CN101856315A - 保湿组合物 - Google Patents
保湿组合物 Download PDFInfo
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- CN101856315A CN101856315A CN201010210877A CN201010210877A CN101856315A CN 101856315 A CN101856315 A CN 101856315A CN 201010210877 A CN201010210877 A CN 201010210877A CN 201010210877 A CN201010210877 A CN 201010210877A CN 101856315 A CN101856315 A CN 101856315A
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Abstract
本发明涉及一种保湿组合物，其包括：植物油与马来酸酐的加合物；和选自水解角蛋白、羟乙基脲、和/或季化氮保湿剂的材料。
Description
本申请是国际申请日为2006年8月24日、国际申请号为PCT/US2006/033162(国家申请号为200680040037.0)、发明名称为“保湿组合物”的原申请的分案申请。
相关申请的交叉参考
本申请要求2005年8月25日提交的美国临时专利申请第60/711,121号的优先权，将其引入本文作为参考。
技术领域
本发明涉及一种组合物，具体涉及一种保湿组合物。
背景技术
给皮肤、毛发、或指甲提供水分已成为许多产物的目的，以防止干燥和/或促进保湿。一些产品已采用作为阻隔剂的材料以防止体内的水分流失。其它产品采用将水分吸收到皮肤上的材料。
期望提供可以提供期望水平的水分，同时对皮肤、毛发、和/或直接具有期望的作用的组合物。
发明内容
一种组合物，其包括：植物油与马来酸酐的加合物；和选自水解角蛋白、羟乙基脲、和/或季化氮保湿剂的材料。另外，一种保湿皮肤、毛发、和/或指甲的方法，其包括施用有效量的该组合物到皮肤、毛发、和/或指甲上。另外，一种将物质沉积到衬底上的方法，其包括将进一步包括该物质的组合物施用到衬底上。
发明详述
自始至终所使用的范围用作描述在该范围之内的每个和全部值的简写。可以选择该范围之内的任意值作为该范围的端点。使用和/或表明，可以单独地选择该序列中的任一个，或者可以选择该序列中的任意组合。
除非相反地指出，否则本文字所述的百分比均为重量百分比，基于该组合物总重(其总计100％)中材料的有效重量。
该组合物包括植物油马来酸酯。该植物油马来酸酯为植物油与马来酸酐的加合物。该植物油马来酸酯可以以获得期望水平的保湿的任意期望量存在。一种实施方式中，该组合物中植物油马来酸酯的存在量为大于0～约2wt％。另一实施方式中，该植物油马来酸酯的存在量为约0.55wt％。
可以利用多种植物油来制备与马来酸酐的加合物，例如，甘油，其中采用相等或者接近相等数量的脂肪酸分子将组成羟基酯化。许多植物油为甘油三酯，即，其中三个脂肪酸分子化学键合于甘油主链的那些甘油酯。适用于本发明的植物油包括、但并非限定于，杏仁、落花生(花生)、鳄梨、蓖麻、椰子、玉米、棉籽、crambie、希蒙得木、lesquerella(豆荚)、亚麻子、橄榄、棕榈、油菜籽(菜籽油)、米糠、桃仁(杏核仁)、红花、芝麻、大豆、向日葵和veronia。
植物油功能性的差异通常归因于它们的各种脂肪酸组分的变化。适用于本发明的植物油中可以存在不同脂肪酸，包括，例如，肉豆蔻酸、十八碳三烯4酮酸、12-羟基油酸、桐酸、蓖麻油酸、棕榈酸、硬脂酸、油酸、亚油酸、亚麻酸、花生酸、二十烯酸、辣木子油酸、芥子酸、palmitiolic酸、docosadienoic酸、lignoseric酸、tetracossenoic酸、十七烷酸、margaroleic酸、顺式9二十碳烯酸、羊脂酸、羊蜡酸、月桂酸、十五烷酸、和十七烷酸。这些脂肪酸也可以在不饱和度方面不同，且它们的羟基可以如典型仲醇一样通过消除或酯化而反应。
植物油马来酸酯的一种实例为马来酸蓖麻酯，其可以通过将蓖麻油与马来酸酐反应形成加合物来制得，如US 6,225,485中所述，将其引入本文作为参考。一种实施方式中，该马来酸蓖麻酯不含自由马来酸酐。该马来酸蓖麻酯可以如下制得，将蓖麻油和环状羧酸酐在75～120℃的温度下反应例如4～24小时的最初时间段，并随后将该反应在室温下继续进行至少一周，以确保实质上全部马来酸酐已反应。
除了植物油马来酸酯之外，该组合物包括选自水解角蛋白、羟乙基脲、和/或季化氮保湿剂的保湿剂。这些中的任一种可以单独使用，或者可以使用这些材料的任意组合。
一种实施方式中，该组合物中存在水解角蛋白。该组合物中可以包括任意的水解角蛋白。一种实施方式中，该水解角蛋白包括山羊毛的提取物。一种实施方式中，该山羊毛为山羊绒。该水解角蛋白可以以获得期望水平的保湿的任意期望量存在于该组合物中。一种实施方式中，该水解角蛋白的存在量为0～约0.005wt％。另一实施方式中，该水解角蛋白的存在量为约0.0005～约0.005wt％。另一实施方式中，该水解角蛋白的存在量为约0.0015wt％。
一种实施方式中，该组合物中存在羟乙基脲。该羟乙基脲可以以获得期望水平的保湿的任意期望量存在于该组合物中。一种实施方式中，该羟乙基脲的存在量为0～约13wt％。一种实施方式中，该羟乙基脲的存在量为约6wt％。
一种实施方式中，该组合物中存在季化氮保湿剂。该季化氮保湿剂为在其结构中含有季化氮的保湿剂。季化氮保湿剂的实例包括、但并非限定于，具有结构
的羟丙基双-羟乙基氯化二甲铵(dimonium)(可从Colonial Chemicals、Inc.以COLATM Moist 200获得)，具有结构
的材料(其描述于US 6,869,977)，胆碱盐(其描述于US 6,475,965和6,265,364，将二者引入本文作为参考)，肉毒碱，及其组合。天然存在的肉毒碱为L-肉毒碱。该季化氮保湿剂可以以获得期望水平的保湿的任意期望量存在于该组合物中。一种实施方式中，该季化氮保湿剂的存在量为0～约5。另一实施方式中，该季化氮保湿剂的存在量为约0.1～约1wt％。另一实施方式中，该水解角蛋白的存在量为约1wt％。
另外，该组合物中与该保湿剂组合地包括甘油。可以包括提供期望水平的保湿的任意期望量的甘油。一种实施方式中，该甘油的存在量为0～约8wt％。其它实施方式中，该甘油的存在量为约6wt％或者约1.5wt％。
该组合物也可以含有肌酸。肌酸可以用于支持皮肤细胞中的能量循环。可以包括任意期望量的肌酸以获得细胞中任意期望水平的能量支持。一种实施方式中，该组合物中肌酸的存在量为0～约2wt％。
该清洁组合物也可以包括一种或多种阴离子表面活性剂、两性表面活性剂、非离子表面活性剂、阳离子表面活性剂、及其组合。本领域普通技术人员将知道适宜的表面活性剂和其它添加剂，可容易地从International CosmeticIngredient Dictionary and Handbook、第10版、(2004)中鉴别。可以包括任意期望量的表面活性剂。一种实施方式中，该组合物中表面活性剂的存在量为0～约40wt％。一种实施方式中，该组合物中表面活性剂的存在量为约1～约40wt％。一种实施方式中，该组合物中表面活性剂的存在量为约5～约40wt％。一种实施方式中，该组合物中表面活性剂的存在量为约1～约10wt％。
保湿身体清洗组合物中可以利用多种阴离子表面活性剂，包括，例如，长链烷基(C6～C22)材料，如长链烷基硫酸酯、长链烷基磷酸酯、长链烷基醚硫酸酯、长链烷基α烯烃磺酸酯、长链烷基牛磺酸盐、长链烷基异硫代硫酸酯(SCI)、长链烷基甘油基醚磺酸酯(AGES)、硫代琥珀酸酯等。这些阴离子表面活性剂可以是烷氧基化的，例如，乙氧基化的，但是烷氧基化并非必须的。这些表面活性剂通常为高水溶性的，如它们的含钠、钾、烷基和铵或烷醇铵的盐形式，且可以提供高发泡清洁能力。可以使用其它等价的阴离子表面活性剂。一种实施方式中，该阴离子表面活性剂包括月桂基聚氧乙烯醚硫酸钠、聚氧乙烯醚硫酸钠、及其组合。可以包括任意期望量的阴离子表面活性剂。一种实施方式中，该组合物中阴离子表面活性剂的存在量为0～约15wt％。一种实施方式中，该组合物中阴离子表面活性剂的存在量为约6～约8wt％。
该组合物中也可以包括两性表面活性剂。这些表面活性剂的特征通常在于高表面活性剂活性、肥皂泡形成和温和的组合。两性表面活性剂包括、但并非限定于，脂肪族仲和叔胺的衍生物，其中脂基可以是支链或支化的和其中一个脂族取代基含有约8～约18个碳原子且一个含有阴离子水溶解性基团，例如，羧基、磺酸盐、硫酸盐、磷酸盐、或膦酸盐。这种化合物的实例包括3-十二烷基氨基丙酸钠、3-十二烷基氨基丙烷磺酸钠、N-烷基牛磺酸和N-高级烷基天门冬氨酸。可以使用其它等价的两性表面活性剂。两性表面活性剂的实例包括、但并非限定于，大量的甜菜碱，包括，例如，高级烷基甜菜碱，如椰油二甲基羧甲基甜菜碱、月桂基二甲基羧甲基甜菜碱、月桂基二甲基α-羧甲基甜菜碱、鲸蜡基二甲基羧甲基甜菜碱、月桂基双-(2-羟乙基)羧甲基甜菜碱、硬脂基双-(2-羟丙基)羧甲基甜菜碱、油烯基二甲基γ-羧丙基甜菜碱、和月桂基双-(2-羟乙基)α-羧乙基甜菜碱，硫代甜菜碱如椰油二甲基硫代丙基甜菜碱、硬脂基二甲基硫代丙基甜菜碱、酰胺基甜菜碱、酰胺基硫代甜菜碱等。具有长链烷基、特别是椰油基的甜菜碱，以及包括酰胺基的那些如椰油酰胺基丙基和椰油酰胺基乙基甜菜碱的那些，可以特别适用。可以包括任意期望量的两性表面活性剂。一种实施方式中，该组合物中两性表面活性剂的存在量为0～约15wt％。一种实施方式中，该组合物中两性表面活性剂的存在量为约4～约6wt％。
非离子表面活性剂的实例包括、但并非限定于，聚山梨酸酯20，具有C8-C22烷基的长链葡糖苷；椰油脂肪酸单乙醇酰胺如椰油酰胺MEA；椰油脂肪酸二乙醇酰胺，脂肪醇乙氧基化物(烷基聚乙二醇)；烷基酚聚乙二醇；烷基硫醇聚乙二醇；脂肪胺乙氧基化物(烷基氨基聚乙二醇)；脂肪酸乙氧基化物(酰基聚乙二醇)；聚丙二醇乙氧基化物(例如可从BASF商购获得的PluronicTM嵌段共聚物)；脂肪酸羟烷基酰胺(脂肪酸酰胺聚乙二醇)；N-烷基-、N-烷氧基多羟基脂肪酸酰胺；蔗糖酯；山梨糖醇酯；聚二醇醚；及其组合。可以包括任意期望量的非离子表面活性剂。一种实施方式中，该组合物中非离子表面活性剂的存在量为0～约3wt％。一种实施方式中，该组合物中非离子表面活性剂的存在量为约0.5～约1.5wt％。
该组合物中也可以包括阳离子表面活性剂。阳离子表面活性剂的实例包括、但并非限定于任意季化或多季化化合物。可以包括任意期望水平的阳离子表面活性剂。一种实施方式中，该组合物中阳离子表面活性剂的存在量为0～约2wt％。一种实施方式中，该组合物中阳离子表面活性剂的存在量为约0.1～约0.3wt％。
多种额外的表面活性剂描述于McCUTCHEON′S DETERGENTS AND EMULSIFIERS(1989)和本领域普通技术人员众所周知的其它参考材料中。
该组合物中可以包括皮肤相容性油。皮肤相容性油包括大量的液体烃，例如线性和支化油如液体石蜡、角鲨烯、角鲨烷、矿物油、低粘度合成烃如聚α烯烃，可从ExxonMobil以商品名Puresyn PAO商购获得，和商品名为PanalaneTM或IndopolTM的聚丁烯。一些情形中轻质(低粘度)高支化烃油也可以适用。其它适用的皮肤相容性油可以为硅酮基的，例如，线性和环状聚二甲基硅氧烷、有机官能硅酮(烷基和烷基芳基)、和氨基硅酮。
其它实施方式中，该组合物可以包括任意期望量的任一种下列材料以在该组合物获得期望的效果(提供了一些实施方式中可以采用的量)：一种或多种碱盐，例如，氯化钠、硫酸钠、碳酸钠、碳酸氢钠和/或它们的等价物(0～5wt％)；发泡剂，例如，癸基葡糖苷、和/或它们的等价物(0～3wt％)；甘油基酯和衍生物，例如，二醇二硬脂酸酯、和/或它们的等价物(0～3wt％)；多价螯合剂，例如，EDTA四钠、和/或它们的等价物(0～2wt％)；杀菌剂，例如，Triclosan(2，4，4’-三氯-2’-羟基二苯基醚)、DMDM乙内酰脲、甲醛和/或咪唑二基脲、和/或它们的等价物(0～2wt％)；有机酸，例如，柠檬酸和/或蚁酸和/或它们的等价物(0～2wt％)；粘度改性剂(0～2wt％)；香料和/或香水(0～5wt％)；防腐剂，例如，苯氧基乙醇、甲醛溶液、对羟基苯甲酸酯类、戊二醇或抗坏血酸(0～2wt％)；光泽剂，例如，二醇二硬脂酸酯，如乙二醇二硬脂酸酯，以及脂肪酸单二醇酯(0～3wt％)；稳定剂，例如，脂肪酸的金属盐，例如，硬脂酸镁、硬脂酸铝和/或硬脂酸锌(0～2wt％)；和许可的且适用于化妆目的的染料与颜料。
该组合物中可以包括水。包含的水的量可以为约90wt％。一种实施方式中，水的存在量为约50％～约90wt％。
一种实施方式中，保湿身体冲洗组合物也利用了，作为增稠剂的，PEG-150二硬脂酸酯和PPG-2羟乙基椰油酰胺的共混物，用于针对与一些保湿身体冲洗组合物中采用的保湿剂浓度相关联的粘度增加。该共混的增稠剂使得该组合物能够获得超过采用常规增稠剂例如仅仅氯化钠所能获得的粘度，且能够在较低浓度下获得适宜粘度。对于可以用来制备该保湿身体冲洗组合物的制备方法来说，用于实现期望粘度的较低浓度也是有利的，由此降低了对于与如果使用其它增稠剂时制备该保湿身体冲洗组合物相关联的更大设备或改进和资本支出的需求。该PEG-150二硬脂酸酯和PPG-2羟乙基椰油酰胺可以以获得期望粘度的任意量存在。一种实施方式中，该组合物中PEG-150二硬脂酸酯的量为0～约2wt％。一种实施方式中，该组合物中PPG-2羟乙基椰油酰胺的量为0～约2wt％。一种实施方式中，该PEG-150二硬脂酸酯和PPG-2羟乙基椰油酰胺的重量比例可以为约3∶1～约1∶3。一种实施方式中，该PEG-150二硬脂酸酯和PPG-2羟乙基椰油酰胺各自存在量为0.0225wt％。该PEG-150二硬脂酸酯和PPG-2羟乙基椰油酰胺可从Uniqema以商品名PROMIDIUMTM LTS以混合物获得。
该组合物可以用于保湿皮肤、毛发、和/或指甲。将该组合物施用到皮肤、毛发、和/或指甲上。如果该组合物为冲洗组合物，将该组合物冲洗掉。可以将该组合物保留任意期望的时间。该组合物可以包含在接触皮肤(包括口腔)、毛发、和/或指甲的任意产品中。该组合物可以用在人或其它动物上。该组合物的形式可以为身体清洗液、洗浴凝胶、洗手液、皂条、洗发剂、调节剂、餐具清洗液、润肤液、遮光剂、泡沫浴、口腔护理产品、牙粉、牙膏、嗽口水、止汗药、除臭剂、或足部浸泡液。
该组合物也可以用于将物质施用到衬底上。该物质包含在该组合物中，并将该组合物施用到衬底上。该衬底可以是任意期望的衬底。一种实施方式中，该衬底可以是皮肤、毛发、和/或指甲。该物质可以吸引到该组合物中的任意物质。一种实施方式中，该物质选自香料、遮光剂、颜料、驱虫剂、和/或疏水材料。
下列实施例仅是示例性的且并非以任意方式限定所述和所要求的本发明的范围。除非相反地指出，用量为该组合物的wt％，基于该材料的有效重量。
具体实施方式
实施例1
可以制备包含水解山羊绒的保湿身体冲洗组合物。下表1中提供了该保湿身体冲洗组合物的配方。表2中显示了该实施例和其它实施例中所用的基料。
表1
| 相 | 成分 | ％Wt.范围 |
| 相A | ||
| 基料 | 70-85 | |
| 相B | ||
| 马来酸蓖麻酯 | 0.1-2 | |
| 甘油 | 1-8 | |
| 山羊绒的提取物 | 0.0005-0.005 | |
| 椰油酰胺基丙基甜菜碱 | 1-15 | |
| 相C | ||
| 香料 | 0.1-3 | |
| 柠檬酸溶液 | 0.001-0.2 | |
| 氯化钠 | 1-5 | |
| 总计 | 100 |
表2
基料
| 成分名称 | ％Wt.范围 |
| 软化水 | 84-87 |
| DMDM乙内酰脲 | 0.2-0.4 |
| 聚季化物-7 | 0.15-0.25 |
| SO3Na Pareth 145-2EO硫酸盐 | 8-10 |
| 椰油酰胺基丙基甜菜碱 | 2.5-4 |
| 成分名称 | ％Wt.范围 |
| 癸基葡糖苷 | 1-2 |
| 乙二胺四乙酸(EDTA) | 0.05-1 |
| 总材料 | 100 |
实施例2
可以制备包括羟乙基脲(例如，HydrovanceTM，从National Starch and Chemical，Bridgewater，NJ商购获得)的保湿身体冲洗组合物。下表3中提供了该保湿身体冲洗组合物的配方。
表3
| 相 | 成分 | ％Wt./Wt. | ％Wt.范围 |
| 相A | |||
| 基料 | 82.31 | 70-85 | |
| 相B | |||
| 马来酸蓖麻酯 | 0.55 | 0.1-2 | |
| 羟乙基脲 | 6 | 1-13 | |
| 椰油酰胺基丙基甜菜碱 | 8 | 1-15 | |
| 相C | |||
| 香料 | 1.1 | 0.1-3 | |
| 柠檬酸溶液 | 0.04 | 0.001-0.2 | |
| 氯化钠 | 2 | 1-5 | |
| 总计 | 100 | 100 |
实施例3
也可以制备下表4中所示的、含有甘油和羟乙基脲的共混物的组合物。
表4
| 相 | 成分 | ％Wt./Wt. | ％Wt.范围 |
| 相A | |||
| 基料 | 78.71 | 70-85 | |
| 相B | |||
| 马来酸蓖麻酯 | 0.55 | 0.1-2 | |
| 甘油 | 3 | 0.1-6 | |
| 羟乙基脲 | 3 | 0.1-6 | |
| 椰油酰胺基丙基甜菜碱 | 8 | 1-15 | |
| 相C | |||
| 乙二醇二硬脂酸酯 | 3.5 | 0.5-7 | |
| DMDM乙内酰脲 | 0.1 | 0.01-0.2 | |
| 相D | |||
| 香料 | 1.1 | 0.1-3 | |
| 柠檬酸溶液 | 0.04 | 0.005-0.1 | |
| 氯化钠 | 2 | 0.1-5 | |
| 总计 | 100 | 100 |
实施例4
另一实施例中，可以将表3配方中6％羟乙基脲用1wt％羟丙基双-羟乙基氯化二甲铵(COLATM Moist 200)和1.5wt％甘油代替。除水之外，所有材料保持相同用量。调节水的量以获得100wt％。
通过将表2中所示的组分组合制得基料，可以制得具有上述各个配方的保湿身体冲洗组合物。该基料，又，用作保湿身体冲洗组合物中的相A。随后将相B组分组合并良好混合以形成相B。随后将相B加到相A中，混合以形成中间组合物。如果期望的话，可以将香料和着色剂加到该中间组合物中并混合直到混合物透明。必要时随后可以加入相C组分并混合以实质上均匀的组合物。需要时随后可以调节该组合物的pH和粘度，由此制得粘度为约12,000～约15,000cPs(采用Brookfield DV-II粘度计第5轴以20rpm在25℃下测量)和pH为约5～6的弱酸性的最终组合物。
除了本文中所述的那些之外，本发明的各种改进对于本领域技术人员从前述说明书来看都是显然的。这些改进也应落入所附权利要求的范围之内。
Claims (17)
1.一种包括蓖麻油的马来酸酯和季铵化氮保湿剂的组合物。
2.权利要求1的组合物，其中包括：
0.1-2重量％的蓖麻油的马来酸酯，和
至多5重量％的季铵化氮保湿剂。
3.权利要求1的组合物，其中进一步包括：
至多15重量％的烷基醚硫酸酯表面活性剂，和
至多15重量％的椰油酰胺基丙基甜菜碱表面活性剂。
4.权利要求1的组合物，其中该季化氮保湿剂选自羟丙基双-羟乙基氯化二甲铵、具有结构：
的材料、胆碱盐、肉毒碱及其组合。
5.权利要求1的组合物，其中该季化氮保湿剂包括羟丙基双-羟乙基氯化二甲铵。
6.权利要求1的组合物，其中该季化氮保湿剂包括肉毒碱。
7.权利要求1的组合物，其中：
所述蓖麻油的马来酸酯的存在量为0.55重量％；和
所述季铵化氮保湿剂的存在量为6重量％。
8.权利要求3的组合物，其中所述烷基醚硫酸酯表面活性剂的存在量为8-10重量％。
9.权利要求3的组合物，其中所述椰油酰胺基丙基甜菜碱表面活性剂存在量为4-6重量％。
10.权利要求1的组合物，其中进一步包括肌酸。
11.权利要求1的组合物，其中进一步包括甘油。
12.权利要求11的组合物，其中所述甘油的存在量基于所述组合物的总重量为1-8重量％。
13.权利要求1的组合物，其中还包括PEG-150二硬脂酸酯和PPG-2羟乙基椰油酰胺。
14.权利要求3的组合物，其中包括：
0.55重量％的蓖麻油的马来酸酯，
6重量％的季铵化氮保湿剂，
8至10重量％的烷基醚硫酸酯表面活性剂，
4至6重量％的椰油酰胺基丙基甜菜碱表面活性剂，和
6重量％的甘油。
15.一种保湿皮肤、毛发和/或指甲的方法，该方法包括施用有效量的权利要求1的组合物到皮肤、毛发和/或指甲上。
16.权利要求15的方法，该方法进一步包括从皮肤、毛发和/或指甲上冲洗该组合物。
17.权利要求1的组合物的用途，用于将选自香料、遮光剂、颜料、驱虫剂和/或疏水材料的物质沉积到皮肤、毛发和/或指甲上，其中所述物质被包括在权利要求1的组合物中，并且所述组合物是施用到皮肤、毛发和/或指甲上。
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US71112105P | 2005-08-25 | 2005-08-25 | |
| US60/711121 | 2005-08-25 |
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| CN2006800400370A Division CN101296684B (zh) | 2005-08-25 | 2006-08-24 | 保湿组合物 |
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| CN101856315A true CN101856315A (zh) | 2010-10-13 |
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| CN2006800400370A Expired - Fee Related CN101296684B (zh) | 2005-08-25 | 2006-08-24 | 保湿组合物 |
| CN2010102108864A Pending CN101897654A (zh) | 2005-08-25 | 2006-08-24 | 保湿组合物 |
| CN201010210877A Pending CN101856315A (zh) | 2005-08-25 | 2006-08-24 | 保湿组合物 |
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| CN2006800400370A Expired - Fee Related CN101296684B (zh) | 2005-08-25 | 2006-08-24 | 保湿组合物 |
| CN2010102108864A Pending CN101897654A (zh) | 2005-08-25 | 2006-08-24 | 保湿组合物 |
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| Country | Link |
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| US (1) | US8703160B2 (zh) |
| EP (3) | EP1916992A2 (zh) |
| KR (3) | KR101228726B1 (zh) |
| CN (3) | CN101296684B (zh) |
| AU (3) | AU2006282979B2 (zh) |
| BR (1) | BRPI0615115A2 (zh) |
| CA (1) | CA2619910C (zh) |
| MX (1) | MX2008002686A (zh) |
| MY (3) | MY151919A (zh) |
| RU (3) | RU2376977C1 (zh) |
| WO (1) | WO2007025093A2 (zh) |
| ZA (1) | ZA200801711B (zh) |
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-
2006
- 2006-08-24 KR KR1020107011412A patent/KR101228726B1/ko not_active Expired - Fee Related
- 2006-08-24 CN CN2006800400370A patent/CN101296684B/zh not_active Expired - Fee Related
- 2006-08-24 MX MX2008002686A patent/MX2008002686A/es not_active Application Discontinuation
- 2006-08-24 EP EP06802302A patent/EP1916992A2/en not_active Ceased
- 2006-08-24 MY MYPI20080333 patent/MY151919A/en unknown
- 2006-08-24 CN CN2010102108864A patent/CN101897654A/zh active Pending
- 2006-08-24 WO PCT/US2006/033162 patent/WO2007025093A2/en active Application Filing
- 2006-08-24 CA CA2619910A patent/CA2619910C/en not_active Expired - Fee Related
- 2006-08-24 BR BRPI0615115-9A patent/BRPI0615115A2/pt not_active IP Right Cessation
- 2006-08-24 RU RU2008111155/15A patent/RU2376977C1/ru not_active IP Right Cessation
- 2006-08-24 KR KR1020087007091A patent/KR101001091B1/ko not_active Expired - Fee Related
- 2006-08-24 EP EP10154399A patent/EP2191817A1/en not_active Ceased
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- 2006-08-24 KR KR1020107011411A patent/KR101228786B1/ko not_active Expired - Fee Related
- 2006-08-24 US US11/466,940 patent/US8703160B2/en active Active
- 2006-08-24 CN CN201010210877A patent/CN101856315A/zh active Pending
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- 2009-08-25 RU RU2009132057/15A patent/RU2009132057A/ru unknown
- 2009-10-19 AU AU2009227846A patent/AU2009227846A1/en not_active Abandoned
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Also Published As
| Publication number | Publication date |
|---|---|
| KR20080037116A (ko) | 2008-04-29 |
| AU2009227847A1 (en) | 2009-11-05 |
| CN101296684A (zh) | 2008-10-29 |
| BRPI0615115A2 (pt) | 2013-01-01 |
| CN101296684B (zh) | 2012-10-10 |
| KR20100061866A (ko) | 2010-06-09 |
| MY179229A (en) | 2020-11-02 |
| MX2008002686A (es) | 2008-03-18 |
| US8703160B2 (en) | 2014-04-22 |
| KR101228786B1 (ko) | 2013-01-31 |
| AU2006282979A1 (en) | 2007-03-01 |
| US20070048235A1 (en) | 2007-03-01 |
| EP2191817A1 (en) | 2010-06-02 |
| KR20100061867A (ko) | 2010-06-09 |
| WO2007025093A3 (en) | 2007-06-14 |
| KR101001091B1 (ko) | 2010-12-14 |
| RU2008111155A (ru) | 2009-09-27 |
| RU2009132056A (ru) | 2011-02-27 |
| CA2619910C (en) | 2012-03-20 |
| EP2189152A1 (en) | 2010-05-26 |
| CN101897654A (zh) | 2010-12-01 |
| RU2376977C1 (ru) | 2009-12-27 |
| KR101228726B1 (ko) | 2013-02-01 |
| CA2619910A1 (en) | 2007-03-01 |
| AU2006282979B2 (en) | 2010-06-10 |
| EP1916992A2 (en) | 2008-05-07 |
| MY177383A (en) | 2020-09-14 |
| RU2009132057A (ru) | 2011-02-27 |
| AU2009227846A1 (en) | 2009-11-05 |
| MY151919A (en) | 2014-07-31 |
| ZA200801711B (en) | 2009-08-26 |
| WO2007025093A2 (en) | 2007-03-01 |
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