[go: up one dir, main page]

CN1026240C - 中草药咖啡色素的配制工艺 - Google Patents

中草药咖啡色素的配制工艺 Download PDF

Info

Publication number
CN1026240C
CN1026240C CN91109976A CN88108307A CN1026240C CN 1026240 C CN1026240 C CN 1026240C CN 91109976 A CN91109976 A CN 91109976A CN 88108307 A CN88108307 A CN 88108307A CN 1026240 C CN1026240 C CN 1026240C
Authority
CN
China
Prior art keywords
leaching
time
filtrate
residue
temperature
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN91109976A
Other languages
English (en)
Other versions
CN1040043A (zh
Inventor
叶春园
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN91109976A priority Critical patent/CN1026240C/zh
Publication of CN1040043A publication Critical patent/CN1040043A/zh
Application granted granted Critical
Publication of CN1026240C publication Critical patent/CN1026240C/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B3/00—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
    • H01B3/18—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances
    • H01B3/30—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes
    • H01B3/40—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes epoxy resins
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
    • C08G59/22—Di-epoxy compounds
    • C08G59/24—Di-epoxy compounds carbocyclic
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/68—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the catalysts used
    • C08G59/686—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the catalysts used containing nitrogen
    • G—PHYSICS
    • G11—INFORMATION STORAGE
    • G11B—INFORMATION STORAGE BASED ON RELATIVE MOVEMENT BETWEEN RECORD CARRIER AND TRANSDUCER
    • G11B7/00—Recording or reproducing by optical means, e.g. recording using a thermal beam of optical radiation by modifying optical properties or the physical structure, reproducing using an optical beam at lower power by sensing optical properties; Record carriers therefor
    • G11B7/08—Disposition or mounting of heads or light sources relatively to record carriers
    • G11B7/09—Disposition or mounting of heads or light sources relatively to record carriers with provision for moving the light beam or focus plane for the purpose of maintaining alignment of the light beam relative to the record carrier during transducing operation, e.g. to compensate for surface irregularities of the latter or for track following
    • G11B7/0908—Disposition or mounting of heads or light sources relatively to record carriers with provision for moving the light beam or focus plane for the purpose of maintaining alignment of the light beam relative to the record carrier during transducing operation, e.g. to compensate for surface irregularities of the latter or for track following for focusing only
    • G11B7/0909—Disposition or mounting of heads or light sources relatively to record carriers with provision for moving the light beam or focus plane for the purpose of maintaining alignment of the light beam relative to the record carrier during transducing operation, e.g. to compensate for surface irregularities of the latter or for track following for focusing only by astigmatic methods
    • G—PHYSICS
    • G11—INFORMATION STORAGE
    • G11B—INFORMATION STORAGE BASED ON RELATIVE MOVEMENT BETWEEN RECORD CARRIER AND TRANSDUCER
    • G11B7/00—Recording or reproducing by optical means, e.g. recording using a thermal beam of optical radiation by modifying optical properties or the physical structure, reproducing using an optical beam at lower power by sensing optical properties; Record carriers therefor
    • G11B7/08—Disposition or mounting of heads or light sources relatively to record carriers
    • G11B7/09—Disposition or mounting of heads or light sources relatively to record carriers with provision for moving the light beam or focus plane for the purpose of maintaining alignment of the light beam relative to the record carrier during transducing operation, e.g. to compensate for surface irregularities of the latter or for track following
    • G11B7/0908—Disposition or mounting of heads or light sources relatively to record carriers with provision for moving the light beam or focus plane for the purpose of maintaining alignment of the light beam relative to the record carrier during transducing operation, e.g. to compensate for surface irregularities of the latter or for track following for focusing only
    • G11B7/0916—Foucault or knife-edge methods
    • G—PHYSICS
    • G11—INFORMATION STORAGE
    • G11B—INFORMATION STORAGE BASED ON RELATIVE MOVEMENT BETWEEN RECORD CARRIER AND TRANSDUCER
    • G11B7/00—Recording or reproducing by optical means, e.g. recording using a thermal beam of optical radiation by modifying optical properties or the physical structure, reproducing using an optical beam at lower power by sensing optical properties; Record carriers therefor
    • G11B7/12—Heads, e.g. forming of the optical beam spot or modulation of the optical beam
    • G11B7/135—Means for guiding the beam from the source to the record carrier or from the record carrier to the detector
    • G11B7/1353—Diffractive elements, e.g. holograms or gratings
    • G—PHYSICS
    • G11—INFORMATION STORAGE
    • G11B—INFORMATION STORAGE BASED ON RELATIVE MOVEMENT BETWEEN RECORD CARRIER AND TRANSDUCER
    • G11B7/00—Recording or reproducing by optical means, e.g. recording using a thermal beam of optical radiation by modifying optical properties or the physical structure, reproducing using an optical beam at lower power by sensing optical properties; Record carriers therefor
    • G11B7/12—Heads, e.g. forming of the optical beam spot or modulation of the optical beam
    • G11B7/135—Means for guiding the beam from the source to the record carrier or from the record carrier to the detector
    • G11B7/1372—Lenses
    • G11B7/1374—Objective lenses
    • G—PHYSICS
    • G11—INFORMATION STORAGE
    • G11B—INFORMATION STORAGE BASED ON RELATIVE MOVEMENT BETWEEN RECORD CARRIER AND TRANSDUCER
    • G11B7/00—Recording or reproducing by optical means, e.g. recording using a thermal beam of optical radiation by modifying optical properties or the physical structure, reproducing using an optical beam at lower power by sensing optical properties; Record carriers therefor
    • G11B7/12—Heads, e.g. forming of the optical beam spot or modulation of the optical beam
    • G11B7/135—Means for guiding the beam from the source to the record carrier or from the record carrier to the detector
    • G11B7/1381—Non-lens elements for altering the properties of the beam, e.g. knife edges, slits, filters or stops
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B3/00—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
    • H01B3/02—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of inorganic substances
    • H01B3/04—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of inorganic substances mica
    • H—ELECTRICITY
    • H02—GENERATION; CONVERSION OR DISTRIBUTION OF ELECTRIC POWER
    • H02K—DYNAMO-ELECTRIC MACHINES
    • H02K3/00—Details of windings
    • H02K3/30—Windings characterised by the insulating material
    • G—PHYSICS
    • G11—INFORMATION STORAGE
    • G11B—INFORMATION STORAGE BASED ON RELATIVE MOVEMENT BETWEEN RECORD CARRIER AND TRANSDUCER
    • G11B7/00—Recording or reproducing by optical means, e.g. recording using a thermal beam of optical radiation by modifying optical properties or the physical structure, reproducing using an optical beam at lower power by sensing optical properties; Record carriers therefor
    • G11B7/12—Heads, e.g. forming of the optical beam spot or modulation of the optical beam
    • G11B7/135—Means for guiding the beam from the source to the record carrier or from the record carrier to the detector
    • G11B7/1372—Lenses
    • G11B2007/13725—Catadioptric lenses, i.e. having at least one internal reflective surface
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/25—Web or sheet containing structurally defined element or component and including a second component containing structurally defined particles
    • Y10T428/251—Mica
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/28—Web or sheet containing structurally defined element or component and having an adhesive outermost layer
    • Y10T428/2852—Adhesive compositions
    • Y10T428/287—Adhesive compositions including epoxy group or epoxy polymer
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/31504—Composite [nonstructural laminate]
    • Y10T428/31511—Of epoxy ether

Landscapes

  • Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Optics & Photonics (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Power Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

一种中草药咖啡色素由玄参为主要原料以生地、甘草、陈皮等中草药为辅助原料，经过反复浸取、过滤、再经浓缩、喷雾干燥等工序制得咖啡色素结晶。本发明的咖啡色素不但具有着色功能，并且具有滋阴、降火、生津解毒之保健功能，可广泛用于饮料，食品，医药等行业。本发明的工艺过程简单，所用溶剂价格低廉，回收率高，具有明显的经济效益。

Description

本发明涉及天然食用色素及其提制工艺。
食品中应用咖啡色素之一的酱色，其制造方法是将砂糖、葡萄糖、淀粉与碱、铵盐焙烧而成，主要用于饮料，点心、酱油。我国专利申请GK88100741“用木糖废液生产食用酱色”和GK88100743“用糖厂酒精废液生产食用酱色”专利申请，均提供了利用废料生产酱色的方法但是已有技术的酱色原料均以糖类为主要成分，酱色本身只起着色作用而没有保健功能。此外至今尚未见过有关用中草药为原料制取咖啡色素的报导。
本发明的目的在于利用我国丰富的中草药资源制取一种有保健作用的咖啡色素，扩大酱色品种并提供其相应的提取工艺。
经过反复研究终于研制出一种利用我国盛产的中草药咖啡色素的配方。配方中的主原料是玄参，它性微寒、无毒，具有滋阴、降火、生津解毒之功能。配方中另一组分的生地，它有补血功能。再辅以常用中草药陈皮、甘草等组分更可提高玄参的功能。本发明的配方原料的重量百分含量为：
玄参    50～100%
生地    30～0%
陈皮    10～0%
甘草    10～0%
本发明的中草药咖啡色素的制取工艺流程为：上述配方中一种或几种原料经过前处理，混合后用含0～5重量%乙醇的离子交换水溶液为浸取剂，经过三次浸取及随后的三次过滤分离，把滤液合并经过后处理，静置澄清液经浓缩，喷雾干燥制得咖啡色素结晶。
其具体工艺过程及工艺参数如下：
（1）中草药原料的前处理：
把上述玄参、生地、陈皮、甘草，按配方取其中一种或几种原料分别洗净，晒干，加工成片或丝状。
（2）混合：
把经过前处理的原料按配方混合在一起。
（3）第一次浸取：
用离子交换纯水或含有0～5重量%乙醇的水溶液为浸取剂，浸取原料混合物，浸取液与原料的液固的重量比为1～1.5∶1，浸取温度为0～50℃，最好30～50℃，浸取时间为3～5小时。
（4）过滤：
上述浸取物经过滤分离为滤液和残留物。
（5）第二次浸取：
把第一次浸取后的残留物用同上浸取剂按浸取液与残留物重量比1∶1的比例进行第二次浸取，浸取温度同前，浸取时间3～5小时。
（6）第二次过滤：
把上述浸取物过滤分离。
（7）第三次浸取：
把（6）的残留物再用同（3）的浸取剂，按浸取液与残留物0.8～1∶1的重量比再浸取，浸取温度同（3），浸取时间3～5小时。
（8）第三次过滤：
把步骤（7）的浸取物过滤分离，取其滤液。
（9）滤液的后处理：
把工序（4）、（6）、（8）三次过滤得到的滤液合并，向滤液中滴入0.05～0.5摩尔NaOH水溶液，滤液中的酒石酸和/或硬脂酸与NaOH起中和反应生成盐类沉淀，滴至不再产生沉淀为止，然后静置1～2小时，吸出澄清液。
（10）浓缩：
经后处理的纯净澄清液投入蒸发器内浓缩，去除大部分水使呈半流体状，浓缩温度不超过100℃。
（11）干燥：
把上述浓缩物经喷雾干燥得到粉状咖啡色素结晶，干燥温度不超过100℃。
本发明的工艺的咖啡色素的回收率为15～20%。
本发明的咖啡色素制品送江西省食品卫生监督检验所进行理化检验的结果如下：
一.外观：本品为咖啡色粉末，无杂质。
二.理化：
干燥失重（%）：8.95
灼烧残渣（%）：2.65
pH：4.68
吸光度E（0.01%溶液1厘米比色皿）0.159
铅（Pa，%）：0.00001
砷（As，%）：0.00008
汞（Hg，%）：0.0000002
铜（Cu，%）：0.00045
试样符合GB5176-85标准的要求。
本发明的咖啡色素制品送江西省食品卫生监督检验所进行食品毒理试验，按试验规定的程序对昆明群系小鼠进行18.5～23.5克/只（体重）剂量的毒性试验，其结果是小鼠口服16000毫克/公斤（体重）剂量，无死亡及不良反应，其结论是：按半数致死量（LD50）分级属无毒级。
本发明的制品还进行了食品毒理实验，对小鼠的微核试验结果为：样品组微核率与阳性组（CP）有显著差别（P＜0.01），与阴性组无显著差别，结论是该样品核试验阴性。
用本发明方法制取的咖啡色素配制成可乐饮料，其外观及口感与美国进口的可乐相似。经口服试验证明具有滋阴、降火、生津解毒之功能，不但有着色作用并且有保健作用，可广泛用于饮料、食品、医药等行业。
本发明的工艺过程简单，所用溶剂价格低廉，回收率高，具有明显的经济效益。
实施例
中草药原料玄参、生地、陈皮、甘草分别经过洗涤、晒干、加工成片或丝，称取经过上述前处理 的原料：玄参700克，生地150克，陈皮70克，甘草80克，用1500毫升经离子交换水乙醇溶液（其中乙醇含量为3%）在40°±10℃浸取4小时后过滤分离，在残留物中再加入1000毫升同上组分浸取液，浸取温度及时间同前，浸取后再过滤分离，残留物中再加入800毫升浸取液再按同前工艺浸取后，再过滤分离，把三次滤液合并。在滤液中滴入0.1摩尔NaOH直至沉淀完全，静置澄清1.5小时，分离出澄清液，经100℃以下温度蒸发浓缩去掉大部分水分后，经100℃以下温度喷雾干燥制得咖啡色素190克。回收率为19%。
用本发明方法制取的咖啡色素，配置成可乐饮料，其外观与口感均接近美国进口的可口可乐，实践证明该饮料具有滋阴、降火、生津解毒功能。

Claims (2)

1、一种中草药咖啡色素的配制工艺，本发明的特征在于：
(1)中草药原料的前处理：
把上述玄参、生地、陈皮、甘草，按配方取其中一种或几种原料分别洗净，晒干，加工成片或丝状。
(2)混合：
把经过前处理的原料按配方(重量百分含量)为：
玄参  50～100%
生地  30～0%
陈皮  10～0%
甘草  10～0%
的组分混合在一起，
(3)第一次浸取：
用离子交换纯水或含有0～5重量%乙醇的水溶液为浸取剂，浸取原料混合物，浸取液与原料的液固的重量比为1～1.5∶1，浸取温度为0～50℃，浸取时间为3～5小时。
(4)过滤：
上述浸取物经过滤分离为滤液和残留物。
(5)第二次浸取：
把第一次浸取后的残留物用同上浸取剂按浸取液与残留物重量比1∶1的比例进行第二次浸取，浸取温度同前，浸取时间3～5小时。
(6)第二次过滤：
把上述浸取物过滤分离。
(7)第三次浸取：
把(6)的残留物再用同(3)的浸取剂，按浸取液与残留物0.8～1∶1的重量比再浸取，浸取温度同(3)，浸取时间3～5小时。
(8)第三次过滤：
把步骤(7)的浸取物过滤分离，取其滤液。
(9)滤液的后处理：
把工序(4)、(6)、(8)三次过滤得到的滤液合并，向滤液中滴入0.05～0.5摩尔NaOH水溶液，滤液中的酒石酸和/或硬脂酸与NaOH起中和反应生成盐类沉淀，滴至不再产生沉淀为止，然后静置1～2小时，吸出澄清液。
(10)浓缩：
经后处理的纯净澄清液投入蒸发器内浓缩，去除大部分水使呈半流体状，浓缩温度不超过100℃。
(11)干燥：
把上述浓缩物经喷雾干燥得到粉状咖啡色素结晶，干燥温度不超过100℃。
2、一种根据权利要求1的中草药咖啡色素的制取工艺，其特征在于：
中草药原料玄参、生地、陈皮、甘草分别经过洗涤、洒干、加工成片或丝，称取经过上述前处理的原料，玄参700克，生地150克，陈皮70克，甘草80克，用1500毫升经离子交换水乙醇溶液（其中乙醇含量为3%）在40°±10℃浸取4小时后过滤分离，在残留物中再加入1000毫升同上组分浸取液，浸取温度及时间同前，浸取后再过滤分离，残留物中再加入800毫升浸取液再按同前工艺浸取后，再过滤分离，把三次滤液合并。在滤液中滴入0.1摩尔NaOH直至沉淀完全，静置澄清1.5小时，分离出澄清液，经100℃以下温度蒸发浓缩去掉大部分水分后经100℃以下温度喷雾干燥制得咖啡色素190克。回收率为19%。
CN91109976A 1988-11-30 1988-11-30 中草药咖啡色素的配制工艺 Expired - Fee Related CN1026240C (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN91109976A CN1026240C (zh) 1988-11-30 1988-11-30 中草药咖啡色素的配制工艺

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN91109976A CN1026240C (zh) 1988-11-30 1988-11-30 中草药咖啡色素的配制工艺

Publications (2)

Publication Number Publication Date
CN1040043A CN1040043A (zh) 1990-02-28
CN1026240C true CN1026240C (zh) 1994-10-19

Family

ID=4835023

Family Applications (1)

Application Number Title Priority Date Filing Date
CN91109976A Expired - Fee Related CN1026240C (zh) 1988-11-30 1988-11-30 中草药咖啡色素的配制工艺

Country Status (1)

Country Link
CN (1) CN1026240C (zh)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101570646B (zh) * 2009-06-09 2013-06-05 福建清源科技有限公司 丹参植物染料的制备方法及其上染棉织物的方法
CN103598584A (zh) * 2013-11-16 2014-02-26 大连杰信生物科技有限公司 一种补气保健膏的制备及其作用
CN105831557A (zh) * 2015-12-16 2016-08-10 云南农业大学 一种咖啡类黑精色素的制备方法

Also Published As

Publication number Publication date
CN1040043A (zh) 1990-02-28

Similar Documents

Publication Publication Date Title
CN101456918B (zh) 黄精多糖及其制备方法以及黄精多糖在制备降血糖、降血脂药物中的应用
CN1282654C (zh) 黄芪总皂苷的制备方法
CN1865290A (zh) 冬枣多糖的提取方法
CN1026240C (zh) 中草药咖啡色素的配制工艺
CN1723981A (zh) 罗汉果提取物用于制备药物辅料的新用途
CN101228958A (zh) 一种从枸杞中提取多糖、红黄色素作为添加物用于红景天饮料中的方法
CN107129541A (zh) 一种牛蒡多糖热解物的制备方法及其应用
KR20070084796A (ko) 당귀 추출물의 제조방법 및 그 조성물
CN1596687A (zh) 一种用于茶叶食品的茶香精及其制备方法
CN1715287A (zh) 一种从生地黄中提取高纯度水苏糖和生产熟地黄的方法
CN1113794A (zh) 清音茶
CN100453108C (zh) 一种具有滋补保健作用的中药组合物及其制备方法
CN1085533C (zh) 鹿茸林蛙油口服液及制备方法
CN107568538A (zh) 一种提高免疫力黄芪中草药保健饮料及其制备方法
GB2160423A (en) A method of producing a crude drug preparation
CN1164600C (zh) 一种利用中药泽兰的块根制取双歧因子低聚糖的方法
CN1457666A (zh) 六味地黄红枣咖啡
CN1205976C (zh) 一种可有效除尽针剂中杂质的中药针剂制备方法
CN1062142C (zh) 银黄冲剂生产工艺
CN1305894C (zh) 西洋参总皂甙提取新工艺及其粉针剂
CN1300604A (zh) 具有增强免疫功能的复方哈士蟆油制剂及其制备方法
CN109288957A (zh) 碱提酸沉法提取益心舒组合物中有效成分的方法及其产品
CN115624576B (zh) 一种甘草提取液的制备及脱色方法
CN113876895B (zh) 一种具有降糖活性的复合提取物制备方法及应用
CN1531870A (zh) 人体所需氨基酸的系列产品

Legal Events

Date Code Title Description
PB01 Publication
SE01 Entry into force of request for substantive examination
C10 Entry into substantive examination
C06 Publication
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
C19 Lapse of patent right due to non-payment of the annual fee