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ES2131273T3 - Procedimiento para la purificacion de (-)-n-isopulegol y composiciones perfumantes de citricos que contienen (-)-n-isopulegol purificado. - Google Patents

Procedimiento para la purificacion de (-)-n-isopulegol y composiciones perfumantes de citricos que contienen (-)-n-isopulegol purificado.

Info

Publication number
ES2131273T3
ES2131273T3 ES95305247T ES95305247T ES2131273T3 ES 2131273 T3 ES2131273 T3 ES 2131273T3 ES 95305247 T ES95305247 T ES 95305247T ES 95305247 T ES95305247 T ES 95305247T ES 2131273 T3 ES2131273 T3 ES 2131273T3
Authority
ES
Spain
Prior art keywords
isopulegol
purified
purification
procedure
perfuming compositions
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES95305247T
Other languages
English (en)
Inventor
Takeshi Yamamoto
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Takasago International Corp
Original Assignee
Takasago International Corp
Takasago Perfumery Industry Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Takasago International Corp, Takasago Perfumery Industry Co filed Critical Takasago International Corp
Application granted granted Critical
Publication of ES2131273T3 publication Critical patent/ES2131273T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • C11B9/022—Refining
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/78—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by condensation or crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C35/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring
    • C07C35/02—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring monocyclic
    • C07C35/08—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring monocyclic containing a six-membered rings
    • C07C35/18—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring monocyclic containing a six-membered rings with unsaturation at least in the ring
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
    • C11B9/0034—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing six carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/07—Optical isomers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Fats And Perfumes (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Cosmetics (AREA)
  • Seasonings (AREA)

Abstract

PARA SU PURIFICACION, EL ISOPULEGOL PRINCIPALMENTE COMPUESTO DE (-)-N-ISOPULEGOL SE ENFRIA PROFUNDAMENTE EN UN SOLVENTE QUE COMPRENDE PRINCIPALMENTE ACETONA PARA OBTENER (-)-N-ISOPULEGOL QUE TIENE UNA PUREZA QUIMICA NO INFERIOR AL 99.7%, Y UNA PUREZA OPTICA NO INFERIOR DE 99.7%E.E. EL (-)-N-ISOPULEGOL ASI PURIFICADO NO TIENE OLOR E IMPARTE UN GUSTO DE FRESCOR, SUAVIDAD Y FRIALDAD A UNA COMPOSICION DE PERFUME DE CITRICO CUANDO ESTA PRESENTE EN UNA CANTIDAD DE ENTRE EL 3% Y EL 30% DE SU PESO.
ES95305247T 1994-07-29 1995-07-27 Procedimiento para la purificacion de (-)-n-isopulegol y composiciones perfumantes de citricos que contienen (-)-n-isopulegol purificado. Expired - Lifetime ES2131273T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP19628294A JP3241542B2 (ja) 1994-07-29 1994-07-29 （−）−ｎ−イソプレゴールの精製方法及びその方法で得られた（−）−ｎ−イソプレゴールを含有するシトラス系香料組成物

Publications (1)

Publication Number Publication Date
ES2131273T3 true ES2131273T3 (es) 1999-07-16

Family

ID=16355215

Family Applications (1)

Application Number Title Priority Date Filing Date
ES95305247T Expired - Lifetime ES2131273T3 (es) 1994-07-29 1995-07-27 Procedimiento para la purificacion de (-)-n-isopulegol y composiciones perfumantes de citricos que contienen (-)-n-isopulegol purificado.

Country Status (5)

Country Link
US (1) US5773410A (es)
EP (1) EP0694514B1 (es)
JP (1) JP3241542B2 (es)
DE (1) DE69508859T2 (es)
ES (1) ES2131273T3 (es)

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US7470244B2 (en) * 1996-01-26 2008-12-30 Harrison Jr Shelton E Flexion-discouraging splint system, method and device
US8512718B2 (en) 2000-07-03 2013-08-20 Foamix Ltd. Pharmaceutical composition for topical application
KR100540669B1 (ko) 2000-11-06 2006-01-11 니뽄 다바코 산교 가부시키가이샤 담배취 소취향료조성물, 담배취 소취제, 및 부류연기취가적은 궐련 및 담배 패키지
DE10112362B4 (de) * 2001-03-15 2004-09-30 Bayerische Motoren Werke Ag Montagevorrichtung
IL152486A0 (en) 2002-10-25 2003-05-29 Meir Eini Alcohol-free cosmetic and pharmaceutical foam carrier
US10117812B2 (en) 2002-10-25 2018-11-06 Foamix Pharmaceuticals Ltd. Foamable composition combining a polar solvent and a hydrophobic carrier
US20080138296A1 (en) 2002-10-25 2008-06-12 Foamix Ltd. Foam prepared from nanoemulsions and uses
US7820145B2 (en) 2003-08-04 2010-10-26 Foamix Ltd. Oleaginous pharmaceutical and cosmetic foam
US9265725B2 (en) 2002-10-25 2016-02-23 Foamix Pharmaceuticals Ltd. Dicarboxylic acid foamable vehicle and pharmaceutical compositions thereof
BR0314916A (pt) 2002-10-25 2005-08-16 Foamix Ltd Espuma farmacêutica e cosmética
US9211259B2 (en) 2002-11-29 2015-12-15 Foamix Pharmaceuticals Ltd. Antibiotic kit and composition and uses thereof
US7700076B2 (en) 2002-10-25 2010-04-20 Foamix, Ltd. Penetrating pharmaceutical foam
US8900554B2 (en) 2002-10-25 2014-12-02 Foamix Pharmaceuticals Ltd. Foamable composition and uses thereof
US9668972B2 (en) 2002-10-25 2017-06-06 Foamix Pharmaceuticals Ltd. Nonsteroidal immunomodulating kit and composition and uses thereof
US8486376B2 (en) 2002-10-25 2013-07-16 Foamix Ltd. Moisturizing foam containing lanolin
US7704518B2 (en) 2003-08-04 2010-04-27 Foamix, Ltd. Foamable vehicle and pharmaceutical compositions thereof
US7575739B2 (en) 2003-04-28 2009-08-18 Foamix Ltd. Foamable iodine composition
US8795693B2 (en) 2003-08-04 2014-08-05 Foamix Ltd. Compositions with modulating agents
US8486374B2 (en) 2003-08-04 2013-07-16 Foamix Ltd. Hydrophilic, non-aqueous pharmaceutical carriers and compositions and uses
RU2375049C2 (ru) * 2005-01-04 2009-12-10 ТЕЙКОКУ ФАРМА ЮЭсЭй, ИНК. Охлаждающий пластырь для местного применения
DE102005040655A1 (de) * 2005-08-26 2007-03-01 Basf Ag Verfahren zur Herstellung von angereichertem Isopulegol
CN101534805A (zh) * 2005-10-24 2009-09-16 帝国制药美国公司 包含n，2，3-三甲基-2-异丙基丁酰胺的局部止痛组合物及其使用方法
US20080260655A1 (en) 2006-11-14 2008-10-23 Dov Tamarkin Substantially non-aqueous foamable petrolatum based pharmaceutical and cosmetic compositions and their uses
US8636982B2 (en) 2007-08-07 2014-01-28 Foamix Ltd. Wax foamable vehicle and pharmaceutical compositions thereof
EP2036875A1 (de) * 2007-09-11 2009-03-18 Basf Se Kontinuierliches Verfahren zur Herstellung von Menthol in reiner oder angereicherter Form
EP2225192B1 (de) * 2007-11-30 2017-05-03 Basf Se Verfahren zur herstellung von optisch aktivem und racemischem menthol
WO2009069006A2 (en) 2007-11-30 2009-06-04 Foamix Ltd. Foam containing benzoyl peroxide
US8518376B2 (en) 2007-12-07 2013-08-27 Foamix Ltd. Oil-based foamable carriers and formulations
WO2009090495A2 (en) 2007-12-07 2009-07-23 Foamix Ltd. Oil and liquid silicone foamable carriers and formulations
WO2009090558A2 (en) 2008-01-14 2009-07-23 Foamix Ltd. Poloxamer foamable pharmaceutical compositions with active agents and/or therapeutic cells and uses
US8992783B2 (en) 2008-09-05 2015-03-31 Max-Planck-Gessellschaft zur förderung der Wissenschaften e.V. Process for enantioseparation of chiral systems with compound formation using two subsequent crystallization steps
KR101686901B1 (ko) 2009-02-17 2016-12-15 나가오카 ＆ 컴퍼니 리미티드 천연 ｌ-멘톨을 제조하기 위한 방법 및 기구
WO2010125470A2 (en) 2009-04-28 2010-11-04 Foamix Ltd. Foamable vehicle and pharmaceutical compositions comprising aprotic polar solvents and uses thereof
CA2769625C (en) 2009-07-29 2017-04-11 Foamix Ltd. Non surfactant hydro-alcoholic foamable compositions, breakable foams and their uses
CA2769677A1 (en) 2009-07-29 2011-02-03 Foamix Ltd. Non surface active agent non polymeric agent hydro-alcoholic foamable compositions, breakable foams and their uses
WO2011064631A1 (en) 2009-10-02 2011-06-03 Foamix Ltd. Surfactant-free, water-free, foamable compositions and breakable foams and their uses
US9849142B2 (en) 2009-10-02 2017-12-26 Foamix Pharmaceuticals Ltd. Methods for accelerated return of skin integrity and for the treatment of impetigo
JP5780933B2 (ja) * 2010-12-01 2015-09-16 高砂香料工業株式会社 光学活性メントールの製造方法
WO2013033501A1 (en) 2011-09-01 2013-03-07 Takasago International Corp. (Usa) Novel substituted cyclohexane compounds
WO2014077323A1 (ja) * 2012-11-15 2014-05-22 高砂香料工業株式会社 光学活性イソプレゴールおよび光学活性メントールの製造方法
MX2017010841A (es) * 2015-02-24 2017-12-11 Takasago Perfumery Co Ltd Composiciones mejoradas de perfume.
US20190048285A1 (en) * 2016-02-24 2019-02-14 Takasago International Corporation Stimulating agent
WO2017146181A2 (en) 2016-02-24 2017-08-31 Takasago International Corporation Household product delivering cooling sensations
WO2017146182A2 (en) 2016-02-24 2017-08-31 Takasago International Corporation Household product delivering warming and/or tingling sensations
BR112019002199B1 (pt) 2016-08-04 2023-02-07 Takasago International Corporation Composto, composição de aquecimento, composição aromatizante ou de fragrância, composição tópica, produto de consumo e método para melhorar, aperfeiçoar ou modificar as propriedades de sabor ou de odor de uma composição aromatizante ou de fragrância
US10398641B2 (en) 2016-09-08 2019-09-03 Foamix Pharmaceuticals Ltd. Compositions and methods for treating rosacea and acne
EP3388411A1 (en) 2017-04-13 2018-10-17 Sulzer Chemtech AG A process for purifying a crude composition including a monoterpene compound, such as a monocyclic monoterpene alcohol, by layer melt crystallization
EP3900697B1 (en) 2020-04-21 2023-03-15 Takasago International Corporation Fragrance composition
ES2948614T3 (es) 2020-04-21 2023-09-14 Takasago Perfumery Co Ltd Composición de fragancia encapsulada

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US3218361A (en) * 1960-06-08 1965-11-16 Glidden Co Process for recovering specific isopulegols
US4217371A (en) * 1978-10-20 1980-08-12 International Flavors & Fragrances Inc. Flavoring with cyclohexene methanol lower alkyl esters
US5545424A (en) * 1994-10-12 1996-08-13 Takasago International Corporation 4-(1-menthoxymethyl)-2-phenyl-1,3-dioxolane or its derivatives and flavor composition containing the same

Also Published As

Publication number Publication date
JP3241542B2 (ja) 2001-12-25
DE69508859D1 (de) 1999-05-12
EP0694514B1 (en) 1999-04-07
EP0694514A3 (en) 1996-03-27
EP0694514A2 (en) 1996-01-31
US5773410A (en) 1998-06-30
DE69508859T2 (de) 1999-10-07
JPH0840959A (ja) 1996-02-13

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