JP4543980B2 - Manufacturing method of extra-thick steel plate with excellent internal properties - Google Patents
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本発明は、厚板圧延における極厚鋼板(製品板厚150〜200mm以上)の製造方法に関し、特に連続鋳造スラブのセンターポロシティー、ザク性欠陥を効果的に消滅(閉鎖―圧着)させて、鋼板内質特性の極めて良好な極厚鋼板を有利に製造する方法を提案する。 The present invention relates to a method for producing a very thick steel plate (product plate thickness of 150 to 200 mm or more) in thick plate rolling, and in particular, by effectively eliminating (closing-crimping) the center porosity and the zaku defect of the continuous cast slab, We propose a method to advantageously manufacture extra-thick steel plates with very good quality.
一般に厚鋼板は、連続鋳造スラフ゛、または鋳型鋳造したインコ゛ットを分塊圧延した造塊スラフ゛を素材とし、これらを厚板圧延する事によって製造される。この両者を比較すると、製造コストの点では前者の方に魅力があるが、連続鋳造スラフ゛の場合、造塊スラフ゛よりも厚みが薄い為、極厚鋼板の製造に際しては、センターホ゜ロシティーの未圧着部分が残存する割合が高く、また現状の厚板圧延機の能力では、連続鋳造スラフ゛の板厚中心位置に必然的に発生するセンターホ゜ロシティーを安定して消滅させる事は困難である。その為、連続鋳造スラフ゛から製造された極厚鋼板について超音波探傷試験を実施すると、圧下率が小さくなるに伴い、鋼板内質不良の発生が多くなる。 In general, a thick steel plate is manufactured by using a continuous casting slab or an ingot slab obtained by split-rolling a mold-cast ingot and rolling them thick. Comparing the two, the former is more attractive in terms of manufacturing cost. However, in the case of continuous casting slabs, the thickness is thinner than the ingot slabs. The ratio of the remaining portion is high, and with the current capacity of the thick plate rolling mill, it is difficult to stably eliminate the center porosity that inevitably occurs at the central position of the continuous cast slab. Therefore, when an ultrasonic flaw detection test is performed on an extremely thick steel plate manufactured from a continuously cast slab, the quality of the steel plate is increased as the rolling reduction decreases.
よって、従来極厚鋼板の製造に当たっては、圧下比(スラフ゛厚/製品厚)に下限値を設け、その下限値を下回るような加工条件で極厚鋼板を製造しなければならない時は、造塊スラフ゛を用いる事が一般的である。例えば、圧力容器用鋼板の一般製造条件を規定したASTM A20では、この圧下比の下限値を3以上としているし、JIS規格ではこのような規定はないが、鋼板製造業者が自主的に管理を行い、製造を行っているのが実情である。 Therefore, in the manufacture of conventional heavy steel plates, when a lower limit is set for the rolling ratio (slave thickness / product thickness) and the heavy steel plates must be manufactured under processing conditions that fall below that lower limit, It is common to use a slough. For example, ASTM A20, which defines general production conditions for steel plates for pressure vessels, sets the lower limit of this reduction ratio to 3 or more, and the JIS standard does not provide such rules, but the steel plate manufacturer manages it voluntarily. The actual situation is that it is done and manufactured.
但し、造塊スラフ゛の場合、製造フ゜ロセス上、押湯部や沈澱晶部の非定常部分の切り捨てや分塊圧延という中間工程を必要とする為、コストの増大や生産性低下を招くという問題がある。 However, in the case of ingot-making slabs, there is a problem in that the production process requires intermediate steps such as truncation of unsteady portions of the feeder and precipitation crystal parts and ingot-rolling, leading to increased costs and reduced productivity. is there.
以上を考慮すると、連続鋳造スラフ゛からの圧下比が小さくとも、鋼板内質特性に優れた極厚鋼板を製造する事が望ましく、その為に下記のような幾つかの提案がある。
非特許文献1には、圧延形状比で定義される数値を大きくする事により、鋼板内質の良好な鋼板を製造することが開示されている。また、特許文献1及び特許文献2には、連続鋳造機の出側でロールまたは平金敷による圧下を施す事によって、連続鋳造スラフ゛のセンターホ゜ロシティーの消滅を図ることが開示されている。更には、特許文献3には、全圧下率が20〜60%の加工条件で125mm厚以上の極厚鋼板を製造するにあたり、厚板圧延に先立ち、連続鋳造スラフ゛の端部を幅方向から鍛造圧下し、元スラフ゛幅から150mm以上減尺させると共に肥厚化させ、スラフ゛厚方向の鍛造圧下を行う事によって、センターホ゜ロシティーの消滅を図ることが開示されている。
Considering the above, it is desirable to produce an extra-thick steel plate excellent in steel sheet quality characteristics even if the reduction ratio from the continuous casting slab is small, and there are several proposals as described below.
Non-Patent Document 1 discloses that a steel sheet having a good steel sheet quality is manufactured by increasing the numerical value defined by the rolling shape ratio.
しかしながら、上記非特許文献1の技術では、鋼板内質の良好な極厚鋼板を得る為に必要な圧延形状比が圧延機の設備仕様により制約される範囲の上限を超える為、実用性に乏しいという問題がある。また上記特許文献1及び特許文献2の技術では、厚板素材用連続鋳造機の設備改良にコストがかかり過ぎるという問題がある。更には、上記特許文献3の技術では、全圧下率が20%を下回る加工条件の極厚鋼板の製造においては、センターホ゜ロシティーの消滅効果が十分でなく、鋼板内質が健全な極厚鋼板の製造は困難であるという問題がある。
However, in the technique of Non-Patent Document 1, the rolling shape ratio necessary for obtaining an extra-thick steel plate with good steel plate quality exceeds the upper limit of the range constrained by the equipment specifications of the rolling mill. There is a problem. Moreover, in the technique of the said patent document 1 and the
これらの点に鑑み、本発明の主たる目的は、比較的簡単な設備で、全圧下率が16%から20%の範囲内の加工条件で、鋼板内質特性の優れた連続鋳造スラフ゛製極厚鋼板の製造技術を提案する事にある。本発明の他の目的は、空隙性欠陥をわずかな連続鋳造スラフ゛の厚み方向圧下率によって、より効果的に消滅させるのに有効な鍛造条件を究明するところにある。 In view of these points, the main object of the present invention is to make a continuous cast slaved ultra-thick steel sheet with excellent quality of steel sheet under processing conditions within a range of 16% to 20% of total rolling reduction with relatively simple equipment. The idea is to propose steel plate manufacturing technology. Another object of the present invention is to investigate forging conditions effective for eliminating void defects more effectively by a slight reduction ratio in the thickness direction of a continuous casting slab.
本発明者らは、上記目的を達成すべく種々検討を行い、連続鋳造スラフ゛の幅方向圧下量に応じたスラフ゛厚方向鍛造に供すべき加工出発スラフ゛の形状とスラフ゛厚方向圧下時の上下鍛造金敷の形状について、望ましい関係を規定すれば、より効果的に連続鋳造スラフ゛のセンターホ゜ロシティーをより効率良く消滅せしめ、鋼板内質特性の優れた連続鋳造スラフ゛製極厚鋼板が得られる事を知見し、本発明をなした。 The inventors of the present invention have made various studies to achieve the above object, and the shape of the starting slab to be used for the slab thickness direction forging according to the width direction reduction amount of the continuous casting slab and the upper and lower forged anvils during the slab thickness direction reduction. If the desired relationship is specified for the shape of the steel, we know that the center porosity of the continuous casting slab can be more effectively eliminated more efficiently, and that a continuous cast slaved extra heavy steel plate with excellent steel quality can be obtained. The present invention has been made.
即ち、連続鋳造スラフ゛を用い、鍛造と厚板圧延を併用して減厚され、全圧下率が16%から20%の範囲内の加工条件で125mm厚以上の極厚鋼板を製造する方法において、連続鋳造スラフ゛の端部を幅方向から鍛造圧下し、スラフ゛幅を元スラフ゛幅から300mm以上減尺させると共に肥厚化させた後、鍛造金敷と連続鋳造スラフ゛の接触長が例えば3倍程度以上異なるような上下非対称の鍛造金敷によりスラフ゛厚方向の鍛造圧下を6%以上行うとする事が望ましい。ここで、上下非対称の鍛造金敷を用いた被鍛造物の内質改善効果は、上下対称に圧下した場合に生じるスラフ゛厚中心位置の引張応力を、意図的にスラフ゛厚方向へずらし、中心位置の静水圧が大きくなる事を利用したFM(Free from Mannesmann effect)鍛造法として、一般的に知られている。そして、センターホ゜ロシティーの消滅のためには、本発明においては、上下非対称の鍛造金敷による鍛造法の中で、上金敷の連続鋳造スラフ゛との接触長さを1としたとき、下金敷の前記連続鋳造スラフ゛との接触長さを3以上として鍛造圧下を行うことにより、スラフ゛厚方向の内質改善作用を高め、センターホ゜ロシティーの完全消滅を達成するものである。 That is, in a method of producing a very thick steel plate with a thickness of 125 mm or more using a continuous casting slab, reduced in thickness by combining forging and thick plate rolling, and under a processing condition in which the total rolling reduction is in the range of 16% to 20%. After forging down the end of the continuous casting slab from the width direction, reducing the slab width by 300 mm or more from the original slab width and increasing the thickness, the contact length between the forged anvil and the continuous casting slab may differ by about 3 times or more. It is desirable that forging reduction in the slab thickness direction is performed by 6% or more by using a forging anvil that is asymmetrical in the vertical direction. Here, the effect of improving the inner quality of the forging using an asymmetrical forged anvil is that the tensile stress at the center of the slab thickness that occurs when the slab is squeezed symmetrically is intentionally shifted in the slab thickness direction. It is generally known as an FM (Free from Mannesmann effect) forging method using the increase in hydrostatic pressure. In order to eliminate the center porosity, in the present invention, when the contact length of the upper anvil with the continuous casting slab is set to 1 in the forging method using the upper and lower asymmetric forging anvil, By performing forging reduction with a contact length of 3 or more with the continuous casting slab, the quality improvement effect in the thickness direction of the slab is enhanced, and the complete disappearance of the center porosity is achieved.
さらに、本発明者らは、連続鋳造スラフ゛について、これをスラフ゛厚方向の鍛造圧下に供するのに望ましいスラフ゛形状について研究した。その結果、連続鋳造スラフ゛の両幅端部における3面冷却部、特に端部よりスラフ゛厚相当内部の3重点と呼ばれる領域には、連続鋳造スラフ゛の幅方向中央部に生成するセンターホ゜ロシティーサイス゛より、大きな内部不良域が存在し、鍛造または圧延におけるスラフ゛厚中心位置の塑性歪量が十分でない場合、この部分にセンターホ゜ロシティー未圧着部が残存し、鋼板内質不良となる事を突き止めた。 Furthermore, the present inventors have studied the shape of a slab that is desirable for subjecting a continuous cast slab to forging pressure in the slab thickness direction. As a result, the three-surface cooling part at both width ends of the continuous casting slab, especially in the region called the triple point inside the slab thickness from the end, is the center porosity size generated at the center in the width direction of the continuous casting slab. When a large internal defect area exists and the amount of plastic strain at the center position of the slab thickness in forging or rolling is not sufficient, it has been found that an uncompressed portion of the center porosity remains in this portion, resulting in poor quality of the steel sheet.
そこで、本発明では図1に示すように連続鋳造スラフ゛の幅方向鍛造圧下をある一定量以上行い、連続鋳造スラフ゛の両幅端部を肥厚化させ、言わゆる断面形状がト゛ック゛ホ゛ーン状として、かつスラフ゛厚方向の鍛造圧下時は、前記したように、鍛造金敷と連続鋳造スラフ゛の接触長が例えば3倍程度以上異なるような上下非対称の鍛造金敷を用いる事によって、上述したセンターホ゜ロシティーは全圧下率が16%から20%の範囲内の加工条件の場合においても、完全に消滅する事が分かった。
Therefore, in the present invention, as shown in FIG. 1, the forging reduction in the width direction of the continuous casting slab is performed for a certain amount or more, both width end portions of the continuous casting slab are thickened, and the so-called cross-sectional shape becomes a dockbone shape, During forging reduction in the slab thickness direction, as described above, by using a forged anvil that is asymmetrical in the vertical direction where the contact length between the forged anvil and the continuous cast slab differs by about 3 times or more, the above-mentioned center porosity is reduced to the total pressure. It was found that even when the processing conditions were within the range of 16% to 20%, the rate disappeared completely.
本発明によれば、全圧下率が20%以下の場合にあっても、適切なスラフ゛幅方向の圧下量に伴うスラフ゛厚の肥厚化と上下非対称の鍛造金敷によるスラフ゛厚方向の圧下を併用する事によって、連続鋳造スラフ゛のセンターホ゜ロシティーを完全に消滅させ、鋼板内質特性の極めて優れた極厚鋼板の生産が可能になった。 According to the present invention, even when the total reduction ratio is 20% or less, the thickening of the slab thickness associated with an appropriate amount of reduction in the slab width direction is combined with the reduction in the slab thickness direction using an asymmetric forged anvil. As a result, the center porosity of the continuous casting slab has completely disappeared, and it has become possible to produce extra-thick steel plates with extremely superior quality characteristics.
本発明では、連続鋳造スラフ゛の幅方向両端部を肥厚化した形状にする為、図1に示すように連続鋳造スラフ゛(1)の幅方向両端部を、鍛造用上下金敷(2,3)にて、幅方向から圧下し、連続鋳造スラフ゛(1)の両端部(E)の厚さを大きくするが、発明者らが行った数々の試験によれば、幅方向圧下による減尺代(r)が300mm以上/両側であれば、連続鋳造スラフ゛厚方向の圧下において、上下非対称の鍛造金敷を用いる事と合わせ、全圧下率が20%以下の場合にあっても、センターホ゜ロシティーの消滅に十分な効果がある事を突き止めた。 In the present invention, both ends in the width direction of the continuous casting slab (1) are formed on the upper and lower anvils for forging (2, 3) as shown in FIG. Therefore, the thickness of both ends (E) of the continuous casting slab (1) is increased by reducing from the width direction, but according to various tests conducted by the inventors, the reduction allowance (r ) Is 300mm or more / both sides, and in combination with the use of an asymmetrical forged anvil in the reduction in the thickness direction of the continuous casting slab, the center porosity disappears even when the total reduction rate is 20% or less. I found out that there was enough effect.
本発明は、上述したセンターホ゜ロシティーの効果的な消滅を図る為に、鍛造と厚板圧延を併用する事により連続鋳造スラフ゛製極厚鋼板を製造する方法である。特に、全圧下率が16%から20%の範囲内の加工条件下においても、健全な鋼板内質特性を確保する為、鍛造時のスラフ゛幅,厚方向圧下量及び厚方向圧下時の要領を規定する。 The present invention is a method for producing a continuous cast slab ultra-thick steel plate by combining forging and thick plate rolling in order to effectively eliminate the above-described center porosity. In particular, to ensure sound steel sheet quality characteristics even under processing conditions where the total rolling reduction is in the range of 16% to 20%, the slab width during forging, the thickness direction rolling amount, and the procedure during thickness direction rolling are specified. Stipulate.
即ち、本発明においては、全圧下率が16%から20%の範囲内の加工条件で125mm厚以上の極厚鋼板を製造する方法において、連続鋳造スラフ゛の端部を幅方向から鍛造圧下し、スラフ゛幅を元スラフ゛幅から300mm以上減尺させると共に肥厚化させた後、鍛造金敷と連続鋳造スラフ゛の接触長が例えば3倍程度以上異なるような上下非対称の鍛造金敷によりスラフ゛厚方向の鍛造圧下を6%以上の加工制御を行う。 That is, in the present invention, in the method for producing an extremely thick steel plate having a thickness of 125 mm or more under a processing condition in which the total reduction ratio is in the range of 16% to 20%, the end of the continuous casting slab is forged and reduced from the width direction. After reducing the slab width by 300 mm or more from the original slab width and increasing the thickness, the forging reduction in the slab thickness direction is achieved by using an asymmetrical forging anvil where the contact length of the forged anvil and continuous casting slab is different by about 3 times or more, for example. Process control of 6% or more.
ここで、全圧下率は次に述べる理由により、16〜20%とする。即ち、全圧下率が20%を超える場合は、上述した連続鋳造スラフ゛幅・厚方向の圧下量及び厚み方向の鍛造圧下要領を実施しなくとも、鍛造と厚板圧延を併用し、加工条件を規定した製造条件によって、健全な鋼板内質特性を有する極厚鋼板の製造が可能である(特許第3528504号公報)。一方、全圧下率が16%未満の場合は、事実上、本規定の鍛造条件を付与しても連続鋳造スラフ゛のセンターホ゜ロシティーは十分圧着されず、板厚中心位置の特性確保が困難である。 Here, the total rolling reduction is set to 16 to 20% for the following reason. In other words, if the total reduction ratio exceeds 20%, the forging and thick plate rolling can be used together without changing the continuous casting slab width / thickness reduction amount and the forging reduction procedure in the thickness direction as described above. According to the specified production conditions, it is possible to produce a very thick steel plate having sound steel quality characteristics (Japanese Patent No. 3528504). On the other hand, if the total rolling reduction is less than 16%, the center porosity of the continuous casting slab will not be sufficiently crimped even if the forging conditions specified here are applied, and it will be difficult to secure the center position of the plate thickness. .
次に、本発明に係る鍛造・圧延方法を用いて極厚鋼板を製造した結果を比較例も交えて説明する。 Next, the result of manufacturing an extremely thick steel plate using the forging / rolling method according to the present invention will be described with reference to a comparative example.
発明者らは、310mm厚の連続鋳造スラフ゛を用いて、鍛造及び厚板圧延の圧下率を変化させ、鋼板の内質特性を超音波探傷試験をJIS G0801に準じて実施した。その結果を表1に示す。
The inventors changed the rolling reduction ratio of forging and thick plate rolling using a continuous casting slab having a thickness of 310 mm, and conducted an ultrasonic flaw detection test according to JIS G0801 for the internal properties of the steel plate. The results are shown in Table 1.
表1より、全圧下率が16〜20%の場合、No.3,7のように連続鋳造スラフ゛幅方向の鍛造圧下量を300mmとし、スラフ゛厚方向鍛造圧下時の上下金敷をスラフ゛接触長が3倍異なる非対称とし、かつ鍛造圧下率を6%として製造した極厚鋼板の内質は良好な結果が得られた。この結果は、一般40キロ鋼に限った例でなく、上下金敷のスラフ゛接触長比を3倍及び5倍とした一般50キロ鋼(No.9,10)、高炭素鋼(No.11,12)及び調質60キロ鋼(No.13,14)に適用した場合も同様に、極厚鋼板の内質は良好な結果が確認された。 From Table 1, when the total reduction ratio is 16 to 20%, the forging reduction amount in the continuous casting slab width direction is 300 mm as in No. 3 and 7, and the upper and lower anvils during the slab thickness direction forging reduction have a slab contact length. Good results were obtained for the quality of extra-thick steel sheets produced with an asymmetry three times different and a forging reduction ratio of 6%. This result is not limited to the general 40kg steel, but the 50% steel (No.9,10), high carbon steel (No.11, Similarly, when applied to tempered 60kg steel (No.13, 14), good results were confirmed for the quality of the extra heavy steel plate.
一方、No.1,2ではスラフ゛厚方向の鍛造圧下率不足や上下対称の金敷を採用した場合では、鋼板内質は不健全である。また、スラフ゛接触長比が5である上下非対称の金敷を用いた場合でも、No.4,5のように、連続鋳造スラフ゛幅方向の鍛造圧下量が300mm未満である場合やNo.6のようにスラフ゛厚方向の鍛造圧下率が6%未満の場合は、同じく不健全な鋼板内質となった。また、No.8のようにスラフ゛接触長比が2である上下非対称金敷を用いた場合は、連続鋳造スラフ゛幅方向の圧下量を350mm、スラフ゛厚方向鍛造圧下率を9%としても良好な鋼板内質は確保できなかった。
On the other hand, in No. 1 and 2, when the forging reduction rate in the slab thickness direction is insufficient or when an anvil is symmetric, the quality of the steel sheet is unhealthy. Even when an asymmetrical anvil with a slab contact length ratio of 5 is used, the forging reduction in the continuous casting slab width direction is less than 300 mm, as in No. 4 and 5, or as in No. 6 On the other hand, when the forging reduction ratio in the slab thickness direction was less than 6%, the quality of the steel sheet was unsatisfactory. In addition, when using an asymmetrical anvil with a slab contact length ratio of 2 such as No. 8, a steel plate that is good even when the rolling reduction in the continuous casting slab width direction is 350 mm and the forging reduction ratio in the slab thickness direction is 9% The internal quality could not be secured.
本発明方法によれば、既設の鍛造プレス機を用いることにより、従来の分塊スラブを素材として製造していた極厚鋼板を連続鋳造スラブにより確実かつ容易に製造できる。
According to the method of the present invention, by using an existing forging press machine, it is possible to reliably and easily manufacture an extremely thick steel plate that has been manufactured using a conventional slab as a raw material by using a continuous cast slab.
1 連続鋳造スラブ
2 鍛造機械の上金敷
3 鍛造機械の下金敷
E 肥厚化部分
r 減尺代
1
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JP5994712B2 (en) * | 2013-03-28 | 2016-09-21 | Jfeスチール株式会社 | Manufacturing method of ultra-thick martensitic stainless steel plate with excellent internal properties |
JP5949629B2 (en) * | 2013-03-28 | 2016-07-13 | Jfeスチール株式会社 | Manufacturing method of extra-thick austenitic stainless steel plate with excellent internal properties and extra-thick austenitic stainless steel plate with excellent internal properties |
JP6070615B2 (en) * | 2014-03-28 | 2017-02-01 | Jfeスチール株式会社 | Manufacturing method of extra heavy steel sheet |
JP6137080B2 (en) * | 2014-07-28 | 2017-05-31 | Jfeスチール株式会社 | Slab forging method |
JP6156459B2 (en) * | 2014-10-02 | 2017-07-05 | Jfeスチール株式会社 | Method for forging steel material and method for producing steel material using the forging method |
JP6156321B2 (en) * | 2014-10-22 | 2017-07-05 | Jfeスチール株式会社 | Hot forging method of slab |
WO2016079978A1 (en) * | 2014-11-18 | 2016-05-26 | Jfeスチール株式会社 | Thick, high toughness, high tension steel sheet with excellent material uniformity and manufacturing method therefor |
JP6879323B2 (en) * | 2018-03-22 | 2021-06-02 | Jfeスチール株式会社 | Manufacturing method of thick steel sheet with excellent fatigue characteristics |
CN112536405B (en) * | 2020-11-19 | 2022-10-18 | 河南科技大学 | Free forging method of large flat square forging |
CN115961202B (en) * | 2022-12-05 | 2024-09-20 | 南京钢铁股份有限公司 | Production method of 1000 MPa-level water-electricity steel plate with thickness of more than 100mm |
Citations (4)
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JPH10263614A (en) * | 1997-03-27 | 1998-10-06 | Kawasaki Steel Corp | Production of extra thick steel plate |
JP2000140906A (en) * | 1998-11-09 | 2000-05-23 | Kawasaki Steel Corp | Manufacture of ultra-heavy steel plate at extremely large reduction ratio |
JP2000263103A (en) * | 1999-03-18 | 2000-09-26 | Kawasaki Steel Corp | Production of extra-thick steel plate using continuously cast slab |
JP2002210502A (en) * | 2001-01-19 | 2002-07-30 | Kawasaki Steel Corp | Manufacturing method for extremely thick steel |
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JPH10263614A (en) * | 1997-03-27 | 1998-10-06 | Kawasaki Steel Corp | Production of extra thick steel plate |
JP2000140906A (en) * | 1998-11-09 | 2000-05-23 | Kawasaki Steel Corp | Manufacture of ultra-heavy steel plate at extremely large reduction ratio |
JP2000263103A (en) * | 1999-03-18 | 2000-09-26 | Kawasaki Steel Corp | Production of extra-thick steel plate using continuously cast slab |
JP2002210502A (en) * | 2001-01-19 | 2002-07-30 | Kawasaki Steel Corp | Manufacturing method for extremely thick steel |
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