CN114053186B - A kind of rose long-acting moisturizing and whitening essence water and preparation method thereof - Google Patents
A kind of rose long-acting moisturizing and whitening essence water and preparation method thereof Download PDFInfo
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- CN114053186B CN114053186B CN202111494999.6A CN202111494999A CN114053186B CN 114053186 B CN114053186 B CN 114053186B CN 202111494999 A CN202111494999 A CN 202111494999A CN 114053186 B CN114053186 B CN 114053186B
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- 239000011716 vitamin B2 Substances 0.000 description 1
- 229940045997 vitamin a Drugs 0.000 description 1
- 230000029663 wound healing Effects 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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Abstract
Description
技术领域technical field
本发明属于化妆品技术领域,具体涉及一种玫瑰长效保湿美白的精华水及其制备方法。The invention belongs to the technical field of cosmetics, and in particular relates to a rose long-acting moisturizing and whitening essence water and a preparation method thereof.
背景技术Background technique
皮肤是人体防御外界伤害的重要屏障。但是,外界气候环境的变化和刺激,会导致皮肤的皮脂腺和汗腺分泌异常,人的皮肤逐渐衰老,皮脂分泌减少,皮肤保存水分的能力会下降,从而使得皮肤变干,皮肤表皮的角质层增厚,产生皮肤角质化、干裂、皮肤的表面变粗糙等问题。The skin is an important barrier for the human body to defend against external damage. However, changes and stimuli in the external climate and environment will lead to abnormal secretion of sebaceous glands and sweat glands in the skin. People's skin will gradually age, sebum secretion will decrease, and the ability of the skin to retain water will decrease, thus making the skin dry and the cuticle of the skin epidermis increased. Thick, resulting in skin keratinization, chapped, rough skin surface and other problems.
近年来随着生活水平的提高,人们越来越重视皮肤的养护。精华水是日常美容护肤必不可少的用品,它能充分补充肌肤角质层中的水分,可用来清洁肌肤、保持肌肤的健康。同时,精华水也具有调整肌肤的酸碱值(即pH值)的功效。In recent years, with the improvement of living standards, people pay more and more attention to skin care. Essence water is an indispensable product for daily beauty and skin care. It can fully replenish the moisture in the stratum corneum of the skin, and can be used to clean the skin and keep the skin healthy. At the same time, essence water also has the effect of adjusting the acid-base value (ie pH value) of the skin.
但是,常见精华水的基质原料多来自于矿物石油的羟类、醇类物质等,配合原料为化工产品着色剂和赋香剂,这些原料含有对人的皮肤有害的成分,长期使用会被皮肤不同程度的吸收,渗入人体,会对人的面部皮肤粘膜产生不良影响。精华水的品质主要由天然成分的多少来决定的,但我国市场化妆品中天然植物成分占比较少,且长效保湿能力较弱,功能较单一。However, the matrix raw materials of common essence water mostly come from the hydroxyls and alcohols of mineral petroleum, and the matching raw materials are chemical product colorants and fragrances. These raw materials contain ingredients harmful to human skin, and long-term use will be damaged by skin. Different degrees of absorption and penetration into the human body will have adverse effects on human facial skin and mucous membranes. The quality of essence water is mainly determined by the amount of natural ingredients, but the proportion of natural plant ingredients in cosmetics in the Chinese market is relatively small, and the long-term moisturizing ability is weak and the function is relatively single.
发明内容Contents of the invention
鉴于上述的分析,本发明旨在提供一种玫瑰长效保湿美白的精华水及其制备方法,解决了现有技术中精华水的天然植物提取物成分占比较少、长效保湿能力较弱、功能较单一的问题。In view of the above analysis, the present invention aims to provide a long-lasting moisturizing and whitening essence water of roses and a preparation method thereof, which solves the problem that the proportion of natural plant extracts in the essence water in the prior art is small, the long-lasting moisturizing ability is weak, A problem with a single function.
本发明的目的主要是通过以下技术方案实现的:The purpose of the present invention is mainly achieved through the following technical solutions:
本发明提供了一种玫瑰长效保湿美白的精华水,其成分按重量百分比计包括:玫瑰提取物50~52、刺梨提取物4~6、罗马洋甘菊精油0.05~1.00、柠檬精油0.02~0.04、透明质酸钠0.01~0.02、维生素E0.08~0.12、甘油6~10、角鲨烷0.08~0.12、山梨酸钾0.04~0.06和pH值调节剂,其余为去离子水。The invention provides a rose long-acting moisturizing and whitening essence water, the composition of which comprises, by weight percentage: 50-52 rose extract, 4-6 prickly pear extract, 0.05-1.00 Roman chamomile essential oil, and 0.02-0.04 lemon essential oil , Sodium Hyaluronate 0.01-0.02, Vitamin E 0.08-0.12, Glycerin 6-10, Squalane 0.08-0.12, Potassium Sorbate 0.04-0.06 and a pH adjuster, and the rest is deionized water.
进一步地,上述精华水的pH值为5.8~6.0,pH调节剂的用量为使精华水的pH值达到5.8~6.0。Further, the pH value of the above-mentioned essence water is 5.8-6.0, and the dosage of the pH regulator is to make the pH value of the essence water reach 5.8-6.0.
进一步地,玫瑰提取物和刺梨提取物均是由纯天然植物新鲜花瓣和新鲜果实为材料制取。Further, both the rose extract and the prickly pear extract are prepared from fresh petals and fresh fruits of pure natural plants.
进一步地,pH调节剂为柠檬酸和三乙醇胺。Further, the pH regulator is citric acid and triethanolamine.
进一步地,玫瑰提取物包括玫瑰纯露和玫瑰精油,两者的质量比为160~170:1。Further, the rose extract includes rose hydrosol and rose essential oil, and the mass ratio of the two is 160-170:1.
进一步地,上述玫瑰长效保湿美白的精华水,其成分按重量百分比计包括:玫瑰提取物50.3、刺梨提取物5、罗马洋甘菊精油0.07、柠檬精油0.03、透明质酸钠0.01、维生素E0.1、甘油7、角鲨烷0.1、山梨酸钾0.05和pH调节剂,其余为去离子水。Further, the above-mentioned rose long-acting moisturizing and whitening essence water, its ingredients include by weight percentage: 50.3 rose extract, 5 pear extract, 0.07 Roman chamomile essential oil, 0.03 lemon essential oil, 0.01 sodium hyaluronate, vitamin E0. 1. Glycerin 7, squalane 0.1, potassium sorbate 0.05 and pH regulator, the rest is deionized water.
进一步地,上述精华水的pH值为5.8。Further, the pH value of the above-mentioned essence water is 5.8.
进一步地,上述溶剂为去离子水。Further, the above-mentioned solvent is deionized water.
本发明还提供了一种玫瑰长效保湿美白的精华水的制备方法,用于制备上述精华水,上述制备方法包括如下步骤:The present invention also provides a preparation method of rose long-acting moisturizing and whitening essence water, which is used to prepare the above essence water. The above preparation method includes the following steps:
步骤1:将玫瑰精油、罗马洋甘菊精油、柠檬精油、角鲨烷、丁二醇、维生素E分次加入到甘油中搅拌混匀后加入玫瑰纯露和刺梨提取物,制得第一混合物;Step 1: Add rose essential oil, Roman chamomile essential oil, lemon essential oil, squalane, butylene glycol, and vitamin E to glycerin, stir and mix well, then add rose hydrosol and prickly pear extract to prepare the first mixture;
步骤2:在搅拌状态下,将透明质酸钠添加到去离子水中,搅拌溶解,然后,添加山梨酸钾,搅拌溶解,制得第二混合物;Step 2: Add sodium hyaluronate to deionized water under stirring, stir to dissolve, then add potassium sorbate, stir to dissolve, and prepare the second mixture;
步骤3:将第一混合物和第二混合物乳化均质后添加柠檬酸和三乙醇胺调节pH值,加去离子定容,经紫外线照射灭菌,灌装瓶中,得到精华水。Step 3: After emulsifying and homogenizing the first mixture and the second mixture, adding citric acid and triethanolamine to adjust the pH value, adding deionization to make up the volume, sterilizing by ultraviolet radiation, filling in bottles, and obtaining essence water.
进一步地,上述步骤2中,去离子水的温度为40~50℃。Further, in the above step 2, the temperature of the deionized water is 40-50°C.
进一步地,上述步骤2中,去离子水的温度为45℃。Further, in the above step 2, the temperature of the deionized water is 45°C.
进一步地,上述步骤1包括如下步骤:Further, the above step 1 includes the following steps:
步骤11:将刺梨提取物、玫瑰精油和玫瑰纯露分别分为两份;Step 11: Divide the prickly pear extract, rose essential oil and rose hydrosol into two parts;
步骤12:将第一份玫瑰精油加入到甘油中搅拌混匀,得到第一初混物;Step 12: adding the first part of rose essential oil to glycerin and stirring to obtain the first primary mixture;
步骤13:将罗马洋甘菊精油、柠檬精油、角鲨烷、丁二醇和维生素E搅拌混匀,得到第二初混物;Step 13: Stir and mix Roman chamomile essential oil, lemon essential oil, squalane, butylene glycol and vitamin E to obtain the second primary mixture;
步骤14:将第一份刺梨提取物和第一份玫瑰纯露加入到第二初混物中,得到第三初混物;Step 14: adding the first part of Rosa roxburghii extract and the first part of rose hydrosol to the second primary mixture to obtain the third primary mixture;
步骤15:将第二份玫瑰精油、第二份刺梨提取物和第二份玫瑰纯露搅拌混匀,得到第四初混物;Step 15: Stir and mix the second part of rose essential oil, the second part of Rosa roxburghii extract and the second part of rose hydrosol to obtain the fourth primary mixture;
步骤16:将第三初混物和第四初混物搅拌乳化均质,制得第一混合物。Step 16: stirring, emulsifying and homogenizing the third primary mixture and the fourth primary mixture to obtain the first mixture.
与现有技术相比,本发明至少可实现如下有益效果之一:Compared with the prior art, the present invention can achieve at least one of the following beneficial effects:
a)本发明提供的玫瑰长效保湿美白的精华水是一种溶剂型精华水,采用天然植物活性提取成分,首次将刺梨提取物应用到精华水中,以兼具美白、保湿作用的玫瑰提取物和刺梨提取物为主要成分,两者同为蔷薇属药食兼用植物的提取物复合使用,充分发挥两者在精华水中保湿美白的作用,取材天然,成分温和;辅以罗马洋甘菊精油、柠檬精油、透明质酸钠、维生素E、甘油等无毒无刺激活性成分,对皮肤温和、无刺激且兼具长效保湿美白的功能,能够满足人们日常皮肤护理的需要,适合多种肤质使用。a) The rose long-acting moisturizing and whitening essence water provided by the present invention is a solvent-based essence water, which adopts natural plant active extract components, and for the first time, Rosa roxburghii extract is applied to the essence water to extract it from roses that have both whitening and moisturizing effects. Rosa roxburghii and Rosa roxburghii extract are the main ingredients, both of which are used in combination with the extracts of Rosa genus medicinal and edible plants, giving full play to the moisturizing and whitening effects of the two in the essence water, with natural materials and mild ingredients; supplemented by Roman chamomile essential oil, Lemon essential oil, sodium hyaluronate, vitamin E, glycerin and other non-toxic and non-irritating active ingredients are mild to the skin, non-irritating and have long-lasting moisturizing and whitening functions, which can meet people's daily skin care needs and are suitable for a variety of skin types use.
b)本发明提供的玫瑰长效保湿美白的精华水中,玫瑰精油和玫瑰纯露是从玫瑰鲜花中通过水蒸馏法制得的高纯度精油和纯露。玫瑰精油具有抗老、防皱、保湿、修复细胞、促进代谢和消炎抗菌等功效,还能淡化斑点,恢复皮肤弹性;玫瑰纯露具有补充水分、保湿、快速消炎、抗过敏、止痒、延缓衰老等作用。本发明的玫瑰长效保湿美白的精华水,采用玫瑰纯露和玫瑰精油复合使用,是因为,大分子的玫瑰精油比较难以直接吸收和渗透,通过添加适量的玫瑰纯露,能够有效促进两者的协同吸收。b) In the rose long-acting moisturizing and whitening essence water provided by the present invention, rose essential oil and rose hydrosol are high-purity essential oils and hydrosols obtained from rose flowers through water distillation. Rose essential oil has anti-aging, anti-wrinkle, moisturizing, repairing cells, promoting metabolism, anti-inflammatory and antibacterial effects, and can also lighten spots and restore skin elasticity; rose hydrosol has moisturizing, moisturizing, rapid anti-inflammatory, anti-allergic, anti-itching, anti-aging effects of aging. The rose long-acting moisturizing and whitening essence water of the present invention uses rose pure dew and rose essential oil in combination, because the macromolecular rose essential oil is difficult to directly absorb and penetrate, and by adding an appropriate amount of rose pure dew, it can effectively promote both. synergistic absorption.
c)本发明提供的玫瑰长效保湿美白的精华水的制备方法中,各混合物的混合顺序以及各个混合物中各个原料的添加顺序均对获得混合均匀和贮存稳定性良好的精华水至关重要,通过分别制备第一混合物(玫瑰精油、罗马洋甘菊精油、柠檬精油、角鲨烷、丁二醇、维生素E、玫瑰纯露和刺梨提取物)和第二混合物(透明质酸钠、水和山梨酸钾),再将第一混合物和第二混合物混合乳化均质后加入pH值调节剂进行pH调节,能够获得混合均匀和贮存稳定性良好的精华水。c) In the preparation method of the rose long-acting moisturizing and whitening essence water provided by the present invention, the mixing order of each mixture and the addition order of each raw material in each mixture are all crucial to obtaining the essence water with uniform mixing and good storage stability, By separately preparing the first mixture (rose essential oil, Roman chamomile essential oil, lemon essential oil, squalane, butylene glycol, vitamin E, rose hydrosol and prickly pear extract) and the second mixture (sodium hyaluronate, water and sorbic acid Potassium acid potassium), and then the first mixture and the second mixture are mixed, emulsified and homogenized, and then a pH regulator is added to adjust the pH, so that the essence water with uniform mixing and good storage stability can be obtained.
d)本发明提供的玫瑰长效保湿美白的精华水的制备方法中,通过将玫瑰精油、玫瑰纯露和刺梨提取物分别分为两份,分多次、多顺序搅拌混匀,制得第一混合物,能够有效促进玫瑰精油、玫瑰纯露和刺梨提取物乳化和混合,从而进一步提高上述精华水的保湿效果和贮存稳定性。d) In the preparation method of rose long-acting moisturizing and whitening essence water provided by the present invention, rose essential oil, rose hydrosol and Rosa roxburghii extract are respectively divided into two parts, which are stirred and mixed evenly in multiple times and in multiple orders to obtain The first mixture can effectively promote the emulsification and mixing of rose essential oil, rose hydrosol and prickly pear extract, thereby further improving the moisturizing effect and storage stability of the above-mentioned essence water.
本发明的其他特征和优点将在随后的说明书中阐述,并且,部分的从说明书中变得显而易见,或者通过实施本发明而了解。本发明的目的和其他优点可通过在所写的说明书中所特别指出的结构来实现和获得。Additional features and advantages of the invention will be set forth in the description which follows, and in part will be apparent from the description, or may be learned by practice of the invention. The objectives and other advantages of the invention may be realized and attained by the structure particularly pointed out in the written description.
具体实施方式Detailed ways
下面具体描述本发明的优选实施例。Preferred embodiments of the present invention are specifically described below.
本发明提供了一种玫瑰长效保湿美白的精华水,其成分按重量百分比计包括:玫瑰提取物50~52、刺梨提取物4~6、罗马洋甘菊精油0.05~1.00、柠檬精油0.02~0.04、透明质酸钠0.01~0.02、维生素E0.08~0.12、甘油6~10、角鲨烷0.08~0.12、山梨酸钾0.04~0.06和pH值调节剂,其余为去离子水,上述精华水的pH值为5.8~6.0,也就是说,pH调节剂的用量可以使精华水的pH值达到5.8~6.0。The invention provides a rose long-acting moisturizing and whitening essence water, the composition of which comprises, by weight percentage: 50-52 rose extract, 4-6 prickly pear extract, 0.05-1.00 Roman chamomile essential oil, and 0.02-0.04 lemon essential oil , Sodium Hyaluronate 0.01-0.02, Vitamin E 0.08-0.12, Glycerin 6-10, Squalane 0.08-0.12, Potassium Sorbate 0.04-0.06 and pH regulator, the rest is deionized water, the above essence water The pH value is 5.8-6.0, that is to say, the dosage of the pH regulator can make the pH value of the essence water reach 5.8-6.0.
需要说明的是,上述精华水中,玫瑰提取物和刺梨提取物均是由纯天然植物新鲜花瓣和新鲜果实为材料制取。It should be noted that the rose extract and roxburghii extract in the above essence water are all made from fresh petals and fresh fruits of pure natural plants.
同样需要说明的是,pH调节剂为柠檬酸和三乙醇胺,两者的添加量以将pH值调节至目标值为准,研究发现,人体皮肤最适合PH为弱酸性,根据原材料的酸碱性调节用量,使得达到精华水的pH值达到5.8~6.0。It should also be noted that the pH regulators are citric acid and triethanolamine. Adjust the dosage so that the pH value of the essence water reaches 5.8-6.0.
与现有技术相比,本发明提供的玫瑰长效保湿美白的精华水是一种溶剂型精华水,采用天然植物活性提取成分,首次将刺梨提取物应用到精华水中,以兼具美白、保湿作用的玫瑰提取物和刺梨提取物为主要成分,两者同为蔷薇属药食兼用植物的提取物复合使用,充分发挥两者在精华水中保湿美白的作用,取材天然,成分温和;辅以罗马洋甘菊精油、柠檬精油、透明质酸钠、维生素E、甘油等无毒无刺激活性成分,对皮肤温和、无刺激且兼具长效保湿美白的功能,能够满足人们日常皮肤护理的需要,适合多种肤质使用。Compared with the prior art, the rose long-acting moisturizing and whitening essence water provided by the present invention is a solvent-based essence water, which adopts natural plant active extract components, and for the first time applies Rosa roxburghii extract to the essence water to have both whitening, Rose extract and Rosa roxburghii extract for moisturizing are the main ingredients, and they are both medicinal and edible plant extracts of the genus Rosa, which are used in combination to give full play to their moisturizing and whitening effects in the essence water. With Roman chamomile essential oil, lemon essential oil, sodium hyaluronate, vitamin E, glycerin and other non-toxic and non-irritating active ingredients, it is mild to the skin, non-irritating and has long-lasting moisturizing and whitening functions, which can meet people's daily skin care needs. Suitable for many skin types.
具体来说,上述玫瑰长效保湿美白的精华水各个成分的作用如下:Specifically, the function of each component of the above-mentioned rose long-lasting moisturizing and whitening essence water is as follows:
玫瑰提取物:玫瑰提取物主要成分是玫瑰精油和玫瑰纯露,是玫瑰新鲜花瓣蒸馏而来,一富含的维生素C、胡萝卜素、维生素B和维生素K,能强壮和收缩微血管、使皮肤紧致;二富含香叶醇、香茅醇、芳樟醇等活性成分,有消炎抗菌等作用,适用所有肤质犹其是成熟干燥或敏感,任何敏感红肿和发炎皮肤;三玫瑰精油具有超强的渗透性,完美的吸收率和100%的安全性,具有较强的美白效果;四玫瑰精油调节内分泌、促进新成代谢、分解色素、淡化皮肤斑点;五玫瑰纯露极溶于水,具有补充水分、保湿等作用,改善皮肤干燥、恢复皮肤弹性,让女性拥有白皙、充满弹性的健康肌肤,是适宜女性保养护肤的芳香提取物。Rose extract: The main components of rose extract are rose essential oil and rose hydrosol, which are distilled from fresh rose petals, rich in vitamin C, carotene, vitamin B and vitamin K, which can strengthen and shrink capillaries, and make skin tight Second, it is rich in geraniol, citronellol, linalool and other active ingredients, which have anti-inflammatory and antibacterial effects, and is suitable for all skin types, especially mature, dry or sensitive skin, any sensitive, red, swollen and inflamed skin; Triple Rose essential oil has super Strong permeability, perfect absorption rate and 100% safety, has a strong whitening effect; Four Roses essential oil regulates endocrine, promotes new metabolism, decomposes pigments, and dilutes skin spots; Five Roses Hydrosol is extremely soluble in water, It has the functions of replenishing water and moisturizing, improving dry skin, restoring skin elasticity, and allowing women to have white, elastic and healthy skin. It is an aromatic extract suitable for women's skin care.
刺梨提取物:以刺梨新鲜果实经过压榨、两次浸提萃取,后经过减压浓缩获得的刺梨提取物。该提取物含有丰富的维生素C、超氧化物歧化酶(SOD)、烟酸,维生素A,维生素B2,维生素K和维生素E等活性物质,具有淡化黑色素,促进黑色素的排出,改善色斑、暗沉,抗氧化,使肌肤白皙,细致、促进胶原蛋白生成,增强肌肤真皮层的弹力与张力等作用。Rosa roxburghii extract: The Rosa roxburghii extract is obtained by pressing the fresh fruit of Rosa roxburghii, extracting twice, and then concentrating under reduced pressure. The extract is rich in active substances such as vitamin C, superoxide dismutase (SOD), niacin, vitamin A, vitamin B2, vitamin K and vitamin E, which can lighten melanin, promote the discharge of melanin, improve pigmentation, dark spots Shen, anti-oxidation, make the skin fair, delicate, promote collagen production, enhance the elasticity and tension of the skin dermis.
罗马洋甘菊精油:主要成分为松萜或蒎烯、莰烯、桧烯、月桂烯、桉树脑、松油精萜品烯、石竹(萜)烯等,纯天然植物精油,可以对改善干性、敏感性皮肤,调节水油平衡。Roman chamomile essential oil: the main components are pine terpene or pinene, camphene, sabinene, myrcene, eucalyptol, pine oil terpinene, caryophyllene, etc., pure natural plant essential oils, which can improve dryness, Sensitive skin, adjust water and oil balance.
柠檬精油:主要成分为柠檬烯、柠檬醛、(牛彪)牛儿酸、香茅油、樟烯等,纯天然植物精油,其含有的柠檬烯特别有益于美白、收敛、平衡油脂分泌、治疗青春痘等油性皮肤症状。Lemon essential oil: the main components are limonene, citral, (niubiao) geranic acid, citronella oil, camphorene, etc., pure natural plant essential oil, the limonene contained in it is especially beneficial for whitening, astringent, balancing oil secretion, and treating acne and other oily skin symptoms.
透明质酸钠:小分子透明质酸钠能渗透到真皮层,促进血液微循环,有利于皮肤对营养物质的吸收,且不受环境湿度限制,具有高保湿性。Sodium hyaluronate: Small molecule sodium hyaluronate can penetrate into the dermis, promote blood microcirculation, and help the skin absorb nutrients. It is not limited by environmental humidity and has high moisturizing properties.
维生素E:一种脂溶性维生素,是最主要的抗氧化剂之一,可延缓衰老,有效减少皱纹的产生,还可保护皮肤免受紫外线和污染的伤害,减少疤痕与色素的沉积,加速伤口的愈合。Vitamin E: A fat-soluble vitamin, one of the most important antioxidants, can delay aging, effectively reduce wrinkles, protect the skin from ultraviolet rays and pollution, reduce scars and pigment deposition, and accelerate wound healing heal.
甘油:具有很强的吸湿性,可隔绝空气、防止水分蒸发还能吸收空气中的水分,具有极强的保湿作用。Glycerin: It has strong hygroscopicity, can isolate air, prevent water from evaporating, and can also absorb moisture in the air, which has a strong moisturizing effect.
角鲨烷:化学稳定性高,对皮肤有较好的亲和性。Squalane: High chemical stability, good affinity to the skin.
山梨酸钾:属于温和、无添加、无刺激的防腐成分,同时具有抗氧化、镇静舒缓的功能。Potassium Sorbate: It is a mild, non-additive, non-irritating antiseptic ingredient, and has anti-oxidation, calming and soothing functions.
示例性地,玫瑰提取物包括玫瑰纯露和玫瑰精油,两者的质量比为160~170:1。其中,玫瑰精油和玫瑰纯露是从玫瑰鲜花水蒸馏的产物。玫瑰精油具有抗老、防皱、保湿、修复细胞、促进代谢、保湿和消炎抗菌等功效,还能淡化斑点,恢复皮肤弹性;玫瑰纯露具有补充水分、保湿、快速消炎、抗过敏、止痒、延缓衰老等作用。本发明的玫瑰长效保湿美白的精华水,采用玫瑰纯露和玫瑰精油复合使用,是因为,大分子的玫瑰精油比较难以直接吸收和渗透,通过添加适量的玫瑰纯露,能够有效促进两者的协同吸收。Exemplarily, the rose extract includes rose hydrosol and rose essential oil, and the mass ratio of the two is 160-170:1. Among them, rose essential oil and rose hydrosol are products of water distillation from rose flowers. Rose essential oil has anti-aging, anti-wrinkle, moisturizing, repairing cells, promoting metabolism, moisturizing, anti-inflammatory and antibacterial effects, and can also lighten spots and restore skin elasticity; rose hydrosol has moisturizing, moisturizing, rapid anti-inflammatory, anti-allergic, anti-itching , anti-aging effects. The rose long-acting moisturizing and whitening essence water of the present invention uses rose pure dew and rose essential oil in combination, because the macromolecular rose essential oil is difficult to directly absorb and penetrate, and by adding an appropriate amount of rose pure dew, it can effectively promote both. synergistic absorption.
在实际应用中,从精华水的综合性能考虑,上述玫瑰长效保湿美白的精华水,其成分按重量百分比计包括:玫瑰提取物50.3、刺梨提取物5、罗马洋甘菊精油0.07、柠檬精油0.03、透明质酸钠0.01、维生素E 0.1、甘油7、角鲨烷0.1、山梨酸钾0.05和pH调节剂,其余为去离子水,精华水的pH值为5.8。In practical application, considering the comprehensive performance of the essence water, the ingredients of the above-mentioned rose long-lasting moisturizing and whitening essence water include by weight percentage: 50.3 rose extract, 5 prickly pear extract, 0.07 Roman chamomile essential oil, 0.03 lemon essential oil , Sodium Hyaluronate 0.01, Vitamin E 0.1, Glycerin 7, Squalane 0.1, Potassium Sorbate 0.05 and a pH regulator, the rest is deionized water, and the pH value of the essence water is 5.8.
考虑到上述精华水中,溶剂是主要成分,为了进一步减少精华水对皮肤的刺激,示例性地,上述溶剂为去离子水。一方面,采用去离子水作为溶剂,能够进一步减少精华水对皮肤的刺激;另一方便,采用去离子水作为溶剂,还能够提高上述精华水内的含水量,进一步提高其保湿功能。Considering that the above-mentioned essence water contains a solvent as a main component, in order to further reduce the skin irritation caused by the essence water, for example, the above-mentioned solvent is deionized water. On the one hand, using deionized water as a solvent can further reduce the irritation of the essence water to the skin; on the other hand, using deionized water as a solvent can also increase the water content in the above essence water and further improve its moisturizing function.
本发明还提供了一种玫瑰长效保湿美白的精华水的制备方法,包括如下步骤:The present invention also provides a preparation method of rose long-acting moisturizing and whitening essence water, comprising the following steps:
步骤1:将玫瑰精油、罗马洋甘菊精油、柠檬精油、角鲨烷、丁二醇、维生素E分次加入到甘油中搅拌混匀后加入玫瑰纯露和刺梨提取物,制得第一混合物;Step 1: Add rose essential oil, Roman chamomile essential oil, lemon essential oil, squalane, butylene glycol, and vitamin E to glycerin, stir and mix well, then add rose hydrosol and prickly pear extract to prepare the first mixture;
步骤2:在搅拌状态下,将透明质酸钠添加到去离子水中,搅拌溶解,然后,添加山梨酸钾,搅拌溶解,制得第二混合物;Step 2: Add sodium hyaluronate to deionized water under stirring, stir to dissolve, then add potassium sorbate, stir to dissolve, and prepare the second mixture;
步骤3:将第一混合物与第二混合物乳化均质后添加柠檬酸和三乙醇胺调节pH值,加去离子水定容,经紫外线照射灭菌,灌装瓶中,得到精华水。Step 3: After emulsifying and homogenizing the first mixture and the second mixture, adding citric acid and triethanolamine to adjust the pH value, adding deionized water to make up the volume, sterilizing by ultraviolet radiation, and filling into bottles to obtain essence water.
与现有技术相比,本发明提供的玫瑰长效保湿美白的精华水的制备方法的有益效果与上述提供的玫瑰长效保湿美白的精华水的有益效果基本相同,在此不一一赘述。Compared with the prior art, the beneficial effect of the preparation method of the rose long-acting moisturizing and whitening essence water provided by the present invention is basically the same as that of the rose long-acting moisturizing and whitening essence water provided above, and will not be repeated here.
具体来说,上述玫瑰长效保湿美白的精华水的制备方法中,各混合物的混合顺序以及各个混合物中各个原料的添加顺序均对获得混合均匀和贮存稳定性良好的精华水至关重要,通过分别制备第一混合物(玫瑰精油、罗马洋甘菊精油、柠檬精油、角鲨烷、丁二醇、维生素E、玫瑰纯露和刺梨提取物)和第二混合物(透明质酸钠、去离子水和山梨酸钾),再将第一混合物和第二混合物混合后加入pH值调节剂进行pH调节,能够获得混合均匀和贮存稳定性良好的精华水。Specifically, in the preparation method of the above-mentioned long-acting moisturizing and whitening essence water of roses, the order of mixing the mixtures and the order of adding each raw material in each mixture are very important to obtain the essence water with uniform mixing and good storage stability. The first mixture (rose essential oil, Roman chamomile essential oil, lemon essential oil, squalane, butylene glycol, vitamin E, rose hydrosol and prickly pear extract) and the second mixture (sodium hyaluronate, deionized water and Potassium sorbate), and then the first mixture and the second mixture are mixed and then added with a pH regulator to adjust the pH, so that the essence water with uniform mixing and good storage stability can be obtained.
为了促进上述玫瑰长效保湿美白的精华水中水乳融合,上述步骤2中,去离子水的温度为40~50℃(例如,45℃)。In order to promote the water-emulsion fusion of the above-mentioned long-lasting moisturizing and whitening essence of rose, in the above step 2, the temperature of the deionized water is 40-50° C. (for example, 45° C.).
考虑到玫瑰精油、玫瑰纯露和刺梨提取物是否混合均匀会直接影响精华水的保湿效果,因此,上述步骤1包括如下步骤:Considering that whether the rose essential oil, rose hydrosol and prickly pear extract are evenly mixed will directly affect the moisturizing effect of the essence water, therefore, the above step 1 includes the following steps:
步骤11:将刺梨提取物、玫瑰精油和玫瑰纯露分别分为两份;Step 11: Divide the prickly pear extract, rose essential oil and rose hydrosol into two parts;
步骤12:将第一份玫瑰精油加入到甘油中搅拌混匀,得到第一初混物;Step 12: adding the first part of rose essential oil to glycerin and stirring to obtain the first primary mixture;
步骤13:将罗马洋甘菊精油、柠檬精油、角鲨烷、丁二醇和维生素E搅拌混匀,得到第二初混物;Step 13: Stir and mix Roman chamomile essential oil, lemon essential oil, squalane, butylene glycol and vitamin E to obtain the second primary mixture;
步骤14:将第一份刺梨提取物和第一份玫瑰纯露加入到第二初混物中,得到第三初混物;Step 14: adding the first part of Rosa roxburghii extract and the first part of rose hydrosol to the second primary mixture to obtain the third primary mixture;
步骤15:将第二份玫瑰精油、第二份刺梨提取物和第二份玫瑰纯露搅拌混匀,得到第四初混物;Step 15: Stir and mix the second part of rose essential oil, the second part of Rosa roxburghii extract and the second part of rose hydrosol to obtain the fourth primary mixture;
步骤16:将第三初混物和第四初混物搅拌混匀,制得第一混合物。Step 16: Stir and mix the third primary mixture and the fourth primary mixture to obtain the first mixture.
这样,通过将刺梨提取物、玫瑰精油和玫瑰纯露分别分为两份,分多次、多顺序搅拌混匀,制得第一混合物,能够有效促进玫瑰精油、玫瑰纯露和刺梨提取物乳化和混合,获得叠加正效应,从而进一步提高上述精华水的保湿效果和贮存稳定性。In this way, the first mixture is obtained by dividing the thorn pear extract, rose essential oil and rose hydrosol into two parts respectively, and stirring and mixing in multiple times and in multiple order, which can effectively promote the extraction of rose essential oil, rose essential oil and thorn pear The emulsification and mixing of substances can obtain superimposed positive effects, thereby further improving the moisturizing effect and storage stability of the above-mentioned essence water.
实施例1(100ml)Example 1 (100ml)
将0.3%玫瑰精油、0.07%罗马洋甘菊精油、0.03%柠檬精油、0.1%维生素E分次加入到10%甘油中搅拌混匀后加入50%玫瑰纯露制得第一混合物,Add 0.3% rose essential oil, 0.07% Roman chamomile essential oil, 0.03% lemon essential oil, and 0.1% vitamin E to 10% glycerin, stir and mix, and then add 50% rose hydrosol to prepare the first mixture.
将0.01%透明质酸钠边搅拌边添加到45℃的去离子水中,搅拌溶解后,添加0.05%山梨酸钾,搅拌溶解制得第二混合物。Add 0.01% sodium hyaluronate to deionized water at 45°C while stirring, stir and dissolve, then add 0.05% potassium sorbate, stir and dissolve to obtain the second mixture.
将第一混合物与第二混合物混合后添加5%刺梨提取物45℃搅拌溶解,添加适量的三乙醇胺和柠檬酸调节pH为5.8加去离子水定容100ml,经紫外线照射灭菌,灌装瓶中,得到精华水。Mix the first mixture with the second mixture, add 5% Rosa roxburghii extract and stir to dissolve at 45°C, add an appropriate amount of triethanolamine and citric acid to adjust the pH to 5.8, add deionized water to make up to 100ml, sterilize by ultraviolet radiation, and fill In the bottle, get the essence water.
实施例2(100ml)Example 2 (100ml)
将1%玫瑰精油、0.09%罗马洋甘菊精油、0.04%柠檬精油、0.12%维生素E分次加入到7%甘油中搅拌混匀后加入50.5%玫瑰纯露制得第一混合物,Add 1% rose essential oil, 0.09% Roman chamomile essential oil, 0.04% lemon essential oil, and 0.12% vitamin E to 7% glycerin, stir and mix, and then add 50.5% rose hydrosol to prepare the first mixture.
将0.02%透明质酸钠边搅拌边添加到50℃的去离子水中,搅拌溶解后,添加0.04%山梨酸钾,搅拌溶解制得第二混合物。Add 0.02% sodium hyaluronate to deionized water at 50°C while stirring, stir and dissolve, then add 0.04% potassium sorbate, stir and dissolve to obtain the second mixture.
将第一混合物与第二混合物混合后添加6%刺梨提取物50℃搅拌溶解,添加适量的三乙醇胺和柠檬酸调节pH为5.8加去离子水定容100ml,经紫外线照射灭菌,灌装瓶中,得到精华水。Mix the first mixture with the second mixture, add 6% Rosa roxburghii extract and stir to dissolve at 50°C, add an appropriate amount of triethanolamine and citric acid to adjust the pH to 5.8, add deionized water to make up to 100ml, sterilize by ultraviolet radiation, and fill In the bottle, get the essence water.
对比例1Comparative example 1
去离子水Deionized water
对比例2Comparative example 2
市售某品牌精华水(有效成分:玫瑰纯露)。A commercially available brand of essence water (active ingredient: rose hydrosol).
对实施例1和对比例1进行安全性测试,参照《化妆品安全技术规范》(2015年版)第五部分人体皮肤封闭型斑贴实验方法,选取30名志愿者,取上述实施例1和对比例1的样品同步进行封闭型斑贴测试,均未见皮肤发红或出现红斑等过敏现象(参见表1),说明实施例1制得的精华水是安全的,没有引起任何不良现象。Carry out safety test to embodiment 1 and comparative example 1, with reference to " cosmetic safety technical specification " (2015 edition) fifth part human skin closed type patch test method, choose 30 volunteers, get above-mentioned embodiment 1 and comparative example The samples of 1 were subjected to the closed patch test simultaneously, and no allergies such as skin redness or erythema occurred (see Table 1), indicating that the essence water prepared in Example 1 was safe and did not cause any adverse phenomena.
表1封闭型斑贴测试结果Table 1 Closed patch test results
对实施例1和对比例2进行3h保湿效果测试,参照QB/T 4256-2011化妆品保湿功效评价指南,每个样品选取20名测试者,取实施例1和对比例2的样品定量涂抹于前臂圈定部位。采用仪器MOISTUREMETERSC MSC1212(DELFIN)及仪器TAPOMETER SWL5167(DELFIN)分别测量使用样品前(未使用样品的初始值)、使用后0h(使用样品的初始值)、1h和3h的皮肤角质层水油含量以及经皮水分流失率数值,记录所得数值并计算平均值,结果参见表2。Carry out 3h moisturizing effect test to embodiment 1 and comparative example 2, refer to QB/T 4256-2011 cosmetic moisturizing effect evaluation guideline, select 20 testers for each sample, take the sample of embodiment 1 and comparative example 2 and smear quantitatively on the forearm Delineate the location. Using MOISTUREMETERSC MSC1212 (DELFIN) and TAPOMETER SWL5167 (DELFIN) to measure the water and oil content of the stratum corneum of the skin before using the sample (the initial value of the unused sample), 0h after using (the initial value of the used sample), 1h and 3h, and Transepidermal water loss rate value, record the obtained value and calculate the average value, see Table 2 for the results.
表2皮肤角质层水油含量Table 2 Water and oil content of skin stratum corneum
试验结果表明,试验组的使用样品初始值(0h)比未使用样品前(使用前)的水分含量从32%提升至63%,水分含量约提升至1.97倍,对比例2从33%提升至57%,水分含量提升至1.73倍,该结果表明实施例1比对比例2在使用初期水分含量提升更显著.Test result shows, the use sample initial value (0h) of test group improves from 32% to 63% than the moisture content before (before use) of sample, and moisture content promotes to 1.97 times approximately, and comparative example 2 promotes from 33% to 63%. 57%, and the moisture content was increased to 1.73 times, and the results showed that the moisture content of Example 1 was more significant than that of Comparative Example 2 at the initial stage of use.
实施例1的含油率从52%降至40%,降幅为12%,对比例2从51%降至42%,降幅为9%,该结果表明实施例1比在使用初期含油量降低幅度大于对比例2。The oil content of embodiment 1 is reduced to 40% from 52%, and the range of decline is 12%, and comparative example 2 is reduced to 42%, and the range of decline is 9%, and this result shows that embodiment 1 compares the reduction range of oil content at the initial stage of use greater than Comparative example 2.
在试验1h和3h时分别检测皮肤水油含量,结果表明,试验1h后,实施例1水分含量和含油量分别为40%和49%,有效促进水油平衡,试验3h后,水分含量和含油量分别为40%和49%,对比使用1h后水油比例,实施例1在3h后也基本保持不变,该结果表明实施例1产品在使用3h后仍能长效持续促进水油平衡,保湿效果显著;而对比例2在试验1h后水油含量分别为36%和51%,3h后水油含量分别为34%和52%,基本恢复到使用前水油比例,结果表明对比例2在使用1h后便无保湿效果。The water and oil content of the skin was detected respectively during the test for 1h and 3h. The results showed that after the test for 1h, the water content and oil content of Example 1 were respectively 40% and 49%, which effectively promoted the balance of water and oil. After the test for 3 hours, the water content and oil content 40% and 49% respectively, compared with the water-oil ratio after 1h of use, Example 1 also remained basically unchanged after 3h. This result shows that the product of Example 1 can still promote water-oil balance for a long time after 3h of use. The moisturizing effect is remarkable; while the water-oil content of Comparative Example 2 was 36% and 51% after 1 hour of the test, and the water-oil content was 34% and 52% after 3 hours, basically returning to the ratio of water and oil before use. No moisturizing effect after 1 hour of use.
对实施例1的精华水进行贮存稳定性检测,结果参见表3,该精华水在冻融循环、耐热/耐寒试验中外观、气味、pH值均无明显变化,具有贮存稳定性。The storage stability of the essence water in Example 1 was tested, and the results are shown in Table 3. The essence water has no obvious changes in appearance, smell, and pH value in the freeze-thaw cycle and heat/cold resistance tests, and has storage stability.
表3精华水贮存稳定性检测结果Table 3 Essence water storage stability testing results
以上所述,仅为本发明较佳的具体实施方式,但本发明的保护范围并不局限于此,任何熟悉本技术领域的技术人员在本发明揭露的技术范围内,可轻易想到的变化或替换,都应涵盖在本发明的保护范围之内。The above is only a preferred embodiment of the present invention, but the scope of protection of the present invention is not limited thereto. Any person skilled in the art within the technical scope disclosed in the present invention can easily think of changes or Replacement should be covered within the protection scope of the present invention.
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