至4,获取标准表的多次标定的标准密度值,以及待测的质量流量计多次输出的密度值;Step 8, under each medium calibration solution, repeat steps 3 to 4 multiple times to obtain the standard density value of multiple calibrations of the standard meter, and the density value output by the mass flowmeter to be tested multiple times;
步骤9,根据多种介质标定溶液下所对应的标准密度值与质量流量计输出的密度值计算质量流量计的精度。In step 9, the accuracy of the mass flowmeter is calculated according to the corresponding standard density values in the calibration solutions of various media and the density values output by the mass flowmeter.
在本实施例中,将上述方法流程展开即可得到如下流程,详述如下:In this embodiment, the following process can be obtained by expanding the process of the above method, which is described in detail as follows:
1.开启工控机(计算机)中质量流量计密度标定系统软件,关闭整套标定系统中的所有电磁阀门;1. Open the mass flowmeter density calibration system software in the industrial computer (computer), and close all the electromagnetic valves in the entire calibration system;
2.将待密度标定的质量流量计仪表按照从前至后(沿着溶液泵的输出方向,即靠近溶液泵的距离为前,远离溶液泵的距离为后)顺序安装于标定管道,确保无泄漏状态;2. Install the mass flowmeter to be calibrated on the calibration pipeline in order from front to back (along the output direction of the solution pump, that is, the distance close to the solution pump is the front, and the distance away from the solution pump is the rear) to ensure no leakage state;
3.上电初始化待密度标定的质量流量和标准表,通讯总线与工控机的总线通讯接口相连通;3. Power on and initialize the mass flow rate and standard table to be calibrated for density, and the communication bus is connected with the bus communication interface of the industrial computer;
4.进行待密度标定的质量流量和标准表的通讯检测,确保在线的每一台质量流量和标准表均与工控机中的质量流量计密度标定系统软件正常通讯;4. Carry out communication detection of the mass flow rate and standard meter to be calibrated to ensure that each online mass flow rate and standard meter communicates normally with the mass flowmeter density calibration system software in the industrial computer;
5.触发工控机中质量流量计密度标定系统,开始在线质量流量计的密度标定流程;5. Trigger the mass flowmeter density calibration system in the industrial computer to start the density calibration process of the online mass flowmeter;
6.延时3分钟左右,使在线待密度标定的质量流量在空管的状态下处于或趋于平稳的工作状态;6. Delay for about 3 minutes, so that the mass flow rate to be calibrated online is in or tends to a stable working state in the state of an empty pipe;
7.按照从前至后的编号顺序,依次采集进行在线待密度标定的质量流量在空管的状态下频率数据;7. According to the numbering sequence from front to back, sequentially collect the mass flow rate data in the state of empty pipe for online density calibration;
8.通过控制总线开启标定管道上的第一电磁阀、第六电磁阀与第十一电磁阀,其它电磁阀处于关闭状态;8. Open the first solenoid valve, the sixth solenoid valve and the eleventh solenoid valve on the calibration pipeline through the control bus, and the other solenoid valves are closed;
9.在溶液泵的驱动下,第一介质溶液装置中的介质溶液流经标定管道、标准表、在线待密度标定的质量流量计,循环后又通过标定管道流回第一介质溶液装置中,在该状态延时工作几(五)分钟左右,直到整个标定管道及在线待密度标定的质量流量计的测量管中完全由第一介质溶液装置中的介质溶液充满而无气泡状态;9. Driven by the solution pump, the medium solution in the first medium solution device flows through the calibration pipeline, the standard meter, and the online mass flowmeter to be calibrated for density, and then flows back to the first medium solution device through the calibration pipeline after circulation. Work in this state for a few (five) minutes, until the entire calibration pipeline and the measuring tube of the mass flowmeter to be calibrated online are completely filled with the medium solution in the first medium solution device without air bubbles;
10.通过控制总线关闭标定管道上的第一电磁阀、第六电磁阀与第十一电磁阀,直到整个标定管道内密度标定介质溶液处于平静且无流动状态,如,采用延时1分钟可达到平静且无流动状态;10. Close the first solenoid valve, the sixth solenoid valve and the eleventh solenoid valve on the calibration pipeline through the control bus until the density calibration medium solution in the entire calibration pipeline is in a calm and non-flowing state. For example, a delay of 1 minute can be used. Achieving a calm and no-flow state;
11.通过总线读取标准表当前输出的标准密度值,按编号顺序依次读取在线待密度标定的质量流量在该状态下输出频率值;11. Read the standard density value currently output by the standard meter through the bus, and read the mass flow rate to be calibrated online in sequence according to the number sequence, and output the frequency value in this state;
12.重复步骤8)-11),完成第二至第五介质溶液装置中介质溶液的密度标定流程;唯一区别即控制的电磁阀不同,具体如下:12. Repeat steps 8)-11) to complete the density calibration process of the medium solution in the second to fifth medium solution devices; the only difference is that the controlled solenoid valves are different, as follows:
第二介质溶液装置的密度标定需要控制的第二电磁阀、第七电磁阀、第十一电磁阀;The density calibration of the second medium solution device needs to control the second solenoid valve, the seventh solenoid valve, and the eleventh solenoid valve;
第三介质溶液装置的密度标定需要控制的第三电磁阀、第八电磁阀、第十一电磁阀;The density calibration of the third medium solution device needs to control the third solenoid valve, the eighth solenoid valve, and the eleventh solenoid valve;
第四介质溶液装置的密度标定需要控制的第四电磁阀、第九电磁阀、第十一电磁阀;The density calibration of the fourth medium solution device needs to control the fourth solenoid valve, the ninth solenoid valve, and the eleventh solenoid valve;
第五介质溶液装置的密度标定需要控制的第五电磁阀、第十电磁阀、第十一电磁阀;The density calibration of the fifth medium solution device needs to control the fifth solenoid valve, the tenth solenoid valve, and the eleventh solenoid valve;
13.依据内部封装的密度标定数学模型,按照顺序依次计算每一台质量流量计的密度系数,将密度系数依次对应的写入到在线质量流量计转换器中;13. Calculate the density coefficient of each mass flowmeter in sequence according to the density calibration mathematical model of the internal package, and write the density coefficients into the online mass flowmeter converter in sequence;
14.重复检测计算在线质量流量计的密度输出精度;14. Repeated detection and calculation of the density output accuracy of the online mass flowmeter;
15.通过控制总线开启标定管道上的第一电磁阀、第六电磁阀与第十一电磁阀,其它电磁阀处于关闭状态;15. Open the first solenoid valve, the sixth solenoid valve and the eleventh solenoid valve on the calibration pipeline through the control bus, and the other solenoid valves are closed;
16.在溶液泵的驱动下,第一介质溶液装置中的介质溶液流经标定管道、标准表、在线待密度标定的质量流量计,循环后又通过标定管道流回第一介质溶液装置中,在该状态延时工作几(五)分钟左右,直到整个标定管道及在线待密度标定的质量流量计的测量管中完全由第一介质溶液装置中的介质溶液充满而无气泡状态;16. Driven by the solution pump, the medium solution in the first medium solution device flows through the calibration pipeline, the standard meter, and the online mass flowmeter to be calibrated for density, and flows back to the first medium solution device through the calibration pipeline after circulation. Work in this state for a few (five) minutes, until the entire calibration pipeline and the measuring tube of the mass flowmeter to be calibrated online are completely filled with the medium solution in the first medium solution device without air bubbles;
17.通过控制总线关闭标定管道上的第一电磁阀、第六电磁阀与第十一电磁阀,直到整个标定管道内密度标定介质溶液处于平静且无流动状态,如,采用延时1分钟可达到平静且无流动状态;17. Close the first solenoid valve, the sixth solenoid valve and the eleventh solenoid valve on the calibration pipeline through the control bus until the density calibration medium solution in the entire calibration pipeline is in a calm and non-flowing state. For example, a delay of 1 minute can be used. Achieving a calm and no-flow state;
18.通过总线读取标准表此时输出的标准密度值,从前至后依次读取在线待密度标定的质量流量在该状态下输出的密度值,且计算质量流量计的精度;18. Read the standard density value output by the standard meter at this time through the bus, read the density value output by the mass flow to be calibrated online in this state from front to back, and calculate the accuracy of the mass flow meter;
19.重复步骤15)-18),第二次检测第一介质溶液装置中介质溶液密度;19. Repeat steps 15)-18), and detect the density of the medium solution in the first medium solution device for the second time;
20.质量流量计密度标定系统软件重复步骤15)-18),第三次检测第一介质溶液装置中介质溶液密度,依次计算出在线质量流量计密度输出的重复性;20. The mass flowmeter density calibration system software repeats steps 15)-18), and detects the medium solution density in the first medium solution device for the third time, and calculates the repeatability of the online mass flowmeter density output in turn;
21.重复步骤15)-20),完成第二至第五介质溶液装置中介质溶液密度输出及重复性的检定;21. Repeat steps 15)-20) to complete the verification of the density output and repeatability of the medium solution in the second to fifth medium solution devices;
22.报告生产用户在线质量流量计密度标定与检测结果(精度和重复性)。22. Report the density calibration and detection results (accuracy and repeatability) of online mass flowmeters for production users.
综上所述,本实用新型通过将原有人工操作的密度标定系统替换为计算机自动控制的密度标定系统,相对于原有密度标定系统每次标定数量由三台变成了十台,提高了产品的标定的效率;采用计算机控制开关切换在不同介质的标定溶液,在每种标定溶液下多次测量质量流量计的密度,标定过程中完全无需人为参与,通过密度标定数学模型计算待测质量流量计的密度,不仅杜绝了传统质量体积方式的标定误差,还大幅度提高了质量流量计密度标定的精度;同时,在密度标定系统中引入了恒压恒流罐,消除了因溶液泵在工作时所产的标定溶液涓流与空气气泡的问题,从本质上提高了质量流量计的标定精度。所以,本实用新型有效克服了现有技术中的种种缺点而具高度产业利用价值。In summary, the utility model replaces the original manually operated density calibration system with a computer automatically controlled density calibration system. Compared with the original density calibration system, the number of each calibration is changed from three to ten, which improves the The efficiency of product calibration; use computer-controlled switches to switch calibration solutions in different media, and measure the density of the mass flowmeter multiple times under each calibration solution. There is no need for human participation in the calibration process, and the mass to be measured is calculated through the density calibration mathematical model. The density of the flowmeter not only eliminates the calibration error of the traditional mass volume method, but also greatly improves the accuracy of the density calibration of the mass flowmeter; at the same time, a constant pressure and constant flow tank is introduced in the density calibration system, eliminating the need for solution pumps The trickle of calibration solution and air bubbles produced during work essentially improve the calibration accuracy of the mass flowmeter. Therefore, the utility model effectively overcomes various shortcomings in the prior art and has high industrial application value.
上述实施例仅例示性说明本实用新型的原理及其功效,而非用于限制本实用新型。任何熟悉此技术的人士皆可在不违背本实用新型的精神及范畴下,对上述实施例进行修饰或改变。因此,举凡所属技术领域中具有通常知识者在未脱离本实用新型所揭示的精神与技术思想下所完成的一切等效修饰或改变,仍应由本实用新型的权利要求所涵盖。The above-mentioned embodiments only illustrate the principles and effects of the present utility model, but are not intended to limit the present utility model. Anyone familiar with this technology can modify or change the above-mentioned embodiments without departing from the spirit and scope of the present invention. Therefore, all equivalent modifications or changes made by those with ordinary knowledge in the technical field without departing from the spirit and technical ideas disclosed in the utility model should still be covered by the claims of the utility model.
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CN106643989A (en) * | 2016-11-22 | 2017-05-10 | 重庆川仪自动化股份有限公司 | Density Calibration System and Method for Mass Flow Meter |
CN108088730A (en) * | 2017-12-21 | 2018-05-29 | 浙江华友钴业股份有限公司 | A kind of accurate dosing method of ternary precursor metal salt solution |
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CN106643989A (en) * | 2016-11-22 | 2017-05-10 | 重庆川仪自动化股份有限公司 | Density Calibration System and Method for Mass Flow Meter |
CN108088730A (en) * | 2017-12-21 | 2018-05-29 | 浙江华友钴业股份有限公司 | A kind of accurate dosing method of ternary precursor metal salt solution |
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