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WO2003035578A1 - Element filtrant ceramique et procede de production associe - Google Patents

Element filtrant ceramique et procede de production associe Download PDF

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Publication number
WO2003035578A1
WO2003035578A1 PCT/RU2002/000453 RU0200453W WO03035578A1 WO 2003035578 A1 WO2003035578 A1 WO 2003035578A1 RU 0200453 W RU0200453 W RU 0200453W WO 03035578 A1 WO03035578 A1 WO 03035578A1
Authority
WO
WIPO (PCT)
Prior art keywords
πορisτοgο
nοsiτelya
filtering
πρi
φilτρuyuschy
Prior art date
Application number
PCT/RU2002/000453
Other languages
English (en)
Russian (ru)
Inventor
Boris Lazarevich Krasny
Sergei Anatolievich Zhuravlev
Petr Petrovich Mamochkin
Andrey Nikolaevich Kislyakov
Khazbechir Asakhmetovich Bazoev
Boris Vasilyevich Parkhaev
Roman Sergeevich Dorodnykh
Original Assignee
Zakrytoe Aktsionernoe Obschestvo Nauchno-Tekhnicheskiy Tsentr 'bakor'
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from RU2001128747/03A external-priority patent/RU2204542C1/ru
Priority claimed from RU2002100715A external-priority patent/RU2200613C1/ru
Application filed by Zakrytoe Aktsionernoe Obschestvo Nauchno-Tekhnicheskiy Tsentr 'bakor' filed Critical Zakrytoe Aktsionernoe Obschestvo Nauchno-Tekhnicheskiy Tsentr 'bakor'
Priority to EA200201305A priority Critical patent/EA004725B1/ru
Publication of WO2003035578A1 publication Critical patent/WO2003035578A1/fr

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/63—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
    • C04B35/632—Organic additives
    • C04B35/634—Polymers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D33/00—Filters with filtering elements which move during the filtering operation
    • B01D33/15—Filters with filtering elements which move during the filtering operation with rotary plane filtering surfaces
    • B01D33/21—Filters with filtering elements which move during the filtering operation with rotary plane filtering surfaces with hollow filtering discs transversely mounted on a hollow rotary shaft
    • B01D33/23—Construction of discs or component sectors thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D39/00—Filtering material for liquid or gaseous fluids
    • B01D39/14—Other self-supporting filtering material ; Other filtering material
    • B01D39/20—Other self-supporting filtering material ; Other filtering material of inorganic material, e.g. asbestos paper, metallic filtering material of non-woven wires
    • B01D39/2068—Other inorganic materials, e.g. ceramics
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D63/00—Apparatus in general for separation processes using semi-permeable membranes
    • B01D63/08—Flat membrane modules
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D63/00—Apparatus in general for separation processes using semi-permeable membranes
    • B01D63/08—Flat membrane modules
    • B01D63/081—Manufacturing thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
    • B01D71/02—Inorganic material
    • B01D71/024—Oxides
    • B01D71/025—Aluminium oxide
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/10—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on aluminium oxide
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/16—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay
    • C04B35/18—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay rich in aluminium oxide
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/63—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B38/00—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
    • C04B38/08—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by adding porous substances
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
    • C04B2111/00793—Uses not provided for elsewhere in C04B2111/00 as filters or diaphragms
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3217—Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/349—Clays, e.g. bentonites, smectites such as montmorillonite, vermiculites or kaolines, e.g. illite, talc or sepiolite
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
    • C04B2235/448—Sulphates or sulphites

Definitions

  • the filtering layer has a significant disintegration, which reduces the set of the filter in the case of filtering.
  • s ⁇ de ⁇ z haschy ⁇ il ⁇ uyuschy ⁇ a ⁇ as with ⁇ il ⁇ uyuschey and vnu ⁇ enney ⁇ ve ⁇ n ⁇ s ⁇ yami
  • vy ⁇ lnenny as ⁇ ug ⁇ v ⁇ g ⁇ se ⁇ a of ⁇ is ⁇ y ⁇ e ⁇ ami ⁇ i with ⁇ y ⁇ ymi ⁇ ami
  • the membrane layer has a significant dispersion of physical and physical properties in the volume of the filter element, which reduces the overall quality of the product.
  • the membranous layer is designed to establish the network of defects due to shrinkage during drying and sintering, depending on the concentration of the liquid in the suspension and the concentration of the concentrate. This leads to a decrease in the productivity of the device.
  • the filter cartridge is subject to electronic particles
  • a ceramic filter element received by the claimed method is provided; on ⁇ ig. 2 - ⁇ ⁇ ⁇ ⁇ ⁇ ⁇ whatsoever ⁇ tica ⁇ tica ⁇ tica ⁇ tica ⁇ . 5 BEST MODE FOR CARRYING OUT THE INVENTION
  • the method of manufacturing a ceramic filter element includes the preparation of a plastic mass containing components
  • the suspension is applied for the formation of the membrane layer, drying and heat treatment.
  • the resulting plastic mass was coagulated by sowing through a system of 1 mm.
  • a disperse system was used, containing 65> electromotive force and 35% EC. After thorough homogenization in the mixer for 40-50 minutes, the disperse system was applied by spraying on the work
  • the membrane was fixed on a direct-coupled carrier with a shift of 13 + 2 °. With an increase in the temperature, the shear stresses decrease significantly.
  • the filtering case 1 is arranged with sparse particles of 6 electrons with a changing ratio of their dimensions in the direction of the output of the filter.
  • the ratio of the particle size of the filtering part to the size of 0 particle size of the internal part is equal to 0.02 - 0.05.
  • the internal cross-section of unit 5 is performed in such a way that it eliminates the volume of fluid not less than the volume of the filter, which is at least a large volume.
  • ⁇ ns ⁇ u ⁇ tsiya ma ⁇ e ⁇ iala s ⁇ en ⁇ ⁇ il ⁇ uyuscheg ⁇ ⁇ a ⁇ asa 1 of 5 vys ⁇ l ⁇ ny ⁇ s ⁇ e ⁇ b ⁇ azny ⁇ chas ⁇ its 6 ele ⁇ unda ⁇ zv ⁇ lyae ⁇ is ⁇ lyuchi ⁇ d ⁇ lni ⁇ elnuyu ⁇ u ⁇ i ⁇ vuyu and ⁇ y ⁇ uyu ⁇ is ⁇ s ⁇ , ch ⁇ snizhae ⁇ she ⁇ va ⁇ s ⁇ s ⁇ en ⁇ ⁇ nitsaemy ⁇ ⁇ and sves ⁇ i ⁇ minimum vnu ⁇ ennee gid ⁇ avliches ⁇ e s ⁇ ivlenie ⁇ il ⁇ uyuscheg ⁇ ⁇ usa 1.
  • the range of particle sizes is 6;
  • the device works as follows
  • a ceramic disk filter is composed of twelve ceramic filter elements.
  • a ceramic filter element of the disk 5 ceramic filter is partially loaded in the media, ⁇ ⁇ ezul ⁇ a ⁇ e ⁇ s ⁇ sa che ⁇ ez ⁇ us ⁇ ely shaft nachinae ⁇ sya ⁇ tsess ⁇ il ⁇ atsii che ⁇ ez ⁇ is ⁇ y ⁇ il ⁇ uyuschy ⁇ a ⁇ as 1 and 2.
  • the other 5 plants are removed, which is removed due to the installation of the input to the device.
  • the cleaned sediment is a ceramic filter element which is convenient for use with the following loading cycles for the material that is in need of service. 10 ⁇ ⁇ ezul ⁇ a ⁇ e mn ⁇ g ⁇ a ⁇ n ⁇ g ⁇ , tsi ⁇ liches ⁇ g ⁇ is ⁇ lz ⁇ vaniya dis ⁇ v ⁇ g ⁇ ⁇ e ⁇ amiches ⁇ g ⁇ ⁇ il ⁇ a on ⁇ il ⁇ uyuschey ⁇ ve ⁇ n ⁇ s ⁇ i ⁇ is ⁇ g ⁇ ⁇ a ⁇ asa 1 ⁇ b ⁇ azue ⁇ sya ⁇ n ⁇ y sl ⁇ y ⁇ il ⁇ vann ⁇ g ⁇ ⁇ sad ⁇ a, ⁇ y not udalyae ⁇ sya s ⁇ eb ⁇ m.
  • This layer increases the hydraulic power 5 and reduces the productivity of the device.
  • the regenerative regeneration of the filtering process is carried out through the use of a filter 1 by means of the inlet of the generating unit. After leaving the 0 part 5, it generates a regenerative component due to excessive pressure in the empty volume 4.
  • a ceramic filter element 0 is used in the following multiple cyclic conditions in the case of a disk ceramic filter.
  • Table 3 shows the comparative technical results of the experiments on the filtering of the pulses of the copper concentrate, at the rate of 90-91%) the class is minus 44. 5 The performed comparative tests showed that the use of the proposed device in comparison with the known one is better at a temperature of 2 - 2.5.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
  • Filtering Materials (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)

Abstract

L'invention concerne des dispositifs de filtration, en particulier la conception d'éléments filtrants de filtres céramiques à disques. L'invention concerne également des procédés de production associés. Pour augmenter l'efficacité du dispositif, la structure de filtration de l'élément filtrant céramique est constituée de particules sphériques d'électrocorindon, le rapport de leurs dimensions changeant en direction de la sortie de filtrat. Des éléments intérieurs sont disposés en rangées parallèles, dans deux directions perpendiculaires, chaque élément étant constitué de deux cônes tronqués, solidaires de la structure de filtration par la base et reliés entre eux par les surfaces de leur coupe transversale. Le procédé de production d'élément filtrant céramique selon l'invention consiste à introduire un électrocorindon M40, une bentonite et une pâte sulfate-alcool sous forme de liant technologique dans un mélange plastique, pendant la préparation de ce mélange. Pendant la formation, deux composants d'un support poreux sont pressés pour obtenir une représentation miroir, et frittés à la température de fusion de la bentonite. Avant l'assemblage, les plans de montage des composants résultants sont traités et des éléments collants sont disposés sur lesdits plans.
PCT/RU2002/000453 2001-10-26 2002-10-15 Element filtrant ceramique et procede de production associe WO2003035578A1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
EA200201305A EA004725B1 (ru) 2001-10-26 2002-10-15 Керамический фильтрующий элемент и способ его изготовления

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
RU2001128747/03A RU2204542C1 (ru) 2001-10-26 2001-10-26 Способ получения керамического фильтрующего элемента
RU2001128747 2001-10-26
RU2002100715A RU2200613C1 (ru) 2002-01-17 2002-01-17 Сектор дискового керамического фильтра
RU2002100715 2002-01-17

Publications (1)

Publication Number Publication Date
WO2003035578A1 true WO2003035578A1 (fr) 2003-05-01

Family

ID=26654100

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/RU2002/000453 WO2003035578A1 (fr) 2001-10-26 2002-10-15 Element filtrant ceramique et procede de production associe

Country Status (2)

Country Link
EA (1) EA004725B1 (fr)
WO (1) WO2003035578A1 (fr)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2004071630A1 (fr) * 2003-02-13 2004-08-26 Itn Nanovation Gmbh Couche inorganique
WO2014191634A1 (fr) * 2013-05-31 2014-12-04 Outotec (Finland) Oy Élément de filtration et son procédé de fabrication
CN108295548A (zh) * 2018-02-06 2018-07-20 烟台桑尼核星环保设备有限公司 一种过滤机用盘片及制造方法

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1036704A1 (ru) * 1981-12-25 1983-08-23 Всесоюзный научно-исследовательский институт фарфоро-фаянсовой промышленности Шихта дл изготовлени пористой керамики
DE3641057A1 (de) * 1985-10-11 1988-06-16 Valmet Oy Verfahren zur plattenherstellung, filterplatte und saugtrocknungsvorrichtung
SU1661167A1 (ru) * 1988-10-03 1991-07-07 Государственный научно-исследовательский институт строительной керамики Способ изготовлени керамических фильтрующих элементов
SU1731762A1 (ru) * 1989-06-01 1992-05-07 Государственный научно-исследовательский институт строительной керамики Способ изготовлени керамических фильтрующих элементов
US5232598A (en) * 1989-10-12 1993-08-03 Ceramesh Limited Porous inorganic membranes
US6074457A (en) * 1996-01-04 2000-06-13 Exxon Chemical Patents Inc. Molecular sieves and processes for their manufacture

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1036704A1 (ru) * 1981-12-25 1983-08-23 Всесоюзный научно-исследовательский институт фарфоро-фаянсовой промышленности Шихта дл изготовлени пористой керамики
DE3641057A1 (de) * 1985-10-11 1988-06-16 Valmet Oy Verfahren zur plattenherstellung, filterplatte und saugtrocknungsvorrichtung
SU1661167A1 (ru) * 1988-10-03 1991-07-07 Государственный научно-исследовательский институт строительной керамики Способ изготовлени керамических фильтрующих элементов
SU1731762A1 (ru) * 1989-06-01 1992-05-07 Государственный научно-исследовательский институт строительной керамики Способ изготовлени керамических фильтрующих элементов
US5232598A (en) * 1989-10-12 1993-08-03 Ceramesh Limited Porous inorganic membranes
US6074457A (en) * 1996-01-04 2000-06-13 Exxon Chemical Patents Inc. Molecular sieves and processes for their manufacture

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2004071630A1 (fr) * 2003-02-13 2004-08-26 Itn Nanovation Gmbh Couche inorganique
WO2014191634A1 (fr) * 2013-05-31 2014-12-04 Outotec (Finland) Oy Élément de filtration et son procédé de fabrication
CN108295548A (zh) * 2018-02-06 2018-07-20 烟台桑尼核星环保设备有限公司 一种过滤机用盘片及制造方法

Also Published As

Publication number Publication date
EA200201305A1 (ru) 2004-04-29
EA004725B1 (ru) 2004-08-26

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