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ES479375A1 - Procedimiento mejorado para la preparacion de n,n,n',n'-te- traacetiletilendiamina. - Google Patents

Procedimiento mejorado para la preparacion de n,n,n',n'-te- traacetiletilendiamina.

Info

Publication number
ES479375A1
ES479375A1 ES479375A ES479375A ES479375A1 ES 479375 A1 ES479375 A1 ES 479375A1 ES 479375 A ES479375 A ES 479375A ES 479375 A ES479375 A ES 479375A ES 479375 A1 ES479375 A1 ES 479375A1
Authority
ES
Spain
Prior art keywords
diacetylethylenediamine
tetraacetylethylenediamine
acetylation
weight
carried out
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES479375A
Other languages
English (en)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hoechst AG
Original Assignee
Hoechst AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE19782816174 external-priority patent/DE2816174A1/de
Priority claimed from DE19792906606 external-priority patent/DE2906606A1/de
Application filed by Hoechst AG filed Critical Hoechst AG
Publication of ES479375A1 publication Critical patent/ES479375A1/es
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/08—Preparation of carboxylic acid amides from amides by reaction at nitrogen atoms of carboxamide groups
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Procedimiento mejorado para la preparación de N,N,N¿,N¿-etraacetiletilendiamina mediante acetilación de N,N¿-diacetiletilendiamina con anhídrido de ácido acético a una temperatura de 120 a 170ºC, caracterizado por a) se utiliza N,N¿-diacetiletilendiamina y anhídric de ácido acético en la proporción de peso de 1:1 hasta 1:10; b) la acetilación se interrumpe antes de establecer el equilibrio de reacción entre N,N¿-diacetiletilendiamina y N,N,N¿,N¿-tetraacetiletilendiamina; c)la mezcla de reacción coloreada de pardo, obtenida, se somete después a antes de la separación de N,N,N¿,N¿-tetraacetiletilendiamina mediante cristalización, a una purificación para eliminar las impurezas coloreadas y D) los componentes de reacción, purificados y recuperados, no reaccionados totalmente para formar N,N,N¿,N¿-tetraacetiletilendiamina, son aportados nuevamente a la acetilación.
ES479375A 1978-04-14 1979-04-06 Procedimiento mejorado para la preparacion de n,n,n',n'-te- traacetiletilendiamina. Expired ES479375A1 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19782816174 DE2816174A1 (de) 1978-04-14 1978-04-14 Verfahren zur herstellung von n,n,n',n'-tetraacetylaethylendiamin
DE19792906606 DE2906606A1 (de) 1979-02-21 1979-02-21 Verfahren zur herstellung von n,n,n'- tetraacetylaethylendiamin

Publications (1)

Publication Number Publication Date
ES479375A1 true ES479375A1 (es) 1979-07-16

Family

ID=25774240

Family Applications (1)

Application Number Title Priority Date Filing Date
ES479375A Expired ES479375A1 (es) 1978-04-14 1979-04-06 Procedimiento mejorado para la preparacion de n,n,n',n'-te- traacetiletilendiamina.

Country Status (10)

Country Link
US (1) US4240980A (es)
EP (1) EP0004919B1 (es)
JP (1) JPS54138512A (es)
AT (1) AT371802B (es)
CA (1) CA1110660A (es)
DE (1) DE2960395D1 (es)
DK (1) DK153379A (es)
ES (1) ES479375A1 (es)
PT (1) PT69485A (es)
YU (1) YU87579A (es)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2078716B (en) * 1980-06-27 1985-04-24 Warwick Chem Ltd Production of amines
GB2143522B (en) * 1980-06-27 1985-09-25 Warwick Chemical Limited Production of amines
DE3042148A1 (de) * 1980-11-08 1982-06-24 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von n,n,n',n'-tetraacetylethylendiamin
DE3609735A1 (de) 1986-03-22 1987-09-24 Henkel Kgaa Verfahren zur reinigung von tetraacetylethylendiamin
DK156052C (da) * 1987-02-11 1989-11-06 Cheminova As Fremgangsmaade til fremstilling af n,n,n',n'-tetraacetylethylendiamin
IT1245724B (it) * 1990-11-09 1994-10-14 Caffaro Spa Ind Chim Procedimento di purificazione della taed
US8258341B2 (en) 2009-07-10 2012-09-04 E.I. Du Pont De Nemours And Company Polyfluorosulfonamido amine and intermediate
CN101891644A (zh) * 2009-11-19 2010-11-24 华东理工大学 一种四乙酰乙二胺的合成方法
CN102030678B (zh) * 2010-11-19 2013-12-04 浙江大学 一种四乙酰乙二胺重结晶的方法
WO2013171492A1 (en) 2012-05-18 2013-11-21 Warwick International Group Limited Activation of peroxygen bleach
US20140021157A1 (en) * 2012-07-20 2014-01-23 Closure Systems International, Inc. Lightweight closure and container package
CN103121960B (zh) * 2013-02-22 2015-04-01 浙江金科日化原料有限公司 一种四乙酰乙二胺的高效重结晶方法
CN103694132B (zh) * 2013-11-28 2016-01-20 浙江金科日化原料有限公司 一种高纯度三乙酰乙二胺的制备方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES257803A1 (es) * 1959-06-06 1960-11-01 Konink Ind Mij Voorheen Noury Un procedimiento para preparar un agente de lavado y o de blanqueo
US3539629A (en) * 1968-03-13 1970-11-10 Fmc Corp Process for producing tetraacetyl derivatives of diamines
US3824286A (en) * 1970-07-07 1974-07-16 Lever Brothers Ltd Preparation of polyacetylalkylene diamines
DE2052822C3 (de) * 1970-10-28 1979-04-19 Basf Ag, 6700 Ludwigshafen Verfahren zur Herstellung von N,N,N',N'-Tetraacetyläthylendiamin
DE2118281A1 (de) * 1971-04-15 1972-11-02 Badische Anilin- & Soda-Fabrik Ag, 6700 Ludwigshafen Verfahren zur kontinuierlichen Herstellung von N,N,N,N-Tetraacetyläthylendiamin
US3755225A (en) 1971-08-17 1973-08-28 Diamond Shamrock Corp Process for preparing homo- and copolymers of vinyl chloride in aqueous emulsion with post addition of a water-soluble ethylene oxide-ethylene glycol adduct
US3886212A (en) * 1973-02-19 1975-05-27 Wacker Chemie Gmbh Process for preparing N,N,N{40 ,N{40 -tetraacetyl compounds

Also Published As

Publication number Publication date
JPS54138512A (en) 1979-10-27
US4240980A (en) 1980-12-23
DE2960395D1 (en) 1981-09-17
EP0004919B1 (de) 1981-06-10
EP0004919A1 (de) 1979-10-31
PT69485A (de) 1979-05-01
DK153379A (da) 1979-10-15
ATA272679A (de) 1982-12-15
YU87579A (en) 1982-08-31
JPS6233223B2 (es) 1987-07-20
CA1110660A (en) 1981-10-13
AT371802B (de) 1983-08-10

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Legal Events

Date Code Title Description
FD1A Patent lapsed

Effective date: 20000201