KR930004340A - 아크릴아미드 단량체의 단독중합체의 안정한 마이크로 에멀션 제조방법 - Google Patents
아크릴아미드 단량체의 단독중합체의 안정한 마이크로 에멀션 제조방법 Download PDFInfo
- Publication number
- KR930004340A KR930004340A KR1019920015661A KR920015661A KR930004340A KR 930004340 A KR930004340 A KR 930004340A KR 1019920015661 A KR1019920015661 A KR 1019920015661A KR 920015661 A KR920015661 A KR 920015661A KR 930004340 A KR930004340 A KR 930004340A
- Authority
- KR
- South Korea
- Prior art keywords
- homopolymer
- stable microemulsion
- acrylamide
- aqueous phase
- acrylamide monomer
- Prior art date
Links
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical group NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 title claims 4
- 239000004530 micro-emulsion Substances 0.000 title claims 4
- 229920001519 homopolymer Polymers 0.000 title claims 2
- 238000004519 manufacturing process Methods 0.000 title 1
- 239000008346 aqueous phase Substances 0.000 claims 3
- 238000000034 method Methods 0.000 claims 2
- 239000000178 monomer Substances 0.000 claims 2
- 239000012074 organic phase Substances 0.000 claims 2
- 239000004215 Carbon black (E152) Substances 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- -1 aliphatic monocarboxylic acids Chemical class 0.000 claims 1
- 150000001991 dicarboxylic acids Chemical class 0.000 claims 1
- 229930195733 hydrocarbon Natural products 0.000 claims 1
- 150000002430 hydrocarbons Chemical class 0.000 claims 1
- 239000002736 nonionic surfactant Substances 0.000 claims 1
- 229920000642 polymer Polymers 0.000 claims 1
- 238000006116 polymerization reaction Methods 0.000 claims 1
- 230000000379 polymerizing effect Effects 0.000 claims 1
- 150000003839 salts Chemical class 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
- 239000004094 surface-active agent Substances 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F20/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride, ester, amide, imide or nitrile thereof
- C08F20/02—Monocarboxylic acids having less than ten carbon atoms, Derivatives thereof
- C08F20/52—Amides or imides
- C08F20/54—Amides, e.g. N,N-dimethylacrylamide or N-isopropylacrylamide
- C08F20/56—Acrylamide; Methacrylamide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F120/00—Homopolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride, ester, amide, imide or nitrile thereof
- C08F120/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
- C08F120/52—Amides or imides
- C08F120/54—Amides, e.g. N,N-dimethylacrylamide or N-isopropylacrylamide
- C08F120/56—Acrylamide; Methacrylamide
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Polymerisation Methods In General (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
- Glass Compositions (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
Description
Claims (2)
- 아크릴아미드 단량체로 구성되는 수성상 및 탄화수소 오일 및 약 6-약 10범위의 HLB를 가지는 비이온성 계면활성제로 구성되는 유기상을 형성하고, 이때, 계면 활성제 대 아크릴아미드의 비가 약 0.3-1.4대 1의 범위이며, 약0.5:1-약 3:1의 수성상 대 유기상의 비로 수성상에 유기상을 첨가하여 마이크로 에멀션을 형성하고, 약 100℃이하로 발열을 유지하면서 상기 단량체를 중합하고 결과로 생긴 깨끗하고 안정한 마이크로 에멀션을 회소하는 것으로 구성되는 외부로부터 첨가된 산염의부재하에 적어도 15%의 중합체 고체 농도의 아크릴아미드 단량체의 단독중합체의 안정한 마이크로 에멀션의 제조방법.
- 제1항에 있어서, 광산, 지방족 모노카르복실산 또는 디카르복실산과 함께 중합하기 앞서 수성상의 pH를 7.0 또는 이하로 조정하는 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US75281091A | 1991-08-30 | 1991-08-30 | |
US7/752810 | 1991-08-30 | ||
US07/752810 | 1991-08-30 |
Publications (2)
Publication Number | Publication Date |
---|---|
KR930004340A true KR930004340A (ko) | 1993-03-22 |
KR100232798B1 KR100232798B1 (ko) | 1999-12-01 |
Family
ID=25027947
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019920015661A KR100232798B1 (ko) | 1991-08-30 | 1992-08-29 | 아크릴아미드 단량체의 단독중합체의 안정한 마이크로에멀션 제조 방법 |
Country Status (15)
Country | Link |
---|---|
US (1) | US5545688A (ko) |
EP (1) | EP0529206B1 (ko) |
JP (1) | JPH05194613A (ko) |
KR (1) | KR100232798B1 (ko) |
AT (1) | ATE141095T1 (ko) |
AU (1) | AU650158B2 (ko) |
BR (1) | BR9203356A (ko) |
CA (1) | CA2077097A1 (ko) |
DE (1) | DE69212627T2 (ko) |
DK (1) | DK0529206T3 (ko) |
ES (1) | ES2090410T3 (ko) |
IE (1) | IE75670B1 (ko) |
MX (1) | MX9204814A (ko) |
TW (1) | TW223088B (ko) |
ZA (1) | ZA926546B (ko) |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5785730A (en) * | 1996-09-12 | 1998-07-28 | Calgon Corporation | Fertilizer and method for preparing the same |
US5776350A (en) * | 1996-09-12 | 1998-07-07 | Calgon Corporation | Separation of raw agricultural waste |
WO2003062289A1 (es) * | 2001-12-31 | 2003-07-31 | Acideka, S.A. | Procedimiento para la produccion de microemulsiones inversas de copolimeros cationicos |
US7918891B1 (en) | 2004-03-29 | 2011-04-05 | Nuvasive Inc. | Systems and methods for spinal fusion |
WO2005103091A1 (en) * | 2004-04-21 | 2005-11-03 | Ciba Specialty Chemicals Water Treatments Limited | Composition and method of preparing high solid emulsions |
US8673005B1 (en) | 2007-03-07 | 2014-03-18 | Nuvasive, Inc. | System and methods for spinal fusion |
US8083796B1 (en) | 2008-02-29 | 2011-12-27 | Nuvasive, Inc. | Implants and methods for spinal fusion |
USD754346S1 (en) | 2009-03-02 | 2016-04-19 | Nuvasive, Inc. | Spinal fusion implant |
US9198765B1 (en) | 2011-10-31 | 2015-12-01 | Nuvasive, Inc. | Expandable spinal fusion implants and related methods |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2524895A1 (fr) * | 1982-04-09 | 1983-10-14 | Inst Francais Du Petrole | Procede de preparation de microlatex en phase huileuse continue par polymerisation en micro-emulsion du type eau dans l'huile d'un monomere hydrosoluble, microlatex obtenus et leur utilisation en recuperation assistee du petrole |
NO165879C (no) * | 1984-06-07 | 1991-04-24 | Inst Francais Du Petrole | Fremgangsmaate for fremstilling av en invers, stabil mikrolateks. |
FR2567525B1 (fr) * | 1984-07-13 | 1987-03-20 | Inst Francais Du Petrole | Procede de preparation de microlatex inverses et les microlatex inverses obtenus |
FR2617172B1 (fr) * | 1987-06-25 | 1993-07-02 | Charbonnages Ste Chimique | Preparation de microlatex inverses utilisables comme adjuvants de flottation et de drainage ainsi que pour l'absorption et la retention de fluides aqueux |
US5041503A (en) * | 1988-12-19 | 1991-08-20 | American Cyanamid Company | Micro-emulsified glyoxalated acrylamide polymers |
-
1992
- 1992-05-25 DE DE69212627T patent/DE69212627T2/de not_active Revoked
- 1992-05-25 ES ES92108768T patent/ES2090410T3/es not_active Expired - Lifetime
- 1992-05-25 DK DK92108768.0T patent/DK0529206T3/da active
- 1992-05-25 AT AT92108768T patent/ATE141095T1/de active
- 1992-05-25 EP EP92108768A patent/EP0529206B1/en not_active Revoked
- 1992-05-27 TW TW081104145A patent/TW223088B/zh active
- 1992-08-20 MX MX9204814A patent/MX9204814A/es not_active IP Right Cessation
- 1992-08-24 JP JP4246026A patent/JPH05194613A/ja active Pending
- 1992-08-27 BR BR929203356A patent/BR9203356A/pt not_active IP Right Cessation
- 1992-08-28 ZA ZA926546A patent/ZA926546B/xx unknown
- 1992-08-28 AU AU21383/92A patent/AU650158B2/en not_active Ceased
- 1992-08-28 CA CA002077097A patent/CA2077097A1/en not_active Abandoned
- 1992-08-28 IE IE922621A patent/IE75670B1/en not_active IP Right Cessation
- 1992-08-29 KR KR1019920015661A patent/KR100232798B1/ko not_active IP Right Cessation
-
1995
- 1995-05-24 US US08/448,947 patent/US5545688A/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
ES2090410T3 (es) | 1996-10-16 |
AU650158B2 (en) | 1994-06-09 |
BR9203356A (pt) | 1993-03-30 |
US5545688A (en) | 1996-08-13 |
AU2138392A (en) | 1993-03-04 |
JPH05194613A (ja) | 1993-08-03 |
DK0529206T3 (da) | 1996-09-02 |
IE922621A1 (en) | 1993-03-10 |
TW223088B (ko) | 1994-05-01 |
DE69212627T2 (de) | 1997-03-06 |
MX9204814A (es) | 1993-02-01 |
EP0529206A1 (en) | 1993-03-03 |
EP0529206B1 (en) | 1996-08-07 |
ZA926546B (en) | 1993-03-05 |
ATE141095T1 (de) | 1996-08-15 |
CA2077097A1 (en) | 1993-03-01 |
DE69212627D1 (de) | 1996-09-12 |
KR100232798B1 (ko) | 1999-12-01 |
IE75670B1 (en) | 1997-09-10 |
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