ES8507478A1 - Un metodo de preparar una sal de acilo c6-c18-oxibencenosulfonato. - Google Patents
Un metodo de preparar una sal de acilo c6-c18-oxibencenosulfonato.Info
- Publication number
- ES8507478A1 ES8507478A1 ES525971A ES525971A ES8507478A1 ES 8507478 A1 ES8507478 A1 ES 8507478A1 ES 525971 A ES525971 A ES 525971A ES 525971 A ES525971 A ES 525971A ES 8507478 A1 ES8507478 A1 ES 8507478A1
- Authority
- ES
- Spain
- Prior art keywords
- synthesis
- sulphonate
- organic compounds
- acyloxybenzene
- reacting
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 230000015572 biosynthetic process Effects 0.000 title abstract 2
- 238000003786 synthesis reaction Methods 0.000 title abstract 2
- 150000002894 organic compounds Chemical class 0.000 title 1
- JXLHNMVSKXFWAO-UHFFFAOYSA-N azane;7-fluoro-2,1,3-benzoxadiazole-4-sulfonic acid Chemical compound N.OS(=O)(=O)C1=CC=C(F)C2=NON=C12 JXLHNMVSKXFWAO-UHFFFAOYSA-N 0.000 abstract 4
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 abstract 1
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 abstract 1
- -1 acyl anhydride Chemical class 0.000 abstract 1
- 150000007933 aliphatic carboxylic acids Chemical class 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 150000001340 alkali metals Chemical class 0.000 abstract 1
- 230000009286 beneficial effect Effects 0.000 abstract 1
- 239000007844 bleaching agent Substances 0.000 abstract 1
- 150000001732 carboxylic acid derivatives Chemical class 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 238000005580 one pot reaction Methods 0.000 abstract 1
- 150000004965 peroxy acids Chemical class 0.000 abstract 1
- 239000002243 precursor Substances 0.000 abstract 1
- 235000017281 sodium acetate Nutrition 0.000 abstract 1
- 239000001632 sodium acetate Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/42—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C309/00—Sulfonic acids; Halides, esters, or anhydrides thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
PROCEDIMIENTO PARA LA PREPARACION DE UNA SAL DE ACILO C6-C18-OXIBENCENOSULFONATO.COMPRENDE LAS SIGUIENTES OPERACIONES: PRIMERA, SE FORMA UNA MEZCLA DE SAL FENOSULFONATO Y UN ANHIDRIDO ALCANOICO DE C2-C3 EN UN MEDIO QUE CONTIENE ACIDO CARBOXILICO ALIFATICO DE C6-C18 SUSTITUIDO O NO SUSTITUIDO; SEGUNDA, SE CALIENTA LA MEZCLA A REFLUJO HASTA UNA TEMPERATURA COMPRENDIDA ENTRE 140 Y 180 GRADOS, HASTA QUE REACCIONE LA SAL FENOL-SULFONATO PARA FORMAR UNA SAL DE ACILO C2-C3-OXIBENCENOSULFONATO; TERCERA, SE ELEVA LA TEMPERATURA DE LA MEZCLA HASTA UN VALOR SUFICIENTE PARA PRODUCIR LA ACIDOLISIS Y PARA LA VOLATILIZACION DEL ACIDO ALCANOICO; Y POR ULTIMO, SE RECUPERA LA SAL DE ACILO C6-C18-OXIBENCENOSULFONATO.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB8227675 | 1982-09-28 | ||
GB838311497A GB8311497D0 (en) | 1983-04-27 | 1983-04-27 | Synthesis of sulphonated organic compounds |
Publications (2)
Publication Number | Publication Date |
---|---|
ES525971A0 ES525971A0 (es) | 1985-09-01 |
ES8507478A1 true ES8507478A1 (es) | 1985-09-01 |
Family
ID=26283972
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES525971A Expired ES8507478A1 (es) | 1982-09-28 | 1983-09-27 | Un metodo de preparar una sal de acilo c6-c18-oxibencenosulfonato. |
Country Status (5)
Country | Link |
---|---|
EP (1) | EP0105672B1 (es) |
CA (1) | CA1211464A (es) |
DE (1) | DE3362937D1 (es) |
ES (1) | ES8507478A1 (es) |
IE (1) | IE56048B1 (es) |
Families Citing this family (22)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB8304990D0 (en) * | 1983-02-23 | 1983-03-30 | Procter & Gamble | Detergent ingredients |
US4537724A (en) * | 1983-05-11 | 1985-08-27 | Ethyl Corporation | Alkanoyloxybenzenesulfonate salt production |
US4814110A (en) * | 1984-12-14 | 1989-03-21 | The Clorox Company | Method for esterifying dihydroxybenzenes |
DE3524052A1 (de) * | 1985-07-05 | 1987-01-08 | Hoechst Ag | Verfahren zur herstellung von acyloxybenzolsulfonsaeuren und deren salzen |
DE3538141A1 (de) * | 1985-10-26 | 1987-04-30 | Hoechst Ag | Kontinuierliches verfahren zur herstellung von acyloxybenzolsulfonsaeuren |
GB8531392D0 (en) * | 1985-12-20 | 1986-02-05 | Unilever Plc | Sulphonated aromated esters |
US4772290A (en) * | 1986-03-10 | 1988-09-20 | Clorox Company | Liquid hydrogen peroxide/peracid precursor bleach: acidic aqueous medium containing solid peracid precursor activator |
US4790952A (en) * | 1986-08-14 | 1988-12-13 | The Clorox Company | Alkyl monoperoxysuccinic acid precursors and method of synthesis |
US4735740A (en) * | 1986-10-03 | 1988-04-05 | The Clorox Company | Diperoxyacid precursors and method |
US4900469A (en) * | 1986-10-21 | 1990-02-13 | The Clorox Company | Thickened peracid precursor compositions |
ES2023916B3 (es) * | 1986-12-05 | 1992-02-16 | Interox Chemicals Ltd | Fabricacion de ester. |
GB8712909D0 (en) * | 1987-06-02 | 1987-07-08 | Interox Chemicals Ltd | Preparation of esters |
DE3824901A1 (de) * | 1988-07-22 | 1990-02-15 | Hoechst Ag | Verfahren zur herstellung von acyloxibenzolsulfonsaeuren oder deren salzen |
DE4106843A1 (de) * | 1991-03-04 | 1992-09-10 | Henkel Kgaa | Verfahren zur herstellung von benzoyloxybenzolsulfonaten |
US5438147A (en) * | 1991-05-04 | 1995-08-01 | Hoechst Ag | Imidocarboxylic acid activators and sulfimidocarboxylic acid activators, processes for their preparation and their use |
US5466840A (en) * | 1994-08-22 | 1995-11-14 | Eastman Chemical Company | Process for preparing purified alkali metal salts of 4-sulfophenyl-[(1-oxyalkanoyl)amino]alkanoate without isolation of intermediates |
US5710296A (en) * | 1995-05-25 | 1998-01-20 | The Clorox Company | Process for preparing phenyl esters |
US6448430B1 (en) | 1999-09-10 | 2002-09-10 | Eastman Chemical Company | Process for the preparation of aryl carboxylate esters |
US6448431B1 (en) | 1999-09-13 | 2002-09-10 | Eastman Chemical Company | Production of aryl carboxylate esters |
DE10233827A1 (de) | 2002-07-25 | 2004-02-12 | Clariant Gmbh | Verfahren zur Herstellung von Acyloxybenzolsulfonaten |
DE10300981A1 (de) | 2003-01-14 | 2004-07-22 | Clariant Gmbh | Verfahren zur Herstellung von Acyloxybenzolsulfonaten |
CA3079120C (en) * | 2013-03-14 | 2020-09-08 | Archer Daniels Midland Company | Process for making hmf from sugars with reduced byproduct formation, and improved stability hmf compositions |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB864798A (en) * | 1958-03-20 | 1961-04-06 | Unilever Ltd | Bleaching processes and compositions |
-
1983
- 1983-09-22 EP EP19830305621 patent/EP0105672B1/en not_active Expired
- 1983-09-22 DE DE8383305621T patent/DE3362937D1/de not_active Expired
- 1983-09-26 CA CA000437521A patent/CA1211464A/en not_active Expired
- 1983-09-27 ES ES525971A patent/ES8507478A1/es not_active Expired
- 1983-09-28 IE IE227983A patent/IE56048B1/en not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
DE3362937D1 (en) | 1986-05-15 |
EP0105672A1 (en) | 1984-04-18 |
EP0105672B1 (en) | 1986-04-09 |
IE56048B1 (en) | 1991-03-27 |
IE832279L (en) | 1984-03-28 |
ES525971A0 (es) | 1985-09-01 |
CA1211464A (en) | 1986-09-16 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FD1A | Patent lapsed |
Effective date: 19971201 |