CN108042457A

CN108042457A - A kind of anti-acne facial cleanser and preparation method thereof

Info

Publication number: CN108042457A
Application number: CN201810014350.1A
Authority: CN
Inventors: 董志强
Original assignee: Hebei Source Of Biological Science And Technology Co Ltd
Current assignee: Hebei Source Of Biological Science And Technology Co Ltd
Priority date: 2018-01-08
Filing date: 2018-01-08
Publication date: 2018-05-18

Abstract

The present invention provides a kind of anti-acne facial cleanser and preparation method thereof, include the component of following parts by weight：10 ~ 50 parts of fulvic acids, 50 250 parts of Chinese medical extract, 10 ~ 50 parts of aloe extracts, 10 ~ 50 parts of Radix et Caulis Opuntiae Dillenii extract, 400 ~ 500 parts of deionized water, 100 ~ 200 parts of surfactant；The present invention plays good effect by adding fulvic acid ingredient to the improvement of face acnes.

Description

A kind of anti-acne facial cleanser and preparation method thereof

Technical field

The present invention relates to skin care item preparation fields, and in particular to a kind of anti-acne facial cleanser and preparation method thereof.

Background technology

Acne is a kind of chronic inflammatory skin of pilosebaceous unit, and clinical manifestation is to be apt to occur in the powder of face With the characteristics of the pleomorphism skin lesion such as thorn, papule, warts, tubercle.The generation of acne is mainly led with hypersteatosis, pilosebaceous follicle The factors such as blockage, bacterium infection and inflammatory reaction are closely related.Adolesce androgen particularly testosterone in descendant's body Horizontal rapid rise, promotes sebaceous glands to develop and generate a large amount of sebums.The dyskeratosis of pilosebaceous duct causes to lead simultaneously Blockage, dyssebacia form horn plug, that is, micro mist thorn.Multiple-microorganism especially propionibacterium acnes is a large amount of in hair follicle Breeding, the lipase that propionibacterium acnes generates decompose sebum generation free fatty, while chemotactic inflammatory cell and medium, finally It induces and aggravates inflammatory reaction.Modern life rhythm is getting faster, and pressure is increasing, and pollution is more and more, often stays up late Overtime work has even more aggravated the degree of fat secretion imbalance and clogging of pores, has caused other inflammation such as facial acne, severe patient Scar.Although there is many Related products currently on the market, mainly based on chemicals, long-time service is easily destroyed skin Skin natural cover causes percutaneous moisture loss to increase extremely, generates the problems such as skin of face is dry, coarse, while generates dependence Property.

The content of the invention

To solve the above problems, the present invention provides a kind of anti-acne facial cleanser and preparation method thereof, by adding fulvic acid Ingredient plays good effect to the improvement of face acnes.

The present invention is to solve the above problems, used technical solution is as follows：

Technical solution one：

A kind of anti-acne facial cleanser includes the component of following parts by weight：10 ~ 50 parts of fulvic acids, 50-250 parts of Chinese medical extract, 10 ~ 50 parts of aloe extracts, 10 ~ 50 parts of Radix et Caulis Opuntiae Dillenii extract, 400 ~ 500 parts of deionized water, 100 ~ 200 parts of surfactant.

As a further improvement on the present invention, the Chinese medical extract includes the component of following weight ratio：Chingma abutilon seed：Horse Bitterroot：Kelp：Cape jasmine：The root of Dahurain angelica：Cimicifugae foetidae is 1-5：1-5:1-5:1-5:1-5:1-5.

As a further improvement on the present invention, present invention additionally comprises 10-50 parts of borneols.

As a further improvement on the present invention, the surfactant is sodium cocoyl glutamate.

As a further improvement on the present invention, the chingma abutilon seed, purslane, kelp, cape jasmine, the root of Dahurain angelica, borneol and cimicifugae foetidae It is the air-dried drug bought from shop of Chinese medicines.

As a further improvement on the present invention, the aloe extract is prepared with the following method：After cleaning and sterilization Aloe is removed the peel, and is cut into small pieces；It is squeezed out aloe juice with juice extractor；200 ~ 300 mesh filter screens of aloe juice are filtered；By filtrate in 2500 ~ 3500r/min speed centrifuges filter, and it is aloe extract to obtain supernatant；

As a further improvement on the present invention, the Radix et Caulis Opuntiae Dillenii extract prepares with the following method：Cactus is removed the peel, and disinfection is clear It washes, is cut into small pieces；It is squeezed out cactus juice with juice extractor；200 ~ 300 mesh filter screens of cactus juice are filtered；By filtrate in 2500 ~ 3500r/min speed centrifuges filter, and it is Radix et Caulis Opuntiae Dillenii extract to obtain supernatant.

As a further improvement on the present invention, the Chinese medical extract is prepared with the following method：By chingma abutilon seed, dent It is spare that amaranth, kelp, cape jasmine, the root of Dahurain angelica, borneol, cimicifugae foetidae etc. are crushed to 80 ~ 100 mesh respectively；

（1）Weigh formula ratio above raw material add in 10 ~ 20 times 50 ~ 80% contents ethyl alcohol, impregnate 1 ~ 2 it is small when after, extract medicine Liquid；It is extracted 3 ~ 5 times by with step；

（2）After more than extracting solution is merged, various impurity are removed in filtered paper hopper filtering；

（3）Filtered fluid is poured into condensate recycling device, is heated, recycles ethyl alcohol, the slightly sticky liquid after being concentrated.

Technical solution two：

A kind of preparation method of anti-acne facial cleanser, includes the following steps：

（1）Chinese medical extract is added in deionized water, then is fed the mixture into blender capable of controlling temperature, stirring is warming up to simultaneously 50~80℃。

（2）It after borneol is crushed to 200-300 mesh, is added in more than liquid and stirs evenly, add fulvic acid, aloe Extract, Radix et Caulis Opuntiae Dillenii extract stir evenly；

（3）Surfactant is added in, is uniformly mixing to obtain brown liquid.

The present invention has the following technical effect that：

Fulvic acid is a kind of a kind of polymolecular raw material extracted from natural humic acid, since its intramolecule contains phenolic hydroxyl group and carboxylic Base determines that it, with faintly acid, is capable of the acid-base value on balance skin surface, does not stimulate mildly；The generation of acne is mainly and skin The factors such as fat hypersecretion, pilosebaceous duct block, bacterium infection and inflammatory reaction are closely related.Fulvic acid is one in itself The hydrophilic colloid of kind, has stronger water absorbing capacity, can prevent skin surface moisture evaporation, keeps skin water and oil balance, drop Low sebum secretion, prevents clogging of pores, so as to prevent the generation of acne；Benzene a pair of horses going side by side-α pyranone in fulvic acid has anti-inflammatory Effect, can inhibit the fungi growth and breeding inside and outside skin, so as to have acne-removing to skin；

The present invention is with the addition of aloe extract, Radix et Caulis Opuntiae Dillenii extract and Chinese medical extract, has wherein in aloe extract a large amount of Anthracene ketone compounds, anthracene ketone compounds have the effects that mostly sterilization, antibacterial, anti-inflammatory, removing toxic substances, promote wound healing, reed Luxuriant growth bitter principle and Barbaloin are respectively provided with sterilization, antiinflammation, the sterilization of aloe, inflammation-diminishing function can effectively eliminate acne, Acne；Containing aromatic amine and polysaccharose substance in cactus extraction, play an important role of that anti-inflammatory is antibacterial；Chingma abutilon seed also known as certain herbaceous plants with big flowers Son, certain herbaceous plants with big flowers vegetable seeds, Semen Abutili, can clearing heat and cooling blood, apocenosis, removing toxic substances, myogenic；Purslane has effects that antibacterial anti-inflammatory；Kelp is sea Thallus with section plant kelp or Alariaceae plant kelp, also referred to as synthetic fibre cloth, extra large kelp, kelp, kelp dish, have apparent Anti-inflammatory effect；Cape jasmine bitter cold in nature, has effects that removing pattogenic heat from the blood and toxic material from the body anti-inflammatory；The root of Dahurain angelica is to face acnes, from the beginning of can dissipate, after bursting It can apocenosis；Cimicifugae foetidae has effects that heat-clearing and detoxication antiphlogistic；Aloe extract, Radix et Caulis Opuntiae Dillenii extract and Chinese medical extract pass through anti-inflammatory Sterilization has effects that skin anti-acne fabulous, but is directly used in facial cleanser, can only be played during face cleaning of short duration Effect, active ingredient can not be stopped in skin surface, and less effective is used alone, and fulvic acid is a kind of glue in itself Body, while have both positive and negative charge, adsorbable zwitterion can be carried aloe extract, cactus by complex reaction The active ingredient in object and Chinese medical extract is taken to save, the protective film rich in nutrition and moisture is formed in skin surface, On the one hand moisture and nutrient loss are prevented, on the other hand can continued slowly to skin Releasing nutrient and moisture, continuous action In skin, good anti-acne effect is played；In addition in fulvic acid molecule there are many active groups, easily with aloe extract, Active ingredient in Radix et Caulis Opuntiae Dillenii extract and Chinese medical extract combines, and the molecular structure of fulvic acid uniqueness makes it have very strong ooze Permeability, the active ingredient that fulvic acid molecule carries anti-acne are absorbed by the skin, and are had more by the cooperation of more than Chinese medicine extract Multiple promotion angiogenesis, nerve ending coincide, the contraposition of skin and subcutaneous tissue, reduce interstitial fluid exudation and promote tissue Interstitial fluid absorbs, and reaches the anti-Cuo of anti-acne, treats scar, promotes scar healing, prevents or reduce the purpose of scar diffusion, and sample is simultaneous It controls.

Specific embodiment

Technical scheme is further elaborated with reference to embodiments.

Embodiment 1：

A kind of anti-acne facial cleanser, is prepared by the following method：

Aloe after cleaning and sterilization is removed the peel, is cut into small pieces, juice extractor is squeezed out aloe juice, by aloe juice with 200 ~ 300 mesh Strainer filtering filters filtrate in 3500r/min speed centrifuges, and it is aloe extract to obtain supernatant；Cactus is removed the peel, Disinfection cleaning, is cut into small pieces, and is squeezed out cactus juice, 200 ~ 300 mesh filter screens of cactus juice is filtered, filtrate with juice extractor It is filtered in 3500r/min speed centrifuges, it is Radix et Caulis Opuntiae Dillenii extract to obtain supernatant；By 5kg chingma abutilon seeds, 6kg purslanes, 5kg kelps, 3kg cape jasmines, the 9kg roots of Dahurain angelica, 2kg cimicifugae foetidaes crush respectively, and with 100 mesh sieves, mixed-powder is added in 15 times of powder The ethyl alcohol of 80% content of last weight, impregnate 2 it is small when after, extract liquid, extracted 5 times by with step, after No. 5 extracting solutions are merged, Various impurity are removed in filtered paper hopper filtering, and filtered fluid is poured into condensate recycling device, is heated, ethyl alcohol is recycled, is concentrated Slightly sticky liquid afterwards is Chinese medical extract；10kg Chinese medical extracts are added in 45kg deionized waters, then will mixing Object is added in blender capable of controlling temperature, and stirring is warming up to 70 DEG C simultaneously；After 2kg borneols are crushed to 300 mesh, it is added in more than liquid It stirs evenly, adds 3.5kg fulvic acids, 3kg aloe extracts, 3kg Radix et Caulis Opuntiae Dillenii extracts stir evenly；Add in 10kg cocounut oil Acyl sodium glutamate surfactant, essence, glycerine are uniformly mixing to obtain brown liquid.

Quality inspection is carried out to facial cleanser described in embodiment 1, sanitary index is shown in Table 1, and sense organ and physical and chemical index are shown in Table 2.

Anti-acne effect inspection is carried out to the facial cleanser described in embodiment 1, the results are shown in Table 3.

Comparative example 1：

For this comparative example in addition to fulvic acid is not added with, remaining is same as Example 1.

Embodiment 2：

A kind of anti-acne facial cleanser, is prepared by the following method：

Aloe after cleaning and sterilization is removed the peel, is cut into small pieces, juice extractor is squeezed out aloe juice, by aloe juice with 200 ~ 300 mesh Strainer filtering filters filtrate in 3500r/min speed centrifuges, and it is aloe extract to obtain supernatant；Cactus is removed the peel, Disinfection cleaning, is cut into small pieces, and is squeezed out cactus juice, 200 ~ 300 mesh filter screens of cactus juice is filtered, filtrate with juice extractor It is filtered in 3500r/min speed centrifuges, it is Radix et Caulis Opuntiae Dillenii extract to obtain supernatant；By 2kg chingma abutilon seeds, 9kg purslanes, 10kg kelps, 5kg cape jasmines, the 2kg roots of Dahurain angelica, 10kg cimicifugae foetidaes crush respectively, and with 100 mesh sieves, mixed-powder is added in 15 times The ethyl alcohol of 80% content of powder weight, impregnate 2 it is small when after, extract liquid, extracted 5 times by with step, No. 5 extracting solutions are merged Afterwards, various impurity are removed in filtered paper hopper filtering, and filtered fluid is poured into condensate recycling device, is heated, ethyl alcohol is recycled, obtains dense Slightly sticky liquid after contracting is Chinese medical extract；5kg Chinese medical extracts are added in 40kg deionized waters, then will be mixed It closes object to add in blender capable of controlling temperature, stirring is warming up to 70 DEG C simultaneously；After 1kg borneols are crushed to 300 mesh, more than liquid is added to In stir evenly, add 5kg fulvic acids, 1kg aloe extracts, 4kg Radix et Caulis Opuntiae Dillenii extracts stir evenly；Add in 15kg cocounut oil Acyl sodium glutamate surfactant, essence, glycerine are uniformly mixing to obtain brown liquid.

Quality inspection is carried out to facial cleanser described in embodiment 2, sanitary index is shown in Table 1, and sense organ and physical and chemical index are shown in Table 2.

Anti-acne effect inspection is carried out to the facial cleanser described in embodiment 2, the results are shown in Table 3.

Comparative example 2：

For this comparative example in addition to fulvic acid is not added with, remaining is same as Example 2.

Embodiment 3：

A kind of anti-acne facial cleanser, is prepared by the following method：

Aloe after cleaning and sterilization is removed the peel, is cut into small pieces, juice extractor is squeezed out aloe juice, by aloe juice with 200 ~ 300 mesh Strainer filtering filters filtrate in 3500r/min speed centrifuges, and it is aloe extract to obtain supernatant；Cactus is removed the peel, Disinfection cleaning, is cut into small pieces, and is squeezed out cactus juice, 200 ~ 300 mesh filter screens of cactus juice is filtered, filtrate with juice extractor It is filtered in 3500r/min speed centrifuges, it is Radix et Caulis Opuntiae Dillenii extract to obtain supernatant；By 10kg chingma abutilon seeds, 10kg purslanes, 2kg kelps, 2kg cape jasmines, the 10kg roots of Dahurain angelica, 5kg cimicifugae foetidaes crush respectively, and with 100 mesh sieves, mixed-powder is added in 15 times of powder The ethyl alcohol of 80% content of last weight, impregnate 2 it is small when after, extract liquid, extracted 5 times by with step, after No. 5 extracting solutions are merged, Various impurity are removed in filtered paper hopper filtering, and filtered fluid is poured into condensate recycling device, is heated, ethyl alcohol is recycled, is concentrated Slightly sticky liquid afterwards is Chinese medical extract；25kg Chinese medical extracts are added in 50kg deionized waters, then will mixing Object is added in blender capable of controlling temperature, and stirring is warming up to 70 DEG C simultaneously；After 5kg borneols are crushed to 300 mesh, it is added in more than liquid It stirs evenly, adds 1kg fulvic acids, 5kg aloe extracts, 5kg Radix et Caulis Opuntiae Dillenii extracts stir evenly；Add in 20kg cocounut oil acyls Sodium glutamate surfactant, essence, glycerine are uniformly mixing to obtain brown liquid.

Quality inspection is carried out to facial cleanser described in embodiment 3, sanitary index is shown in Table 1, and sense organ and physical and chemical index are shown in Table 2.

Anti-acne effect inspection is carried out to the facial cleanser described in embodiment 3, the results are shown in Table 3.

Comparative example 3：

Embodiment 4：

A kind of anti-acne facial cleanser, is prepared by the following method：

Aloe after cleaning and sterilization is removed the peel, is cut into small pieces, juice extractor is squeezed out aloe juice, by aloe juice with 200 ~ 300 mesh Strainer filtering filters filtrate in 3500r/min speed centrifuges, and it is aloe extract to obtain supernatant；Cactus is removed the peel, Disinfection cleaning, is cut into small pieces, and is squeezed out cactus juice, 200 ~ 300 mesh filter screens of cactus juice is filtered, filtrate with juice extractor It is filtered in 3500r/min speed centrifuges, it is Radix et Caulis Opuntiae Dillenii extract to obtain supernatant；By 6kg chingma abutilon seeds, 2kg purslanes, 3.5kg kelps, 10kg cape jasmines, the 7kg roots of Dahurain angelica, 7.5kg cimicifugae foetidaes crush respectively, and with 100 mesh sieves, mixed-powder is added in 15 times In the ethyl alcohol of 80% content of powder weight, impregnate 2 it is small when after, extract liquid, extracted 5 times by with step, No. 5 extracting solutions are closed After and, various impurity are removed in filtered paper hopper filtering, and filtered fluid is poured into condensate recycling device, is heated, ethyl alcohol is recycled, obtains Slightly sticky liquid after concentration is Chinese medical extract；18kg Chinese medical extracts are added in 45kg deionized waters, then will Mixture is added in blender capable of controlling temperature, and stirring is warming up to 70 DEG C simultaneously；After 2kg borneols are crushed to 300 mesh, it is added to upper liquid It is stirred evenly in body, adds 5kg fulvic acids, 5kg aloe extracts, 1kg Radix et Caulis Opuntiae Dillenii extracts stir evenly；Add in 20kg coconut palms Oleoyl sodium glutamate surfactant, essence, glycerine are uniformly mixing to obtain brown liquid.

Quality inspection is carried out to facial cleanser described in embodiment 4, sanitary index is shown in Table 1, and sense organ and physical and chemical index are shown in Table 2.

Anti-acne effect inspection is carried out to the facial cleanser described in embodiment 4, the results are shown in Table 3.

Comparative example 4：

The anti-acne effect of embodiment 1-4 and comparative example 1-4 are examined with the following method：

The volunteer that choosing 240 faces has acne participates in experiment, is equally divided into 8 groups, every group of 30 people, and every group of average age is 15-30 Sui, men and women's number is equal, and the age is evenly distributed；240 volunteers are without other diseases that may influence this observation result Disease before the experiments takes pictures every volunteer's face as a comparison, and test period is 50 days, and it is clean that other are not used during experiment Face product；8 groups of volunteers respectively using the facial cleanser described in embodiment 1-4 and comparative example 1-4, face cleaning frequency for twice a day, Time be morning 7-9 points and evening 7-9 points by 50 days experiment after, respectively statistics improve it is apparent, more apparent, unconspicuous Number is recorded in table 2.Wherein with after photo comparison before experiment, volunteer's face acnes completely disappear or disappear substantially, red and swollen complete It totally disappeared and move back or substantially disappear to improve substantially；Face acnes quantity, red and swollen area regression half to 2/3rds are brighter to improve It is aobvious；Face acnes quantity, red and swollen area disappear less than 1/3rd as improvement unobvious.

1 sanitary index of table

2 sense organ of table and physical and chemical index

Sanitary index, sense organ and the physical and chemical index of facial cleanser described in embodiment 1-4 and comparative example 1-4 meet QB/T1645- 2004《Facial cleanser/cream》Regulation.

From Tables 1 and 2, sanitary index, sense organ and the physics and chemistry of the facial cleanser described in embodiment 1-4 and comparative example 1-4 Index is according to QB/T1645-2004《Facial cleanser/cream》Regulation is tested, and inspection result meets professional standard, specific to examine Proved recipe method is the generally known common knowledge of those of ordinary skill in the art, is no longer specifically repeated herein.

3 anti-acne effect statistical form of table

As shown in Table 3, the addition of fulvic acid can improve anti-acne effect, and anti-acne effect is more after fulvic acid is combined with Chinese medicine composition It is good.

The foregoing description of the disclosed embodiments enables professional and technical personnel in the field to realize or use the present invention. A variety of modifications of these embodiments will be apparent for those skilled in the art, it is as defined herein General Principle can be realized in other embodiments without departing from the spirit or scope of the present invention.Therefore, it is of the invention The embodiments shown herein is not intended to be limited to, and is to fit to and the principles and novel features disclosed herein phase one The most wide scope caused.

Claims

1. a kind of anti-acne facial cleanser, which is characterized in that it includes the component of following parts by weight：10 ~ 50 parts of fulvic acids, 50-250 parts Chinese medical extract, 10 ~ 50 parts of aloe extracts, 10 ~ 50 parts of Radix et Caulis Opuntiae Dillenii extract, 400 ~ 500 parts of deionized water, surface-active 100 ~ 200 parts of agent；The fulvic acid is mineral fulvic acid.

2. a kind of anti-acne facial cleanser according to claim 1, which is characterized in that the Chinese medical extract includes following weight Measure the component of ratio：Chingma abutilon seed：Purslane：Kelp：Cape jasmine：The root of Dahurain angelica：Cimicifugae foetidae is 1-5:1-5:1-5:1-5:1-5.

3. a kind of anti-acne facial cleanser according to claim 2, which is characterized in that further include 10-50 parts of borneols.

4. a kind of anti-acne facial cleanser according to claim 3, which is characterized in that the surfactant is cocounut oil acyl paddy ammonia Sour sodium.

5. a kind of anti-acne facial cleanser according to claim 4, which is characterized in that the chingma abutilon seed, purslane, kelp, Cape jasmine Son, the root of Dahurain angelica, borneol and cimicifugae foetidae are the air-dried drug bought from shop of Chinese medicines.

6. a kind of anti-acne facial cleanser according to claim 5, which is characterized in that the aloe extract is with the following method It prepares：Aloe after cleaning and sterilization is removed the peel, is cut into small pieces；It is squeezed out aloe juice with juice extractor；By aloe juice with 200 ~ 300 Mesh filter screen filters；Filtrate is filtered in 2500 ~ 3500r/min speed centrifuges, it is aloe extract to obtain supernatant.

7. a kind of anti-acne facial cleanser according to claim 6, which is characterized in that the Radix et Caulis Opuntiae Dillenii extract uses such as lower section It is prepared by method：Cactus is removed the peel, and disinfection cleaning is cut into small pieces；It is squeezed out cactus juice with juice extractor；By cactus juice with 200 ~ 300 mesh filter screens filter；Filtrate is filtered in 2500 ~ 3500r/min speed centrifuges, it is cactus extraction to obtain supernatant Object.

8. a kind of anti-acne facial cleanser according to claim 7, which is characterized in that the Chinese medical extract is with the following method It prepares：

（1）Weigh that be crushed to 80 ~ 100 mesh respectively after chingma abutilon seed, purslane, kelp, cape jasmine, the root of Dahurain angelica and cimicifugae foetidae spare；

（2）More than raw material is added in the ethyl alcohol of 10 ~ 20 times of 50 ~ 80% contents, impregnate 1 ~ 2 it is small when after, by liquid by 200 ~ 300 mesh filter screens obtain filtrate and collect, and are extracted 3 ~ 5 times by above step, collected filtrate is extracting solution；

（3）After more than extracting solution is merged, various impurity are removed in filtered paper hopper filtering；

（4）Filtered fluid is poured into condensate recycling device, is heated, recycles ethyl alcohol, during the slightly sticky liquid after being concentrated is Medicament extract.

9. a kind of preparation method of anti-acne facial cleanser as claimed in claim 8, which is characterized in that include the following steps：

（1）Chinese medical extract is added in deionized water, then is fed the mixture into blender capable of controlling temperature, stirring is warming up to simultaneously 50~80℃；

（2）It after borneol is crushed to 200-300 mesh, is added in more than liquid and stirs evenly, add fulvic acid, aloe extraction Object, Radix et Caulis Opuntiae Dillenii extract stir evenly；

（3）Surfactant is added in, is uniformly mixing to obtain brown liquid.