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KR900000463A - 윤활유 조성물 및 농축물 - Google Patents

윤활유 조성물 및 농축물 Download PDF

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Publication number
KR900000463A
KR900000463A KR1019890007127A KR890007127A KR900000463A KR 900000463 A KR900000463 A KR 900000463A KR 1019890007127 A KR1019890007127 A KR 1019890007127A KR 890007127 A KR890007127 A KR 890007127A KR 900000463 A KR900000463 A KR 900000463A
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KR
South Korea
Prior art keywords
oil composition
group
polyamine
alcohol
composition
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Application number
KR1019890007127A
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English (en)
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KR930010526B1 (en
Inventor
유진 리플 데이빗
윌리엄 슈록 캘빈
Original Assignee
지이 아아르 힐
더 루우브리졸 코오포레이션
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Publication of KR900000463A publication Critical patent/KR900000463A/ko
Application granted granted Critical
Publication of KR930010526B1 publication Critical patent/KR930010526B1/ko

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Abstract

내용 없음

Description

윤활유 조성물 및 농축물
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
제1도는 주워진 점도를 유지시키는데 필요한 중합체 점도 항상제 및 두 분산제의 농도의 관계를 나타내는 그래프이다.

Claims (105)

  1. (A) 윤활 점도의 오일다량, (B) (B-1)값이 약 1300 내지 약 5000이고값이 약 1.5 내지 약 4.5인 것을 특징으로 하는 폴리알켄으로부터 치환체 기와 숙신산 기로 이루어져 있으며, 그 구조내에 치환체 기 각각의 당량에 대해 평균적으로 최소한 1.3의 숙신산 기가 존재하는 것을 특징으로 하는, 최소한 하나의 치환된 숙신산 아실화제 1당량당(B-2) 그 구조내에 최소한 하나의 HN＜기가 존재하는 것을 특징으로 하는, 최소한 하나의 아민 약 0.70당량-1당량을 반응시킴으로써 제조된, 최소한 하나의 카르복실산 유도체 조성물 소량, 및 (C), (C-1) 디티오인산은, 최소한 10몰%의 이소프로필 알코올 및 약 3-약13개의 탄소 원자를 함유하는 최소한 하나의 일차 지방족 알코올을 포함하는 알코올 혼합물과 오황화인을 반응시킴으로써 제조되고, (C-2) 금속은 제Ⅱ족 금속, 알루미늄, 주석, 철, 코발트, 납, 몰리브덴, 망간, 니켈 또는 구리인, 디히드로카르빌 디티오인산의, 최소한 하나의 금속염 소량을 포함하는, 내부 연소 엔진을 위한 윤활유 조성물.
  2. 제1항에 있어서, 카르복실산 유도체 조성물(B)를 최소한 약 2중량% 함유하는 오일 조성물.
  3. 제1항에 있어서, 카르복실산 유도체 조성물(B)를 최소한 약 2.5중량% 함유하는 오일 조성물.
  4. 제1항에 있어서, (B)에서의값이 최소한 약 1500인 오일 조성물.
  5. 제1항에 있어서, (B)에서의값이 최소한 약 2.0인 오인 조성물.
  6. 제1항에 있어서, (B)에서의 치환체 기가, 2-약 6개의 탄소 원자를 갖는 말단 올레핀의 인터폴리머 및 호모폴리머로 구성된 군으로부터 선택된 하나 이상의 폴리알켄(단, 상기 인터폴리머는 약 6개 이하의 탄소 원자를 갖는 내부 올레핀으로부터 유도된 폴리머 단위체를 약 25% 이하 함유할 수 있음)으로부터 유도되는 오일 조성물.
  7. 제1항에 있어서, (B)에서의 치환체 기가, 폴리부텐, 에틸렌-프로필렌 코폴리머, 폴리프로필렌, 및 이들 중 두개 이상의 어떤 것의 혼합물로 구성된 군으로부터 선택된 요소로부터 유도되는 오일 조성물.
  8. 제1항에 있어서, (B)에서의 치환체 기가 폴리부덴으로부터 유도되고 부텐으로부터 유도된 전체 단위체중 최소한 약 50%는 이소부텐으로부터 유도되는 오일 조성물.
  9. 제1항에 있어서, (B)에서, 1당량의 아실화제(B-1) 당 약 0.70 -약 0.95 당량의 아민(B-2)을 반응시키는 오일 조성물.
  10. 제1항에 있어서, 아민(B-2)이 지방족, 환식지방족 또는 방향족 폴리아민인 오일 조성물.
  11. 제1항에 있어서, 아민(B-2)이 히드록시-치환 모노아민, 폴리아민, 또는 이들의 혼합물인 오일 조성물.
  12. 제1항에 있어서, 아민(B-2)이 하기 일반식(Ⅷ)을 갖는 것을 특징으로 하는 오일 조성물.
    상기식에서, n은 정수 1-약 10이며, 각각의 R3는 독립적으로 수소 원자, 히드로카르빌 기 또는 약 30 개 이하의 원자를 갖는 아미노-치환 또는 히드록시-치환 히드로키르빌 기이거나, 다른 질소 원자 상의 두개의 R3기가 함께 결합하여 U기를 형성할 수 있고, 단, 최소한 하나의 R3기는 수소 원자이고 U는 약 2-약 10개의 탄소 원자를 갖는 알킬렌 기이다.
  13. 제1항에 있어서, (C-1)에서의 일차 지방족 알코일이 약 6-약 13개의 탄소 원자를 함유하는 오일 조성물.
  14. 제1항에 있어서, (C-2)의 금속이 아연, 구리, 또는 아연과 구리의 혼합물인 오일 조성물.
  15. 제1항에 있어서, (C-2)의 금속이 아연인 오일 조성물.
  16. 제1항에 있어서, (C-1)에서의 알코올 혼합물이 최소한 20몰%의 이소프로필 알코올을 포함하는 오일 조성물.
  17. 제1항에 있어서, 하기 일반식(Ⅸ) :
    (상기식에서, R1및 R2는 3-약 10개의 탄소 원자를 함유하는 히드로카르빌 기이고, M은 제 Ⅰ족 금속, 제 Ⅱ족 금속, 알루미늄, 주석, 철, 코발트, 납, 몰리브덴, 망간, 니켈 또는 구리이며, n은 M의 원자가와 같은 정수임)을 특징으로 하는 디히드로카르빌 디티오인산의, 최소한 하나의 부가적인 금속염을 함유하는 오일 조성물.
  18. 제17항에 있어서, 일반식(Ⅸ)에서의 히드로카르빌 기중 최소한 하나가 제이 탄소 원가를 통해 산소원자에 부착된 오일 조성물.
  19. 제17항에 있어서, 일반식(Ⅸ)에서의 R1및 R2가 제이 탄소 원자를 통해 산소원자에 부착된 히드로카르빌 기인 오일 조성물.
  20. 제1항에 있어서, (D)(D-1) 최소한 하나의 치환된 숙신산 아실화제와 (D-2) 하기 일반식(Ⅹ) :
    R3(OH)m (Ⅹ)
    (상기식에서, R3는 탄소결합을 통해 -OH기에 연결된 일가 또는 다가의 유기기이며, m은 정수 1- 약 10임)을 갖는 최소한 하나의 알코올을 반응시킴으로써 제조된 최소한 하나의 카르복실산 에스테르 유도체 조성물을 함유하는 오일 조성물.
  21. 제20항에 있어서, (D-1)에서의 치환된 숙신산 아실화제가,값이 최소한 약 700인 치환제 기 및 숙신산 기로 구성된 오일 조성물.
  22. 제21항에 있어서, (D-1)에서의 치환제 기가, 약 700-약 5000의값을 갖는 폴리알켄으로부터 유도되는 오일 조성물.
  23. 제20항에 있어서, 일반식(Ⅹ)의 알코올(D-2)이 40개 이하의 지방족 탄소 원자룰 함유하는 일가 또는 다가 알코올인 오일 조성물.
  24. 제21항에 있어서, (D-1)에서의 치환제 기가, 폴리부텐, 에틸렌-프롤필렌 코폴리머, 폴리프로필렌, 및 이들 중 두개 이상의 어떤 것의 혼합물로 구성된 군으로부터 선택된 요소로부터 유도되는 오일 조성물.
  25. 제21항에 있어서, (D-1)에서의 치환제 기가 폴리부텐으로부터 유도되고, 폴리부텐으로부터 유도된 전체 단위체 중 최소한 약 50%는 이소부텐으로부터 유도되는 오일 조성물.
  26. 제20항에 있어서 알코올(D-2)이 네오펜틸 글리콜, 에틸렌, 글리콜, 글리세롤, 펜타에리트리톨, 솔리톨, 폴리(옥시알킬렌) 글리콜의 모노-아릴 또는 모노-알킬 에테르, 또는 이들 중 어떤 것의 혼합물인 오일 조성물.
  27. 제20항에 있어서, 약 0.1-약 2몰의 알코올(D-2)을 1몰의 치환된 숙신산 아실화제(D-1)와 반응시키는 오일 조성물.
  28. 제20항에 있어서, 일반식(Ⅹ)에서의 m이 최소한 2인 오일 조성물.
  29. 제20항에 있어서, 아실화제(D-1)와 알코올(D-2)을 반응시킴으로써 제조된 카르복실산 에스테르 유도체 조성물(D)을, (D-3) 최소한 하나의 HM＜기를 함유하는 최소한 하나의 아민과 반응시키는 오일 조성물.
  30. 제29항에 있어서, 아민(D-3)이 폴리아민인 오일 조성물.
  31. 제30항에 있어서, 폴리아민(D-3)이 지방족, 환식지방족 또는 방향족 폴리아민인 오일 조성물.
  32. 제30항에 있어서, 폴리아민(D-3)이 알킬렌 폴리아민인 오일 조성물.
  33. 제30항에 있어서, 폴리아민(D-3)이 하기 일반식(Ⅷ)을 갖는 것을 특징으로 하는 오일 조성물:
    (Ⅷ)
    상기식에서, n은 정수 1-약 10이며, 각각의 R3는 독립적으로 수소 원자, 히드로카르빌 기 또는 약 30개 이하의 원자를 갖는 아미노-치환 또는 히드록시 -치환 히드로카르빌 기이거나, 다른 질소 원자 사의 두개의 R3기가 함께 결합하여 U기를 형성할 수 있고, 단, 최소한 하나의 R3기는 수소 원자이며, U는 약 2 내지 약 10개의 탄소 원자를 갖는 알킬렌 기이다.
  34. 제20항에 있어서, 치환된 숙신산 아실화제(D-1)가,값이 약 1300 내지 약 5000이고값이 약 1.5 내지 약 4.5인 것을 특징으로 하는 폴리알켄으로부터 유도된 치환체 기와 숙신산 기로 구성되고, 그 구조내에 치환제가 각각의 당량에 대해 최소한 약 1.3의 숙신산 기가 존재하는 것을 특징으로 하는 오일 조성물.
  35. 제34항에 있어서, (D-1)에서의 폴리알켄이 최소한 약 1500의 Mn 값과 약 2 내지 약 4의값을 갖는 것을 특징으로 하는 오일 조성물.
  36. 제34항에 있어서, 아실화제의 알코올을 반응시킴으로써 제조된 카르복실산 에스테르를, (D-3) 최소한 하나의 HN＜기를 함유하는 최소한 하나의 아민과 반응시키는 오일 조성물.
  37. 제36항에 있어서, 아민(D-3)이 폴리아민인 오일 조성물.
  38. 제37항에 있어서, 폴리아민(D-3)이 지방족, 환식지방족 또는 방향족 폴리아민인 오일 조성물.
  39. 제37항에 있어서, 폴리아민(D-3)인 알킬렌 폴리아민인 오일 조성물.
  40. 제37항에 있어서, 폴리아민(D-3)이 하기 일반식(Ⅷ)을 갖는 것을 특징으로 하는 오일 조성물 :
    (Ⅷ)
    상기식에서, n은 정수 1- 약 10 개이며, 각각의 R3는 독립적으로 수소 원자, 히드로카르빌 기 또는 약 30개 이하의 원자를 갖는 아미노-치환 또는 히드록시-치환 히드로카르빌 기이거나, 다른 질소 원자 상의 두개의 R3기가 함께 결합하여 U기를 형성할 수 있고, 단, 최소한 하나의 R3기는 수소 원자이며, U는 약 2 내지 약 10개의 탄소 원자를 갖는 알킬렌 기이다.
  41. 제1항에 있어서, (E) 최소한 하나의 산성 유기 화합물의, 최소한 하나의 중성 또는 염기성 알킬리 토금속 염을 함유하는 오일 조성물.
  42. 제41항에 있어서, (E)에서의 산성 유기 화합물이 황산, 카르복실산, 인산, 페놀 또는 이들의 혼합물인 오일 조성물.
  43. 제41항에 있어서, (E)에서의 알칼리 토금속이 칼슘, 마그네슘, 또는 칼슘과 마그네슘의 혼합물인 오일 조성물.
  44. 제41항에 있어서, 알칼리 토금속염(E)이 최소한 약 2의 금속비를 갖는 염기성 금속염인 오일 조성물.
  45. 제41항에 있어서, (E)에서의 산성 화합물이 최소한 하나의 유기 설폰산인 옹리 조성물.
  46. 제45항에 있어서, 유기 설폰산이, 각각 하기 일반식(ⅩⅠ) 및 (ⅩⅡ)로 나타낸 히드록카르빌-치환 방향족 설폰산, 또는 지방족 설폰산인 오일 조성물 :
    Rx-T-(SO3H)y (ⅩⅠ)
    R'-(SO3H)r (ⅩⅡ)
    상기식들에서, R 및 R'는 각각 독립적으로 약 60개 이하의 탄소 원자를 함유하는 지방족기이고, T는 방향족 탄화수소 핵이며, x는 1 내지 3이고, r 및 y는 1 내지 2이다.
  47. 제45항에 있어서, 설폰산이 알킬화된 벤젠 설폰산인 오일 조성물.
  48. 제1항에 있어서, (F) 다가 알코올의, 최소한 하나의 부분적 지방산 에스테르를 함유하는 오일 조성물.
  49. 제48항에 있어서, 다가 알코올의 지방산 에스테르가 글리세롤의 부분적 지방산 에스테르인 오일 조성물.
  50. 제48항에 있어서, 지방산이 약 10-약 22개의 탄소 원자를 함유하는 오일 조성물.
  51. (A) 윤활 점도의 오일다량, (B) (B-1)값이 약 1300 내지 약 5000이고 Mw/Mn 값이 약 2 내지 약 4.5인 것을 특징으로 하는 폴리알켄으로부터 유도된 치환제 기와, 숙신산 기로 이루어져 있으며, 그 구조내에 치환체 기 각각의 당량에 대해 평균적으로 최소한 1.3의 숙신산 기가 존재하는 것을 특징으로 하는, 최소한 하나의 치환된 숙신산 아실화제 1당량 당 (B-2) 그 구조내에 최소한 하나의 HN＜기가 존재하는 것을 특징으로 하는, 최소한 하나의 아민 약 0.70당량-약 0.95당량을 반응시킴으로써 제조된, 최소한 하나의 카르복실산 유도체 조성물 약 0.5-약 10중량% (C) (C-1) 디티오인산은, 최소한 10몰%의 이소프로필 알코올 및 약 3-약 13개의 탄소원자를 함유하는 최소한 하나의 일차 지방족 알코올을 포함하는 알코올 혼합물과 오황화인을 반응시킴으로써 제조되고, (C-2)금속은 제Ⅱ족 금속, 알루미늄, 주석, 철, 코발트, 납, 몰리브덴, 망간, 니켈, 또는 구리인, 디리드로카르빌 디티오인산의, 최소한 하나의 금속염 약 0.05-약 5중량%, (D) (D-1) 최소한 하나의 치환된 숙신산 아실화제와 (D-2)하기 일반식(Ⅹ) :
    R3(OH)m (Ⅹ)
    (상기식에서, R는 탄소 결합을 통해 -OH기에 연결된 일가 또는 다가 유기기이고, m은 정수 2- 약 10임)을 갖는 최소한 하나의 알코올을 반응시킴으로써 제조된, 최소한 하나의 카르복실산 에스테르 유도체 조성물 0.1 내지 약 10%, 및 (E) 황산, 카르복실산, 인산, 페놀, 및 상기 산들의 혼합물로 구성된 군으로부터 선택된 유기산 화합물의, 최소한 하나의 알카리 토금속염 약 0.01- 약 5중량%를 포함하는, 내부 연소 엔진을 위한 윤활유 조성물.
  52. 제51항에 있어서, 카르복실산 유도체 조성물(B)를 최소한 약 2.0중량% 함유하는 오일 조성물.
  53. 제51항에 있어서, 카르복실산 유도체 조성물(B)를 최소한 약 2.5중량%를 함유하는 오일 조성물.
  54. 제51항에 있어서, 아민(B-2)이 하기 일반식(Ⅷ)을 갖는 것을 특징으로 하는 오일 조성물:
    상기식에서, n은 정수 1- 약 10이며, 각각의 R3는 독립적으로 수소 원자. 히드로카르빌 기 또는 약 30개 이하의 원자를 갖는 아미노-치환 또는 히드록시-치환 히드로카르빌 기이거나, 다른 질소 원자 상의 두개의 R3가기 함께 결합하여 U기를 형성할 수 있고, 단, 최소한 하나의 R3기는 수소 원자이며, U는 약 2- 약 10개의 탄소 원자를 갖는 알킬렌 기이다.
  55. 제51항에 있어서, (C-1)에서의 일차 지방족 알코올이 약 6-약13개의 탄소 원자를 함유하는 오일 조성물.
  56. 제51항에 있어서, (C-2)의 금속이 아연, 구리, 또는 아연과 구리의 혼합물인 오일 조성물.
  57. 제51항에 있어서, (C-2)의 금속이 아연인 오일 조성물.
  58. 제51항에 있어서, (C-1)에서의 알코올 혼합물이 최소한 20몰%의 이소프로필 알코올을 포함하는 오일 조성물.
  59. 제51항에 있어서, 치환된 숙신산 아실화제(D-1)가, 최소한 약700의값을 갖는 치환체 기와 숙신산 기로 구성되는 오일 조성물.
  60. 제51항에 있어서, 치환제 기가, 약 700-약 5000의값을 갖는 폴리알켄으로부터 유도되는 오일 조성물.
  61. 제51항에 있어서, 알코올(D-2)이 40개 이하의 지방족 탄소 원자를 함유하는 일가 또는 다가 알코올인 오일 조성물.
  62. 제59항에 있어서, 치환체 기가, 폴리부텐, 에틸렌-프로필렌 코폴리머, 폴리프로필렌, 및 이들 중 두 개 이상의 어떤 것의 혼합물로 구성된 군으로부터 선택된 요소로부터 유도되는 오일 조성물.
  63. 제59항에 있어서, 치환체 기가 폴리부텐으로부터 유도되고, 폴리부텐으로부터 유도된 전체 단위체충 최소한 약 50%는 이소부텐으로부터 유도되는 오일 조성물.
  64. 제51항에 있어서, 알코올(D-2)이 네로펜틸 글리콜, 에틸렌글리콜, 글리세롤, 펜타에리트리톨, 솔비톨, 폴리(옥시알킬렌) 글리콜의 모노-아릴 또는 모노-알킬 에테르, 또는 이들 중 어떤 것의 혼합물인 오일 조성물.
  65. 제51항에 있어서, 약 0.1 -약 2몰의 알코올(D-2)을 1몰의 치횐된 숙신산 아실화체(D-1)와 반응시키는 오일 조성물.
  66. 제51항에 있어서, 일반식(Ⅹ)에서의 m이 최소한 2인 오일 조성물.
  67. 제51항에 있어서, (D)의 카르복실산 에스테르를, 최소한 하나의 HN＜기를 함유하는 최소한 하나의 폴리아민(D-3)과 반응시키는 오일 조성물.
  68. 제67항에 있어서, 아민(D-3)이 최소한 하나의 폴리아민인 오일 조성물.
  69. 제68항에 있어서, 폴리아민(D-3)이 지방족, 환식지방족 또는 방향족 폴리아민인 오일 조성물.
  70. 제68항에 있어서, 폴리아민(D-3)이 하기 일반식(Ⅷ)을 갖는 특징으로 하는 오일 조성물 :
    상기식에서, n은 정수 1-약 10이며, 각각의 R3는 독립적으로 수소 원자, 히드로카르빌 기 또는 약 30개 이하의 원자를 갖는 아미노-치환 또는 히드록시-치환 히드로카르빌 기이거나, 다른 질소 원자 상의 두개의 R3기가 함께 결합하여 U기를 형성할 수 있고, 단, 최소한 하나의 R3기는 수소 원자이며, U는 약 2 내지 약 10개의 탄소 원자를 갖는 알킬렌 기이다.
  71. 제51항에 있어서, Mn 값이 약 1300 내지 약 5000이고 Mw/Mn 값이 약 1.5 내지 약 4.5인 것을 특징으로 하는 폴리알켄으로부터 유도된 치환제 기와 숙신산 기로 구성되고, 그 구조내에 치환체 기 각각의 당량에 대해 최소한 약 1.3의 숙신산 기가 존재하는 것을 특징으로 하는, 치환된 숙신산 아실화제(D-1)를, 알코올(D-2)과 반응시키는 오일 조성물.
  72. 제71항에 있어서, 폴리알켄이 최소한 약 1500의 Mn값과 약 2 내지약 4.5의값을 갖는 것을 특징으로 하는 오일 조성물.
  73. 제71항에 있어서, 카르복실산 에스테르 유도체 조성물을, 최소한 하나의 HN＜기를 함유하는 최소한 하나의 폴리하민(D-3)과 반응시키는 오일 조성물.
  74. 제73항에 있어서, 아민이 폴리아민인 오일 조성물.
  75. 제74항에 있어서, 폴리아민이 지방족, 환식지방종 또는 방향족 폴리아민인 오일 조성물.
  76. 제74항에 있어서, 폴리아민이 알킬렌 폴리아민인 오일 조성물.
  77. 제74항에 있어서, 폴리아민이 하기 일반식(Ⅷ)을 갖는 것을 특징으로 하는 오일 조성물
    상기식에서, n은 정수 1-약 10이며, 각각의 R3는 독립적으로 수소 원자. 히드로카르빌 기 또는 약 30개 이하의 원자를 갖는 아미노-치환 또는 히드록시-치환 히드로카르빌 기이거나, 다른 질소 원자 상의 두개의 R3기가 함께 결합하여 U기를 형성할 수 있고, 단, 최소한 하나의 R2기는 수소 원자이며, U는 약 2 내지 약 10개의 탄소 원자를 갖는 알킬렌 기이다.
  78. 제51항에 있어서, (F) 다가 알코올의, 최소한 하나의 부분적 지방산 에스테르를 약 0.01-2중량% 함유하는 오일 조성물.
  79. 제78항에 있어서, 다가 알코올이 글리세롤인 오일 조성물.
  80. 제78항에 있어서, 지방산이 약 10-약 22개의 탄소 원자를 함유하는 오일 조성물.
  81. (A) 윤활 점도의 오일다량, (B) (B-1) Mn 값이 약 1300 내지 약 5000이고값이 약 2 내지 4인 것을 특징으로 하는 폴리알켄으로부터 유도된 치환체 기와 숙신산 기로 이루어져 있으며, 그 구조내에 치환체 기 각각의 당량에 대해 평균적으로 최소한 1.3의 숙신산 기가 존재하는 것을 특징으로 하는, 최소한 하나의 치환된 숙신산 아실화제 1당량 당(B-2) 그 구조내에 최소한 하나의 HN＜기가 존재하는 것을 특징으로 하는, 최소한 하나의 폴리아민 약 0.75 당량-약 0.90당량을 반응시킴으로써 제조된, 최소한 하나의 카르복실산 유도체 조성물 약 2-약 10중량%, (C)(C-1) 디티오인산은, 최소한 약 20몰%의 이소프로필 알코올 및 약 6 - 약 13개의 탄소원자를 함유하는 최소한 하나의 일차 지방족 알코올을 포함하는 알코올 혼합물과 오황화인을 반응시킴으로써 제조되고, (C-2) 금속은 제Ⅱ족 금속, 알루미늄, 주석, 철 코발트, 납 몰리브덴, 망간, 니켈, 또는 구리인, 디히드로카르빌 디티오인산의, 최소한 하나의 금속염 약 0.05-약 5중량%, (D)(D-1) 최소한 하나의 치환된 숙신산 아실화제 1몰당 (D-2) 네오펜틸 글리콜, 에틸렌 글리콘, 글리세롤, 펜타에리트리톨, 솔비톨, 폴리(옥시알킬렌) 글리콜의 모노-아릴 또는 모노-알킬 에테르 또는 이들중 두개 이상의 어떤 것의 혼합물로 구성된 군으로부터 선택된, 최소한 하나의 폴리히드록시 화합물 약 0.1-약 2몰을 반응시킴으로서 제조된, 최소한 하나의 카르복실산 에스테르 유도체 조성물 0.1 내지 약 10%, 및 (E) 설폰산, 카르복실산, 페놀, 및 상기 산들의 혼합물로 구성된 군으로부터 선택된 유기산 화합물의, 최소한 하나의 알카리 토금속염 약 0.01-약 5중량%를 포함하는, 내부 연소 엔진을 위한 윤활유 조성물.
  82. 제81항에 있어서, 카르복실산 유도체 조성물(B)를 최소한 약 2.5중량% 함유하는 오일 조성물.
  83. 제81항에 있어서, 폴리아민(B-2)이 하기 일반식(Ⅷ)을 갖는 것을 특징으로 하는 폴리아민인 오일 조성물 :
    상기식에서, n은 정수 1-약 10이며, 각각의 R3는 독립적으로 수소 원자, 히드로카르빌 기 또는 약 30개 이하의 원자를 갖는 아미노-치환 또는 히드록시-치환 히드로카르빌 기이거나, 다른 질소 원자 상의 두개의 R3기가 함꼐 결합하여 U기를 형성할 수 있고, 단, 최소한 하나의 R3기는 수소 원자이며, U는 약 2 내지 약 10개의 탄소 원자를 갖는 알킬렌 기이다.
  84. 제81항에 있어서, (C-1)에서의 알코올 혼합물이 최소한 약 40몰%의 이소프로필 알코올을 포함하는 오일 조성물.
  85. 제81항에 있어서, (C-2)의 금속이 아연인 오일 조성물.
  86. 제81항에 있어서, 치환된 숙신산 아실화제(D-1)가, 약 700-약 5000의 Mn 값을 갖는 치환체 기와 숙산산 기로 구성되는 오일 조성물.
  87. 제86항에 있어서, 치환체 기가, 폴리부텐, 에틸렌-프로필렌 코폴리머, 폴리프로필렌, 및 이들중 두개 이상의 어떤 것의 혼합물로 구성되는 군으로부터 선택되는 요소로부터 유도되는 오일 조성물.
  88. 제86항에 있어서, 치환체 기가 폴리부텐으로부터 유도되고, 폴리부텐으로부터 유도된 전체 단위체중 최소한 약 50%는 이소부텐으로부터 유도되는 오일 조성물.
  89. 제81항에 있어서, (D)의 카르복실산 에스테르를, 최소한 하나의 HN＜기를 함유하는 최소한 하나의 폴리아민(D-3)과 반응시키는 오일 조성물.
  90. 제89항에 있어서, 폴리아민(D-3)이 지방족, 환식지방족 또는 방향족 폴리아민인 조성물.
  91. 제89항에 있어서, 폴리아민(D-3)이 하기 일반식(Ⅷ)을 갖는 것을 특징으로 하는 오일 조성물 :
    상기식에서, n은 정수 1-약 10이며, 각각의 R3는 독립적으로 수소 원자ㅡ 히드로카르빌 기 또는 약 30개 이하의 원자를 갖는 아미노-치환 또는 히드록시-치환 히드로카르빌 기이거나, 다른 질소 원자 상의 두개의 R3기가 함께 결합하여 U기를 형성할 수 있고, 단, 최소한 하나의 R3기는 수소 원자이며, U는 약 2 - 약 10개의 탄소 원자를 갖는 알킬렌 기이다.
  92. 제81항에 있어서,값이 약 1300 내지 약 5000이고의 값이 약 1.5 내지 약 4인 것을 특징으로 하는 폴리알켄으로부터 유도된 치환체 기와 수신산 기로 구성되고, 그 구조내에 치환체가 각각의 당량에 대해 최소한 약 1.3의 숙신산 기가 존재하는 것을 특징으로 하는, 치환된 숙신산 아실화제(D-1)를 폴리히드록시 화합물(D-2)과 반응시키는 오일 조성물.
  93. 제92항에 있어서, 카르복실산 에스테르 유도체 조성물을, 최소한 하나의 HN＜기를 함유하는 최소한 하나의 폴리아민(D-3)과 반응시키는 오일 조성물.
  94. 제93항에 있어서, 폴리아민이 지방족, 환식지방족 또는 방향족 폴리아민인 오일 조성물.
  95. 제93항에 있어서, 폴리아민이 알킬렌 폴리아민인 오일 조성물.
  96. 제81항에 있어서, (F) 글리세롤의, 최소한 하나의 부분적 지방산 에스테르를 약 0.01-2중량% 함유하는 오일 조성물.
  97. 제96항에 있어서, 지방산이 약 10- 약 22개의 탄소 원자를 함유하는 오일 조성물.
  98. 일반적으로 액체이고, 본질적으로 불활성인 유기 희석제/용매 약 20-약 90중량%, (B) (B-1)값이 약 1300 내지 약 5000이고값이 약 1.5 내지 약 4.5인 것을 특징으로 하는 폴리알켄으로부터 유도된 치환체 기와 숙신산 기로 이루어져 있으며, 그 구조내에 치환체 기 각각의 당량에 대해 평균적으로 최소한 1.3의 숙신산 기가 존재하는 것을 특징으로 하는, 최소한 하나의 치환된 숙신산 아실화제 1당량 당(B-2) 그 구조내에 최소한 하나의 HN＜기가 존재하는 것을 특징으로 하는, 최소한 하나의 아민 1당량 이하를 반응시킴으로서, 제조된 최소한 하나의 카르복실신 유도체 조성물 약 10-약 50중량% 및 (C)(C-1) 디티오인산은, 최소한 10몰%의 이소프로필 알코올 및 약 3-약 13개의 탄소 원자를 함유하는 최소한 하나의 일차 지방족 알코올을 포함하는 알코올 혼합물과 오황화인을 반응시킴으로써 제조되고, (C-2)금속은 제Ⅱ족 금속, 알루미늄, 주석, 철, 코발트, 납, 몰리브덴, 망간, 니켈, 또는 구리인, 디히드로카르빌 디티오인산의, 최소한 하나의 금속염 약 0.001 - 약 15중량%를 포함하는, 윤활유 조성물을 배합하기 위한 농축물.
  99. 제98항에 있어서, (D)(D-1) 최소한 하나의 치환된 숙신산 아실화제와 (D-2) 하기 일반식(Ⅹ) :
    R3(OH)m (X)
    (상기식에서, R3는 탄소 결합을 통해 -OH기에 연결된 일가 또는 다가 유기기이고, m은 정수 1- 약 10임)을 갖는 최소한 하나의 알코올을 반응시킴으로써 제조된, 최소한 하나의 카르복실산 에스테르 유도체 조성물을 약 1- 약 30중량% 함유하는 농축물.
  100. 제99항에 있어서, 아실화제(D-1)와 알코올(D-2)을 반응시킴으로써 제조된 카르복실산 에스테르(D)를, 최소한 하나의 HN＜기를 함유하는, 최소한 하나의 아민(D-3)과 반응시키는 농축물.
  101. 제98항에 있어서, (E) 최소한 하나의 산성 유기 화합물의 최소한 하나의 중성 또는 염기성 알칼리 토금속염을 약 1-약 20중량% 함유하는 농축물.
  102. 제99항에 있어서, (E) 최소한 하나의 산성 유기 화합물의, 최소한 하나의 중성 또는 염기성 알칼리 토금속염을 약 1-약 20중량% 함유하는 농축물.
  103. 제98항에 있어서, (F) 다가 알코올의, 최소한 하나의 부분적 지지방산 에스테르를 약 0.001-약 10중량% 함유하는 농축물.
  104. 제99항에 있어서, (F) 다가 알코올의, 최소한 하나의 부분적 지지방산 에스테르를 약 0.001-약 10중량% 함유하는 농축물.
  105. 제104항에 있어서, (E) 최소한 하나의 산성 유기 화합물의 최소한 하나의 중성 또는 염기성 알카리 토금속염을 약 1-약 20중량% 함유하는 농축물.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
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