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GB675341A - Manufacture of finely divided silica - Google Patents

Manufacture of finely divided silica

Info

Publication number
GB675341A
GB675341A GB2522050A GB2522050A GB675341A GB 675341 A GB675341 A GB 675341A GB 2522050 A GB2522050 A GB 2522050A GB 2522050 A GB2522050 A GB 2522050A GB 675341 A GB675341 A GB 675341A
Authority
GB
United Kingdom
Prior art keywords
silica
collected
formation
silicon tetrafluoride
finely divided
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB2522050A
Inventor
Donald Beddoes Broughton
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Godfrey L Cabot Inc
Original Assignee
Godfrey L Cabot Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Godfrey L Cabot Inc filed Critical Godfrey L Cabot Inc
Priority to GB2522050A priority Critical patent/GB675341A/en
Publication of GB675341A publication Critical patent/GB675341A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/113Silicon oxides; Hydrates thereof
    • C01B33/12Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C01B33/181Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by a dry process
    • C01B33/183Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by a dry process by oxidation or hydrolysis in the vapour phase of silicon compounds such as halides, trichlorosilane, monosilane
    • C01B33/184Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by a dry process by oxidation or hydrolysis in the vapour phase of silicon compounds such as halides, trichlorosilane, monosilane by hydrolysis of tetrafluoride
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/10Solid density
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/12Surface area

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Silicon Compounds (AREA)

Abstract

Amorphous finely divided silica is produced by reacting silicon tetrafluoride vapour with steam at a temperature which prevents the formation of moisture, collecting the silica after its formation and maintaining the collected silica at a sufficiently high temperature, to prevent the formation of moisture therein, and until the hydrofluoric acid has been separated therefrom. Fluorite (CaF2), sand, and sulphuric acid are reacted to produce silicon tetrafluoride vapour, which is contacted with steam, and the resultant silica is collected in a bag filter. The hydrofluoric acid may be collected and passed through sand to produce silicon tetrafluoride for re-use in the process. The silica has a density of 4 pounds per cubic foot and a specific surface area of 100-200 sq. m. per gram.
GB2522050A 1950-10-17 1950-10-17 Manufacture of finely divided silica Expired GB675341A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB2522050A GB675341A (en) 1950-10-17 1950-10-17 Manufacture of finely divided silica

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB2522050A GB675341A (en) 1950-10-17 1950-10-17 Manufacture of finely divided silica

Publications (1)

Publication Number Publication Date
GB675341A true GB675341A (en) 1952-07-09

Family

ID=10224152

Family Applications (1)

Application Number Title Priority Date Filing Date
GB2522050A Expired GB675341A (en) 1950-10-17 1950-10-17 Manufacture of finely divided silica

Country Status (1)

Country Link
GB (1) GB675341A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2805956A (en) * 1952-05-28 1957-09-10 Columbia Southern Chem Corp Silica pigment and method of preparing same
US3123497A (en) * 1964-03-03 Process for depositing silicon dioxide dielectric coatings

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3123497A (en) * 1964-03-03 Process for depositing silicon dioxide dielectric coatings
US2805956A (en) * 1952-05-28 1957-09-10 Columbia Southern Chem Corp Silica pigment and method of preparing same

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