HUP0104484A2 - Eljárás alkánszulfonsavak előállítására - Google Patents
Eljárás alkánszulfonsavak előállításáraInfo
- Publication number
- HUP0104484A2 HUP0104484A2 HU0104484A HUP0104484A HUP0104484A2 HU P0104484 A2 HUP0104484 A2 HU P0104484A2 HU 0104484 A HU0104484 A HU 0104484A HU P0104484 A HUP0104484 A HU P0104484A HU P0104484 A2 HUP0104484 A2 HU P0104484A2
- Authority
- HU
- Hungary
- Prior art keywords
- nitrogen oxides
- sulfonic acid
- nitric acid
- alkane sulfonic
- producing
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 2
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 title 1
- 150000001335 aliphatic alkanes Chemical class 0.000 title 1
- MWUXSHHQAYIFBG-UHFFFAOYSA-N nitrogen oxide Inorganic materials O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 abstract 9
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 abstract 3
- 229910017604 nitric acid Inorganic materials 0.000 abstract 3
- 239000002253 acid Substances 0.000 abstract 2
- 230000003647 oxidation Effects 0.000 abstract 2
- 238000007254 oxidation reaction Methods 0.000 abstract 2
- BWGNESOTFCXPMA-UHFFFAOYSA-N Dihydrogen disulfide Chemical compound SS BWGNESOTFCXPMA-UHFFFAOYSA-N 0.000 abstract 1
- 150000007513 acids Chemical class 0.000 abstract 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 239000006227 byproduct Substances 0.000 abstract 1
- 230000001590 oxidative effect Effects 0.000 abstract 1
- 239000001301 oxygen Substances 0.000 abstract 1
- 229910052760 oxygen Inorganic materials 0.000 abstract 1
- 229920001021 polysulfide Polymers 0.000 abstract 1
- 239000005077 polysulfide Substances 0.000 abstract 1
- 150000008117 polysulfides Polymers 0.000 abstract 1
- 230000008929 regeneration Effects 0.000 abstract 1
- 238000011069 regeneration method Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/02—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
- C07C303/16—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof by oxidation of thiols, sulfides, hydropolysulfides, or polysulfides with formation of sulfo or halosulfonyl groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
A találmány tárgya eljárás alkánszulfonsavak előállítására. Atalálmány szerint úgy járnak el, hogy alkántiolt és/vagy dialkil-diszulfidot és/vagy dialkil-poliszulfidot salétromsavval víz,nitrogén-oxidok és más melléktermékek keletkezése mellett a megfelelőalkánszulfonsavvá oxidálnak, majd a keletkezett nitrogén-oxidokatoxigénnel salétromsavvá regenerálják, és az így kapott salétromsavatvisszaforgatják az oxidációs lépésbe. Az oxidációt és a nitrogén-oxidok regenerálását egymástól elkülönített reaktortérben hajtjákvégre. Ó
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19854428A DE19854428A1 (de) | 1998-11-25 | 1998-11-25 | Verfahren zur Herstellung von Alkansulfonsäuren |
| PCT/EP1999/008994 WO2000031027A1 (de) | 1998-11-25 | 1999-11-22 | Verfahren zur herstellung von alkansulfonsäuren |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| HUP0104484A2 true HUP0104484A2 (hu) | 2002-03-28 |
| HUP0104484A3 HUP0104484A3 (en) | 2003-07-28 |
Family
ID=7889013
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| HU0104484A HUP0104484A3 (en) | 1998-11-25 | 1999-11-22 | Method of producing alkane sulfonic acid |
Country Status (20)
| Country | Link |
|---|---|
| US (1) | US6531629B1 (hu) |
| EP (1) | EP1133470B1 (hu) |
| JP (1) | JP4294874B2 (hu) |
| KR (1) | KR100599637B1 (hu) |
| CN (1) | CN1163479C (hu) |
| AT (1) | ATE240938T1 (hu) |
| AU (1) | AU765481B2 (hu) |
| BR (1) | BR9915651B1 (hu) |
| CA (1) | CA2350490C (hu) |
| DE (2) | DE19854428A1 (hu) |
| ES (1) | ES2200582T3 (hu) |
| HU (1) | HUP0104484A3 (hu) |
| IN (1) | IN207425B (hu) |
| MX (1) | MXPA01004496A (hu) |
| PL (1) | PL197882B1 (hu) |
| RU (1) | RU2230735C2 (hu) |
| SK (1) | SK7152001A3 (hu) |
| UA (1) | UA66896C2 (hu) |
| WO (1) | WO2000031027A1 (hu) |
| ZA (1) | ZA200104256B (hu) |
Families Citing this family (38)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7820145B2 (en) * | 2003-08-04 | 2010-10-26 | Foamix Ltd. | Oleaginous pharmaceutical and cosmetic foam |
| JP4441726B2 (ja) * | 2003-01-24 | 2010-03-31 | 石原薬品株式会社 | スズ又はスズ合金の脂肪族スルホン酸メッキ浴の製造方法 |
| US20060272950A1 (en) * | 2003-05-12 | 2006-12-07 | Martyak Nicholas M | High purity electrolytic sulfonic acid solutions |
| US9399618B2 (en) * | 2003-05-12 | 2016-07-26 | Arkema Inc. | High purity electrolytic sulfonic acid solutions |
| US7282603B2 (en) * | 2003-06-21 | 2007-10-16 | Richards Alan K | Anhydrous processing of methane into methane-sulfonic acid, methanol, and other compounds |
| FR2935142B1 (fr) * | 2008-08-20 | 2010-11-19 | Arkema France | Dimethyldisulfure issu au moins partiellement de matieres renouvellables |
| JP5675642B2 (ja) | 2008-12-23 | 2015-02-25 | ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ | 硫化水素含有ガスの圧縮方法 |
| PH12012500874A1 (en) | 2009-11-03 | 2013-01-07 | Basf Se | Method for handling aqueous methanesulfonic acid solutions |
| GB201100531D0 (en) | 2011-01-13 | 2011-03-02 | Phosphonics | Functionalised materials, processes for the production and uses thereof |
| KR101947205B1 (ko) | 2011-04-14 | 2019-02-12 | 바스프 에스이 | 시스템의 표면 상의 스케일의 침착을 억제하고/하거나 용해시키는 방법 |
| US8648026B2 (en) | 2011-11-30 | 2014-02-11 | Basf Se | Composition comprising an alkanesulfonic acid for dissolving and/or inhibiting deposition of scale on a surface of a system |
| US9290722B2 (en) | 2012-04-12 | 2016-03-22 | Basf Se | Cleaning composition for dishwashing |
| WO2015077737A1 (en) | 2013-11-25 | 2015-05-28 | Basf Se | Cleaning concentrate for removing scale from a surface of a system |
| WO2015085522A1 (en) | 2013-12-11 | 2015-06-18 | Evonik Industries Ag | Process for preparing alkanesulphonic acids |
| WO2015086424A1 (en) | 2013-12-11 | 2015-06-18 | Evonik Industries Ag | A catalyst for oxidation reactions, a method for its preparation and the use thereof |
| CA2941399A1 (en) | 2014-03-04 | 2015-09-11 | Basf Se | Method for degumming and esterification of an oil |
| WO2015134496A1 (en) | 2014-03-04 | 2015-09-11 | Basf Se | Method of delinting cotton seeds |
| EP3035046A1 (de) | 2014-12-19 | 2016-06-22 | Evonik Degussa GmbH | Verfahren zur Bestimmung eines Dialkyldisulfids |
| KR20180067563A (ko) | 2015-09-28 | 2018-06-20 | 바스프 에스이 | 코튼 시드의 중화 방법 |
| MX375979B (es) | 2015-11-10 | 2025-03-06 | Basf Se | Proceso para reprocesar acido alcansulfonico. |
| EP3374346B1 (de) | 2015-11-10 | 2019-07-24 | Basf Se | Verfahren zur aufreinigung von alkansulfonsäuren |
| EP3173405A1 (de) | 2015-11-30 | 2017-05-31 | Evonik Degussa GmbH | Verfahren zur herstellung einer alkansulfonsäure |
| MX392504B (es) | 2016-06-20 | 2025-03-24 | Basf Se | Proceso de produccion de etanol a partir de maiz. |
| CA3027747A1 (en) | 2016-06-20 | 2017-12-28 | Basf Se | Process for producing ethanol from corn comprising dry-milling and adding alkanesulfonic acid to the separated corn fiber |
| EP3472330A1 (en) | 2016-06-20 | 2019-04-24 | Basf Se | Process for producing ethanol from corn comprising dry-milling and adding alkanesulfonic acid to the fermented mash |
| CN109477225A (zh) | 2016-07-18 | 2019-03-15 | 巴斯夫欧洲公司 | 用于缩合反应的低腐蚀链烷磺酸 |
| TW201841881A (zh) | 2017-04-18 | 2018-12-01 | 德商巴斯夫歐洲公司 | 純化烷烴磺酸酐的方法及使用純化的烷烴磺酸酐製造烷烴磺酸的方法 |
| CA3062417C (en) | 2017-05-11 | 2023-07-04 | Arkema Inc. | Processes and systems for recovering methanesulfonic acid in purified form |
| WO2018219728A1 (en) * | 2017-05-30 | 2018-12-06 | Basf Se | Process for the manufacturing of methane sulfonic acid |
| EP3453447B1 (en) | 2017-09-06 | 2020-12-23 | Evonik Operations GmbH | Process for the preparation of alkanesulfonic acid |
| EP3456708B1 (en) | 2017-09-13 | 2020-07-01 | Evonik Operations GmbH | Process for operating a plant for preparing an alkanesulfonic acid |
| CN107698468A (zh) * | 2017-10-18 | 2018-02-16 | 辽宁省轻工设计院有限公司 | 甲基磺酸的制备工艺 |
| SG11202007292TA (en) * | 2018-02-07 | 2020-08-28 | Basf Se | Process for the manufacturing of alkanesulfonic acids |
| WO2020126855A1 (en) * | 2018-12-21 | 2020-06-25 | Basf Se | Mixture comprising methanesulfonic acid and sulfuric acid |
| MX2022001602A (es) | 2019-08-07 | 2022-03-11 | Basf Se | Recuperacion de acido metansulfonico libre de agua del flujo de fondo de una columna de destilacion. |
| EP4038051B1 (en) * | 2019-10-01 | 2023-09-20 | Basf Se | Process for manufacturing alkanesulfonic acids |
| CN113214120B (zh) * | 2021-03-25 | 2022-10-04 | 四川上氟科技有限公司 | 一种全氟己基乙基磺酸盐的制备方法 |
| KR20240149900A (ko) * | 2022-02-18 | 2024-10-15 | 바스프 에스이 | 알킬 설폰산의 제조 방법 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2697722A (en) | 1951-01-13 | 1954-12-21 | Standard Oil Co | Manufacture of sulfonic acids |
| US2727920A (en) * | 1951-04-20 | 1955-12-20 | Standard Oil Co | Oxidation of mercaptans to sulfonic acids |
| AU5714698A (en) | 1997-02-10 | 1998-08-26 | Innochem Inc. | Preparation of alkane sulfonic acids and sulfonyl chlorides by oxidation of alkanethiols and dialkyl disulfides |
-
1998
- 1998-11-25 DE DE19854428A patent/DE19854428A1/de not_active Withdrawn
-
1999
- 1999-11-22 SK SK715-2001A patent/SK7152001A3/sk unknown
- 1999-11-22 BR BRPI9915651-2A patent/BR9915651B1/pt not_active IP Right Cessation
- 1999-11-22 KR KR1020017006113A patent/KR100599637B1/ko not_active Expired - Lifetime
- 1999-11-22 EP EP99962150A patent/EP1133470B1/de not_active Expired - Lifetime
- 1999-11-22 UA UA2001064423A patent/UA66896C2/uk unknown
- 1999-11-22 AU AU18593/00A patent/AU765481B2/en not_active Ceased
- 1999-11-22 CN CNB998136883A patent/CN1163479C/zh not_active Expired - Lifetime
- 1999-11-22 DE DE59905681T patent/DE59905681D1/de not_active Expired - Lifetime
- 1999-11-22 WO PCT/EP1999/008994 patent/WO2000031027A1/de active IP Right Grant
- 1999-11-22 JP JP2000583855A patent/JP4294874B2/ja not_active Expired - Fee Related
- 1999-11-22 PL PL347973A patent/PL197882B1/pl unknown
- 1999-11-22 US US09/831,362 patent/US6531629B1/en not_active Expired - Lifetime
- 1999-11-22 ES ES99962150T patent/ES2200582T3/es not_active Expired - Lifetime
- 1999-11-22 AT AT99962150T patent/ATE240938T1/de active
- 1999-11-22 HU HU0104484A patent/HUP0104484A3/hu unknown
- 1999-11-22 CA CA002350490A patent/CA2350490C/en not_active Expired - Fee Related
- 1999-11-22 RU RU2001117526/04A patent/RU2230735C2/ru not_active IP Right Cessation
-
2001
- 2001-05-04 MX MXPA01004496 patent/MXPA01004496A/es unknown
- 2001-05-24 ZA ZA200104256A patent/ZA200104256B/xx unknown
- 2001-05-25 IN IN725CH2001 patent/IN207425B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| KR20010092744A (ko) | 2001-10-26 |
| MX217997B (hu) | 2003-12-08 |
| AU765481B2 (en) | 2003-09-18 |
| SK7152001A3 (en) | 2002-01-07 |
| UA66896C2 (uk) | 2004-06-15 |
| ES2200582T3 (es) | 2004-03-01 |
| ZA200104256B (en) | 2002-05-24 |
| CA2350490A1 (en) | 2000-06-02 |
| DE19854428A1 (de) | 2000-05-31 |
| JP2002530369A (ja) | 2002-09-17 |
| DE59905681D1 (de) | 2003-06-26 |
| CA2350490C (en) | 2008-03-04 |
| WO2000031027A1 (de) | 2000-06-02 |
| PL197882B1 (pl) | 2008-05-30 |
| PL347973A1 (en) | 2002-05-06 |
| IN207425B (hu) | 2007-06-29 |
| CN1328544A (zh) | 2001-12-26 |
| HUP0104484A3 (en) | 2003-07-28 |
| MXPA01004496A (es) | 2002-03-01 |
| KR100599637B1 (ko) | 2006-07-12 |
| BR9915651A (pt) | 2001-08-07 |
| RU2230735C2 (ru) | 2004-06-20 |
| US6531629B1 (en) | 2003-03-11 |
| CN1163479C (zh) | 2004-08-25 |
| AU1859300A (en) | 2000-06-13 |
| BR9915651B1 (pt) | 2011-07-26 |
| JP4294874B2 (ja) | 2009-07-15 |
| EP1133470B1 (de) | 2003-05-21 |
| EP1133470A1 (de) | 2001-09-19 |
| ATE240938T1 (de) | 2003-06-15 |
| IN2001CH00725A (hu) | 2006-08-25 |
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