GB322750A - Improvements in the manufacture and production of condensation products of the anthraquinone series - Google Patents
Improvements in the manufacture and production of condensation products of the anthraquinone seriesInfo
- Publication number
- GB322750A GB322750A GB2561728A GB2561728A GB322750A GB 322750 A GB322750 A GB 322750A GB 2561728 A GB2561728 A GB 2561728A GB 2561728 A GB2561728 A GB 2561728A GB 322750 A GB322750 A GB 322750A
- Authority
- GB
- United Kingdom
- Prior art keywords
- condensation
- carried out
- dichloranthraquinone
- aminoaryl
- anthraquinones
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B1/00—Dyes with anthracene nucleus not condensed with any other ring
- C09B1/16—Amino-anthraquinones
- C09B1/20—Preparation from starting materials already containing the anthracene nucleus
- C09B1/26—Dyes with amino groups substituted by hydrocarbon radicals
- C09B1/32—Dyes with amino groups substituted by hydrocarbon radicals substituted by aryl groups
- C09B1/325—Dyes with no other substituents than the amino groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
322,750. Johnson, J. Y., (I. G. Farbenindustrie Akt.-Ges.). Sept. 6, 1928. 1 : 5 - Di- (o - carboxyarylamino)-anthraquinones are prepared by effecting the condensation of 1: 5-dihalogen anthraquinones with aminoaryl-ocarboxylic acds or salts thereof in presence of acid binding agents and a copper compound as catalyst, in alcohols at temperatures above 150‹ C. Pressure may be used if necessary, and the process results in better yields of purer products than are otherwise obtained. The aminoaryl-o-carboxylic acids are preferably employed as salts and in quantities in excess of theroetical requirements. In examples, (1) the condensation of potassium anthranilate with the 1: 5-dichloranthraquinone is carried out in n-butyl alcohol (or ethyl alcohol) in an autoclave at 150‹ -180‹ C.; the product is condensed to the diacridone by warming with chlorsulphonic acid. (2) The condensation of the same materials is carried out in benzyl alcohol at 170‹ C. (3) The condensation of sodium 5-chloranthranilate with 1: 5-dichloranthraquinone is carried out in n-butyl alcohol at 170‹-175‹ C. in an autoclave. Reference has been directed by the Comptroller to Specification 312,678.
Priority Applications (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DEI34791D DE503205C (en) | 1928-06-30 | 1928-06-30 | Process for the preparation of condensation products of the anthraquinone series |
GB2561728A GB322750A (en) | 1928-09-06 | 1928-09-06 | Improvements in the manufacture and production of condensation products of the anthraquinone series |
US371714A US1929847A (en) | 1928-06-30 | 1929-06-17 | Production of condensation products of 1.5-dihalogen anthraquinones |
FR676857D FR676857A (en) | 1928-06-30 | 1929-06-19 | Process for the preparation of condensation products of the anthraquinone series |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB2561728A GB322750A (en) | 1928-09-06 | 1928-09-06 | Improvements in the manufacture and production of condensation products of the anthraquinone series |
Publications (1)
Publication Number | Publication Date |
---|---|
GB322750A true GB322750A (en) | 1929-12-06 |
Family
ID=10230557
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB2561728A Expired GB322750A (en) | 1928-06-30 | 1928-09-06 | Improvements in the manufacture and production of condensation products of the anthraquinone series |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB322750A (en) |
-
1928
- 1928-09-06 GB GB2561728A patent/GB322750A/en not_active Expired
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