CN103520072B - Fulvic acid containing anti-acne mask and preparation method thereof - Google Patents

Abstract

The invention discloses an acne-removing facial mask containing fulvic acid and a preparation method thereof. It is prepared by using fulvic acid, pearl powder, motherwort, lavender, moisturizing oil, thickener, moisturizing agent and surfactant as raw materials. The present invention adds fulvic acid, a natural product with anti-inflammatory, pain-relieving, and endocrine-regulating effects, to the facial mask to achieve the effect of removing acne. The effect of relieving acne marks, this invention does not contain preservatives, and four kinds of traditional Chinese medicine ingredients including fulvic acid are added to the base of the mask. Acne and repair damaged skin, easy to use, quality controllable.

Description

A kind of anti-acne mask containing fulvic acid and preparation method thereof

technical field

The invention relates to an acne-removing facial mask containing fulvic acid and a preparation method thereof, belonging to the technical field of cosmetics mainly composed of traditional Chinese medicines.

Background technique

Acne, commonly known as acne, is a common and frequently-occurring disease in dermatology. According to statistics, 95% of adolescent males and 85% of females have suffered from different degrees of acne. The main clinical manifestations of acne are blackheads, whiteheads, inflammatory papules, Pustules, nodules, and cysts are easy to form pigmentation, enlarged pores, and even scar-like lesions, which cause great troubles to adolescents who are very image-conscious. Nowadays, there are countless acne-removing products on the market, but most of their ointments and creams are harmful to skin. The skin will produce different degrees of irritation and damage, and there are certain side effects at the same time. In addition, the products added with hormones are very easy to rebound and cause acne recurrence. There are many traditional Chinese medicine products for the treatment of acne. The ingredients are complex and easy to cause unstable quality. An acne-removing product with stable quality and no side effects, especially an acne-removing mask is very necessary.

There are many patents for facial masks, 95% of which are whitening, moisturizing, freckle-removing, and anti-wrinkle. There are only a dozen patents for acne-removing, such as CN1927148A special mask for acne prevention and treatment. Because of the bad smell of eggs, the use is limited; CN1954799A acne mask is formulated with onion liquid with medicinal ingredients, honey, and royal jelly. Honey has a large molecular weight and is easy to clog pores. It is not suitable for people with oily skin and hair follicle inflammation. Use: CN1554381A acne-removing, wrinkle-removing and whitening traditional Chinese medicine face mask element, the medicinal ingredients are Angelica dahurica, Bletilla striata, Bletilla striata, Trichosanthum pollen, Polygonatum odoratum, Artemisia annua, Chuanxiong, almond and other multi-flavored Chinese medicinal materials, the medicinal ingredients are too complicated and the quality is difficult to control; The purpose of the present invention is to provide a mask with simple composition, controllable quality, obvious acne-removing effect, whitening and repairing damaged skin and a preparation method thereof for the deficiency of the acne-removing facial mask in the current market.

Fulvic acid is the part of humic acid with the smallest molecular weight, the highest solubility, and the strongest biological activity. It contains many active functional groups and is easily absorbed and utilized by the human body. The medicinal research of fulvic acid has been done for many years. Li Shizhen of the Ming Dynasty wrote "Compendium of Materia Medica" "Recounts a kind of "Wujin San", which is used to treat diseases such as infectious ulcers and women's bleeding. In fact, "Wujin San" is the current humic acid. Its medicinal value was discovered as early as 1500 years ago. Humic acid It has the functions of antibacterial, anti-inflammatory, hemostasis and muscle growth, and has a definite effect on the treatment of acne; pearl powder has the functions of whitening, oil control, muscle growth, beauty, anti-aging, and UV isolation; motherwort can promote blood circulation, remove blood stasis, and smooth acne marks; Lavender has the effect of repairing, promoting the regeneration of epidermal cells, and it is also a natural fragrance agent.

After searching, there are no facial mask products and technologies that use fulvic acid as the main medicinal ingredient at home and abroad. For the first time, the present invention combines fulvic acid, which has antibacterial, anti-inflammatory, pain-relieving, hemostatic, and endocrine-regulating effects, with pearl powder, Motherwort and lavender auxiliary components are added to the matrix to prepare a mask. The mask is mild in nature, has no stimulating effect on the skin, and can effectively remove acne and repair damaged skin. It adds a new variety to the market and has broad application prospects.

Contents of the invention

The object of the present invention is to provide a kind of anti-acne facial mask containing fulvic acid, which is prepared according to the following raw materials, each raw material and its mass percentage are: 10-20% of Chinese medicine extract, emollient Fat 10~25%, sodium carboxymethylcellulose 2~3%, lanolin 0.1~1.5%, glycerin 5~15%, butylene glycol 5~10%, allantoin 0.1~0.5%, hyaluronic acid 0.01% ~0.1%, surfactant 1~10%, vitamin E 1~5%, deionized water 30~40%, the mass percentage of all substances is based on the sum of the mass of each raw material;

The Chinese medicine extract is prepared from the following raw materials: 10-25 parts by weight of fulvic acid, 5-10 parts by weight of pearl powder, 5-10 parts by weight of motherwort extract, and 4-8 parts by weight of lavender extract;

The emollient oil of the present invention is one or both of polydimethylsiloxane and glyceryl monostearate mixed in a ratio of 1:1 to 1:1.5;

The surfactant of the present invention is one of potassium laurate, fatty acid polyoxyethylene ether, and Tween 80.

Another object of the present invention is to provide the preparation method of the acne-removing mask containing fulvic acid, which specifically includes the following steps:

(1) Heat and sterilize fulvic acid, pearl powder, motherwort extract, and lavender extract at 80-95°C for 40-60 minutes, and set aside;

(2) Mix emollient oil, sodium carboxymethyl cellulose, lanolin, glycerin, butylene glycol, allantoin, surfactant and water, heat to 75~85°C, stir evenly, and emulsify for 5~ 10 minutes;

(3) Add the mixture obtained in step (1), hyaluronic acid and vitamin E when cooled to 45~50°C, stir and cool down, and homogenize for 3~5 minutes when the temperature is 35~45°C to obtain yellow rancid acne mask;

(4) Packaging and inspection to get the finished product.

The fulvic acid described in the present invention is pharmaceutical grade fulvic acid or the fulvic acid prepared by referring to the method in the patent application 200810233669.X "Method for Oxidative Degradation of Lignite to Produce Humic Acid and Its Salt" (using non-polluting hydrogen peroxide As an oxidizing agent, and after purification to obtain fulvic acid), commercially available refined fulvic acid can also be used after the heavy metal detection does not exceed the standard.

The motherwort extract and lavender extract of the present invention are all commercially available extracts.

The beneficial effects of the present invention are:

(1) The acne-removing facial mask containing fulvic acid described in the present invention has the effect of removing acne, and the production process is simple, easy to use, fast, stable in quality, and practical;

(2) The anti-acne facial mask containing fulvic acid of the present invention utilizes the natural antibacterial effect of fulvic acid, does not need to add preservatives that damage the skin, is mild in nature, has no stimulating effect on the skin, and is safe to use;

(3) The acne-removing facial mask containing fulvic acid of the present invention utilizes the natural aroma of lavender without the need of fragrance chemicals, which can relieve the pressure of patients and reduce the troubles of treatment.

Detailed ways

The present invention will be described in further detail below in conjunction with the examples, but the protection scope of the present invention is not limited to the content described.

Example 1

The acne-removing facial mask containing fulvic acid described in this example is prepared according to the following raw materials, each raw material and its mass percentage are: 20% of Chinese medicine extract, 20% of emollient oil, 2% of sodium carboxymethyl cellulose, wool 0.1% fat, 15% glycerin, 5% butanediol, 0.1% allantoin, 0.01% hyaluronic acid, 1% surfactant, 1% vitamin E, 35.79% deionized water;

The emollient grease described in the present embodiment is polydimethylsiloxane;

The surfactant described in this embodiment is potassium laurate.

The preparation method of the acne-removing facial mask containing fulvic acid described in the present embodiment specifically comprises the steps:

(1) Take 100g of fulvic acid, 100g of pearl powder, 50g of motherwort extract, and 40g of lavender extract, and mix them to obtain a traditional Chinese medicine extract;

(2) Take 200 g of the Chinese medicine extract obtained in step (1) and heat and sterilize it at 80° C. for 60 minutes to obtain the sterilized Chinese medicine extract;

(3) Mix 200g of polydimethylsiloxane, 20g of sodium carboxymethylcellulose, 1g of lanolin, 150g of glycerin, 50g of butanediol, 1g of allantoin, 10g of potassium laurate and 357.9g of water, and heat to 75°C, stir evenly, homogeneously emulsify for 10 minutes;

(4) When cooling to 45°C, add the traditional Chinese medicine extract obtained in step (2), hyaluronic acid, vitamin E, stir and continue to cool down, when the temperature is 45°C, homogenize for 3 minutes, and the material is discharged to obtain the yellow rot sour acne mask;

(5) Packing and inspection to get the finished product.

The acne-removing facial mask containing fulvic acid described in this example is used to improve the condition of facial skin. There are 6 subjects, 3 females and 3 males, aged 19-26 years. They use the mask containing fulvic acid for two days. Use the anti-acne mask once, and observe the facial skin changes after two consecutive months. The statistical results are shown in Table 1:

Table 1 Treatment effect

Example 2

The acne-removing facial mask containing fulvic acid described in this embodiment is prepared according to the following raw materials, and the raw materials and their mass percentages are: 10% of Chinese medicine extract, 25% of emollient oil, 3% of sodium carboxymethyl cellulose, wool 1.5% fat, 5% glycerin, 10% butanediol, 0.4% allantoin, 0.1% hyaluronic acid, 10% surfactant, 5% vitamin E, 30% deionized water;

The emollient oil described in this embodiment is polydimethylsiloxane and glyceryl monostearate mixed in a ratio of 1:1.5;

The surfactant described in this embodiment is potassium laurate.

The preparation method of the acne-removing facial mask containing fulvic acid described in the present embodiment specifically comprises the steps:

(1) Take 250g of fulvic acid, 500g of pearl powder, 100g of motherwort extract, and 80g of lavender extract, and mix them to obtain a traditional Chinese medicine extract;

(2) Heat and sterilize 100 g of the Chinese medicine extract obtained in step (1) at 95° C. for 40 minutes to obtain a sterilized Chinese medicine extract;

(3) Mix polydimethylsiloxane 100g, glyceryl monostearate 150g, sodium carboxymethylcellulose 30g, lanolin 15g, glycerin 50g, butylene glycol 100g, allantoin 40g, potassium laurate 100g Mix with 300g of water, heat to 85°C, stir evenly, and emulsify for 5 minutes;

(4) When cooling to 50°C, add the traditional Chinese medicine extract obtained in step (2), hyaluronic acid, vitamin E, stir and continue to cool down, and when the temperature is 35°C, homogenize for 5 minutes, and the material is discharged to obtain the yellow rot Sour acne mask.

(5) Packing and inspection to get the finished product.

The acne-removing facial mask containing fulvic acid described in this example is used to improve the condition of facial skin. There are 6 subjects, 2 females and 4 males, aged 20-25 years. They use the mask containing fulvic acid for two days. After one month of continuous use of the anti-acne mask, observe the changes in the facial skin. The statistical results are shown in Table 2:

Table 2 Treatment effect

Example 3

The acne-removing facial mask containing fulvic acid described in this example is prepared according to the following raw materials, and the raw materials and their mass percentages are: 12% of Chinese medicine extract, 22.92% of emollient oil, 2.5% of sodium carboxymethyl cellulose, wool 1% lipid, 10% glycerin, 6% butanediol, 0.5% allantoin, 0.08% hyaluronic acid, 3% surfactant, 2% vitamin E, 40% deionized water;

The emollient oil described in the present embodiment is glyceryl monostearate;

The surfactant described in this embodiment is fatty acid polyoxyethylene ether.

The preparation method of the acne-removing facial mask containing fulvic acid described in the present embodiment specifically comprises the steps:

(1) Take 160g of fulvic acid, 70g of pearl powder, 60g of motherwort extract, and 50g of lavender extract, and mix them to obtain a traditional Chinese medicine extract;

(2) Heat and sterilize 120 g of the Chinese medicine extract obtained in step (1) at 95° C. for 40 minutes to obtain a sterilized Chinese medicine extract;

(3) Mix 229.2g of glyceryl monostearate, 25g of sodium carboxymethylcellulose, 10g of lanolin, 100g of glycerin, 60g of butanediol, 5g of allantoin, 30g of polyoxyethylene fatty acid ether and 40g of water, and heat At 78°C, stir evenly and emulsify for 6 minutes;

(4) When cooling to 46°C, add the traditional Chinese medicine extract obtained in step (2), 0.8g of hyaluronic acid, and 20g of vitamin E, stir and continue to cool down, and when the temperature is 40°C, homogenize for 4 minutes, and the material is ready Acne-fighting mask with fulvic acid.

(5) Packing and inspection to get the finished product.

The acne-removing facial mask containing fulvic acid described in this example is used to improve the facial skin condition. There are 6 subjects, 4 females and 2 males, aged 18-23 years. They use the facial mask containing fulvic acid for two days. Use the anti-acne mask once, and observe the changes in the facial skin after one month. The statistical results are shown in Table 3:

Table 3 Treatment effect

Example 4

The acne-removing facial mask containing fulvic acid described in this example is prepared according to the following raw materials, and the raw materials and their mass percentages are: 15% of Chinese medicine extract, 22% of emollient oil, 2.6% of sodium carboxymethyl cellulose, wool 1.3% fat, 8% glycerin, 7% butanediol, 0.3% allantoin, 0.06% hyaluronic acid, 6% surfactant, 3% vitamin E, 34.74% deionized water;

The emollient oil described in the present embodiment is polydimethylsiloxane and glyceryl monostearate mixed in a ratio of 1:1;

The surfactant described in this example is Tween 80.

The preparation method of the acne-removing facial mask containing fulvic acid described in the present embodiment specifically comprises the steps:

(1) Take 200g of fulvic acid, 90g of pearl powder, 80g of motherwort extract, and 70g of lavender extract, and mix them to obtain a traditional Chinese medicine extract;

(2) Heat and sterilize 150 g of the Chinese medicine extract obtained in step (1) at 96° C. for 50 minutes to obtain a sterilized Chinese medicine extract;

(3) Mix 110g dimethylsiloxane, 110g glyceryl monostearate, 26g sodium carboxymethylcellulose, 13g lanolin, 80g glycerin, 70g butanediol, 3g allantoin, 60g Tween 80 and 347.4 mixed with water, heated to 78°C, stirred evenly, and emulsified for 8 minutes;

(4) When cooling to 48°C, add the sterilized Chinese medicine extract obtained in step (2), hyaluronic acid 0.6g, vitamin E 30g, stir and continue to cool down, and when the temperature is 40°C, homogenize for 5 minutes , and the acne-removing mask containing fulvic acid can be obtained immediately;

(5) Packing and inspection to get the finished product.

The acne-removing facial mask containing fulvic acid described in this example is used to improve the facial skin condition. There are 6 subjects, 4 females and 2 males, aged 20-25 years. They use the mask containing fulvic acid for two days. Use the anti-acne mask once, and observe the facial skin changes after two consecutive months. The statistical results are shown in Table 4:

Table 4 Treatment effect

Claims (2)

1. A acne-removing facial mask containing fulvic acid is characterized in that it is prepared by the following raw materials, each raw material and its mass percentage are: 10-20% of Chinese medicine extract, 10-25% of moisturizing oil, carboxymethyl fiber Sodium 2~3%, lanolin 0.1~1.5%, glycerin 5~15%, butanediol 5~10%, allantoin 0.1~0.5%, hyaluronic acid 0.01~0.1%, surfactant 1~10% %, vitamin E 1~5%, deionized water 30-40%, the mass percentages of all substances are based on the sum of the mass of each raw material; The Chinese medicine extract is prepared from the following raw materials: 10-25 parts by weight of fulvic acid, 5-10 parts by weight of pearl powder, 5-10 parts by weight of motherwort extract, and 4-8 parts by weight of lavender extract; The emollient oil is one or both of polydimethylsiloxane and glyceryl monostearate mixed in a ratio of 1:1 to 1:1.5; The surfactant is one of potassium laurate and Tween 80. 2. the preparation method of the acne-removing mask containing fulvic acid according to claim 1, is characterized in that comprising the steps: (1) Heat and sterilize fulvic acid, pearl powder, motherwort extract, and lavender extract at 80-95°C for 40-60 minutes, and set aside; (2) Mix emollient oil, sodium carboxymethyl cellulose, lanolin, glycerin, butylene glycol, allantoin, surfactant and water, heat to 75~85°C, stir evenly, and emulsify for 5~ 10 minutes; (3) Add the mixture obtained in step (1) when cooled to 45~50°C, hyaluronic acid and vitamin E, stir and cool down, and homogenize for 3~5 minutes when the temperature is 35~45°C to obtain yellow rancid acne mask; (4) Packaging and inspection to get the finished product.