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WO2016076392A1 - Huile/matière grasse en poudre, aliment/boisson comprenant de l'huile/de la matière grasse en poudre, et procédé de production d'huile/de matière grasse en poudre - Google Patents

Huile/matière grasse en poudre, aliment/boisson comprenant de l'huile/de la matière grasse en poudre, et procédé de production d'huile/de matière grasse en poudre Download PDF

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Publication number
WO2016076392A1
WO2016076392A1 PCT/JP2015/081850 JP2015081850W WO2016076392A1 WO 2016076392 A1 WO2016076392 A1 WO 2016076392A1 JP 2015081850 W JP2015081850 W JP 2015081850W WO 2016076392 A1 WO2016076392 A1 WO 2016076392A1
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WIPO (PCT)
Prior art keywords
oil
fat
mass
powdered
treated starch
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PCT/JP2015/081850
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English (en)
Japanese (ja)
Inventor
友希 北谷
伊藤　隆史
野田　竜治
Original Assignee
日清オイリオグループ株式会社
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
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Priority claimed from JP2015215604A external-priority patent/JP6609162B2/ja
Application filed by 日清オイリオグループ株式会社 filed Critical 日清オイリオグループ株式会社
Priority to MYPI2017701684A priority Critical patent/MY194365A/en
Priority to CN201580061704.2A priority patent/CN107109294B/zh
Priority to KR1020177013102A priority patent/KR102509515B1/ko
Priority to EP15859634.6A priority patent/EP3219779B1/fr
Publication of WO2016076392A1 publication Critical patent/WO2016076392A1/fr
Priority to US15/592,706 priority patent/US10993455B2/en

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Classifications

    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS OR COOKING OILS
    • A23D9/00—Other edible oils or fats, e.g. shortenings or cooking oils
    • A23D9/007—Other edible oils or fats, e.g. shortenings or cooking oils characterised by ingredients other than fatty acid triglycerides
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom

Definitions

  • the present invention relates to powdered oil and fat, food and drink containing the powdered oil and fat, and a method for producing the powdered oil and fat.
  • Medium-chain fatty acid triglycerides are more easily digested and absorbed than common vegetable oils, and are easy to use as energy. Therefore, medium-chain fatty acid triglycerides have been used in the medical field for the purpose of energy supplementation for patients with reduced digestive absorption function and recovery of physical strength of patients after surgery. In addition, medium-chain fatty acid triglycerides have been used in the food field for the purpose of increasing the calorie content of the diet of elderly people. When using medium-chain fatty acid triglycerides for the purpose of adding to pharmaceuticals, foods, etc., medium-chain fatty acid triglycerides are not only used as liquid fats but may be used after being prepared in the form of powdered fats and oils. .
  • Powdered oils and fats are used in a wide range of fields because they are easier to mix with other powder raw materials than liquid or solid oils and fats and are easily dispersed and dissolved in water and do not require emulsification. Yes. Techniques relating to the preparation of powdered oils and fats include techniques described in Patent Documents 1 to 3.
  • Powdered oils and fats are required to be easy to handle and have an appearance that does not deteriorate during dissolution. Therefore, powders and fats are required to have high solubility and fluidity as powders and less oil floating during dissolution.
  • medium-chain fatty acid triglycerides are blended with powdered fats and oils at a high rate (for example, 65% by mass or more with respect to the whole powdered fats and oils), the oils are excellent in solubility and fluidity. There was a possibility that a powdered oil with little floating could not be obtained.
  • the present invention has been made in view of such circumstances, and an object of the present invention is to provide powdered fats and oils that contain medium-chain fatty acid triglycerides at a high ratio, have excellent solubility and fluidity, and have less oil floating during dissolution.
  • the present inventors blend an octenyl succinic acid-treated starch mixture containing at least two octenyl succinic acid-treated starches having different viscosities with a medium-chain fatty acid triglyceride in a predetermined ratio and a dextrin having a dextrose equivalent of 10 or more.
  • the present inventors have found that the above-mentioned problems can be solved and completed the present invention.
  • the present invention provides the following.
  • the octenyl succinic acid-treated starch mixture is a first octenyl succinic acid-treated starch whose viscosity at 25 ° C. of a 10% by mass aqueous solution is less than 30 mPa ⁇ s, and the viscosity at 25 ° C. of a 10% by mass aqueous solution is 30 mPa ⁇ s or more.
  • the content of the second octenyl succinic acid-treated starch is 12% by mass or more and 45% by mass or less based on the whole octenyl succinic acid-treated starch mixture,
  • the dextrose equivalent of the dextrin is 10 or more,
  • Content of the said medium chain fatty acid triglyceride is powder oil and fat which is 65 to 85 mass% with respect to the whole said powder oil and fat.
  • a food or drink containing the powdered fat according to any one of (1) to (4).
  • octenyl succinic acid-treated starch mixture containing medium chain fatty acid triglyceride, octenyl succinic acid-treated starch mixture, dextrin, and water; Preparing a powdered fat by dry-pulverizing the oil-in-water emulsion, and
  • the octenyl succinic acid-treated starch mixture is a first octenyl succinic acid-treated starch whose viscosity at 25 ° C. of a 10% by mass aqueous solution is less than 30 mPa ⁇ s, and the viscosity at 25 ° C. of a 10% by mass aqueous solution is 30 mPa ⁇ s or more.
  • the content of the second octenyl succinic acid-treated starch is 12% by mass or more and 45% by mass or less based on the whole octenyl succinic acid-treated starch mixture,
  • the dextrose equivalent of the dextrin is 10 or more,
  • Content of the said medium chain fatty acid triglyceride is a manufacturing method of powdered oil and fat which is 65 to 85 mass% with respect to the said whole powdered oil and fat.
  • a powdered fat that contains a medium-chain fatty acid triglyceride at a high ratio, has excellent solubility and fluidity, and has less oil floating during dissolution.
  • the powdery fat of the present invention comprises medium chain fatty acid triglyceride, octenyl succinic acid treated starch mixture, and dextrin.
  • the powdered fat of the present invention has a structure in which fine oil droplets containing medium-chain fatty acid triglycerides and the like are coated with an octenyl succinic acid-treated starch mixture, dextrin and the like.
  • each component which comprises the powdered fats and oils of this invention is demonstrated.
  • the medium chain fatty acid triglyceride is also referred to as MCT (Medium Chain Triglycerides), and is a triglyceride whose constituent fatty acid is a saturated fatty acid having 6 to 12 carbon atoms (preferably 8 to 10 carbon atoms) (coconut oil decomposing fatty acid and the like).
  • MCT Medium Chain Triglycerides
  • saturated fatty acid having 6 to 12 carbon atoms examples include n-hexanoic acid, n-heptanoic acid, n-octanoic acid, n-nonanoic acid, n-decanoic acid, n-undecanoic acid, and n-dodecanoic acid.
  • saturated fatty acids having an even number of carbon atoms are preferred, and any one or more of saturated fatty acids (n-octanoic acid, n-decanoic acid, and n-dodecanoic acid) having 8, 10, and 12 carbon atoms are preferred.
  • a combination is more preferable, and a saturated fatty acid having 8 and / or 10 carbon atoms (n-octanoic acid and / or n-decanoic acid) is more preferable.
  • the content of medium-chain fatty acid triglycerides in the powdered fats and oils is 65% by mass or more and 85% by mass or less, preferably 70% by mass or more and 85% by mass or less, more preferably 75% by mass or more and 85% with respect to the entire powdered fats and oils. It is below mass%.
  • powder oil and fat containing 65% by mass or more of medium chain fatty acid triglyceride with respect to the whole powder oil and fat is prepared, it is difficult to obtain powder oil and fat having excellent solubility and fluidity and less oil floating at the time of dissolution. there were.
  • the present invention by blending the octenyl succinic acid-treated starch mixture and dextrin, which will be described later, together with the medium chain fatty acid triglyceride, it has excellent solubility and fluidity while containing a medium chain fatty acid triglyceride at a high ratio, It is possible to obtain a powdered oil and fat that has little oil floating and that can impart richness to food.
  • an octenyl succinic acid-treated starch mixture and dextrin which will be described later, in an amount sufficient to exert the effect. Can be blended.
  • fats and oils other than medium chain fatty acid triglycerides may be blended in the powdered fats and oils.
  • Fats and oils other than medium chain fatty acid triglycerides are not particularly limited as long as they are edible fats and oils, but vegetable oils (rapeseed oil, corn oil, soybean oil, cottonseed oil, safflower oil, palm oil, rice bran oil, etc.), animal fats and oils (Beef tallow, lard, milk fat, fish oil, etc.), hardened oil or transesterified oil of these fats, or liquid oil or solid fat obtained by fractionating these fats and oils.
  • These fats and oils may use 1 type (s) or 2 or more types.
  • the content of the fats and oils is preferably 0.0% by mass or more and 10% by mass or less, more preferably 0.0% by mass with respect to the entire powdered fats and oils.
  • the content is 5.0% by mass or less and most preferably 0.0% by mass or more and 3.0% by mass or less. Since the blending in the present invention is particularly suitable when the fat is a medium chain fatty acid triglyceride, it is preferable that the fat or oil other than the medium chain fatty acid triglyceride is not contained in the powdered fat.
  • the content of all fats and oils in the powdered fats and oils is preferably 65 mass% or more and 85 mass% or less, more preferably 70 mass% or more and 85 mass% or less, and most preferably 75 mass% or more and 85 mass% or less.
  • the medium chain fatty acid triglyceride can be produced by a conventionally known method.
  • the medium chain fatty acid triglyceride can be produced by esterifying a medium chain fatty acid and glycerin by a conventional method.
  • the medium chain fatty acid used as a raw material for the medium chain fatty acid triglyceride can be obtained, for example, by hydrolyzing palm kernel oil or palm oil containing the medium chain fatty acid and then refining it.
  • commercially available edible oils and fats such as “ODO” (manufactured by Nissin Oilio Group Co., Ltd.) may be used.
  • the content of medium-chain fatty acid triglycerides in the powdered fats and oils is measured by the following method. First, after the powdered fats and oils are dissolved in hot water, the fats and oils in the powdered fats and oils are extracted by applying the Rose Goth Reeve method. Next, the composition of triglyceride in the oil and fat is measured by gas chromatography, and the content of medium chain fatty acid triglyceride is specified. As a column in gas chromatography, for example, “DB-1ht” manufactured by Agilent Technologies can be used.
  • the powdered fats and oils of the present invention are the first octenyl succinic acid-treated starch whose viscosity at 25 ° C. of a 10% by mass aqueous solution is less than 30 mPa ⁇ s, and second viscosity whose viscosity at 25 ° C. of the 10% by mass aqueous solution is 30 mPa ⁇ s or more. And an octenyl succinic acid-treated starch mixture.
  • the viscosity of the first octenyl succinic acid-treated starch is preferably 1.0 mPa ⁇ s or more and 25 mPa ⁇ s or less, more preferably 2.0 mPa ⁇ s or more and 20 mPa ⁇ s or less, most preferably in a 10% by mass aqueous solution (25 ° C.). Is 5.0 mPa ⁇ s or more and 10 mPa ⁇ s or less.
  • the viscosity of the second octenyl succinic acid-treated starch is preferably 30 mPa ⁇ s or more and 60 mPa ⁇ s or less, more preferably 35 mPa ⁇ s or more and 55 mPa ⁇ s or less, and most preferably 35 mPa ⁇ s, in a 10% by mass aqueous solution (25 ° C.). It is 45 mPa ⁇ s or less.
  • the viscosity of the octenyl succinic acid-treated starch mixture is preferably 8.0 mPa ⁇ s or more and 14.0 mPa ⁇ s or less at 25 ° C. in a 10% by mass aqueous solution.
  • the content of the second octenyl succinic acid-treated starch is 12% by mass or more and 45% by mass or less, preferably 15% by mass or more and 40% by mass or less, more preferably 15% by mass with respect to the whole octenyl succinic acid-treated starch mixture. It is 35 mass% or less, More preferably, it is 15 mass% or more and 30 mass% or less, Most preferably, it is 20 mass% or more and 25 mass% or less.
  • two kinds of octenyl succinic acid-treated starches having different viscosities are blended in the powdered oil and fat, and the first octenyl succinic acid-treated starch is blended more than the second octenyl succinic acid-treated starch, and a high ratio
  • the blending amount of the second octenyl succinic acid-treated starch is less than 12% by mass with respect to the whole octenyl succinic acid-treated starch mixture, the emulsification of the powdered fat becomes unstable, and the fluidity of the powdered fat is likely to be inferior. Oil floatation is likely to occur when powdered oils and fats are dissolved.
  • the blending amount of the second octenyl succinic acid-treated starch is more than 45% by mass with respect to the whole octenyl succinic acid-treated starch mixture, the viscosity of the oil-in-water emulsion prepared from the powdered fats and oils increases, resulting in decreased productivity. Or the solubility of powdered oils and fats tends to decrease.
  • the content of the octenyl succinic acid-treated starch mixture in the powder fat is not particularly limited, but is preferably 5.0% by mass or more and 20% by mass or less, and more preferably 7.0% by mass or more and 18% by mass with respect to the whole powder oil or fat. % Or less, most preferably 10% by mass or more and 15% by mass or less.
  • the content of the octenyl succinic acid-treated starch mixture in the powdered fat is in the above range, it is easy to obtain powdered fat having excellent solubility and fluidity.
  • the octenyl succinic acid-treated starch is not particularly limited as long as the viscosity satisfies the above-mentioned requirements.
  • plant-derived starch potato starch, tapioca starch, corn starch, waxy corn starch, etc.
  • a hydrolyzate thereof with octenyl succinic acid The esterified product can be preferably used.
  • the octenyl succinic acid-treated starch obtained through esterification include those in which one carboxylic acid group in octenyl succinic acid and starch or a hydrolyzate thereof constitute an ester.
  • the other carboxylic acid group that does not constitute the ester in octenyl succinic acid may be free and constitutes a salt such as sodium, potassium, ammonia, or amines. Also good. From the viewpoint that the effect of the present invention is easily achieved, in the octenyl succinic acid-treated starch, the other carboxylic acid group that does not constitute an ester in octenyl succinic acid constitutes a sodium salt (that is, sodium octenyl succinate starch) Is preferred.
  • the first octenyl succinic acid-treated starch and the second octenyl succinic acid-treated starch may be the same type of starch, but may be different types of starch.
  • Each of the first and second octenyl succinic acid-treated starches may be composed of the same kind of starch, but may be one in which different types of starch are mixed to adjust the viscosity.
  • hydrochloric acid, sulfuric acid is used for the octenyl succinic acid-treated starch obtained by esterifying the starch (or the hydrolyzate of the starch) with octenyl succinic acid.
  • a method of treating with acid degradation by amylase and enzymatic degradation with amylase is used for the octenyl succinic acid-treated starch obtained by esterifying the starch (or the hydrolyzate of the starch) with octenyl succinic acid.
  • first and second octenyl succinic acid-treated starches may be those in which the viscosity is adjusted by combining two or more starches within the viscosity range of the first or second octenyl succinic acid-treated starch. Good.
  • the viscosities of the first and second octenyl succinic acid-treated starches are specified by the method shown in the examples.
  • the trade name “Purity Gum BE” (manufactured by Indy Graon)
  • the trade name “Purity Gum 1773” (manufactured by Indy Graon)
  • the trade name “Capsule” (manufactured by Indy Graon)
  • Commercial products such as trade name “Emalstar A1” (manufactured by Matsutani Chemical Co., Ltd.) and trade name “Emalstar 500” (manufactured by Matsutani Chemical Co., Ltd.) may be used.
  • a commercially available product such as “N Creamer 46” (manufactured by Indy Greon) may be used.
  • the content of the octenyl succinic acid-treated starch mixture in powdered oils and fats shall apply mutatis mutandis to the “starch sodium octenyl succinate purity test (1) (2)” described in “Standards for Food, Additives, etc. (Food Sanitation Law)”. Specified by.
  • the powdered fats and oils of this invention contain the dextrin whose dextrose equivalent is 10 or more.
  • the solubility of the powdered oil and fat is easily increased.
  • the shaping property improves by mix
  • dextrin and the above-mentioned octenyl succinic acid-treated starch mixture in combination even if it contains medium-chain fatty acid triglycerides in a high ratio, it is excellent in solubility and fluidity, and it is a powdered oil that has less oil floating when dissolved Can be stably prepared.
  • the dextrose equivalent of dextrin is excellent in solubility and fluidity, and particularly a powdered oil and fat with less oil floating at the time of dissolution is obtained, and further, from the viewpoint of suppressing the sweetness of the powdered oil and fat and suppressing the decrease in flavor of other materials, Preferably they are 10 or more and 50 or less, More preferably, they are 10 or more and 40 or less, More preferably, they are 10 or more and 30 or less, Most preferably, they are 10 or more and 20 or less.
  • the content of dextrin in the powdered oil and fat is preferably 5.0% by mass or more and 30% by mass or less, more preferably, based on the whole of the powdered fat and oil, from the viewpoint that it is easy to obtain powdered oil and fat having good solubility and fluidity. Is 7.0% by mass or more and 20% by mass or less, and most preferably 10% by mass or more and 15% by mass or less.
  • the dextrose equivalent is also called DE (Dextrose Equivalent) and is an index representing the degree of hydrolysis of starch. The higher the value, the more advanced the hydrolysis.
  • the method for producing dextrin is not particularly limited, but hydrolyzes plant-derived starch (rice starch, wheat starch, corn starch, potato starch, tapioca starch, sweet potato starch, starch starch, corn starch, etc.) with acid or enzyme The method of doing is mentioned.
  • the content of dextrin in powdered fats and oils is specified by high performance liquid chromatography.
  • the powdered fats and oils of the present invention may contain known additives as long as the effects of the present invention are not impaired.
  • the kind and blending amount can be appropriately adjusted according to the effect to be obtained.
  • the powdered fats and oils of this invention may contain a small amount of water less than 3.0 mass% with respect to the whole powdered fats and oils.
  • additives include sugars (eg lactose, sucrose, glucose etc.), vitamins (eg vitamin C and vitamin E etc.), thickening polysaccharides (eg gelatin, xanthan gum, gum arabic, gellan gum, locust) Bean gum, tamarind seed gum, carrageenan, agar, pectin, etc.), trace nutrients (eg, calcium, potassium, magnesium, iron, zinc, etc.), antioxidants, fragrances and the like.
  • sugars eg lactose, sucrose, glucose etc.
  • vitamins eg vitamin C and vitamin E etc.
  • thickening polysaccharides eg gelatin, xanthan gum, gum arabic, gellan gum, locust
  • Bean gum tamarind seed gum
  • carrageenan agar
  • pectin agar
  • trace nutrients eg, calcium, potassium, magnesium, iron, zinc, etc.
  • the powdered fats and oils of the present invention may contain at least medium chain fatty acid triglyceride, octenyl succinic acid-treated starch mixture, and dextrin as raw materials.
  • Conventional powdered fats and oils contain proteins (casein and the like) as excipients. In the present invention, even if such proteins are not contained, the powdered fats and oils in which oil floating during dissolution is suppressed. Is obtained.
  • the powdered fats and oils of the present invention do not contain protein, or are prepared as powdered fats and oils containing a very small amount of protein, so that the acidic food (yogurt, vegetable beverages, etc.) that can have an action of aggregating proteins ) And foods for patients with kidney disease that are restricted in protein intake.
  • the powdered fat of the present invention can be obtained by dry-pulverizing an oil-in-water emulsion containing the above-mentioned components (medium chain fatty acid triglyceride, octenyl succinic acid-treated starch mixture, dextrin, etc.).
  • the oil-in-water emulsion is obtained by a known emulsion preparation method.
  • an aqueous phase obtained by dissolving an octenyl succinic acid-treated starch mixture and dextrin in water and an oil phase containing medium-chain fatty acid triglycerides are mixed. After stirring with a homomixer or the like, it can be obtained by homogenizing with a homogenizer or the like.
  • the viscosity of the oil-in-water emulsion is preferably 1200 mPa ⁇ s or less, more preferably 1000 mPa ⁇ s or less.
  • the viscosity of the oil-in-water emulsion is specified with a B-type viscometer (55 ° C., 20 rpm, rotor No. 1 is used. However, if it exceeds 500 mPa ⁇ s, rotor No. 2 is used).
  • the median diameter of the oil droplets of the oil-in-water emulsion is not particularly limited, but is preferably 0.3 ⁇ m or more and 1.5 ⁇ m or less, and more preferably 0 from the viewpoint of easily obtaining a powdered oil with less oil floating when dissolved. 0.5 ⁇ m or more and 1.0 ⁇ m or less, and most preferably 0.6 ⁇ m or more and 0.8 ⁇ m or less.
  • the median diameter of the oil droplets of the oil-in-water emulsion is specified by measuring with a laser diffraction particle size distribution meter described in the examples.
  • a known spray drying method, vacuum freeze drying method, vacuum drying method or the like can be used, but the spray drying method is preferred from the viewpoint of easy preparation of powdered oils and fats.
  • the powdered fats and oils of the present invention are general foods and beverages (bread, Japanese confectionery, Western confectionery, prepared dishes, fried foods, soups, beverages, marine products, mixed powders, etc.), seasonings, health foods, nursing foods (especially kidney diseases) It can be suitably used as a raw material in foods for patients) or the like, or as a material to be added when eating these foods.
  • the powdered fats and oils of the present invention do not need to contain protein, they can be suitably used for foods for patients with kidney disease and acidic foods.
  • the powdered fats and oils of this invention can be ingested as it is, or can be ingested by dissolving in water or the like.
  • the powdered fats and oils of the present invention contain medium-chain fatty acid triglycerides at a high ratio, they are excellent in solubility and fluidity and have less oil floating during dissolution.
  • the solubility of powdered oil / fat refers to the ease of dissolving the powdered oil / fat in water.
  • the fluidity of powdered fats and oils refers to the ease of flow of powdered fats and oils as a powder.
  • oil floating at the time of dissolution refers to oil floating on the surface of an aqueous solution when powdered fats and oils are dissolved in warm water.
  • solubility, fluidity, and oil float at the time of dissolution are evaluated by the method described in the examples.
  • each oil and fat described in Tables 1 and 2 was adjusted to 70 ° C. to prepare an oil phase.
  • the water phase was prepared by dissolving octenyl succinic acid starch, dextrin, and lactose in each oil and fat described in Tables 1 and 2, octenyl succinic acid-treated starch, each dextrin, and water having the same mass as the total mass of lactose.
  • the water phase and the oil phase were homogenized at a pressure of 150 kg / cm 2 using a pressure homogenizer to obtain an oil-in-water emulsion.
  • the obtained oil-in-water emulsion was spray-dried using a nozzle spray dryer to obtain a powdered oil having a water content of 1.8% by mass.
  • the inlet temperature of the spray drying air was set to 210 ° C.
  • Fats and oils B Soybean oil (trade name “soybean white squeezed oil”, manufactured by Nisshin Oillio Group, Inc.)
  • Oil C Hardened rapeseed oil (melting point 36 ° C., manufactured by Miyoshi Oil & Fat Co., Ltd.)
  • Oil D Medium chain fatty acid triglyceride-2 (constituent fatty acid: n-octanoic acid 40% by mass, n-decanoic acid 40% by mass, n-dodecano
  • each octenyl succinic acid-treated starch described in Tables 1 and 2 The details of each octenyl succinic acid-treated starch described in Tables 1 and 2 are as follows.
  • the viscosity of each octenyl succinic acid-treated starch was specified as a viscosity after 30 seconds of measurement with a vibration viscometer (trade name “VIBRO VISCOMETER SV-10”, manufactured by A & D) at 25 ° C. in a 10% by mass solution.
  • octenyl succinate starch sodium A, B, and C correspond to “first octenyl succinate-treated starch”
  • octenyl succinate starch sodium D corresponds to “second octenyl succinate-treated starch”.
  • Sodium octenyl succinate starch A (viscosity 2.22 mPa ⁇ s, trade name “Emulstar A1”, manufactured by Matsutani Chemical Co., Ltd.)
  • Sodium octenyl succinate starch B (viscosity 2.34 mPa ⁇ s, trade name “Capsule”, manufactured by Indy Greon)
  • Sodium octenyl succinate starch C (viscosity 7.14 mPa ⁇ s, trade name “Purity Gum BE”, manufactured by Indy Graon)
  • Sodium octenyl succinate starch D (viscosity 38.7 mPa ⁇ s, trade name “N Creamer 46”, manufactured by Indy Graon)
  • Dextrin D 40, trade name “Paindex # 6”, manufactured by Matsutani Chemical Industry Co., Ltd.)
  • Dextrin E 45, trade name “MR25-45”, manufactured by Shikishima Starch Co., Ltd.)
  • lactose described in Tables 1 and 2 are as follows. Lactose (Brand name “American Grande Dactose 80 Mesh”, made by Grande Custom Ingredients)
  • the ratio of octenyl succinic acid-treated starch D is the ratio of octenyl succinic acid starch D to “amount of octenyl succinic acid-treated starch mixture”.
  • Viscosity of oil-in-water emulsion The viscosity of each oil-in-water emulsion was measured using a B-type viscometer (manufactured by Nihon Keiki Co., Ltd.) at a rotational speed of 20 rpm and a rotor No. 1 or 2 (When exceeding 500 mPa ⁇ s, rotor No. 2 was used.), Measured at a temperature of 55 ° C. for 30 seconds. The results are shown in Tables 1 and 2 under “Viscosity of emulsion before spray drying”.
  • the powdered fats and oils of the present invention were excellent in solubility and fluidity, and had less oil floating during dissolution. Particularly good results were obtained when dextrin having a dextrose equivalent of 11 or 18 was used (Examples 1-5, 7, 12). Furthermore, the “ratio of octenyl succinic acid-treated starch sodium D” (this value corresponds to the content of the second octenyl succinic acid-treated starch with respect to the whole octenyl succinic acid-treated starch mixture) is 16.7% by mass or more and 25.0%. When the content was within the range of mass% or less, remarkably good results were obtained (Examples 2 to 5 and 12).
  • Test 3 Addition and evaluation of powdered fats and oils to miso soup
  • 6 g of the powdered fats and oils of Example 3 were added to 1 cup (160 mL) of a commercial instant miso soup and mixed with a spoon, the powdered fats and oils were quickly dissolved in the miso soup, and no undissolved residue or oil floating was observed.
  • the resulting miso soup had a rich taste and did not impair the original flavor of the miso soup.

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Abstract

L'objectif de la présente invention est de fournir une huile/une matière grasse en poudre qui comprend une proportion élevée d'un triglycéride d'acide gras à chaîne moyenne, présente une solubilité et une fluidité excellentes, et donne lieu à peu de flottaison d'huile durant la dissolution. La présente invention concerne une huile/une matière grasse en poudre qui comprend un triglycéride d'acide gras à chaîne moyenne, un mélange d'amidon traité avec de l'acide octénylsuccinique, et une dextrine, où : le mélange d'amidon traité avec de l'acide octénylsuccinique comprend un premier amidon traité avec de l'acide octénylsuccinique dont la viscosité d'une solution aqueuse de 10 % en masse à 25°C est inférieure à 30 mPa·S, et un second amidon traité avec de l'acide octénylsuccinique dont la viscosité d'une solution aqueuse de 10 % en masse à 25°C est de 30 mPa·S ou plus ; la teneur du second amidon traité avec de l'acide octénylsuccinique est de 12 à 45 % en masse, inclus, par rapport au mélange entier d'amidon traité avec de l'acide octénylsuccinique ; le poids équivalent en dextrose de la dextrine est de 10 ou plus ; et la teneur en triglycéride d'acide gras à chaîne moyenne est de 65 à 85 % en masse, inclus, par rapport à l'huile/à la matière grasse en poudre entière.
PCT/JP2015/081850 2014-11-13 2015-11-12 Huile/matière grasse en poudre, aliment/boisson comprenant de l'huile/de la matière grasse en poudre, et procédé de production d'huile/de matière grasse en poudre WO2016076392A1 (fr)

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MYPI2017701684A MY194365A (en) 2014-11-13 2015-11-12 Powdered oil and/or fat, food and drink containing powdered oil and/or fat, and method for manufacturing powdered oil and/or fat
CN201580061704.2A CN107109294B (zh) 2014-11-13 2015-11-12 粉末油脂、包含该粉末油脂的食品、以及该粉末油脂的制造方法
KR1020177013102A KR102509515B1 (ko) 2014-11-13 2015-11-12 분말유지, 당해 분말유지를 포함하는 음식품, 및 당해 분말유지의 제조방법
EP15859634.6A EP3219779B1 (fr) 2014-11-13 2015-11-12 Huile/matière grasse en poudre, aliment/boisson comprenant de l'huile/de la matière grasse en poudre, et procédé de production d'huile/de matière grasse en poudre
US15/592,706 US10993455B2 (en) 2014-11-13 2017-05-11 Powdered oil and/or fat, food and drink containing powdered oil and/or fat, and method for manufacturing powdered oil and/or fat

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JP2021145602A (ja) * 2020-03-18 2021-09-27 日清オイリオグループ株式会社 改良発酵食品及びその製造方法

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CN109414059A (zh) * 2016-07-04 2019-03-01 日本烟草产业株式会社 吸附剂、具有该吸附剂的吸烟物品用过滤嘴、及具有该吸烟物品用过滤嘴的吸烟物品
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JP2021145602A (ja) * 2020-03-18 2021-09-27 日清オイリオグループ株式会社 改良発酵食品及びその製造方法
JP7604105B2 (ja) 2020-03-18 2024-12-23 日清オイリオグループ株式会社 改良発酵食品及びその製造方法

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