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FR2985991A1 - Nouveau procede de preparation de silices precipitees - Google Patents

Nouveau procede de preparation de silices precipitees Download PDF

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Publication number
FR2985991A1
FR2985991A1 FR1200212A FR1200212A FR2985991A1 FR 2985991 A1 FR2985991 A1 FR 2985991A1 FR 1200212 A FR1200212 A FR 1200212A FR 1200212 A FR1200212 A FR 1200212A FR 2985991 A1 FR2985991 A1 FR 2985991A1
Authority
FR
France
Prior art keywords
acid
preparation
new process
silicate
added
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR1200212A
Other languages
English (en)
Other versions
FR2985991B1 (fr
Inventor
Emmanuelle Allain
Sylvaine Neveu
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Rhodia Operations SAS
Original Assignee
Rhodia Operations SAS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR1200212A priority Critical patent/FR2985991B1/fr
Application filed by Rhodia Operations SAS filed Critical Rhodia Operations SAS
Priority to CA2862473A priority patent/CA2862473A1/fr
Priority to CN201380006528.3A priority patent/CN104066682A/zh
Priority to US14/373,797 priority patent/US9695054B2/en
Priority to PCT/EP2013/051234 priority patent/WO2013110655A1/fr
Priority to AU2013211587A priority patent/AU2013211587A1/en
Priority to EP13713364.1A priority patent/EP2807118A1/fr
Priority to BR112014018028A priority patent/BR112014018028A8/pt
Priority to MX2014009000A priority patent/MX354838B/es
Priority to KR1020147023224A priority patent/KR20140116524A/ko
Priority to RU2014134531/05A priority patent/RU2581407C2/ru
Publication of FR2985991A1 publication Critical patent/FR2985991A1/fr
Application granted granted Critical
Publication of FR2985991B1 publication Critical patent/FR2985991B1/fr
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/126—Preparation of silica of undetermined type
    • C01B33/128—Preparation of silica of undetermined type by acidic treatment of aqueous silicate solutions
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C01B33/187—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
    • C01B33/193—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates of aqueous solutions of silicates

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Silicon Compounds (AREA)
  • Paper (AREA)

Abstract

L'invention concerne un procédé de préparation de silices précipitées dans lequel : (i) on forme un pied de cuve de pH de 2 à 5, (ii) on y ajoute, simultanément, du silicate et de l'acide, de telle manière que le pH du milieu réactionnel soit entre 2 et 5, (iii) on ajoute du silicate jusqu'à un pH de 7 à 10, (iv) on ajoute, simultanément, du silicate et de l'acide, de telle manière que le pH soit entre 7 et 10, (v) on ajoute de l'acide jusqu'à un pH de 2,5 à 5,3, (vi) on met en contact le milieu réactionnel avec de l'acide et du silicate, de telle manière que le pH soit entre 2,5 et 5,3, dans lequel l'acide utilisé dans au moins une de ses étapes est un acide concentré.
FR1200212A 2012-01-25 2012-01-25 Nouveau procede de preparation de silices precipitees Expired - Fee Related FR2985991B1 (fr)

Priority Applications (11)

Application Number Priority Date Filing Date Title
FR1200212A FR2985991B1 (fr) 2012-01-25 2012-01-25 Nouveau procede de preparation de silices precipitees
MX2014009000A MX354838B (es) 2012-01-25 2013-01-23 Proceso novedoso para preparar sílices precipitadas.
US14/373,797 US9695054B2 (en) 2012-01-25 2013-01-23 Process for preparing precipitated silica
PCT/EP2013/051234 WO2013110655A1 (fr) 2012-01-25 2013-01-23 Procede de preparation de silices precipitees
AU2013211587A AU2013211587A1 (en) 2012-01-25 2013-01-23 Method for preparing precipitated silica
EP13713364.1A EP2807118A1 (fr) 2012-01-25 2013-01-23 Procede de preparation de silices precipitees
CA2862473A CA2862473A1 (fr) 2012-01-25 2013-01-23 Procede de preparation de silices precipitees
CN201380006528.3A CN104066682A (zh) 2012-01-25 2013-01-23 用于制备沉淀二氧化硅的方法
KR1020147023224A KR20140116524A (ko) 2012-01-25 2013-01-23 침강 실리카의 제조 방법
RU2014134531/05A RU2581407C2 (ru) 2012-01-25 2013-01-23 Новый способ получения осажденных диоксидов кремния
BR112014018028A BR112014018028A8 (pt) 2012-01-25 2013-01-23 Processo para preparação de sílicas precipitadas

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR1200212A FR2985991B1 (fr) 2012-01-25 2012-01-25 Nouveau procede de preparation de silices precipitees

Publications (2)

Publication Number Publication Date
FR2985991A1 true FR2985991A1 (fr) 2013-07-26
FR2985991B1 FR2985991B1 (fr) 2014-11-28

Family

ID=48044728

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1200212A Expired - Fee Related FR2985991B1 (fr) 2012-01-25 2012-01-25 Nouveau procede de preparation de silices precipitees

Country Status (11)

Country Link
US (1) US9695054B2 (fr)
EP (1) EP2807118A1 (fr)
KR (1) KR20140116524A (fr)
CN (1) CN104066682A (fr)
AU (1) AU2013211587A1 (fr)
BR (1) BR112014018028A8 (fr)
CA (1) CA2862473A1 (fr)
FR (1) FR2985991B1 (fr)
MX (1) MX354838B (fr)
RU (1) RU2581407C2 (fr)
WO (1) WO2013110655A1 (fr)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2984870B1 (fr) 2011-12-23 2014-03-21 Rhodia Operations Nouveau procede de preparation de silices precipitees.
JP5868520B2 (ja) 2011-12-23 2016-02-24 ローディア オペレーションズ 沈澱シリカ製造方法
FR2985990B1 (fr) 2012-01-25 2014-11-28 Rhodia Operations Nouveau procede de preparation de silices precipitees a morphologie, granulometrie et porosite particulieres
FR2985993B1 (fr) 2012-01-25 2014-11-28 Rhodia Operations Nouveau procede de preparation de silices precipitees
FR2985992B1 (fr) 2012-01-25 2015-03-06 Rhodia Operations Nouveau procede de preparation de silices precitees
PT3555000T (pt) * 2016-12-19 2021-07-06 Evonik Operations Gmbh Sílica compatível com estanho
US11958980B2 (en) * 2017-12-27 2024-04-16 Rhodia Operations Precipitated silica and process for its manufacture
EP3990389B1 (fr) * 2019-06-27 2023-07-19 Rhodia Operations Silice précipitée et son procédé de fabrication

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0520862A1 (fr) * 1991-06-26 1992-12-30 Rhone-Poulenc Chimie Procédé de préparation de silice précipitée, silices précipitées obtenues et leur utilisation au renforcement des élastomères
EP0754650A1 (fr) * 1995-07-20 1997-01-22 Degussa Ag Silice précipitée
WO2011026895A1 (fr) * 2009-09-03 2011-03-10 Rhodia Operations Nouveau procede de preparation de silices precipitees

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3639845A1 (de) 1986-11-21 1988-06-01 Degussa Faellungskieselsaeuren, verfahren zu ihrer herstellung und verwendung
FR2646673B1 (fr) * 1989-05-02 1991-09-06 Rhone Poulenc Chimie Silice sous forme de bille, procede de preparation et son utilisation au renforcement des elastomeres
CA2150369C (fr) * 1993-09-29 2001-05-01 Yvonick Chevallier Silice precipitee
FR2763581B1 (fr) * 1997-05-26 1999-07-23 Rhodia Chimie Sa Silice precipitee utilisable comme charge renforcante pour elastomeres
US7700062B2 (en) 2000-10-13 2010-04-20 University Of Cincinnati Methods for synthesizing precipitated silica and use thereof
FR2818966B1 (fr) * 2000-12-28 2003-03-07 Rhodia Chimie Sa Procede de preparation de silice precipitee contenant de l'aluminium
CN101412515B (zh) * 2001-08-13 2011-02-09 罗狄亚化学公司 具有特定孔隙尺寸和/或粒度分布的硅石和它的用途,尤其用于增强聚合物
US6869595B2 (en) * 2001-12-21 2005-03-22 J.M. Huber Corporation Abrasive compositions for clear toothpaste
FR2902781B1 (fr) * 2006-06-27 2008-09-05 Rhodia Recherches Et Technologies Sas Silice precipitee pour application papier
WO2010022544A1 (fr) 2008-09-01 2010-03-04 Evonik Degussa Gmbh Procédé de préparation de silices précipitées, silices précipitées et leur utilisation
FR2949455B1 (fr) * 2009-09-03 2011-09-16 Rhodia Operations Nouveau procede de preparation de silices precipitees
FR2962996B1 (fr) 2010-07-23 2012-07-27 Rhodia Operations Nouveau procede de preparation de silices precipitees
JP5868520B2 (ja) 2011-12-23 2016-02-24 ローディア オペレーションズ 沈澱シリカ製造方法
FR2984870B1 (fr) 2011-12-23 2014-03-21 Rhodia Operations Nouveau procede de preparation de silices precipitees.
FR2985993B1 (fr) 2012-01-25 2014-11-28 Rhodia Operations Nouveau procede de preparation de silices precipitees
FR2985992B1 (fr) 2012-01-25 2015-03-06 Rhodia Operations Nouveau procede de preparation de silices precitees
FR2985990B1 (fr) 2012-01-25 2014-11-28 Rhodia Operations Nouveau procede de preparation de silices precipitees a morphologie, granulometrie et porosite particulieres

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0520862A1 (fr) * 1991-06-26 1992-12-30 Rhone-Poulenc Chimie Procédé de préparation de silice précipitée, silices précipitées obtenues et leur utilisation au renforcement des élastomères
EP0754650A1 (fr) * 1995-07-20 1997-01-22 Degussa Ag Silice précipitée
WO2011026895A1 (fr) * 2009-09-03 2011-03-10 Rhodia Operations Nouveau procede de preparation de silices precipitees

Also Published As

Publication number Publication date
BR112014018028A8 (pt) 2017-07-11
WO2013110655A1 (fr) 2013-08-01
RU2581407C2 (ru) 2016-04-20
CA2862473A1 (fr) 2013-08-01
EP2807118A1 (fr) 2014-12-03
FR2985991B1 (fr) 2014-11-28
MX2014009000A (es) 2015-03-05
KR20140116524A (ko) 2014-10-02
CN104066682A (zh) 2014-09-24
AU2013211587A1 (en) 2014-08-07
US20150037235A1 (en) 2015-02-05
RU2014134531A (ru) 2016-03-20
US9695054B2 (en) 2017-07-04
BR112014018028A2 (fr) 2017-06-20
MX354838B (es) 2018-03-21

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