GB1148874A - The production of carbon fibres - Google Patents
The production of carbon fibresInfo
- Publication number
- GB1148874A GB1148874A GB1077965A GB1077965A GB1148874A GB 1148874 A GB1148874 A GB 1148874A GB 1077965 A GB1077965 A GB 1077965A GB 1077965 A GB1077965 A GB 1077965A GB 1148874 A GB1148874 A GB 1148874A
- Authority
- GB
- United Kingdom
- Prior art keywords
- fibres
- carbon fibres
- oxidizing atmosphere
- polyacrylonitrile
- produced
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title abstract 5
- 229910052799 carbon Inorganic materials 0.000 title abstract 5
- 238000010438 heat treatment Methods 0.000 abstract 4
- 229920002239 polyacrylonitrile Polymers 0.000 abstract 4
- 230000001590 oxidative effect Effects 0.000 abstract 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 abstract 2
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 abstract 1
- 238000005727 Friedel-Crafts reaction Methods 0.000 abstract 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 abstract 1
- 229910052786 argon Inorganic materials 0.000 abstract 1
- 229920001577 copolymer Polymers 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 abstract 1
- 239000000178 monomer Substances 0.000 abstract 1
- 229920001568 phenolic resin Polymers 0.000 abstract 1
- 239000005011 phenolic resin Substances 0.000 abstract 1
- 229920000642 polymer Polymers 0.000 abstract 1
- 229920001897 terpolymer Polymers 0.000 abstract 1
Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
- D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
- D01F9/20—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products
- D01F9/21—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D01F9/22—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from polyacrylonitriles
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Inorganic Fibers (AREA)
Abstract
1,148,874. Carbon fibres. NATIONAL RESEARCH DEVELOPMENT CORP. 15 June, 1966 [15 March, 1965], No. 10779/65. Heading C1A. Carbon fibres are produced by heating polyacrylonitrile fibres in a non-oxidizing atmosphere from ambient to a temperature of 1000‹ C. over a period of 2-24 hours whilst the fibres are held under a tension sufficient to cause the polyacrylonitrile fibres to elongate from their initial length so that the carbon fibres produced from them are of greater length than the original polyacrylonitrile fibres. Preferably the non-oxidizing atmosphere is a vacuum or hydrogen and the carbon fibres produced may be subjected to a further heat treatment wherein they are heated to a temperature of 1500‹ C. in not less than 2 hours followed by further heating to a higher temperature not exceeding 3300‹ C. in a non- oxidizing atmosphere, e.g. argon. The further heat treatment may be performed as a separate step and the fibres may be tensioned during this step so that they elongate even more during this treatment. The term polyacrylonitrile fibres is used in the Specification to also mean, copolymers or terpolymers of acrylonitrile with other monomers, e.g. methyl methaorylate or vinyl acetate, either alone or to which have been added polymers compatible with them, e.g. phenolic resins, or Friedel-Crafts condensates.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB1077965A GB1148874A (en) | 1965-03-15 | 1965-03-15 | The production of carbon fibres |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB1077965A GB1148874A (en) | 1965-03-15 | 1965-03-15 | The production of carbon fibres |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1148874A true GB1148874A (en) | 1969-04-16 |
Family
ID=9974107
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1077965A Expired GB1148874A (en) | 1965-03-15 | 1965-03-15 | The production of carbon fibres |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB1148874A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3652221A (en) * | 1969-07-30 | 1972-03-28 | Union Carbide Corp | Process for producing carbon fibers |
-
1965
- 1965-03-15 GB GB1077965A patent/GB1148874A/en not_active Expired
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3652221A (en) * | 1969-07-30 | 1972-03-28 | Union Carbide Corp | Process for producing carbon fibers |
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