GB1355433A - Production of titanium - Google Patents
Production of titaniumInfo
- Publication number
- GB1355433A GB1355433A GB3553571A GB1355433DA GB1355433A GB 1355433 A GB1355433 A GB 1355433A GB 3553571 A GB3553571 A GB 3553571A GB 1355433D A GB1355433D A GB 1355433DA GB 1355433 A GB1355433 A GB 1355433A
- Authority
- GB
- United Kingdom
- Prior art keywords
- titanium
- temperature
- chloride
- passed
- arc
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 title abstract 4
- 239000010936 titanium Substances 0.000 title abstract 4
- 229910052719 titanium Inorganic materials 0.000 title abstract 4
- 239000003513 alkali Substances 0.000 abstract 2
- 229910052784 alkaline earth metal Inorganic materials 0.000 abstract 2
- 239000000463 material Substances 0.000 abstract 2
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 abstract 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 abstract 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 229910001514 alkali metal chloride Inorganic materials 0.000 abstract 1
- 229910001617 alkaline earth metal chloride Inorganic materials 0.000 abstract 1
- 150000001342 alkaline earth metals Chemical class 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- 239000012159 carrier gas Substances 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 150000001805 chlorine compounds Chemical class 0.000 abstract 1
- 238000010891 electric arc Methods 0.000 abstract 1
- 230000005611 electricity Effects 0.000 abstract 1
- 238000005868 electrolysis reaction Methods 0.000 abstract 1
- 239000007789 gas Substances 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 229910052751 metal Inorganic materials 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1263—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction
- C22B34/1268—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams
- C22B34/1272—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams reduction of titanium halides, e.g. Kroll process
Landscapes
- Chemical & Material Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
- Electrolytic Production Of Metals (AREA)
Abstract
1355433 Extracting titanium ELECTRICITY COUNCIL 13 July 1972 [28 July 1971] 35535/71 Heading C7D Elemental titanium is obtained by reducing titanium tetrachloride in vapour form with a vapourized alkali or alkaline earth metal, the vapours being heated by hydrogen as carrier gas passed through an electric arc. The reacting materials are maintained at a temperature at which elemental titanium is liquid and falls to the bottom of the reactor vessel 12, and at a temperature at which the temperature of the materials is above that of the boiling point of the alkali or alkaline earth metal chloride formed so that the chloride thus formed may be removed from the reaction vessel 12 through 24. The metal contained in this chloride is obtained by electrolysis in tank 29 and passed into the reactor vessel 12 through ports 21. The titanium tetrachloride is passed through port 20 and the arc is struck between the cathode tip 15 and anode 16, a swirling action of the gas passed down through nozzle 17 being caused by the effect of an electrically energized coil 18 on the arc struck.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB3553571 | 1971-07-28 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1355433A true GB1355433A (en) | 1974-06-05 |
Family
ID=10378818
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB3553571A Expired GB1355433A (en) | 1971-07-28 | 1971-07-28 | Production of titanium |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US3825415A (en) |
| JP (1) | JPS5110803B1 (en) |
| AU (1) | AU459240B2 (en) |
| CA (1) | CA964471A (en) |
| GB (1) | GB1355433A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2231883A (en) * | 1989-05-24 | 1990-11-28 | Nkr Co Ltd | Method for manufacturing titanium powder or titanium composite powder |
| WO2008039047A1 (en) * | 2006-09-25 | 2008-04-03 | Ervins Blumbergs | Method and apparatus for continuous producing of metallic titanium and titanium-based alloys |
Families Citing this family (42)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4080194A (en) * | 1976-11-26 | 1978-03-21 | Westinghouse Electric Corporation | Titanium or zirconium reduction process by arc heater |
| US4102765A (en) * | 1977-01-06 | 1978-07-25 | Westinghouse Electric Corp. | Arc heater production of silicon involving alkali or alkaline-earth metals |
| US4162291A (en) * | 1977-10-12 | 1979-07-24 | Westinghouse Electric Corp. | Liquid silicon casting control mechanism |
| LU81469A1 (en) * | 1979-07-05 | 1981-02-03 | Luniversite Libre Bruxelles | PROCESS AND PLANT FOR THE PRODUCTION OF REACTIVE METALS BY REDUCTION OF THEIR HALIDES |
| US4468248A (en) * | 1980-12-22 | 1984-08-28 | Occidental Research Corporation | Process for making titanium metal from titanium ore |
| FI103033B (en) * | 1990-07-25 | 1999-04-15 | Anglo Amer Corp South Africa | Process for the recovery of titanium |
| WO1992014851A1 (en) * | 1991-02-21 | 1992-09-03 | The University Of Melbourne | Process for the production of metallic titanium and intermediates useful in the processing of ilmenite and related minerals |
| US5160532A (en) * | 1991-10-21 | 1992-11-03 | General Electric Company | Direct processing of electroslag refined metal |
| US20030145682A1 (en) * | 1994-08-01 | 2003-08-07 | Kroftt-Brakston International, Inc. | Gel of elemental material or alloy and liquid metal and salt |
| US20030061907A1 (en) * | 1994-08-01 | 2003-04-03 | Kroftt-Brakston International, Inc. | Gel of elemental material or alloy and liquid metal and salt |
| US7435282B2 (en) | 1994-08-01 | 2008-10-14 | International Titanium Powder, Llc | Elemental material and alloy |
| US7445658B2 (en) | 1994-08-01 | 2008-11-04 | Uchicago Argonne, Llc | Titanium and titanium alloys |
| BR9508497A (en) * | 1994-08-01 | 1997-12-23 | Kroftt Brakston International | Processes for producing an elementary material or an alloy thereof from a halide or mixtures thereof and for continuously producing a metal or non-metal or an alloy of the same |
| US8891583B2 (en) * | 2000-11-15 | 2014-11-18 | Ati Properties, Inc. | Refining and casting apparatus and method |
| US6496529B1 (en) | 2000-11-15 | 2002-12-17 | Ati Properties, Inc. | Refining and casting apparatus and method |
| US7442227B2 (en) * | 2001-10-09 | 2008-10-28 | Washington Unniversity | Tightly agglomerated non-oxide particles and method for producing the same |
| US20050284824A1 (en) * | 2002-09-07 | 2005-12-29 | International Titanium Powder, Llc | Filter cake treatment apparatus and method |
| UA79310C2 (en) * | 2002-09-07 | 2007-06-11 | Int Titanium Powder Llc | Methods for production of alloys or ceramics with the use of armstrong method and device for their realization |
| CN100482820C (en) * | 2002-09-07 | 2009-04-29 | 国际钛金属粉末公司 | Method for Separating Ti from Ti Slurry |
| US20060107790A1 (en) * | 2002-10-07 | 2006-05-25 | International Titanium Powder, Llc | System and method of producing metals and alloys |
| AU2003263082A1 (en) * | 2002-10-07 | 2004-05-04 | International Titanium Powder, Llc. | System and method of producing metals and alloys |
| US7794580B2 (en) * | 2004-04-21 | 2010-09-14 | Materials & Electrochemical Research Corp. | Thermal and electrochemical process for metal production |
| US7410562B2 (en) * | 2003-08-20 | 2008-08-12 | Materials & Electrochemical Research Corp. | Thermal and electrochemical process for metal production |
| US20070180951A1 (en) * | 2003-09-03 | 2007-08-09 | Armstrong Donn R | Separation system, method and apparatus |
| US20070017319A1 (en) | 2005-07-21 | 2007-01-25 | International Titanium Powder, Llc. | Titanium alloy |
| US7803211B2 (en) * | 2005-09-22 | 2010-09-28 | Ati Properties, Inc. | Method and apparatus for producing large diameter superalloy ingots |
| US7578960B2 (en) * | 2005-09-22 | 2009-08-25 | Ati Properties, Inc. | Apparatus and method for clean, rapidly solidified alloys |
| US7803212B2 (en) * | 2005-09-22 | 2010-09-28 | Ati Properties, Inc. | Apparatus and method for clean, rapidly solidified alloys |
| EP1945394A2 (en) | 2005-10-06 | 2008-07-23 | International Titanium Powder, LLC. | Titanium boride |
| US8381047B2 (en) * | 2005-11-30 | 2013-02-19 | Microsoft Corporation | Predicting degradation of a communication channel below a threshold based on data transmission errors |
| US20080031766A1 (en) * | 2006-06-16 | 2008-02-07 | International Titanium Powder, Llc | Attrited titanium powder |
| US7753989B2 (en) * | 2006-12-22 | 2010-07-13 | Cristal Us, Inc. | Direct passivation of metal powder |
| EP2109691B1 (en) * | 2007-01-22 | 2016-07-13 | Materials And Electrochemical Research Corporation | Metallothermic reduction of in-situ generated titanium chloride |
| US8748773B2 (en) * | 2007-03-30 | 2014-06-10 | Ati Properties, Inc. | Ion plasma electron emitters for a melting furnace |
| KR101433415B1 (en) * | 2007-03-30 | 2014-08-26 | 에이티아이 프로퍼티즈, 인코퍼레이티드 | A fused furnace comprising a wire discharge ion plasma electron emitter |
| US9127333B2 (en) * | 2007-04-25 | 2015-09-08 | Lance Jacobsen | Liquid injection of VCL4 into superheated TiCL4 for the production of Ti-V alloy powder |
| US7798199B2 (en) | 2007-12-04 | 2010-09-21 | Ati Properties, Inc. | Casting apparatus and method |
| US8747956B2 (en) | 2011-08-11 | 2014-06-10 | Ati Properties, Inc. | Processes, systems, and apparatus for forming products from atomized metals and alloys |
| AU2012358205B2 (en) | 2011-12-22 | 2017-10-12 | Universal Achemetal Titanium, Llc | A system and method for extraction and refining of titanium |
| KR101617351B1 (en) * | 2014-12-19 | 2016-05-03 | 한국생산기술연구원 | reduction device using liquid metal |
| BR112019005038B1 (en) | 2016-09-14 | 2022-12-20 | Universal Achemetal Titanium, Llc | A METHOD TO PRODUCE TITANIUM-ALUMINUM-VANADIUM ALLOY |
| RU2763465C2 (en) | 2017-01-13 | 2021-12-29 | ЮНИВЕРСАЛ АКЕМЕТАЛ ТИТАНИУМ, ЭлЭлСи | TITANIUM LIGATURE FOR ALLOYS BASED ON Ti-Al |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2768074A (en) * | 1949-09-24 | 1956-10-23 | Nat Res Corp | Method of producing metals by decomposition of halides |
| US2816828A (en) * | 1956-06-20 | 1957-12-17 | Nat Res Corp | Method of producing refractory metals |
| US2955333A (en) * | 1957-04-11 | 1960-10-11 | Ici Ltd | Electric arc furnaces |
-
1971
- 1971-07-28 GB GB3553571A patent/GB1355433A/en not_active Expired
-
1972
- 1972-07-20 CA CA147,547A patent/CA964471A/en not_active Expired
- 1972-07-21 US US00274006A patent/US3825415A/en not_active Expired - Lifetime
- 1972-07-27 AU AU45076/72A patent/AU459240B2/en not_active Expired
- 1972-07-27 JP JP47074706A patent/JPS5110803B1/ja active Pending
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2231883A (en) * | 1989-05-24 | 1990-11-28 | Nkr Co Ltd | Method for manufacturing titanium powder or titanium composite powder |
| GB2231883B (en) * | 1989-05-24 | 1993-07-07 | N K R Company Ltd | Method for manufacturing titanium powder or titanium composite powder |
| WO2008039047A1 (en) * | 2006-09-25 | 2008-04-03 | Ervins Blumbergs | Method and apparatus for continuous producing of metallic titanium and titanium-based alloys |
| US7776128B2 (en) | 2006-09-25 | 2010-08-17 | Baltic Titan Limited | Continuous production of metallic titanium and titanium-based alloys |
| AU2007300818B2 (en) * | 2006-09-25 | 2010-11-25 | Baltic Titan Limited | Method and apparatus for continuous producing of metallic titanium and titanium-based alloys |
| EA014948B1 (en) * | 2006-09-25 | 2011-04-29 | Ервинс Блумбергс | Method and apparatus for continuous producing of metallic titanium and titanium-based alloys |
| CN101517103B (en) * | 2006-09-25 | 2011-10-05 | 埃尔温斯·布卢姆伯格斯 | Method and equipment for continuous production of titanium metal or titanium alloy |
| US8157885B2 (en) | 2006-09-25 | 2012-04-17 | Baltic Titan Limited | Continuous production of metallic titanium and titanium-based alloys |
Also Published As
| Publication number | Publication date |
|---|---|
| CA964471A (en) | 1975-03-18 |
| JPS5110803B1 (en) | 1976-04-07 |
| AU4507672A (en) | 1974-01-31 |
| AU459240B2 (en) | 1975-03-20 |
| US3825415A (en) | 1974-07-23 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |