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GB436194A - A process and solvent for separating mineral oil products - Google Patents

A process and solvent for separating mineral oil products

Info

Publication number
GB436194A
GB436194A GB12798/35A GB1279835A GB436194A GB 436194 A GB436194 A GB 436194A GB 12798/35 A GB12798/35 A GB 12798/35A GB 1279835 A GB1279835 A GB 1279835A GB 436194 A GB436194 A GB 436194A
Authority
GB
United Kingdom
Prior art keywords
solvent
naphthenic
mixture
solvents
water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB12798/35A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HANS POELL
Original Assignee
HANS POELL
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by HANS POELL filed Critical HANS POELL
Publication of GB436194A publication Critical patent/GB436194A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G21/00Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents
    • C10G21/06Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents characterised by the solvent used
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G21/00Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents
    • C10G21/06Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents characterised by the solvent used
    • C10G21/12Organic compounds only
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G21/00Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents
    • C10G21/06Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents characterised by the solvent used
    • C10G21/12Organic compounds only
    • C10G21/27Organic compounds not provided for in a single one of groups C10G21/14 - C10G21/26

Landscapes

  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Mineral oils are separated into their paraffinic and naphthenic components by treating with an anhydrous mixture of crude cresol and a liquid water-repellent solvent, whereby paraffins are removed, and then saturating the extract with water to separate the naphthenic component leaving an aqueous mixture of solvents containing resins, aromatic and asphaltic substances. The major part of the aromatic and resinous fraction may be removed in a pretreatment with a mixture of the solvents containing water whereby a more pure naphthenic fraction is obtained. A mineral lubricating or spindleoil distillate or a residue is treated with three portions of a mixture of cresol containing 10 to 30 per cent by volume of nitrobenzene at or near atmospheric temperature, or the oil is completely dissolved by warming with the solvents and then cooled to separate into layers. After removal of the paraffinic layer the solvent layer is saturated with water by passage through a pump and the naphthenic layer is separated in a centrifuge and the separated naphthenic and paraffinic fractions p are distilled to remove solvent and are finally treated with an adsorbent earth. Final traces of solvent are removed by superheated steam. The naphthenic fraction may be further purified by extraction with anhydrous solvent mixture at a low temperature. The aqueous mixture of solvents is distilled removing water and solvents, leaving an asphaltic oil. Water repellent solvents specified are:--nitrotoluene, nitrobenzene, toluidines, aniline, xylidines, ethyl aniline, dichlorbenzenes, or dichlordiethyl ether. The separation may also be effected by counter-flowing the oil and solvent mixture in a treating tower. Specification 432,249 is referred to.
GB12798/35A 1934-05-05 1935-04-29 A process and solvent for separating mineral oil products Expired GB436194A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
AT436194X 1934-05-05

Publications (1)

Publication Number Publication Date
GB436194A true GB436194A (en) 1935-10-07

Family

ID=3674164

Family Applications (1)

Application Number Title Priority Date Filing Date
GB12798/35A Expired GB436194A (en) 1934-05-05 1935-04-29 A process and solvent for separating mineral oil products

Country Status (1)

Country Link
GB (1) GB436194A (en)

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