CN108815084A - A kind of dandruff control shampoo containing and preparation method thereof containing Herba Lophatheri extract - Google Patents
A kind of dandruff control shampoo containing and preparation method thereof containing Herba Lophatheri extract Download PDFInfo
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- CN108815084A CN108815084A CN201810972696.2A CN201810972696A CN108815084A CN 108815084 A CN108815084 A CN 108815084A CN 201810972696 A CN201810972696 A CN 201810972696A CN 108815084 A CN108815084 A CN 108815084A
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- China
- Prior art keywords
- dandruff
- extract
- herba lophatheri
- zpt
- shampoo
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- 238000002360 preparation method Methods 0.000 title claims abstract description 15
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- 229910052711 selenium Inorganic materials 0.000 description 1
- 230000035807 sensation Effects 0.000 description 1
- 229940095673 shampoo product Drugs 0.000 description 1
- 230000003997 social interaction Effects 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 235000007586 terpenes Nutrition 0.000 description 1
- 229940124597 therapeutic agent Drugs 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
- A61K8/416—Quaternary ammonium compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4926—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having six membered rings
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4933—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having sulfur as an exocyclic substituent, e.g. pyridinethione
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9771—Ginkgophyta, e.g. Ginkgoaceae [Ginkgo family]
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- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
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Abstract
The invention discloses a kind of dandruff control shampoo containing and preparation method thereof containing Herba Lophatheri extract.The dandruff control shampoo containing includes the raw material of following weight percentage：Anti-dandruff agent 0.35-0.60%, wherein the weight ratio of ZPT and OCT is (0.25-0.5):0.1, Herba Lophatheri extract 0.005-1%, other plant extract 0-3%, conditioner 0.1-5%, anionic surfactant 10-40%, nonionic surfactant 0.5-10%, amphoteric surfactant 1.0-10%, thickener 0.15-0.7%, preservative 0-0.50%, essence 0-1%, deionized water surplus.The shampoo has good anti-dandruff and itching-relieving and avoids hair and dry scalp and other effects on the basis of safely cleaning hair, and the crowd for having dandruff is suitble to use.
Description
Technical field
The invention belongs to field of daily chemicals, and in particular to a kind of dandruff control shampoo containing and its system containing Herba Lophatheri extract
Preparation Method.
Background technique
Shampoo is the important hair cleaning supplies that hair and scalp cleaning health are kept in life.With shampoo formula
With the development of technique, shampoo no longer limits to cleaning purpose, it is also necessary to which good anti-dandruff effect will more take into account south and north
Square market.
Dandruff is a kind of common scalp affections, often shows as sticking the sheet scales of skin that peel off on scalp and hair,
Disease incidence about 50% in crowd, it is common and serious in young man.Since dandruff shows as dry skin, furfur, quilt
Referred to as capitis pityriasis.Dandruff makes people generate itching of the scalp, stimulate, the discomforts such as exsiccation of feeling nervous, the social interaction for people
It has a negative impact.
In view of the clinical characters of dandruff, current therapeutic agent mainly has cutin the cracking-off agent such as coal tar, sulphur of external application
The antifungal drug of sulphur and salicylic acid etc. and wide spectrum.It is wherein preferable with the clinical effectiveness of antifungal drug, and hair washing is made more
Shampoo carry out using.Main anti-dandruff agent is mainly with ZPT, climbazole, piroctone olamine salt etc. currently on the market.Due to
ZPT has outstanding antibacterial effect and price low, nearly 45% shampoo using it as main anti-dandruff component, but due to
ZPT itself belongs to minerals, and is deposited on scalp, when this also results in the drying of northern winter, in single use amount lower part
Crowd is divided to itch using rear scalp hair shaft.Piroctone olamine salt is the anti-dandruff and itching-relieving that uniquely can be used for disposable class hair care product
Agent, the anti-dandruff and itching-relieving agent that can be retained on scalp and hair-care, but since its price is high compared with ZPT price, it is single in cost consideration to make
With being just provided with limitation.If guaranteeing that dandruff control shampoo containing price is easy to be esthetically acceptable to the consumers, there is anti-dandruff effect, and can be simultaneously
The anti-dandruff demand for meeting southern and northern Various Seasonal, is a technological difficulties in current anti-dandruff shampoo product development.Therefore it is badly in need of
Invent the dandruff control shampoo containing that one kind can have good anti-dandruff effect and southern and northern market Various Seasonal.
Summary of the invention
The first purpose of the invention is to provide a kind of dandruff control shampoo containing containing Herba Lophatheri extract, which is used
ZPT (zinc pyrithione), OCT (piroctone olamine salt) and Herba Lophatheri extract are used in compounding can be in the base of safely cleaning hair
Effective anti-dandruff and itching-relieving, avoids hair and dry scalp on plinth；In addition, Herba Lophatheri extract and conditioner in the dandruff control shampoo containing
(guar hydroxypropyltrimonium ammonium chloride, polyquaternium, albumen etc.) synergistic effect can reach good conditioning performance, preferably
Avoid hair and dry scalp.Product of the present invention reduces production cost, is suitble to different zones (especially southern and northern), different seasons
Section has dandruff crowd use.
A second object of the present invention is to provide the preparation methods of the above-mentioned dandruff control shampoo containing containing Herba Lophatheri extract.
In order to achieve the above objectives, the present invention adopts the following technical solutions：
A kind of dandruff control shampoo containing containing Herba Lophatheri extract, active constituent include anti-dandruff agent and Herba Lophatheri extract, institute
Stating anti-dandruff agent includes ZPT, OCT, and the weight ratio of ZPT and OCT is (0.25-0.50):0.1；The sum of weight of ZPT, OCT with it is light
The weight ratio of bamboo extractive is (0.35-0.60):(0.005-1.5).
As an optimal technical scheme of the invention, the anti-dandruff agent is made of ZPT, OCT.
If active constituent of the present invention is primarily referred to as avoiding hair and scalp dry with anti-dandruff and itching-relieving without specified otherwise
Dry active constituent.
Further, the dandruff control shampoo containing containing Herba Lophatheri extract, wherein the weight ratio of ZPT and OCT is (0.25-
0.50):0.1；The sum of weight of ZPT, OCT and the weight ratio of Herba Lophatheri extract are (0.35-0.60):(0.005-1.0).
Specifically, the dandruff control shampoo containing containing Herba Lophatheri extract, wherein the weight ratio of ZPT and OCT can be 0.25:
0.1,0.40:0.1 or 0.5:0.1；And/or the sum of weight of ZPT, OCT and the weight ratio of Herba Lophatheri extract can be 0.35:
0.005、0.5:0.01、0.6:1.00。
Preferably, the dandruff control shampoo containing containing Herba Lophatheri extract, wherein the weight ratio of ZPT and OCT is 0.4:0.1；
The sum of weight of ZPT, OCT and the weight ratio of Herba Lophatheri extract are 0.5:0.01.
Further, in the dandruff control shampoo containing containing Herba Lophatheri extract, the weight of ZPT, OCT, Herba Lophatheri extract
The sum of content is 0.355-1.6%.
In above-mentioned active constituent proportional region, those skilled in the art can be adjusted as needed, this can be achieved
Goal of the invention.
Conventionally used ZPT is its suspension, and active component content 48-50% is commercially available to buy.
The content of ZPT is in terms of its sterling in dandruff control shampoo containing of the present invention.
In the case where not influencing the above-mentioned effect of shampoo of the present invention, ability can be added in those skilled in the art as needed
The available other active components in domain or auxiliary agent.
Further, also containing the other plant as active constituent in the dandruff control shampoo containing containing Herba Lophatheri extract
One or more of extract, including ginkgo biloba extract, camomile extract, chrysanthemum extract, wolfberry fruit extract etc..This hair
It is bright the study found that ZPT, OCT and Herba Lophatheri extract and above-mentioned other plant extract act synergistically, be more advantageous to it is anti-dandruff only
Itch, avoid hair and dry scalp；Better effect when especially selecting ginkgo biloba extract.
Further, in the dandruff control shampoo containing containing Herba Lophatheri extract, the weight of the other plant extract contains
Amount is 0-3%, preferably 0.1-3%.
Further, appropriate conditioner can be also contained in the dandruff control shampoo containing of the present invention containing Herba Lophatheri extract；?
The synergistic effect of these conditioners can reach good conditioning performance, preferably avoid hair and dry scalp, meet consumer
Demand.The dosage of the conditioner can routinely be needed to be adjusted by this field.
Specifically, the conditioner include guar hydroxypropyltrimonium chloride, polyquaternium -7, Polyquaternium-10,
Avocado Oil, Ah's glycerol, hydrolytic collagen and/or albumen, panthenol, glycine betaine, pearly-lustre dibasic acid esters, hexadecanol, menthol, silicone emulsion etc.
One or more of.
Further, appropriate anionic surface can be also contained in the dandruff control shampoo containing of the present invention containing Herba Lophatheri extract
Activating agent and/or nonionic surfactant and/or amphoteric surfactant；Its dosage can routinely be adjusted by this field
It is whole.
Specifically, the anionic surfactant includes laureth sulfuric ester ammonium, laurel alcohol sulfuric ester ammonium, laurel
One of alcohol polyethers sodium sulfovinate, laruyl alcohol sodium sulfovinate, sodium lauroyl sarcosine, cocoamido sodium propionate etc. are several
Kind.
Specifically, the nonionic surfactant includes coconut oleoyl amine DEA, lauryl glucoside, amine oxide, cocounut oil acyl
One or more of amine monoethanolamine etc..
Specifically, the amphoteric surfactant includes Cocoamidopropyl betaine amine, cocounut oil acyl both sexes base oxalic acid
One or more of disodium etc..
Further, in the dandruff control shampoo containing of the present invention containing Herba Lophatheri extract can also containing appropriate thickener and/
Or preservative and/or essence, dosage can routinely be needed to be adjusted by this field.
Specifically, the thickener includes one or more of U20, ETD2020, TAB etc..
Specifically, the preservative includes sodium benzoate, 1,2- hexylene glycol/pungent glycol/tropolone, in DMDM second
One or more of uride, methylisothiazolinone, methyl hydroxybenzoate etc..
Further, also contain in the dandruff control shampoo containing of the present invention containing Herba Lophatheri extract and gone as primary solvent
Ionized water.
Specifically, the dandruff control shampoo containing of the present invention containing Herba Lophatheri extract, containing following weight percentage components：
Anti-dandruff agent 0.35-0.60%, wherein the weight ratio of ZPT and OCT is preferably (0.25-0.5):0.1, Herba Lophatheri extract
0.005-1%, other plant extract 0-3%, conditioner 0.1-5%, anionic surfactant 10-40%, nonionic table
Face activating agent 0.5-10%, amphoteric surfactant 1.0-10%, thickener 0.15-0.7%, preservative 0-0.50%, essence
0-1%, deionized water surplus.
More specifically, the dandruff control shampoo containing containing Herba Lophatheri extract, containing following weight percentage components：It is anti-dandruff
Agent 0.35-0.60%, wherein the weight ratio of ZPT and OCT is preferably (0.25-0.5):0.1, Herba Lophatheri extract 0.01-
0.5%, other plant extract 0-3%, conditioner 0.1-5%, anionic surfactant 10-40%, non-ionic surface are lived
Property agent 0.5-10%, amphoteric surfactant 1.0-10%, thickener 0.15-0.7%, 0-0.50 parts of preservative, essence 0-
1%, deionized water surplus.
Preferably, the dandruff control shampoo containing containing Herba Lophatheri extract, containing following weight percentage components：Anti-dandruff agent
0.5%, wherein the weight ratio of ZPT and OCT is preferably 0.4:0.1, Herba Lophatheri extract 0.01%, other plant extract 0-
3%, conditioner 0.1-5%, anionic surfactant 10-40%, nonionic surfactant 0.5-10%, amphoteric surface are living
Property agent 1.0-10%, thickener 0.15-0.7%, 0-0.50 parts of preservative, essence 0-1%, deionized water surplus.
Lophatherum gracile is the drying cauline leaf of grass henon bamboo leaf.Li Shizhen of the Ming Dynasty exists《Compendium of Materia Medica》It is middle to discuss it：Sweet,
It is cold, nontoxic, go dysphoria with smothery sensation, diuresis, clear away heart-fire.Modern research shows that：Contain a large amount of flavone compound and biology in lophatherum gracile
Active polysaccharide and other active components, such as phenolic acid compound, anthraquinone analog compound, terpene lactone, amino acid and manganese, zinc, selenium
Equal microelements.It clinically commonly uses lophatherum gracile and controls thirsty pyreticosis, vexed, aphthous stomatitis tongue boil, swelling and aching of gum etc..In formula of the invention
In, Herba Lophatheri extract can act synergistically with other plants extracts such as anti-dandruff agent (ZPT and OCT) and ginkgo biloba extracts,
Lower anti-dandruff agent dosage, reaches effect of the health of anti-dandruff, maintenance hair and scalp.
Further, the Herba Lophatheri extract is alcohol extract, and principle active component is bamboo-leaves flavones, general flavone content >=
24.0%；It is commercially available to buy.Such as purchased from Zhejiang Shengshi Biological Product Co., Ltd.
Further, the ginkgo leaf is extracted as water extract (liquid), and principle active component is total flavonol glycosides, content
It is >=0.1%；It is commercially available to buy.Such as purchased from Shanghai Jia Kai Biotechnology Co., Ltd.
Further, the camomile extract is water extract (liquid), and principle active component is chlorogenic acid, content is >=
0.1%；It is commercially available to buy.Such as purchased from Shanghai Jia Kai Biotechnology Co., Ltd.
Further, the chrysanthemum extract is water extract (liquid), and principle active component is galuteolin, content is >=
0.1%；It is commercially available to buy.Such as purchased from Shanghai Jia Kai Biotechnology Co., Ltd.
Further, the wolfberry fruit extract is water extract (liquid), and principle active component is polysaccharides, content is >=
0.2%；It is commercially available to buy.Such as purchased from Shanghai Jia Kai Biotechnology Co., Ltd.
Dandruff control shampoo containing of the present invention containing Herba Lophatheri extract can be prepared by conventional method in that art.
Specific body, the present invention also provides the preparation method of the above-mentioned dandruff control shampoo containing containing Herba Lophatheri extract, this method packets
It includes：Main tank is added in deionized water, is warming up to 75 DEG C -85 DEG C, sequentially add conditioner, thickener, anionic surfactant,
Amphoteric surfactant, nonionic surfactant, Herba Lophatheri extract, after be cooled to 45-55 DEG C, it is anti-dandruff to sequentially add low temperature
Agent, low temperature conditioner, plant extracts, preservative, essence stir evenly, formed solution to get.
Furthermore, it is to be understood that herein, also included in the meaning of terms such as "include", "comprise", " containing " " by ...
Composition ", " by ... constitute ", " by ... it is made " etc..
Each raw material of the present invention is commercially available to be bought or prepares by conventional method in that art.
On the basis of common knowledge of the art, above-mentioned each optimum condition can be combined with each other each preferably to get the present invention
Example.
Beneficial effects of the present invention are as follows：
Herba Lophatheri extract, OCT and ZPT three collaboration in dandruff control shampoo containing provided by the invention containing Herba Lophatheri extract
Effect, so that product has good anti-dandruff performance, meanwhile, by the stringent screening of other conditioning ingredients in formula so that this is washed
Shampoo has good moisturizing and conditioning efficiency, the crowd demand of more suitable the South and the North Various Seasonal.Dandruff control shampoo containing of the present invention exists
On the basis of safely cleaning hair, there is good anti-dandruff performance, the crowd for having dandruff is suitble to use.
Specific embodiment
In order to illustrate more clearly of the present invention, below with reference to preferred embodiment, the present invention is described further.Ability
Field technique personnel should be appreciated that following specifically described content is illustrative and be not restrictive, this should not be limited with this
The protection scope of invention.
ZPT used below is its suspension, and active component content 50% is purchased from Mitsubishi Chemical
Corporation。
OCT used below is white powder, and active component content is 98%-101.5% (potentiometric titration), is purchased from India
Ku Ma company.
Herba Lophatheri extract used below is alcohol extract, and principle active component is bamboo-leaves flavones, general flavone content is >=
24%；Purchased from Zhejiang Shengshi Biological Product Co., Ltd.
Ginkgo leaf is extracted as Aqueous extracts, and principle active component is total flavonol glycosides, and content is >=0.1%；Purchased from upper
Hai Jiakai Biotechnology Co., Ltd.
Camomile extract is Aqueous extracts, and principle active component is chlorogenic acid, and content is >=0.1%；It is triumphant purchased from Shanghai Ka
Biotechnology Co., Ltd.
Chrysanthemum extract is Aqueous extracts, and principle active component is galuteolin, and content is >=0.1%；It is triumphant purchased from Shanghai Ka
Biotechnology Co., Ltd.
Wolfberry fruit extract is water extract liquid, and principle active component is polysaccharides, content 0.2%；It is triumphant purchased from Shanghai Ka
Biotechnology Co., Ltd.
1 dandruff control shampoo containing of embodiment
Formula composition：Anti-dandruff agent 0.35% (ZPT 0.25%, OCT 0.1%), Herba Lophatheri extract 0.005%, ocean are sweet
Chrysanthemum extract 1%, chrysanthemum extract 1%, wolfberry fruit extract 1%, guar hydroxypropyltrimonium chloride 0.3%, polyquaternary amine
Salt -7 2%, Polyquaternium-10 0.3%, panthenol 0.2%, pearly-lustre dibasic acid esters 1.5%, hexadecanol 0.4%, menthol 0.3%, cream
SiClx oil 3%, laureth sulfuric ester ammonium 8%, laurel alcohol sulfuric ester ammonium 2%, coconut oleoyl amine monoethanolamine 3%, lauryl
Glucoside 7%, cocounut oil acyl both sexes base diethyl acid disodium 10.0%, TAB 0.5%, 1,2- hexylene glycol/pungent glycol/cycloheptatriene phenol
Ketone 0.50%, deionized water surplus.(note：In the formula, ZPT is the content in terms of its sterling.)
Preparation process：
Main tank is added in deionized water, guar hydroxypropyltrimonium chloride, poly- season are sequentially added under stirring
Ammonium salt -10 is uniformly dispersed, and then addition laureth sulfuric ester ammonium, laurel alcohol sulfuric ester ammonium are warming up to 85 DEG C and are uniformly dissolved,
It adds pearly-lustre dibasic acid esters, hexadecanol and Herba Lophatheri extract is added after TAB heat preservation half an hour and be cooled to 70 DEG C, coconut oleoyl amine is added
Monoethanolamine, lauryl glucoside and cocounut oil acyl both sexes base diethyl acid disodium, after be cooled to 55 DEG C, OCT and scattered is added
ZPT, polyquaternium -7, camomile extract, chrysanthemum extract, wolfberry fruit extract stir evenly, and 45 DEG C of 1,2- of addition hexylene glycols/
Pungent glycol/tropolone, the menthol being pre-dissolved, panthenol, silicone emulsion formed solution to get.
2 dandruff control shampoo containing of embodiment
Formula composition：Anti-dandruff agent 0.6% (ZPT 0.5%, OCT 0.1%), ETD2020 0.2%, Herba Lophatheri extract
1.0%, ginkgo biloba extract 1%, laureth sodium sulfovinate 16%, laruyl alcohol sodium sulfovinate 2%, coconut oleoyl amine DEA
0.5%, sodium lauroyl sarcosine 11%, cocoamido sodium propionate 11%, Cocoamidopropyl betaine 1%, melon rubber hydroxyl
Hydroxypropyltrimonium chloride 0.15%, albumen 0.1%, glycine betaine 0.5%, methylisothiazolinone 0.08%, methyl hydroxybenzoate
0.1%, deionized water surplus.(note：In the formula, ZPT is the content in terms of its sterling.)
Preparation process：
Main tank is added in deionized water, it is equal that guar hydroxypropyltrimonium chloride dispersion is sequentially added under stirring
It is even, soaked ETD2020, laureth sodium sulfovinate, laruyl alcohol sodium sulfovinate, methyl hydroxybenzoate is then added and is warming up to 85
It DEG C is uniformly dissolved after heat preservation half an hour and Herba Lophatheri extract is added is cooled to 70 DEG C, coconut oleoyl amine DEA, Hamposyl L is added
Sodium, cocoamido sodium propionate, Cocoamidopropyl betaine are cooled to 55 DEG C after mixing evenly, and OCT and scattered is added
ZPT, ginkgo biloba extract, glycine betaine stir evenly, 45 DEG C of addition methylisothiazolinones, albumen formed solution to get.
3 dandruff control shampoo containing of embodiment
Formula composition：Anti-dandruff agent 0.35% (ZPT 0.25%, OCT 0.1%), U20 0.7%, Herba Lophatheri extract
0.005%, laureth sulfuric ester ammonium 8%, laurel alcohol sulfuric ester ammonium 2%, coconut oleoyl amine monoethanolamine 3%, melon rubber hydroxyl
Hydroxypropyltrimonium chloride 0.2%, Ah's glycerol 0.1%, Avocado Oil 0.1%, hydrolytic collagen 0.05%, DMDM hydantoin
0.30%, essence 1.0%, deionized water surplus.(note：In the formula, ZPT is the content in terms of its sterling.)
Preparation process：
Main tank is added in deionized water, it is equal that guar hydroxypropyltrimonium chloride dispersion is sequentially added under stirring
It is even, soaked U20, laureth sulfuric ester ammonium, laurel alcohol sulfuric ester ammonium is then added and is warming up to 85 DEG C and is uniformly dissolved, protects
Herba Lophatheri extract is added after warm half an hour and is cooled to 70 DEG C, coconut oleoyl amine monoethanolamine is added, after be cooled to 55 DEG C, be added
OCT and scattered ZPT, Ah's glycerol, Avocado Oil, hydrolytic collagen stir evenly, 45 DEG C of additions DMDM hydantoin, essence, shape
At solution to get.
4 dandruff control shampoo containing of embodiment
Formula composition：Anti-dandruff agent 0.5% (ZPT 0.4%, OCT 0.1%), U20 0.2%, Herba Lophatheri extract
0.01%, ginkgo biloba extract 0.1%, laureth sulfuric ester ammonium 17%, laurel alcohol sulfuric ester ammonium 4%, melon rubber hydroxypropyl
Trimethyl ammonium chloride 0.2%, Polyquaternium-10 0.2%, coconut oleoyl amine DEA0.6%, Cocoamidopropyl betaine 5% are general
Alcohol 0.2%, glycine betaine 0.5%, pearly-lustre dibasic acid esters 1.5%, hexadecanol 0.4%, menthol 0.1%, silicone emulsion 3%, DMDM second
Interior uride 0.30%, methylisothiazolinone 0.03%, essence 0.4%, deionized water surplus.(note：In the formula, ZPT be with
The content of its sterling meter.)
Preparation process：
Main tank is added in deionized water, guar hydroxypropyltrimonium chloride, poly- season are sequentially added under stirring
Ammonium salt -10 is uniformly dispersed, and soaked U20, laureth sulfuric ester ammonium, laurel alcohol sulfuric ester ammonium is then added and is warming up to 85
It DEG C is uniformly dissolved, adds coconut oleoyl amine DEA, pearly-lustre dibasic acid esters, Herba Lophatheri extract cooling is added after hexadecanol heat preservation half an hour
To 70 DEG C, Cocoamidopropyl betaine is added, after be cooled to 55 DEG C, OCT, scattered ZPT, panthenol, glycine betaine is added and stirs
It mixes uniformly, 45 DEG C of addition silicone emulsions, DMDM hydantoin, methylisothiazolinone, essence and the pre- solution of menthol, ginkgo
Extract formed solution to get.
1 dandruff control shampoo containing of comparative example
Its difference for being formulated with embodiment 4 is only that without OCT；The content of anti-dandruff agent ZPT is 0.5%.Preparation process ginseng
According to embodiment 4.(note：In the formula, ZPT is the content in terms of its sterling.)
2 dandruff control shampoo containing of comparative example
Its difference for being formulated with embodiment 4 is only that without ZPT；The content of anti-dandruff agent OCT is 0.5%.Preparation process ginseng
According to embodiment 4.
3 dandruff control shampoo containing of comparative example
Its difference for being formulated with embodiment 4 is only that without Herba Lophatheri extract；The content of ginkgo biloba p.e is
0.11%.Preparation process is referring to embodiment 4.
4 dandruff control shampoo containing of comparative example
Its difference for being formulated with embodiment 4 is only that without ginkgo biloba p.e.Preparation process is referring to embodiment 4.
Test example 1
With shampoo prepared by embodiment 4 and comparative example 1, hair washing effect assessment is carried out.
Test crowd：20 people of test crowd quantity, wherein men and women is fifty-fifty, and long hair bob ratio respectively accounts for about half.
Test method：Hair is divided into two parts from head middle position, the left side uses 4 shampoo of embodiment, and the right makes
With 1 shampoo of comparative example of equivalent, gently massaging scalp, then rinses two parts with clear water respectively.Compare anti-dandruff effect, hair
Salubrious degree, antipruritic effect and scalp moisturization degree situation.
Evaluation result using 1 shampoo of 4 shampoo of embodiment and comparative example is as follows：
| Serial number | Performance indicator | It is better than | Quite | It is worse than | Positive rating |
| 1 | Anti-dandruff effect | 11 | 9 | 0 | 55% |
| 2 | Hair is clearly spent | 12 | 6 | 2 | 60% |
| 3 | Antipruritic effect | 16 | 4 | 0 | 85% |
| 4 | Scalp moisturization degree | 17 | 2 | 1 | 80% |
Note：" being better than "：4 shampoo performance indicator effect of embodiment is better than 1 shampoo of comparative example；" suitable "：Embodiment 4 is washed
Flood suitable with 1 shampoo performance indicator effect of comparative example；" being worse than "：4 shampoo performance indicator effect of embodiment is worse than comparison
1 shampoo of example.(positive rating=better than/sum, similarly hereinafter)
The result shows that：The anti-dandruff effect of 4 shampoo of embodiment, hair clearly spend, antipruritic effect, scalp moisturization degree are obviously excellent
In 1 shampoo of comparative example.
Test example 2
With shampoo prepared by embodiment 4 and comparative example 2, hair washing effect assessment is carried out.
Test crowd：20 people of test crowd quantity, wherein men and women is fifty-fifty, and long hair bob ratio respectively accounts for about half.
Test method：Hair is divided into two parts from head middle position, the left side uses 4 shampoo of embodiment, and the right makes
With 2 shampoo of comparative example of equivalent, gently massaging scalp, then rinses two parts with clear water respectively.Compare anti-dandruff effect, hair
Salubrious degree, antipruritic effect and scalp moisturization degree situation.
Evaluation result using 2 shampoo of 4 shampoo of embodiment and comparative example is as follows：
| Serial number | Performance indicator | It is better than | Quite | It is worse than | Positive rating |
| 1 | Anti-dandruff effect | 18 | 0 | 2 | 90% |
| 2 | Hair is clearly spent | 16 | 2 | 2 | 80% |
| 3 | Antipruritic effect | 13 | 3 | 4 | 65% |
| 4 | Scalp moisturization degree | 10 | 4 | 6 | 50% |
Note：" being better than "：4 shampoo performance indicator effect of embodiment is better than 2 shampoo of comparative example；" suitable "：Embodiment 4 is washed
Flood suitable with 2 shampoo performance indicator effect of comparative example；" being worse than "：4 shampoo performance indicator effect of embodiment is worse than comparison
2 shampoo of example.
The result shows that：The anti-dandruff effect of 4 shampoo of embodiment, hair clearly spend, antipruritic effect, scalp moisturization degree are obviously excellent
In 2 shampoo of comparative example.
Test example 3
With shampoo prepared by embodiment 4 and comparative example 3, hair washing effect assessment is carried out.
Test crowd：20 people of test crowd quantity, wherein men and women is fifty-fifty, and long hair bob ratio respectively accounts for about half.
Test method：Hair is divided into two parts from head middle position, the left side uses 4 shampoo of embodiment, and the right makes
With 3 shampoo of comparative example of equivalent, gently massaging scalp, then rinses two parts with clear water respectively.Compare anti-dandruff effect, hair
Salubrious degree, antipruritic effect and scalp moisturization degree situation.
Evaluation result using 3 shampoo of 4 shampoo of embodiment and comparative example is as follows：
| Serial number | Performance indicator | It is better than | Quite | It is worse than | Positive rating |
| 1 | Anti-dandruff effect | 14 | 6 | 0 | 70% |
| 2 | Hair is clearly spent | 10 | 10 | 0 | 50% |
| 3 | Antipruritic effect | 11 | 8 | 1 | 55% |
| 4 | Scalp moisturization degree | 12 | 3 | 5 | 60% |
Note：" being better than "：4 shampoo performance indicator effect of embodiment is better than 3 shampoo of comparative example；" suitable "：Embodiment 4 is washed
Flood suitable with 3 shampoo performance indicator effect of comparative example；" being worse than "：4 shampoo performance indicator effect of embodiment is worse than comparison
3 shampoo of example.
The result shows that：The anti-dandruff effect of 4 shampoo of embodiment, hair clearly spend, antipruritic effect, scalp moisturization degree are obviously excellent
In 3 shampoo of comparative example.
Test example 4
With shampoo prepared by embodiment 4 and comparative example 4, hair washing effect assessment is carried out.
Test crowd：20 people of test crowd quantity, wherein men and women is fifty-fifty, and long hair bob ratio respectively accounts for about half.
Test method：Hair is divided into two parts from head middle position, the left side uses 4 shampoo of embodiment, and the right makes
With 4 shampoo of comparative example of equivalent, gently massaging scalp, then rinses two parts with clear water respectively.Compare anti-dandruff effect, hair
Salubrious degree, antipruritic effect and scalp moisturization degree situation.
Evaluation result using 4 shampoo of 4 shampoo of embodiment and comparative example is as follows：
| Serial number | Performance indicator | It is better than | Quite | It is worse than | Positive rating |
| 1 | Anti-dandruff effect | 15 | 5 | 0 | 75% |
| 2 | Hair is clearly spent | 10 | 7 | 3 | 50% |
| 3 | Antipruritic effect | 12 | 4 | 4 | 60% |
| 4 | Scalp moisturization degree | 11 | 5 | 4 | 55% |
Note：" being better than "：4 shampoo performance indicator effect of embodiment is better than 4 shampoo of comparative example；" suitable "：Embodiment 4 is washed
Flood suitable with 4 shampoo performance indicator effect of comparative example；" being worse than "：4 shampoo performance indicator effect of embodiment is worse than comparison
4 shampoo of example.
The result shows that：The anti-dandruff effect of 4 shampoo of embodiment, hair clearly spend, antipruritic effect, scalp moisturization degree are obviously excellent
In 4 shampoo of comparative example.
Test example 5
With shampoo prepared by comparative example 1 and comparative example 4, hair washing effect assessment is carried out.
Test crowd：20 people of test crowd quantity, wherein men and women is fifty-fifty, and long hair bob ratio respectively accounts for about half.
Test method：Hair is divided into two parts from head middle position, the left side uses 1 shampoo of comparative example, and the right makes
With 4 shampoo of comparative example of equivalent, gently massaging scalp, then rinses two parts with clear water respectively.Compare anti-dandruff effect, hair
Salubrious degree, antipruritic effect and scalp moisturization degree situation.
Evaluation result using 4 shampoo of 1 shampoo of comparative example and comparative example is as follows：
Note：" being better than "：4 shampoo performance indicator effect of comparative example is better than 1 shampoo of comparative example；" suitable "：Comparative example 4 is washed
Flood suitable with 1 shampoo performance indicator effect of comparative example；" being worse than "：4 shampoo performance indicator effect of comparative example is worse than comparison
1 shampoo of example.
The result shows that：The anti-dandruff effect of 4 shampoo of comparative example, hair clearly spend, antipruritic effect, scalp moisturization degree are obviously excellent
In 1 shampoo of comparative example.
Test example 6
With shampoo prepared by comparative example 2 and comparative example 4, hair washing effect assessment is carried out.
Test crowd：20 people of test crowd quantity, wherein men and women is fifty-fifty, and long hair bob ratio respectively accounts for about half.
Test method：Hair is divided into two parts from head middle position, the left side uses 2 shampoo of comparative example, and the right makes
With 4 shampoo of comparative example of equivalent, gently massaging scalp, then rinses two parts with clear water respectively.Compare anti-dandruff effect, hair
Salubrious degree, antipruritic effect and scalp moisturization degree situation.
Evaluation result using 4 shampoo of 2 shampoo of comparative example and comparative example is as follows：
| Serial number | Performance indicator | It is better than | Quite | It is worse than | Positive rating |
| 1 | Anti-dandruff effect | 16 | 3 | 1 | 80% |
| 2 | Hair is clearly spent | 11 | 7 | 2 | 55% |
| 3 | Antipruritic effect | 13 | 5 | 2 | 65% |
| 4 | Scalp moisturization degree | 10 | 4 | 6 | 50% |
Note：" being better than "：4 shampoo performance indicator effect of comparative example is better than 2 shampoo of comparative example；" suitable "：Comparative example 4 is washed
Flood suitable with 2 shampoo performance indicator effect of comparative example；" being worse than "：4 shampoo performance indicator effect of comparative example is worse than comparison
2 shampoo of example.
The result shows that：The anti-dandruff effect of 4 shampoo of comparative example, hair clearly spend, antipruritic effect, scalp moisturization degree are obviously excellent
In 2 shampoo of comparative example.
Test example 7
With shampoo prepared by comparative example 3 and comparative example 4, hair washing effect assessment is carried out.
Test crowd：20 people of test crowd quantity, wherein men and women is fifty-fifty, and long hair bob ratio respectively accounts for about half.
Test method：Hair is divided into two parts from head middle position, the left side uses 3 shampoo of comparative example, and the right makes
With 4 shampoo of comparative example of equivalent, gently massaging scalp, then rinses two parts with clear water respectively.Compare anti-dandruff effect, hair
Salubrious degree, antipruritic effect and scalp moisturization degree situation.
Evaluation result using 4 shampoo of 3 shampoo of comparative example and comparative example is as follows：
| Serial number | Performance indicator | It is better than | Quite | It is worse than | Positive rating |
| 1 | Anti-dandruff effect | 13 | 5 | 2 | 65% |
| 2 | Hair is clearly spent | 10 | 5 | 5 | 50% |
| 3 | Antipruritic effect | 12 | 2 | 6 | 60% |
| 4 | Scalp moisturization degree | 11 | 3 | 6 | 55% |
Note：" being better than "：4 shampoo performance indicator effect of comparative example is better than 3 shampoo of comparative example；" suitable "：Comparative example 4 is washed
Flood suitable with 3 shampoo performance indicator effect of comparative example；" being worse than "：4 shampoo performance indicator effect of comparative example is worse than comparison
3 shampoo of example.
The result shows that：The anti-dandruff effect of 4 shampoo of comparative example, hair clearly spend, antipruritic effect, scalp moisturization degree are obviously excellent
In 3 shampoo of comparative example.
As it can be seen that the anti-dandruff effect of the dandruff control shampoo containing containing Herba Lophatheri extract, hair are clearly spent, the moist degree of scalp is slightly good
In single shampoo containing ZPT and the single shampoo containing OCT；Further ginkgo biloba p.e can further improve shampoo
Anti-dandruff effect.
Obviously, the above embodiment of the present invention be only to clearly illustrate example of the present invention, and not be pair
The restriction of embodiments of the present invention may be used also on the basis of the above description for those of ordinary skill in the art
To make other variations or changes in different ways, all embodiments can not be exhaustive here, it is all to belong to this hair
The obvious changes or variations that bright technical solution is extended out are still in the scope of protection of the present invention.
Claims (10)
1. a kind of dandruff control shampoo containing containing Herba Lophatheri extract, which is characterized in that its active constituent includes anti-dandruff agent and lophatherum gracile
Extract, the anti-dandruff agent includes ZPT, OCT, and the weight ratio of ZPT and OCT is (0.25-0.50):0.1；The weight of ZPT, OCT
The sum of amount and the weight ratio of Herba Lophatheri extract are (0.35-0.60):(0.005-1.5).
2. dandruff control shampoo containing according to claim 1, which is characterized in that the sum of weight of ZPT, OCT is extracted with lophatherum gracile
The weight ratio of object is (0.35-0.60):(0.005-1.0).
3. dandruff control shampoo containing according to claim 1, which is characterized in that the anti-dandruff shampoo containing Herba Lophatheri extract
Water, wherein the weight ratio of ZPT and OCT is 0.4:0.1；The sum of weight of ZPT, OCT and the weight ratio of Herba Lophatheri extract are
0.5:0.01。
4. dandruff control shampoo containing according to claim 1-3, which is characterized in that described to be gone containing Herba Lophatheri extract
It considers to be worth doing in shampoo, the sum of ZPT, OCT, weight content of Herba Lophatheri extract are 0.355-1.6%.
5. dandruff control shampoo containing according to claim 1-4, which is characterized in that the Herba Lophatheri extract is alcohol extracting
Object, preferably general flavone content >=24.0%.
6. dandruff control shampoo containing according to claim 1-5, which is characterized in that also containing as active constituent its
His plant extracts；Other described extracts include ginkgo biloba extract, camomile extract, chrysanthemum extract, wolfberry fruit extract
One or more of；
Preferably, the weight content of the other plant extract is 0-3%, more preferably 0.1-3%.
7. dandruff control shampoo containing according to claim 1-6, which is characterized in that also contain appropriate conditioner；It is described
Conditioner includes guar hydroxypropyltrimonium chloride, polyquaternium -7, Polyquaternium-10, Avocado Oil, Ah's glycerol, hydrolysis
One or more of collagen and/or albumen, panthenol, glycine betaine, pearly-lustre dibasic acid esters, hexadecanol, menthol, silicone emulsion；With/
Or,
The dandruff control shampoo containing also contains appropriate anionic surfactant and/or nonionic surfactant and/or both sexes table
Face activating agent and/or thickener and/or preservative and/or essence；
Preferably, the anionic surfactant includes that laureth sulfuric ester ammonium, laurel alcohol sulfuric ester ammonium, laruyl alcohol are poly-
One or more of ether sodium sulfovinate, laruyl alcohol sodium sulfovinate, sodium lauroyl sarcosine, cocoamido sodium propionate；
The nonionic surfactant includes coconut oleoyl amine DEA, lauryl glucoside, amine oxide, coconut oleoyl amine monoethanolamine
One or more of；
The amphoteric surfactant includes one of Cocoamidopropyl betaine amine, cocounut oil acyl both sexes base diethyl acid disodium
Or it is several；
The thickener includes one or more of U20, ETD2020, TAB；
The preservative includes that sodium benzoate, 1,2- hexylene glycol/pungent glycol/tropolone, DMDM hydantoin, methyl are different
One or more of thiazolinone, methyl hydroxybenzoate.
8. dandruff control shampoo containing according to claim 1-7, which is characterized in that the group containing following weight percent
Point：Anti-dandruff agent 0.35-0.60%, wherein the weight ratio of ZPT and OCT is preferably (0.25-0.5):0.1, Herba Lophatheri extract
0.005-1%, other plant extract 0-3%, conditioner 0.1-5%, anionic surfactant 10-40%, nonionic table
Face activating agent 0.5-10%, amphoteric surfactant 1.0-10%, thickener 0.15-0.7%, preservative 0-0.50%, essence
0-1%, deionized water surplus.
9. dandruff control shampoo containing according to claim 8, which is characterized in that containing following weight percentage components：It is anti-dandruff
Agent 0.35-0.60%, wherein the weight ratio of ZPT and OCT is (0.25-0.5):0.1, Herba Lophatheri extract 0.01-0.5%,
He is plant extracts 0-3%, conditioner 0.1-5%, anionic surfactant 10-40%, nonionic surfactant 0.5-
10%, amphoteric surfactant 1.0-10%, thickener 0.15-0.7%, 0-0.50 parts of preservative, essence 0-1%, deionization
Water surplus；
It is highly preferred that the dandruff control shampoo containing containing Herba Lophatheri extract, containing following weight percentage components：Anti-dandruff agent
0.5%, wherein the weight ratio of ZPT and OCT is preferably 0.4:0.1, Herba Lophatheri extract 0.01%, other plant extract 0-
3%, conditioner 0.1-5%, anionic surfactant 10-40%, nonionic surfactant 0.5-10%, amphoteric surface are living
Property agent 1.0-10%, thickener 0.15-0.7%, 0-0.50 parts of preservative, essence 0-1%, deionized water surplus.
10. the preparation method of any dandruff control shampoo containing containing Herba Lophatheri extract of claim 1-9, which is characterized in that packet
It includes：Main tank is added in deionized water, is warming up to 75 DEG C -85 DEG C, sequentially adds conditioner resistant to high temperature, thickener, anion table
Face activating agent, amphoteric surfactant, nonionic surfactant, Herba Lophatheri extract, after be cooled to 45-55 DEG C, successively plus
Enter low temperature anti-dandruff agent, low temperature conditioner, plant extracts, preservative, essence to stir evenly, formed solution to get.
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Application publication date: 20181116 |
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