CN116637733A - Temperature calibration test method for in-situ heating of centrifugal machine under high rotation speed and high temperature - Google Patents
Temperature calibration test method for in-situ heating of centrifugal machine under high rotation speed and high temperature Download PDFInfo
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
- B04B—CENTRIFUGES
- B04B1/00—Centrifuges with rotary bowls provided with solid jackets for separating predominantly liquid mixtures with or without solid particles
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
- B04B—CENTRIFUGES
- B04B13/00—Control arrangements specially designed for centrifuges; Programme control of centrifuges
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
- B04B—CENTRIFUGES
- B04B15/00—Other accessories for centrifuges
- B04B15/02—Other accessories for centrifuges for cooling, heating, or heat insulating
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
- B04B—CENTRIFUGES
- B04B7/00—Elements of centrifuges
- B04B7/08—Rotary bowls
- B04B7/12—Inserts, e.g. armouring plates
- B04B7/16—Sieves or filters
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
- B04B—CENTRIFUGES
- B04B9/00—Drives specially designed for centrifuges; Arrangement or disposition of transmission gearing; Suspending or balancing rotary bowls
- B04B9/12—Suspending rotary bowls ; Bearings; Packings for bearings
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Abstract
Description
技术领域technical field
本发明涉及金属材料原位加热领域的一种离心机加热校温控制方法,尤其涉及了一种用于高转速-高温作用下金属材料的离心机原位加热的校温测试方法。The invention relates to a centrifuge heating and temperature calibration control method in the field of in-situ heating of metal materials, in particular to a temperature calibration test method for in-situ heating of a centrifuge for metal materials under the action of high rotation speed and high temperature.
背景技术Background technique
国家标准GB/T 38822-2020《金属材料蠕变-疲劳试验方法》和GB/T6825.1-2008《静单轴试验机的检验第1部分:拉力和(或)压力试验机测力系统的检验与校准》均规定金属材料力学性能的测试方法,但这些标准规定的测试环境均为1G(G=9.8m/s2),可以满足金属材料本身力学性能的研究。然而,在涡轮推进系统,如航空发动机、航天发动机、工业和舰艇用燃气轮机、汽车和火车用涡轮增压器等动力系统的关键部件,如压气机叶片、风扇叶片、涡轮工作叶片等在正常工作时均处于高速旋转状态,即服役环境通常为离心超重力环境。National standard GB/T 38822-2020 "Creep-fatigue test method for metal materials" and GB/T6825.1-2008 "Inspection of static uniaxial testing machine Part 1: Tensile and (or) compression testing machine force measurement system "Inspection and Calibration" all stipulate the test methods for the mechanical properties of metal materials, but the test environment specified in these standards is 1G (G=9.8m/s 2 ), which can satisfy the research on the mechanical properties of metal materials themselves. However, in turbo propulsion systems, such as aeroengines, aerospace engines, gas turbines for industry and ships, turbochargers for automobiles and trains, and other key components of power systems, such as compressor blades, fan blades, turbine working blades, etc. They are always in a state of high-speed rotation, that is, the service environment is usually a centrifugal hypergravity environment.
涡轮推进系统通常是一种将燃料燃烧后的热能经导向叶片在工作叶片上通过热膨胀做功带动涡轮将热能转换成机械能的涡轮动力装置,涡轮增压器是利用柴油(汽油)发动机的废气在涡轮上热膨胀做功将发动机余热转换成机械能的动力装置。服役时这些动力装置的涡轮工作叶片绕发动机轴线高速旋转,其作用是燃气膨胀做功,将燃气的位能和热能转换为转子的机械功,所以服役过程中涡轮工作叶片承受的载荷包括气动力、离心力和热载荷。其中,高速旋转产生的离心力属于体积力,主要使叶片产生径向拉应力,对于扭转结构叶片,同时会产生扭转应力。若叶片的积叠线与径向线不完全重合,离心力也使叶片产生弯曲应力。热载荷产生的热应力与叶片的温度梯度和几何约束密切相关,叶片的温度梯度越大,热应力越大。但目前用于设计涡轮推进系统涡轮叶片的关键材料力学性能数据均来自1G条件下的持久、蠕变、疲劳等试验机通过测试标准试样获取材料静态、单轴应力状态下的力学性能数据。虽然标准试样力学性能数据在一定程度上能为涡轮推进系统涡轮叶片强度设计提供设计依据,但由于叶片具有复杂的几何形状,其复杂的应力状态和标准试样不同,通过标准试样得到的材料力学性能数据,没看考虑高转速、叶片几何结构等对其结构可靠性的影响,不能直接用来评估涡轮叶片的寿命。The turbine propulsion system is usually a turbine power device that converts the heat energy of fuel combustion into mechanical energy through the guide vanes on the working blades through thermal expansion to drive the turbine to convert heat energy into mechanical energy. The thermal expansion works to convert the waste heat of the engine into mechanical energy. When in service, the turbine working blades of these power plants rotate around the engine axis at high speed, and their function is to expand the gas to do work, converting the potential energy and thermal energy of the gas into the mechanical work of the rotor, so the loads on the turbine working blades during service include aerodynamic force, Centrifugal forces and thermal loads. Among them, the centrifugal force generated by high-speed rotation belongs to body force, which mainly causes radial tensile stress on the blade, and torsional stress on the blade with torsion structure at the same time. If the stacking line of the blade does not completely coincide with the radial line, the centrifugal force will also cause the blade to generate bending stress. The thermal stress generated by thermal load is closely related to the temperature gradient and geometric constraints of the blade. The greater the temperature gradient of the blade, the greater the thermal stress. However, the key material mechanical performance data currently used to design the turbine blades of the turbine propulsion system come from the durability, creep, fatigue and other testing machines under 1G conditions to obtain the mechanical performance data of the material under static and uniaxial stress states by testing standard specimens. Although the mechanical performance data of the standard sample can provide a design basis for the strength design of the turbine blade of the turbine propulsion system to a certain extent, due to the complex geometry of the blade, its complex stress state is different from that of the standard sample. The mechanical performance data of materials cannot be directly used to evaluate the life of turbine blades without considering the influence of high speed, blade geometry, etc. on its structural reliability.
发明内容Contents of the invention
针对目前1G下金属材料静态力学性能测试的不足,针对目前没有适合高转速-高温作用下金属材料力学性能测试过程中的原位加热及校温方法,本发明提供了一种可在高速旋转环境下给金属材料施加原位加热校温方法,解决高转速-高温作用下金属材料力学性能测试过程的原位加热、温度校核及智能控温的关键难题。In view of the shortcomings of the current static mechanical performance test of metal materials under 1G, and the lack of in-situ heating and temperature calibration methods suitable for the test process of the mechanical properties of metal materials under the action of high speed and high temperature, the present invention provides a method that can be used in a high-speed rotation environment. The method of in-situ heating and temperature calibration is applied to metal materials to solve the key problems of in-situ heating, temperature calibration and intelligent temperature control in the process of testing the mechanical properties of metal materials under the action of high speed and high temperature.
本发明所述的高转速环境下金属材料原位加热是指在金属材料或部件力学性能测试过程中,高速旋转的测试材料或部件始终处于原位加热状态,直至测试结束。The in-situ heating of metal materials in a high-rotational environment in the present invention means that during the mechanical performance testing process of metal materials or components, the test materials or components rotating at high speed are always in a state of in-situ heating until the end of the test.
本发明所述的高转速环境下金属材料原位加热系统的温度校核是指在金属材料或部件力学性能测试过程中,在高速旋转状态或静止状态给测试材料或部件的温度分布进行原位测温和校准。The temperature check of the metal material in-situ heating system under the high-speed environment of the present invention refers to the in-situ temperature distribution of the test material or component in the high-speed rotating state or static state during the test process of the mechanical properties of the metal material or component. Temperature measurement and calibration.
本发明所述的高温是指实验时施加给试样指定区域的加热温度不低于500℃,且原位加热持续的时间不低于测试时间。The high temperature mentioned in the present invention means that the heating temperature applied to the designated area of the sample during the experiment is not lower than 500°C, and the duration of in-situ heating is not lower than the test time.
本发明所述的高转速是指实验时离心机的最高转速不低于5000转/min。The high rotational speed in the present invention means that the maximum rotational speed of the centrifuge during the experiment is not less than 5000 rpm.
本发明采用的技术方案:The technical scheme adopted in the present invention:
第一步:根据实验条件确定离心机的主轴转速和轮盘半径;Step 1: Determine the spindle speed and disc radius of the centrifuge according to the experimental conditions;
第二步:确定测试试样中质量块的尺寸和重量、标距段的尺寸和几何中心;The second step: determine the size and weight of the mass block in the test sample, the size and geometric center of the gauge length section;
第三步:确定试验温度和标距段几何中心施加的离心应力,进而确定标距段的几何中心的离心应力对应的转速,确定标距段几何中心到离心机的主轴中心之间的距离;Step 3: Determine the test temperature and the centrifugal stress applied by the geometric center of the gauge section, and then determine the rotational speed corresponding to the centrifugal stress of the geometric center of the gauge section, and determine the distance between the geometric center of the gauge section and the center of the main shaft of the centrifuge;
第四步:在样品卡盘的一个卡槽中安装一个校温试样和其余卡槽中安装测试试样,在测试试样旁边安装校温试样;在校温试样的各个热电偶孔中均插入热电偶,且在测试试样和校温试样的标距段几何中心位置均固定上控温热电偶;Step 4: Install a temperature calibration sample in one slot of the sample chuck and the test sample in the remaining slots, and install the temperature calibration sample next to the test sample; in each thermocouple hole of the temperature calibration sample Thermocouples are inserted in the middle, and the temperature control thermocouples are fixed at the geometric center of the gauge length section of the test sample and the temperature calibration sample;
第五步:在不启动离心机情况下,样品卡盘及其上面的测试试样和校温试样均保持静止,对环境进行抽真空,然后启动感应加热系统、循环水冷却系统和控温系统,通过控温系统控制感应加热系统、循环水冷却系统工作对测试试样和校温试样施加温度载荷,待温度到达预定温度后并保温一段时间;Step 5: Without starting the centrifuge, keep the sample chuck and the test sample and temperature calibration sample on it still, vacuumize the environment, and then start the induction heating system, circulating water cooling system and temperature control System, through the temperature control system to control the induction heating system and the circulating water cooling system to apply temperature load to the test sample and the temperature calibration sample, and keep it warm for a period of time after the temperature reaches the predetermined temperature;
通过测试试样和校温试样的控温热电偶以及校温试样的各个热电偶孔中的热电偶测量获得的温度数据进行分析处理获得正式试验测量时的上感应线圈和下感应线圈的通电电流、电流交变频率以及上感应线圈和下感应线圈之间的间距的参数;The temperature data obtained by the temperature control thermocouples of the test sample and the temperature calibration sample and the thermocouples in each thermocouple hole of the temperature calibration sample are analyzed and processed to obtain the upper induction coil and the lower induction coil during the formal test measurement. Parameters of energizing current, current alternating frequency and distance between the upper induction coil and the lower induction coil;
第六步:从样品卡盘的卡槽上撤下校温试样、换上测试试样,再启动离心机,使离心机的主轴旋转且转速达到离心应力对应的转速进行正式试验测试,按照第五步获得的参数控制上感应线圈和下感应线圈之间的间距和通电电流、电流交变频率,保持参数不变,直到测试试样被拉断断裂。Step 6: Remove the temperature calibration sample from the slot of the sample chuck, replace it with the test sample, and then start the centrifuge, so that the main shaft of the centrifuge rotates and the speed reaches the speed corresponding to the centrifugal stress to conduct a formal test. The parameters obtained in the five steps control the distance between the upper induction coil and the lower induction coil, the energizing current, and the alternating frequency of the current, and keep the parameters unchanged until the test sample is broken.
方法采用校温测试装置,装置包括样品卡盘、感应加热系统、循环水冷却系统和控温系统;所述的样品卡盘同轴安装在离心机的主轴上且随离心机的主轴同步旋转,所述的样品卡盘上安装测试试样和校温试样,感应加热系统同轴安装在离心机上且不随离心机的主轴旋转,感应加热系统和循环水冷却系统连接,控温系统分别和循环水冷却系统、测试试样连接。The method uses a temperature calibration test device, which includes a sample chuck, an induction heating system, a circulating water cooling system, and a temperature control system; the sample chuck is coaxially installed on the main shaft of the centrifuge and rotates synchronously with the main shaft of the centrifuge. The test sample and the temperature calibration sample are installed on the sample chuck, the induction heating system is installed coaxially on the centrifuge and does not rotate with the main shaft of the centrifuge, the induction heating system is connected with the circulating water cooling system, and the temperature control system is connected with the circulating water cooling system respectively. Water cooling system, test specimen connection.
所述的样品卡盘包括盘体、卡槽和法兰,盘体中心的两端同轴安装有法兰,盘体通过法兰和离心机的主轴同轴固定连接,盘体周围沿周向开设有多个卡槽,多个卡槽沿周向间隔布置,每个卡槽用于安装一个测试试样。The sample chuck includes a disc body, a card slot and a flange. Flanges are coaxially installed at both ends of the center of the disc body. The disc body is fixedly connected with the main shaft of the centrifuge through the flange. A plurality of draw-in slots are provided, and the plurality of draw-in slots are arranged at intervals along the circumferential direction, and each draw-in slot is used for installing a test sample.
所述的测试试样呈条状,包括依次衔接的质量块、标矩段、承力段和装配榫头,质量块、标矩段、承力段和装配榫头均沿测试试样的条状依次布置,装配榫头嵌装在样品卡盘的卡槽中。The test sample is in the shape of a strip, including successively connected mass blocks, standard moment sections, load-bearing sections and assembly tenons, and the mass blocks, standard moment sections, load-bearing sections and assembly tenons are all sequentially Arrangement, the assembly tenon is embedded in the slot of the sample chuck.
所述的校温试样和测试试样结构、形状、尺寸相同,不同的是在所述的校温试样内部开设有多个不同深度的热电偶孔,每个热电偶孔均沿样品卡盘的盘体的径向开设布置,每个热电偶孔均安装有一个热电偶。The temperature calibration sample and the test sample have the same structure, shape and size, the difference is that a plurality of thermocouple holes with different depths are opened inside the temperature calibration sample, and each thermocouple hole is along the sample card. The disk body of the disk is arranged radially, and each thermocouple hole is equipped with a thermocouple.
所述的感应加热系统包括上感应线圈、上固定板、下感应线圈和下固定板;上固定板和下固定板分别上下间隔平行地固定布置,上固定板和下固定板之间的间隔中布置样品卡盘;环形的上感应线圈和下感应线圈分别通过上感应线圈绝缘层、下感应线圈绝缘层固定在上固定板的底面和下固定板和顶面。The induction heating system includes an upper induction coil, an upper fixed plate, a lower induction coil and a lower fixed plate; the upper fixed plate and the lower fixed plate are fixedly arranged in parallel at intervals up and down, and in the interval between the upper fixed plate and the lower fixed plate The sample chuck is arranged; the ring-shaped upper induction coil and the lower induction coil are respectively fixed on the bottom surface of the upper fixing plate, the lower fixing plate and the top surface through the upper induction coil insulation layer and the lower induction coil insulation layer.
上感应线圈和下感应线圈分别被包裹在上感应线圈绝缘层、下感应线圈绝缘层的内腔中,上感应线圈绝缘层和下感应线圈绝缘层的内腔之间通过管道连通,上感应线圈绝缘层、下感应线圈绝缘层分别通过上固定螺杆、下固定螺杆固定于上固定板的底面和下固定板和顶面。The upper induction coil and the lower induction coil are respectively wrapped in the inner chambers of the upper induction coil insulation layer and the lower induction coil insulation layer, and the inner chambers of the upper induction coil insulation layer and the lower induction coil insulation layer are connected through pipes, and the upper induction coil The insulating layer and the insulating layer of the lower induction coil are respectively fixed on the bottom surface of the upper fixing plate, the lower fixing plate and the top surface through the upper fixing screw rod and the lower fixing screw rod.
所述的循环水冷却系统包括设置在感应加热系统中的管道组件以及流通进水管、流通出水管、正电极、内绝缘套、金属套管、负电极、铜管、绝缘压套、固定法兰、绝缘压套、压紧圆螺母、密封件、电极绝缘压套、外接出水管、外接正电极板、外接进水管和外接负电极板;铜管外套装有用于和金属套管绝缘的绝缘压套,绝缘压套外套装有金属套管;金属套管中部通过绝缘压套和轴用密封圈密封套装在固定法兰的中心孔中,固定法兰固定于离心机的实验腔盖上,铜管、绝缘压套和金属套管的两端分别通过内绝缘套和密封件固定密封安装;铜管一端穿过内绝缘套后和流通出水管同轴对接,且在铜管一端穿过内绝缘套后的端部设置正电极;外接正电极板通过电极绝缘压套和铜管电连接,使得正电极直接经铜管后和外接正电极板电连接;铜管另一端和外接出水管对接,使得流通出水管直接经铜管和外接出水管流通;绝缘压套和金属套管之间具有环形管道间隙用于作为进水通道,进水通道一端经金属管道和流通进水管连通连接,流通进水管在端部附近设置负电极;外接负电极板通过压紧圆螺母和金属套管电连接,使得负电极依次经金属管道、金属套管后和外接负电极板电连接;金属套管在连接密封件的的一端管壁开设有通槽,通槽和外接进水管流通连接,使得流通进水管依次经金属管道、进水通道、通槽后和外接进水管流通。The circulating water cooling system includes a pipe assembly set in the induction heating system, a water inlet pipe, a water outlet pipe, a positive electrode, an inner insulating sleeve, a metal sleeve, a negative electrode, a copper pipe, an insulating pressure sleeve, and a fixing flange , insulating pressure sleeve, compression round nut, seal, electrode insulation pressure sleeve, external water outlet pipe, external positive electrode plate, external water inlet pipe and external negative electrode plate; the copper tube jacket is equipped with insulation pressure for insulation from the metal casing The outer cover of the insulating pressure sleeve is equipped with a metal sleeve; the middle part of the metal sleeve is sealed in the center hole of the fixed flange through the insulating pressure sleeve and the shaft seal ring, and the fixed flange is fixed on the experimental chamber cover of the centrifuge. The two ends of the pipe, insulating sleeve and metal sleeve are respectively fixed and sealed through the inner insulating sleeve and the seal; one end of the copper pipe passes through the inner insulating sleeve and is coaxially connected with the flow outlet pipe, and one end of the copper pipe passes through the inner insulation The end behind the sleeve is provided with a positive electrode; the external positive electrode plate is electrically connected to the copper tube through the electrode insulation pressure sleeve, so that the positive electrode is directly electrically connected to the external positive electrode plate through the copper tube; the other end of the copper tube is connected to the external water outlet pipe. Make the circulation outlet pipe flow directly through the copper pipe and the external outlet pipe; there is an annular pipe gap between the insulating pressure sleeve and the metal sleeve as the water inlet channel, and one end of the water inlet channel is connected through the metal pipe and the circulation inlet pipe. The water pipe is provided with a negative electrode near the end; the external negative electrode plate is electrically connected to the metal sleeve through the compression round nut, so that the negative electrode is electrically connected to the external negative electrode plate after passing through the metal pipe and the metal sleeve; the metal sleeve is connected The pipe wall at one end of the sealing element is provided with a through groove, and the through groove is fluidly connected with the external water inlet pipe, so that the circulation water inlet pipe flows through the metal pipe, the water inlet channel, the through groove and the external water inlet pipe in turn.
所述的管道组件包括加热进水管、进水管密封套、加热出水管和出水管密封套;加热进水管、加热出水管的一端分别经进水管密封套、出水管密封套和流通进水管、流通出水管连接,加热进水管和加热出水管的另一端分别连通到感应加热系统中的上感应线圈和下感应线圈所在的内腔环境中,上感应线圈和下感应线圈所在的内腔环境相互连通。The pipeline assembly includes a heating water inlet pipe, a water inlet pipe sealing sleeve, a heating water outlet pipe and a water outlet pipe sealing sleeve; The outlet pipe is connected, and the other ends of the heating water inlet pipe and the heating outlet pipe are respectively connected to the inner cavity environment where the upper induction coil and the lower induction coil are located in the induction heating system, and the inner cavity environment where the upper induction coil and the lower induction coil are located are connected to each other .
所述的外接出水管和外接进水管分别连接到循环水机的进水口和出水口。The external water outlet pipe and the external water inlet pipe are respectively connected to the water inlet and water outlet of the circulating water machine.
所述的正电极和负电极分别电连接到上感应线圈和下感应线圈,所述的外接正电极板和外接负电极板分别连接到外部电源的正负极。The positive electrode and the negative electrode are electrically connected to the upper induction coil and the lower induction coil respectively, and the external positive electrode plate and the external negative electrode plate are respectively connected to the positive and negative electrodes of the external power supply.
所述的控温系统包括热电偶、热电偶延长线、高速滑环、数据采集模块、数据转换传输模块和高频交流电源柜;所述的感应加热系统的上感应线圈和下感应线圈所正对应的测试试样表面上均固定设有热电偶,热电偶经热电偶延长线、高速滑环和数据采集模块连接,数据采集模块经数据转换传输模块和高频交流电源柜通信连接、高频交流电源柜和循环水冷却系统的外接正电极板、外接负电极板电连接。The temperature control system includes a thermocouple, a thermocouple extension wire, a high-speed slip ring, a data acquisition module, a data conversion transmission module and a high-frequency AC power supply cabinet; the upper induction coil and the lower induction coil of the induction heating system are positive The corresponding test samples are fixed with thermocouples on the surface, and the thermocouples are connected to the data acquisition module through the thermocouple extension line, the high-speed slip ring, and the data acquisition module is connected to the high-frequency AC power supply cabinet through the data conversion and transmission module. The AC power supply cabinet is electrically connected to the external positive electrode plate and the external negative electrode plate of the circulating water cooling system.
由于加热系统在试件外通过感应加热,使得试件外表面温度会高于内部温度,产生屈服效应,试件里面温度低,外部温度高,这样试件各处的温度并不均匀,导致试件测试和试验的有效性大大降低,测试误差增大。Since the heating system is heated by induction outside the test piece, the temperature of the outer surface of the test piece will be higher than the internal temperature, resulting in a yield effect. The effectiveness of component testing and testing is greatly reduced, and the test error is increased.
为了避免这样的问题,本发明才设计了校温装置和校温过程,通过校温装置和校温过程使得正式试验时的测试试样在被加热时能够温度分布均匀,各处温度均达到预设温度,误差不大于五摄氏度。In order to avoid such problems, the present invention has just designed a temperature calibration device and a temperature calibration process. By means of the temperature calibration device and the temperature calibration process, the test sample in the formal test can have a uniform temperature distribution when heated, and the temperature everywhere reaches the predetermined temperature. Set the temperature with an error not greater than five degrees Celsius.
本发明的校温是能够保证试件沿垂直离心力方向的温度均匀无梯度,沿离心力方向的温度可以不均匀有梯度。The temperature calibration of the present invention can ensure that the temperature of the test piece along the vertical direction of centrifugal force is uniform without gradient, and the temperature along the direction of centrifugal force can be uneven and have gradient.
本发明的有益效果是:The beneficial effects of the present invention are:
(1)解决了目前高转速下辐射加热只能校核环境温度而无法精确校核试样温度的不足,本发明提供的校温测试方法,可以在高转速下直接校核试样温度,使测试部件温度更加精准;(1) It solves the problem that the current radiation heating can only check the ambient temperature but cannot accurately check the temperature of the sample at high rotational speeds. The temperature calibration test method provided by the invention can directly check the temperature of the sample at high rotational speeds, so that The temperature of the test part is more accurate;
(2)通过改变校核试样的形状和安装校温热电偶间距与深度,可以根据需要校核试样任何位置的温度。(2) By changing the shape of the check sample and installing the spacing and depth of the thermocouples, the temperature at any position of the sample can be checked as needed.
附图说明Description of drawings
图1是样品卡盘1的结构示意图;Fig. 1 is the structural representation of sample chuck 1;
图2是测试试样1.1的结构示意图;Fig. 2 is the structural representation of test sample 1.1;
图3是感应加热系统2的结构示意图;Fig. 3 is the structural representation of induction heating system 2;
图4是循环水冷却系统3的结构示意图;Fig. 4 is the structural representation of circulating water cooling system 3;
图5是控温系统4的示意图;Fig. 5 is the schematic diagram of temperature control system 4;
图6是一种测试样品1.1的结构示意图;Fig. 6 is a structural representation of a test sample 1.1;
图7是一种测试样品1.1的结构示意图;Fig. 7 is a schematic structural view of a test sample 1.1;
图8是一种测试样品1.1的结构示意图;Fig. 8 is a schematic structural view of a test sample 1.1;
图9是样品卡盘1、感应加热系统2在离心机上的安装示意图;Fig. 9 is a schematic diagram of the installation of the sample chuck 1 and the induction heating system 2 on the centrifuge;
图10是加热具体实施一的工艺路线图;Fig. 10 is a process route diagram of specific implementation one of heating;
图11是加热具体实施二的工艺路线图;Fig. 11 is the process roadmap of specific implementation two of heating;
图12是加热具体实施三的工艺路线图;Fig. 12 is the process roadmap of specific implementation three of heating;
图13是校温试样5的结构示意图;Fig. 13 is the structural representation of temperature calibration sample 5;
图14是测试试样1.1、校温试样5、样品卡盘1和感应加热系统2共同安装后的布局图。Fig. 14 is a layout diagram after the test sample 1.1, the temperature calibration sample 5, the sample chuck 1 and the induction heating system 2 are installed together.
图中:In the picture:
样品卡盘1:测试试样1.1、卡槽1.2、法兰1.3;Sample chuck 1: test sample 1.1, slot 1.2, flange 1.3;
质量块1.1.1、标矩段1.1.2、承力段1.1.3、装配榫头1.1.4;Mass block 1.1.1, standard moment section 1.1.2, bearing section 1.1.3, assembly tenon 1.1.4;
感应加热系统2:上感应线圈2.1、上感应线圈绝缘层2.2、上固定板2.3、上固定螺杆2.4、下感应线圈2.5、下感应线圈绝缘层2.6、下固定板2.7、下固定螺杆2.8、连接杆2.9、螺帽2.10、加热进水管2.11、进水管密封套2.12、加热出水管2.13、出水管密封套2.14;Induction heating system 2: upper induction coil 2.1, upper induction coil insulating layer 2.2, upper fixing plate 2.3, upper fixing screw 2.4, lower induction coil 2.5, lower induction coil insulating layer 2.6, lower fixing plate 2.7, lower fixing screw 2.8, connection Rod 2.9, nut 2.10, heating water inlet pipe 2.11, water inlet pipe sealing sleeve 2.12, heating water outlet pipe 2.13, water outlet pipe sealing sleeve 2.14;
循环水冷却系统3:流通进水管3.1、连接螺母3.2、流通出水管3.3、连接螺母3.4、正电极3.5、内绝缘套3.6、负电极3.8、铜管3.9、绝缘压套3.10、固定法兰3.11、固定螺杆3.12、轴用密封圈3.13、绝缘压套3.14、压紧圆螺母3.15、顶紧螺母3.16、绝缘件3.17、密封件3.18、电极绝缘压套3.19、密封螺母3.20、外接出水管3.21、外接正电极板3.22、外接进水管3.23和外接负电极板3.24;Circulating water cooling system 3: circulating water inlet pipe 3.1, connecting nut 3.2, circulating water outlet pipe 3.3, connecting nut 3.4, positive electrode 3.5, inner insulating sleeve 3.6, negative electrode 3.8, copper pipe 3.9, insulating pressure sleeve 3.10, fixed flange 3.11 , fixed screw rod 3.12, shaft sealing ring 3.13, insulating gland 3.14, compression round nut 3.15, top tightening nut 3.16, insulator 3.17, seal 3.18, electrode insulation gland 3.19, sealing nut 3.20, external outlet pipe 3.21, External positive electrode plate 3.22, external water inlet pipe 3.23 and external negative electrode plate 3.24;
控温系统4:热电偶4.1、热电偶延长线4.2、高速滑环4.3、数据采集模块4.4、控制软件4.5、数据转换传输模块4.6、高频交流电源柜4.7;Temperature control system 4: thermocouple 4.1, thermocouple extension wire 4.2, high-speed slip ring 4.3, data acquisition module 4.4, control software 4.5, data conversion and transmission module 4.6, high-frequency AC power supply cabinet 4.7;
校温试样5:热电偶孔5-1、热电偶孔5-2、热电偶孔5-3、热电偶孔5-4、热电偶孔5-5、热电偶孔5-6、热电偶孔5-7。Calibration sample 5: thermocouple hole 5-1, thermocouple hole 5-2, thermocouple hole 5-3, thermocouple hole 5-4, thermocouple hole 5-5, thermocouple hole 5-6, thermocouple Holes 5-7.
具体实施方式Detailed ways
下面结合附图和具体实施对本发明作进一步说明。The present invention will be further described below in conjunction with the accompanying drawings and specific implementation.
如图9所示,具体实施中设计了校温测试装置,装置包括样品卡盘1、感应加热系统2、循环水冷却系统3和控温系统4;样品卡盘1同轴安装在离心机的主轴上且随离心机的主轴同步旋转,样品卡盘1上安装测试试样1.1和校温试样5,感应加热系统2同轴安装在离心机上且不随离心机的主轴旋转而保持固定,感应加热系统2和循环水冷却系统3连接,控温系统4分别和循环水冷却系统3、测试试样1.1连接。As shown in Figure 9, a temperature calibration test device is designed in the specific implementation, and the device includes a sample chuck 1, an induction heating system 2, a circulating water cooling system 3 and a temperature control system 4; the sample chuck 1 is coaxially installed on the centrifuge The main shaft rotates synchronously with the main shaft of the centrifuge. The test sample 1.1 and the temperature calibration sample 5 are installed on the sample chuck 1. The induction heating system 2 is coaxially installed on the centrifuge and does not keep fixed with the main shaft rotation of the centrifuge. The heating system 2 is connected to the circulating water cooling system 3, and the temperature control system 4 is respectively connected to the circulating water cooling system 3 and the test sample 1.1.
离心机为超重力离心机。The centrifuge is an ultra-gravity centrifuge.
如图1所示,样品卡盘1的作用是用于安装测试试样且通过主轴与离心机相连,包括盘体、卡槽1.2和法兰1.3,盘体中心的两端同轴固定安装有法兰1.3,盘体通过法兰1.3和离心机的主轴同轴固定连接,盘体周围沿周向开设有多个卡槽1.2,多个卡槽1.2沿周向间隔布置,每个卡槽1.2用于安装一个测试试样1.1。As shown in Figure 1, the function of the sample chuck 1 is to install the test sample and connect with the centrifuge through the main shaft, including the disc body, the slot 1.2 and the flange 1.3, and the two ends of the disc center are coaxially fixed with Flange 1.3, the disc body is coaxially fixedly connected with the main shaft of the centrifuge through flange 1.3, a plurality of card slots 1.2 are arranged around the disc body along the circumferential direction, and the plurality of card slots 1.2 are arranged at intervals along the circumferential direction, each card slot 1.2 For mounting a test specimen 1.1.
法兰1.3是用来将样品卡盘1与离心机主轴相连,实验时通过离心机主轴高速旋转带动样品卡盘1旋转,借此给测试试样1.1施加离心载荷。The flange 1.3 is used to connect the sample chuck 1 with the main shaft of the centrifuge. During the experiment, the high-speed rotation of the main shaft of the centrifuge drives the sample chuck 1 to rotate, thereby applying a centrifugal load to the test sample 1.1.
卡槽1.2主要用来固定高速旋转的测试试样1.1,测试试样1.1的装配榫头1.1.4安装在卡槽1.2,使样品卡盘1在旋转时带动测试试样1.1一起旋转。The slot 1.2 is mainly used to fix the test sample 1.1 rotating at high speed, and the assembly tenon 1.1.4 of the test sample 1.1 is installed in the slot 1.2, so that the sample chuck 1 drives the test sample 1.1 to rotate together when rotating.
3、根据权利要求1一种高转速-高温作用下离心机原位加热的校温测试方法,其特征在于:3. According to claim 1, a method for calibrating the temperature of a centrifuge heated in situ under the action of high rotating speed and high temperature, characterized in that:
如图2所示,测试试样1.1是由测试性能的金属材料加工而成,呈条状,包括依次衔接的质量块1.1.1、标矩段1.1.2、承力段1.1.3和装配榫头1.1.4,质量块1.1.1、标矩段1.1.2、承力段1.1.3和装配榫头1.1.4均沿测试试样1.1的条状依次布置,具体地质量块1.1.1、标矩段1.1.2、承力段1.1.3和装配榫头1.1.4从样品卡盘1的卡槽1.2中径向向外依次布置,装配榫头1.1.4嵌装在样品卡盘1的卡槽1.2中。As shown in Figure 2, the test sample 1.1 is processed by the metal material for testing performance, and is in the shape of a strip, including the sequentially connected mass block 1.1.1, standard moment section 1.1.2, load-bearing section 1.1.3 and assembly Tenon 1.1.4, quality block 1.1.1, standard moment section 1.1.2, load-bearing section 1.1.3 and assembly tenon 1.1.4 are arranged sequentially along the strip of test sample 1.1, specifically mass block 1.1.1, The standard moment section 1.1.2, the load-bearing section 1.1.3 and the assembly tenon 1.1.4 are arranged radially outward from the slot 1.2 of the sample chuck 1, and the assembly tenon 1.1.4 is embedded in the clamp of the sample chuck 1 slot 1.2.
具体实施中装配榫头1.1.4的宽度和样品卡盘1的卡槽1.2的槽宽均大于质量块1.1.1、标矩段1.1.2和承力段1.1.3的宽度,使得测试试样1.1在被样品卡盘1带动高速旋转时能够稳定嵌装定位。In the specific implementation, the width of the assembly tenon 1.1.4 and the groove width of the sample chuck 1 are larger than the width of the mass block 1.1.1, the standard moment section 1.1.2 and the load-bearing section 1.1.3, so that the test sample 1.1 When driven by the sample chuck 1 to rotate at high speed, it can be stably embedded and positioned.
质量块1.1.1用来在高转速下通过自身重量产生的离心力给标矩段1.1.3施加一个离心应力。质量块1.1.1的质量为m,有效半径为r,转速为ω,则质量快1.1.1产生的离心力F=mrω2。质量块1.1.1的重量m取决于实验条件下材料的断裂强度。The mass block 1.1.1 is used to apply a centrifugal stress to the standard moment section 1.1.3 by the centrifugal force generated by its own weight at high rotational speed. The mass of the mass block 1.1.1 is m, the effective radius is r, and the rotational speed is ω, then the centrifugal force F=mrω 2 generated by the mass block 1.1.1 is fast. The mass m of the mass 1.1.1 depends on the breaking strength of the material under the experimental conditions.
标距段1.1.2与质量块1.1.1相连,用来承载质量块1.1.1在高速旋转和高温下施加的离心应力和热应力载荷。标距段1.1.2的形状可以根据实际需要进行改变。The gauge length section 1.1.2 is connected with the mass block 1.1.1, and is used to carry the centrifugal stress and thermal stress load imposed by the mass block 1.1.1 under high-speed rotation and high temperature. The shape of gauge length section 1.1.2 can be changed according to actual needs.
承力段1.1.3用来连接标距段1.1.2和装配榫头1.1.4。The load-bearing section 1.1.3 is used to connect the gauge length section 1.1.2 and the assembly tenon 1.1.4.
根据实验需要,测试试样1.1可设计如图2、图6-图8的结构。According to the needs of the experiment, the test sample 1.1 can be designed with the structure shown in Figure 2, Figure 6-Figure 8.
如图13所示,校温试样5和测试试样1.1结构、形状、尺寸相同,不同的是在校温试样5内部开设有多个不同深度的热电偶孔,每个热电偶孔均沿样品卡盘1的盘体的径向开设布置,每个热电偶孔均安装有一个热电偶。As shown in Figure 13, the temperature calibration sample 5 and the test sample 1.1 have the same structure, shape, and size. The difference is that there are multiple thermocouple holes with different depths inside the temperature calibration sample 5, and each thermocouple hole is Arranged along the radial direction of the disc body of the sample chuck 1, each thermocouple hole is equipped with a thermocouple.
具体实施中,校温试样5在沿样品卡盘1的盘体径向的外端面上开设不同深度的热电偶孔5-1、热电偶孔5-2、热电偶孔5-3、热电偶孔5-4、热电偶孔5-5、热电偶孔5-6、热电偶孔5-7,每个热电偶孔均安装一个热电偶,热电偶装入热电偶孔内的底部。In specific implementation, the temperature calibration sample 5 is provided with thermocouple holes 5-1, thermocouple holes 5-2, thermocouple holes 5-3, thermoelectric Couple holes 5-4, thermocouple holes 5-5, thermocouple holes 5-6, thermocouple holes 5-7, each thermocouple hole is equipped with a thermocouple, and the thermocouple is packed into the bottom of the thermocouple hole.
为了校核校温试样5上A、B、C、D、E、F、G截面的温度,在校温试样5上打热电偶孔5-1、热电偶孔5-2、热电偶孔5-3、热电偶孔5-4、热电偶孔5-5、热电偶孔5-6、热电偶孔5-7分别对应A、B、C、D、E、F、G截面。校核时,将热电偶分别插入热电偶孔5-1、热电偶孔5-2、热电偶孔5-3、热电偶孔5-4、热电偶孔5-5、热电偶孔5-6、热电偶孔5-7,然后将热电偶与控温系统4相连。具体实验时,热电偶孔的数量和深度可调整。In order to check the temperature of sections A, B, C, D, E, F, and G on the temperature calibration sample 5, a thermocouple hole 5-1, a thermocouple hole 5-2, and a thermocouple hole 5-1 are punched on the temperature calibration sample 5. Hole 5-3, thermocouple hole 5-4, thermocouple hole 5-5, thermocouple hole 5-6, and thermocouple hole 5-7 correspond to sections A, B, C, D, E, F, and G, respectively. When checking, insert the thermocouple into thermocouple hole 5-1, thermocouple hole 5-2, thermocouple hole 5-3, thermocouple hole 5-4, thermocouple hole 5-5, thermocouple hole 5-6 , thermocouple holes 5-7, and then connect the thermocouples to the temperature control system 4. In specific experiments, the number and depth of thermocouple holes can be adjusted.
测试试样1.1和校温试样5的标距段1.1.2的中心布置有热电偶和应变片的其中之一或者两者。One or both of thermocouples and strain gauges are arranged in the center of the gauge length section 1.1.2 of the test sample 1.1 and the temperature calibration sample 5.
如图3所示,感应加热系统2的作用是用于给高速旋转试样原位加热,给测试试样1.1指定区域施加温度载荷。包括上感应线圈2.1、上固定板2.3、下感应线圈2.5和下固定板2.7;上固定板2.3和下固定板2.7分别上下间隔平行地固定布置,具体实施中,离心机的主轴可旋转地穿过上固定板2.3布置。上固定板2.3和下固定板2.7之间的间隔中布置样品卡盘1;上固定板2.3和下固定板2.7之间通过连接杆2.9支撑固定,连接杆2.9外端设置螺帽2.10安装。环形的上感应线圈2.1和下感应线圈2.5分别通过上感应线圈绝缘层2.2、下感应线圈绝缘层2.6固定在上固定板2.3的底面和下固定板2.7和顶面。As shown in Figure 3, the function of the induction heating system 2 is to heat the high-speed rotating sample in situ, and to apply temperature load to the designated area of the test sample 1.1. It includes an upper induction coil 2.1, an upper fixed plate 2.3, a lower induction coil 2.5 and a lower fixed plate 2.7; the upper fixed plate 2.3 and the lower fixed plate 2.7 are respectively fixed and arranged at intervals up and down in parallel, and in specific implementation, the main shaft of the centrifuge can rotate through 2.3 Arrangement over the fixed plate. The sample chuck 1 is arranged in the interval between the upper fixed plate 2.3 and the lower fixed plate 2.7; the upper fixed plate 2.3 and the lower fixed plate 2.7 are supported and fixed by the connecting rod 2.9, and the outer end of the connecting rod 2.9 is provided with a nut 2.10 for installation. The annular upper induction coil 2.1 and the lower induction coil 2.5 are respectively fixed on the bottom surface of the upper fixing plate 2.3 and the lower fixing plate 2.7 and the top surface through the upper induction coil insulation layer 2.2 and the lower induction coil insulation layer 2.6.
上固定板2.3和下固定板2.7均为环形的板,上感应线圈2.1和下感应线圈2.5均为整体环形的线圈。The upper fixing plate 2.3 and the lower fixing plate 2.7 are ring-shaped plates, and the upper induction coil 2.1 and the lower induction coil 2.5 are overall ring-shaped coils.
具体地,上感应线圈2.1和下感应线圈2.5分别被包裹在上感应线圈绝缘层2.2、下感应线圈绝缘层2.6的内腔中,上感应线圈绝缘层2.2和下感应线圈绝缘层2.6的内腔之间通过管道连通,上感应线圈绝缘层2.2、下感应线圈绝缘层2.6分别通过上固定螺杆2.4、下固定螺杆2.8固定于上固定板2.3的底面和下固定板2.7和顶面。Specifically, the upper induction coil 2.1 and the lower induction coil 2.5 are respectively wrapped in the inner cavity of the upper induction coil insulating layer 2.2 and the lower induction coil insulating layer 2.6, and the inner cavity of the upper induction coil insulating layer 2.2 and the lower induction coil insulating layer 2.6 The upper induction coil insulating layer 2.2 and the lower induction coil insulating layer 2.6 are respectively fixed on the bottom surface of the upper fixing plate 2.3 and the lower fixing plate 2.7 and the top surface through the upper fixing screw 2.4 and the lower fixing screw 2.8.
其中,上感应线圈2.1包裹在上感应线圈绝缘层2.2内部,防止导电,用于绝缘;然后通过上固定螺杆2.4将带有绝缘层的上感应线圈2.1固定在上固定板2.3,组成上感应线圈;下感应线圈2.5包裹在下感应线圈绝缘层2.6内部,也通过下固定螺杆2.8将带有绝缘层的下感应线圈2.5固定在下固定板2.7,组成下感应线圈;随后,上固定板2.3和下固定板2.7之间通过连接杆2.9和螺帽2.10组装在一起。Among them, the upper induction coil 2.1 is wrapped inside the upper induction coil insulation layer 2.2 to prevent conduction and is used for insulation; then the upper induction coil 2.1 with the insulation layer is fixed on the upper fixing plate 2.3 by the upper fixing screw 2.4 to form the upper induction coil The lower induction coil 2.5 is wrapped inside the lower induction coil insulating layer 2.6, and the lower induction coil 2.5 with the insulating layer is also fixed on the lower fixing plate 2.7 by the lower fixing screw 2.8 to form the lower induction coil; subsequently, the upper fixing plate 2.3 and the lower fixing The plates 2.7 are assembled together by connecting rods 2.9 and nuts 2.10.
在通交流电情况下,放置在上感应线圈2.1、下感应线圈2.5之间的金属材料在交变磁场作用下产生感应电流I或涡流,涡流通过有电阻的导体产生热,在通过热传导的方式加热金属材料,其中感应电流I产生的焦耳热Q=I2RtR为金属材料的电阻,t为时间,感应加热过程中,通过调节交流电频率f、试样距离上感应线圈2.1与下感应线圈2.5之间的距离、加热功率来控制加热温度。In the case of alternating current, the metal material placed between the upper induction coil 2.1 and the lower induction coil 2.5 generates an induced current I or an eddy current under the action of an alternating magnetic field, and the eddy current generates heat through a resistive conductor, which is heated by heat conduction For metal materials, the Joule heat Q=I 2 RtR generated by the induced current I is the resistance of the metal material, and t is time. During the induction heating process, by adjusting the frequency f of the alternating current and the sample distance between the upper induction coil 2.1 and the lower induction coil 2.5 The distance between them and the heating power are used to control the heating temperature.
如图4所示,循环水冷却系统3的作用是用于给感应加热系统2中上感应线圈2.1和下感应线圈2.5中的铜管冷却。包括设置在感应加热系统2中的管道组件以及流通进水管3.1、流通出水管3.3、正电极3.5、内绝缘套3.6、金属套管3.7、负电极3.8、铜管3.9、绝缘压套3.10、固定法兰3.11、绝缘压套3.14、压紧圆螺母3.15、密封件3.18、电极绝缘压套3.19、外接出水管3.21、外接正电极板3.22、外接进水管3.23和外接负电极板3.24;As shown in FIG. 4 , the function of the circulating water cooling system 3 is to cool the copper tubes in the upper induction coil 2.1 and the lower induction coil 2.5 in the induction heating system 2 . Including the pipeline assembly set in the induction heating system 2, the circulation inlet pipe 3.1, the circulation outlet pipe 3.3, the positive electrode 3.5, the inner insulating sleeve 3.6, the metal sleeve 3.7, the negative electrode 3.8, the copper pipe 3.9, the insulating pressure sleeve 3.10, the fixing Flange 3.11, insulating gland 3.14, compression round nut 3.15, seal 3.18, electrode insulating gland 3.19, external water outlet pipe 3.21, external positive electrode plate 3.22, external water inlet pipe 3.23 and external negative electrode plate 3.24;
铜管3.9外径向向外依次同轴套装设有绝缘压套3.10和金属套管3.7,铜管3.9外固定同轴套装有用于和金属套管3.7绝缘的绝缘压套3.10,绝缘压套3.10外同轴套装有金属套管3.7,这样铜管3.9和金属套管3.7之间保持绝缘;金属套管3.7中部通过绝缘压套3.14和轴用密封圈3.13密封套装在固定法兰3.11的中心孔中,固定法兰3.11通过固定螺杆3.12固定于离心机的实验腔盖上,铜管3.9、绝缘压套3.10和金属套管3.7的两端分别通过内绝缘套3.6和密封件3.18固定密封安装,通过内绝缘套3.6和密封件3.18绝缘和防止漏水;The outer radial direction of the copper tube 3.9 is set coaxially with an insulating sleeve 3.10 and a metal sleeve 3.7, and the outer fixed coaxial sleeve of the copper tube 3.9 is equipped with an insulating sleeve 3.10 and an insulating sleeve 3.10 for insulation from the metal sleeve 3.7 The outer coaxial sleeve is equipped with a metal sleeve 3.7, so that the insulation between the copper tube 3.9 and the metal sleeve 3.7 is maintained; the middle part of the metal sleeve 3.7 is sealed and fitted in the center hole of the fixed flange 3.11 through the insulating pressure sleeve 3.14 and the shaft sealing ring 3.13 Among them, the fixed flange 3.11 is fixed on the experimental chamber cover of the centrifuge through the fixed screw rod 3.12, and the two ends of the copper tube 3.9, the insulating sleeve 3.10 and the metal sleeve 3.7 are respectively fixed and sealed through the inner insulating sleeve 3.6 and the seal 3.18, Insulate and prevent water leakage through the inner insulating sleeve 3.6 and the seal 3.18;
铜管3.9一端穿过内绝缘套3.6后和流通出水管3.3同轴对接,且在铜管3.9一端穿过内绝缘套3.6后的端部设置正电极3.5;外接正电极板3.22通过多个电极绝缘压套3.19和铜管3.9电连接,具体地,至少两个电极绝缘压套3.19通过螺纹套装铜管3.9的外螺纹上,其中相邻两个电极绝缘压套3.19之间被压紧安装有外接正电极板3.22,外接正电极板3.22穿过相邻两个电极绝缘压套3.19之间的间隙和外接正电极板3.22保持电连接。这样使得正电极3.5直接经铜管3.9后和外接正电极板3.22电连接;One end of the copper pipe 3.9 passes through the inner insulating sleeve 3.6 and is coaxially connected with the circulation outlet pipe 3.3, and a positive electrode 3.5 is set at the end of the copper pipe 3.9 after passing through the inner insulating sleeve 3.6; the external positive electrode plate 3.22 passes through multiple electrodes The insulating gland 3.19 is electrically connected to the copper pipe 3.9. Specifically, at least two electrode insulating glands 3.19 are threaded onto the external threads of the copper pipe 3.9, wherein two adjacent electrode insulating glands 3.19 are compressed and installed with The externally connected positive electrode plate 3.22, the externally connected positive electrode plate 3.22 passes through the gap between two adjacent electrode insulating sleeves 3.19 and maintains electrical connection with the externally connected positive electrode plate 3.22. In this way, the positive electrode 3.5 is directly electrically connected to the external positive electrode plate 3.22 through the copper tube 3.9;
铜管3.9另一端通过密封螺母3.20和外接出水管3.21对接,这样使得流通出水管3.3直接经铜管3.9和外接出水管3.21流通;The other end of the copper pipe 3.9 is connected to the external outlet pipe 3.21 through the sealing nut 3.20, so that the circulation outlet pipe 3.3 is directly circulated through the copper pipe 3.9 and the external outlet pipe 3.21;
绝缘压套3.10和金属套管3.7之间具有环形管道间隙用于作为进水通道,进水通道在靠近内绝缘套3.6的一端经金属管道和流通进水管3.1连通连接,流通进水管3.1在端部附近设置负电极3.8;外接负电极板3.24通过多个压紧圆螺母3.15和金属套管3.7电连接,具体地,至少两个压紧圆螺母3.15通过螺纹套装金属套管3.7的外螺纹上,其中相邻两个压紧圆螺母3.15之间被压紧安装有外接负电极板3.24,外接负电极板3.24穿过相邻两个压紧圆螺母3.15之间的间隙和外接负电极板3.24保持电连接。这样使得负电极3.8依次经金属管道、金属套管3.7后和外接负电极板3.24电连接;There is an annular pipe gap between the insulating gland 3.10 and the metal sleeve 3.7 for the water inlet channel, and the water inlet channel is connected to the metal pipe and the circulation water inlet pipe 3.1 at the end close to the inner insulation sleeve 3.6, and the circulation water inlet pipe 3.1 is at the end The negative electrode 3.8 is set near the center; the external negative electrode plate 3.24 is electrically connected to the metal sleeve 3.7 through a plurality of compression round nuts 3.15, specifically, at least two compression round nuts 3.15 are threaded on the external thread of the metal sleeve 3.7 , wherein an external negative electrode plate 3.24 is compressed and installed between two adjacent compression round nuts 3.15, and the external negative electrode plate 3.24 passes through the gap between two adjacent compression round nuts 3.15 and the external negative electrode plate 3.24 Stay electrically connected. In this way, the negative electrode 3.8 is electrically connected to the external negative electrode plate 3.24 after sequentially passing through the metal pipe and the metal sleeve 3.7;
金属套管3.7在连接密封件3.18的、设置外接正电极板3.22和外接负电极板3.24之间的一端管壁开设有通槽,通槽和外接进水管3.23流通连接,具体地,通槽周围的金属套管3.7上通过顶紧螺母3.16套装绝缘件3.17,外接进水管3.23穿过绝缘件3.17上的通孔和通槽连通;这样使得流通进水管3.1依次经金属管道、进水通道、通槽后和外接进水管3.23流通;The metal casing 3.7 is provided with a through groove on the pipe wall at one end of the connecting seal 3.18, between the external positive electrode plate 3.22 and the external negative electrode plate 3.24, and the through groove is connected to the external water inlet pipe 3.23. Specifically, around the through groove The metal casing 3.7 is set with the insulator 3.17 through the top tightening nut 3.16, and the external water inlet pipe 3.23 passes through the through hole and the through groove on the insulator 3.17 to communicate; in this way, the circulation inlet pipe 3.1 passes through the metal pipe, the water inlet channel, and the through channel in turn. After the tank, it communicates with the external water inlet pipe 3.23;
其中更具体地,铜管3.9是一根空心长铜管,外周安装绝缘压套3.10用于绝缘,安装密封圈可用于防止实验腔体漏气。More specifically, the copper tube 3.9 is a long hollow copper tube, and an insulating compression sleeve 3.10 is installed on the periphery for insulation, and a sealing ring is installed to prevent air leakage from the experimental cavity.
流通进水管3.1通过连接螺母3.2与感应加热系统2的加热进水管2.11连接;流通出水管3.3通过连接螺母3.4与感应加热系统2的加热出水管2.13连接;正电极3.5安装在流通出水管3.3外周,确保冷却水能够冷却到正电极3.5;负电极3.8安装在流通进水管3.1外周,确保冷却水能够冷却到负电极3.8。The circulation inlet pipe 3.1 is connected to the heating water inlet pipe 2.11 of the induction heating system 2 through the connection nut 3.2; the circulation outlet pipe 3.3 is connected to the heating outlet pipe 2.13 of the induction heating system 2 through the connection nut 3.4; the positive electrode 3.5 is installed on the periphery of the circulation outlet pipe 3.3 , to ensure that the cooling water can be cooled to the positive electrode 3.5; the negative electrode 3.8 is installed on the periphery of the circulation inlet pipe 3.1, to ensure that the cooling water can be cooled to the negative electrode 3.8.
金属套管3.7外通过法兰3.11用6个固定螺杆3.12安装在实验腔的腔盖上,然后通过轴用密封圈3.13防止漏气,用绝缘压套3.14绝缘防止漏电;在绝缘压套3.14上面,通过三个压紧圆螺母3.15固定安装外接负电极板3.24;通过顶紧螺母3.16、绝缘件3.17使外接进水管3.23与铜管3.9的通槽联通,且通过顶紧螺母3.16方便更换或维修外接进水管3.23,绝缘件3.17防止电机漏电;在密封件3.18上面,通过电极绝缘压套3.19固定外接正电极板3.22;在电极绝缘压套3.19上面,通过密封螺母3.20使外接出水管3.21与流通出水管3.3的铜管联通。The metal casing 3.7 is installed on the chamber cover of the experimental chamber with 6 fixed screw rods 3.12 through the flange 3.11, and then the shaft seal ring 3.13 is used to prevent air leakage, and the insulation pressure sleeve 3.14 is used to insulate to prevent leakage; on the insulation pressure sleeve 3.14 , the external negative electrode plate 3.24 is fixedly installed through three compression round nuts 3.15; the external water inlet pipe 3.23 is connected with the through groove of the copper pipe 3.9 through the tightening nut 3.16 and the insulator 3.17, and the replacement or maintenance is facilitated by the tightening nut 3.16 The external water inlet pipe 3.23 and the insulator 3.17 prevent electric leakage of the motor; on the seal 3.18, the external positive electrode plate 3.22 is fixed through the electrode insulating pressure sleeve 3.19; on the electrode insulating pressure sleeve 3.19, the external water outlet pipe 3.21 is connected to the circulation The copper pipe Unicom of outlet pipe 3.3.
管道组件包括加热进水管2.11、进水管密封套2.12、加热出水管2.13和出水管密封套2.14;加热进水管2.11、加热出水管2.13的一端分别经进水管密封套2.12、出水管密封套2.14和流通进水管3.1、流通出水管3.3连接,加热进水管2.11和加热出水管2.13的另一端分别连通到感应加热系统2中的上感应线圈2.1和下感应线圈2.5所在的内腔环境中,上感应线圈2.1和下感应线圈2.5所在的内腔环境相互连通。The pipeline assembly includes a heating water inlet pipe 2.11, a water inlet pipe sealing sleeve 2.12, a heating outlet pipe 2.13 and an outlet pipe sealing sleeve 2.14; The circulation inlet pipe 3.1 and the circulation outlet pipe 3.3 are connected, and the other ends of the heating water inlet pipe 2.11 and the heating outlet pipe 2.13 are respectively connected to the inner cavity environment where the upper induction coil 2.1 and the lower induction coil 2.5 in the induction heating system 2 are located. The inner chamber environment where the coil 2.1 and the lower induction coil 2.5 are located communicate with each other.
具体地,加热进水管2.11的另一端分别经进水管密封套2.12、连接螺母3.2和流通进水管3.1连接,加热出水管2.13的另一端分别经出水管密封套2.14、连接螺母3.4和流通出水管3.3连接。Specifically, the other end of the heating water inlet pipe 2.11 is respectively connected through the water inlet pipe sealing sleeve 2.12, the connecting nut 3.2 and the circulation water inlet pipe 3.1, and the other end of the heating water outlet pipe 2.13 is respectively connected through the water outlet pipe sealing sleeve 2.14, the connection nut 3.4 and the circulation outlet pipe 3.3 Connections.
外接出水管3.21和外接进水管3.23分别连接到循环水机的进水口和出水口。具体实施中,外接出水管3.21与循环水机进水管连接,外接进水管3.23与循环水机出水管连接,组成一个封闭的循环水冷却系统,给感应加热系统2降温。The external water outlet pipe 3.21 and the external water inlet pipe 3.23 are respectively connected to the water inlet and the water outlet of the circulating water machine. In specific implementation, the external outlet pipe 3.21 is connected to the water inlet pipe of the circulating water machine, and the external water inlet pipe 3.23 is connected to the outlet pipe of the circulating water machine to form a closed circulating water cooling system to cool down the induction heating system 2 .
正电极3.5和负电极3.8分别电连接到上感应线圈2.1和下感应线圈2.5,外接正电极板3.22和外接负电极板3.24分别连接到外部电源的正负极。具体实施中,外接正电极板3.22与作为交流电源的高频交流电源柜4.7的正极连接,外接负电极板3.24与作为交流电源的高频交流电源柜4.7的负极连接,组成一个闭环电路,给感应加热系统2提供电源。The positive electrode 3.5 and the negative electrode 3.8 are electrically connected to the upper induction coil 2.1 and the lower induction coil 2.5 respectively, and the external positive electrode plate 3.22 and the external negative electrode plate 3.24 are respectively connected to the positive and negative poles of the external power supply. In specific implementation, the externally connected positive electrode plate 3.22 is connected to the positive pole of the high-frequency AC power supply cabinet 4.7 as an AC power supply, and the externally connected negative electrode plate 3.24 is connected to the negative pole of the high-frequency AC power supply cabinet 4.7 as an AC power supply to form a closed-loop circuit. The induction heating system 2 provides power.
上感应线圈2.1所在的内腔与加热进水管2.11连接,加热进水管2.11通过进水管密封套2.12与循环水冷却系统3的流通进水管3.1连接;下感应线圈2.5所在的内腔与加热出水管2.13连接,加热出水管2.13通过与出水管密封套2.14与循环水冷却系统3的流通出水管3.3连接,通过冷却系统3提供的冷却水给铜管降温。The inner chamber where the upper induction coil 2.1 is located is connected to the heating water inlet pipe 2.11, and the heating water inlet pipe 2.11 is connected to the circulating water inlet pipe 3.1 of the circulating water cooling system 3 through the water inlet pipe sealing sleeve 2.12; the inner chamber where the lower induction coil 2.5 is located is connected to the heating water outlet pipe 2.13 connection, the heating outlet pipe 2.13 is connected with the outlet pipe sealing sleeve 2.14 and the circulating water outlet pipe 3.3 of the circulating water cooling system 3, and the cooling water provided by the cooling system 3 cools down the copper pipe.
如图5所示,控温系统4的作用是用于通过控制感应电源加热功率,确保给测试试样1.1加热到预定温度且保持该温度直到实验结束。包括热电偶4.1、热电偶延长线4.2、高速滑环4.3、数据采集模块4.4、数据转换传输模块4.6和高频交流电源柜4.7;感应加热系统2的上感应线圈2.1和下感应线圈2.5所正对应的测试试样1.1表面上均固定设有热电偶4.1,热电偶4.1经热电偶延长线4.2、高速滑环4.3和数据采集模块4.4连接,热电偶延长线4.2穿设过样品卡盘1的盘体、离心机的主轴后和高速滑环4.3电连接,高速滑环4.3布置在离心机的主轴上,数据采集模块4.4经数据转换传输模块4.6和高频交流电源柜4.7通信连接、高频交流电源柜4.7和循环水机、循环水冷却系统3的外接正电极板3.22、外接负电极板3.24电连接。As shown in FIG. 5 , the function of the temperature control system 4 is to ensure that the test sample 1.1 is heated to a predetermined temperature by controlling the heating power of the induction power supply and maintain this temperature until the end of the experiment. Including thermocouple 4.1, thermocouple extension wire 4.2, high-speed slip ring 4.3, data acquisition module 4.4, data conversion and transmission module 4.6 and high-frequency AC power supply cabinet 4.7; the upper induction coil 2.1 and the lower induction coil 2.5 of the induction heating system 2 are positive The surface of the corresponding test sample 1.1 is fixed with a thermocouple 4.1, and the thermocouple 4.1 is connected with the thermocouple extension line 4.2, the high-speed slip ring 4.3 and the data acquisition module 4.4, and the thermocouple extension line 4.2 passes through the sample chuck 1. The disc body and the main shaft of the centrifuge are electrically connected to the high-speed slip ring 4.3, and the high-speed slip ring 4.3 is arranged on the main shaft of the centrifuge. The data acquisition module 4.4 is connected to the high-frequency AC power supply cabinet 4.7 through the data conversion and transmission module 4.6. The AC power cabinet 4.7 is electrically connected to the external positive electrode plate 3.22 and the external negative electrode plate 3.24 of the circulating water machine and the circulating water cooling system 3 .
具体实施中还设置控制软件4.5,控制软件4.5分别和数据采集模块4.4、数据转换传输模块4.6连接。In the specific implementation, control software 4.5 is also set, and the control software 4.5 is respectively connected with the data acquisition module 4.4 and the data conversion transmission module 4.6.
实验时热电偶4.1焊接在上感应线圈2.1和下感应线圈2.5对应测试试样1.1的中心部位,然后将热电偶4.1通过热电偶延长线4.2通过离心机空心主轴与高速滑环4.3相连,再通过导线与数据采集模块4.4、控制软件4.5、数据转换传输模块4.6相连,最后将控制信号线与高频交流电源柜4.7相连,组成一个温度调控系统。During the experiment, the thermocouple 4.1 was welded to the center of the upper induction coil 2.1 and the lower induction coil 2.5 corresponding to the test sample 1.1, and then the thermocouple 4.1 was connected to the high-speed slip ring 4.3 through the hollow spindle of the centrifuge through the thermocouple extension line 4.2, and then passed The wire is connected with the data acquisition module 4.4, the control software 4.5, and the data conversion transmission module 4.6, and finally the control signal line is connected with the high-frequency AC power supply cabinet 4.7 to form a temperature control system.
本发明还设计不同的试样,以更好地进行进行试件金属材料的力学性能测试。The present invention also designs different samples to better test the mechanical properties of the metal material of the test piece.
第一种测试试样1.1的结构,见图2,为凹槽试样及其相关类似结构;The structure of the first test sample 1.1, see Figure 2, is a groove sample and related similar structures;
第二种测试试样1.1的结构,见图6,为平板试样及其相关类似结构;The structure of the second test sample 1.1, see Figure 6, is a flat plate sample and related similar structures;
第三种测试试样1.1的结构,见图7,为圆棒试样及其相关类似结构;The structure of the third test sample 1.1, as shown in Figure 7, is a round bar sample and related similar structures;
第四种测试试样1.1的结构,见图8,结构梯度试样及其相关类似结构。The structure of the fourth test sample 1.1, see Fig. 8, the structural gradient sample and its related similar structures.
校温装置下还可提供了多种用于高转速环境下的原位加热模式,为开展不同温度、不同转速条件下材料性能测试提供新的实验条件。其中,本发明的加热模式包括但不限于如下几种情况:The temperature calibration device can also provide a variety of in-situ heating modes for high-speed environments, providing new experimental conditions for material performance tests at different temperatures and different speeds. Wherein, the heating mode of the present invention includes but not limited to the following situations:
加热模式一:高转速下对测试试样1.1的标矩段1.1.2实施均温加热模式,图10。Heating mode 1: Implement uniform temperature heating mode on the standard moment section 1.1.2 of the test sample 1.1 at high speed, as shown in Figure 10.
实验材料类型相同,实验过程中标矩段1.1.2与上感应线圈2.1和下感应线圈2.5之间的距离h保持相同,且加热功率和加热频率在t时间内保持不变,给标矩段1.1.2施加一个恒定且均匀的温度场。The type of experimental material is the same, the distance h between the standard moment section 1.1.2 and the upper induction coil 2.1 and the lower induction coil 2.5 remains the same during the experiment, and the heating power and heating frequency remain unchanged within t time, the standard moment section 1.1 .2 Apply a constant and uniform temperature field.
加热模式二:高转速下对测试试样1.1的标矩段1.1.2实施周期性变化的交变温加热模式,图11。Heating mode 2: Under the high rotation speed, the alternating temperature heating mode is implemented to periodically change the standard moment section 1.1.2 of the test sample 1.1, as shown in Fig. 11 .
实验材料类型相同,实验过程中标矩段1.1.2与上感应线圈2.1和下感应线圈2.5之间的距离h保持相同,加热频率不变,但在t时间内使加热功率周期性变化,给标矩段1.1.2在t1时间内施加T1、在t2时间内施加T2的交变温度场。The experimental material type is the same, the distance h between the standard moment section 1.1.2 and the upper induction coil 2.1 and the lower induction coil 2.5 remains the same during the experiment, the heating frequency is constant, but the heating power is periodically changed within the time t, and the standard Section 1.1.2 is an alternating temperature field in which T1 is applied during t1 and T2 is applied within t2.
加热模式三:高转速下对测试试样1.1的标矩段1.1.2实施恒温的温度梯度的加热模式,图12。Heating mode three: a heating mode in which a constant temperature gradient is applied to the standard moment section 1.1.2 of the test sample 1.1 at a high rotational speed, as shown in FIG. 12 .
实验材料类型相同,将测试试样1.1的标矩段1.1.2加工成半径为R的圆弧,实验过程中标矩段1.1.2圆弧最低端与上感应线圈2.1和下感应线圈2.5之间的距离h保持相同,且加热功率和加热频率在t时间内保持不变。由于圆弧状的标矩段1.1.2到感应线圈2.1和下感应线圈2.5的距离连续变化,根据感应加热原理,相同功率和频率条件下,样品加热温度与其到感应线圈的距离成反比,由此给测试试样1.1的标矩段1.1.2实施一个恒温的温度梯度。The experimental material type is the same, the standard moment section 1.1.2 of the test sample 1.1 is processed into a circular arc with a radius of R, and the distance between the lowest end of the standard moment section 1.1.2 arc and the upper induction coil 2.1 and the lower induction coil 2.5 during the experiment The distance h remains the same, and the heating power and heating frequency remain unchanged for t time. Since the distance from the arc-shaped standard moment section 1.1.2 to the induction coil 2.1 and the lower induction coil 2.5 changes continuously, according to the principle of induction heating, under the same power and frequency conditions, the heating temperature of the sample is inversely proportional to the distance from the induction coil to the induction coil. This implements a constant temperature gradient for the standard moment section 1.1.2 of the test specimen 1.1.
本发明具体实施过程如下:The concrete implementation process of the present invention is as follows:
根据实验条件确定实验温度和离心机转速。Determine the experimental temperature and centrifuge speed according to the experimental conditions.
下面以图10为例,说明高转速-高温作用下材料力学性能高通量测试:Take Figure 10 as an example below to illustrate the high-throughput testing of mechanical properties of materials under the action of high speed and high temperature:
第一步:根据实验条件确定离心机的主轴转速和轮盘半径;Step 1: Determine the spindle speed and disc radius of the centrifuge according to the experimental conditions;
第二步:确定测试试样1.1中质量块1.1.1的尺寸和重量、标距段1.1.2的尺寸和几何中心;The second step: determine the size and weight of the mass block 1.1.1 in the test sample 1.1, the size and the geometric center of the gauge length section 1.1.2;
第三步:确定试验温度和标距段1.1.2几何中心施加的离心应力,进而通过有限元计算确定标距段1.1.2的几何中心的离心应力对应的转速,确定标距段1.1.2几何中心到离心机的主轴中心之间的距离;Step 3: Determine the test temperature and the centrifugal stress imposed by the geometric center of the gauge length section 1.1.2, and then determine the rotational speed corresponding to the centrifugal stress at the geometric center of the gauge length section 1.1.2 through finite element calculations, and determine the gauge length section 1.1.2 The distance between the geometric center and the center of the main shaft of the centrifuge;
第四步:按照第三步的距离在样品卡盘1的一个卡槽1.2中安装一个校温试样5和其余卡槽1.2中安装测试试样1.1,在测试试样1.1旁边安装校温试样5;在校温试样5的各个热电偶孔中均插入热电偶,且在测试试样1.1和校温试样5的标距段1.1.2几何中心位置焊接均固定上各自的控温热电偶4.1,控温热电偶4.1经温度延长导线4.2与控温系统4相连;Step 4: Install a temperature calibration sample 5 in one slot 1.2 of the sample chuck 1 and test sample 1.1 in the remaining slots 1.2 according to the distance of the third step, and install a temperature calibration test sample next to the test sample 1.1. Sample 5; thermocouples are inserted in each thermocouple hole of the temperature calibration sample 5, and the respective temperature control tubes are fixed at the geometric center positions of the gauge length section 1.1.2 of the test sample 1.1 and the temperature calibration sample 5. Thermocouple 4.1, temperature control thermocouple 4.1 is connected with temperature control system 4 through temperature extension wire 4.2;
校温试样5和测试测试试样1.1在相同的环境下,认为校核试样5中获得的温度分布与测试测试试样1.1的温度分布相同。Calibration sample 5 and test test sample 1.1 are in the same environment, it is considered that the temperature distribution obtained in the calibration sample 5 is the same as that of the test test sample 1.1.
第五步:在不启动离心机情况下,样品卡盘1及其上面的测试试样1.1和校温试样5均保持静止,对离心机内部的环境进行抽真空,然后启动感应加热系统2、循环水冷却系统3和控温系统4,通过控温系统4控制感应加热系统2、循环水冷却系统3工作对测试试样1.1和校温试样5施加温度载荷,待温度到达预定温度后并保温一段时间30min;Step 5: Without starting the centrifuge, keep the sample chuck 1 and the test sample 1.1 on it and the temperature calibration sample 5 still, vacuumize the environment inside the centrifuge, and then start the induction heating system 2 , the circulating water cooling system 3 and the temperature control system 4, through the temperature control system 4 to control the induction heating system 2, the circulating water cooling system 3 work to apply a temperature load to the test sample 1.1 and the temperature calibration sample 5, after the temperature reaches the predetermined temperature And keep warm for 30 minutes;
通过测试试样1.1和校温试样5的控温热电偶4.1以及校温试样5的各个热电偶孔中的热电偶测量获得温度随时间变化的温度数据进行分析处理获得正式试验测量时的上感应线圈2.1和下感应线圈2.5的通电电流、电流交变频率和功率以及上感应线圈2.1和下感应线圈2.5之间的间距的参数;By testing the temperature control thermocouple 4.1 of the test sample 1.1 and the temperature calibration sample 5 and the thermocouple measurement in each thermocouple hole of the temperature calibration sample 5, the temperature data obtained by the temperature change with time is analyzed and processed to obtain the formal test measurement. Parameters of the energizing current, current alternating frequency and power of the upper induction coil 2.1 and the lower induction coil 2.5, and the distance between the upper induction coil 2.1 and the lower induction coil 2.5;
第六步:从样品卡盘1的卡槽1.2上撤下校温试样5、换上测试试样1.1,使得样品卡盘1的每个卡槽1.2中均安装测试试样1.1,再启动离心机,使离心机的主轴旋转且转速达到离心应力对应的转速进行正式试验测试,按照第五步获得的参数控制上感应线圈2.1和下感应线圈2.5之间的间距和通电电流、电流交变频率和功率,保持参数不变,直到测试试样1.1被拉断断裂。Step 6: Remove the temperature calibration sample 5 from the slot 1.2 of the sample chuck 1 and replace it with the test sample 1.1, so that the test sample 1.1 is installed in each slot 1.2 of the sample chuck 1, and then start the centrifugation machine, make the main shaft of the centrifuge rotate and the rotational speed reaches the rotational speed corresponding to the centrifugal stress to conduct a formal test, and control the distance between the upper induction coil 2.1 and the lower induction coil 2.5 according to the parameters obtained in the fifth step, and the energized current and current alternating frequency and power, keep the parameters constant until the test specimen 1.1 is pulled off and broken.
从离心机的主轴开始旋转到测试试样1.1被拉断断裂之间的过程中,通过控温热电偶4.1和应变片实时采集温度变化和应力变化的数据,试件测量试验的数据。During the process from when the main shaft of the centrifuge starts to rotate to when the test sample 1.1 is broken, the data of temperature change and stress change are collected in real time through the temperature control thermocouple 4.1 and the strain gauge, and the data of the test sample is measured.
这样方法通过校温装置来检测每个点的温度,也通过校温过程来设定参数调整后续试验施加的条件,使得在试验时的试件温度梯度越小。In this way, the temperature of each point is detected by the temperature calibration device, and the parameters are set through the temperature calibration process to adjust the conditions applied in the subsequent test, so that the temperature gradient of the specimen during the test is smaller.
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