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DE69508859D1 - Verfahren zur Reinigung von (-)-n-Isopulegol sowie gereinigtes (-)-n-Isopulegol enthaltende Zitrusparfümzusammensetzungen - Google Patents

Verfahren zur Reinigung von (-)-n-Isopulegol sowie gereinigtes (-)-n-Isopulegol enthaltende Zitrusparfümzusammensetzungen

Info

Publication number
DE69508859D1
DE69508859D1 DE69508859T DE69508859T DE69508859D1 DE 69508859 D1 DE69508859 D1 DE 69508859D1 DE 69508859 T DE69508859 T DE 69508859T DE 69508859 T DE69508859 T DE 69508859T DE 69508859 D1 DE69508859 D1 DE 69508859D1
Authority
DE
Germany
Prior art keywords
isopulegol
purified
purification
perfume compositions
containing citrus
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69508859T
Other languages
English (en)
Other versions
DE69508859T2 (de
Inventor
Takeshi Yamamoto
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Takasago International Corp
Original Assignee
Takasago International Corp
Takasago Perfumery Industry Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Takasago International Corp, Takasago Perfumery Industry Co filed Critical Takasago International Corp
Publication of DE69508859D1 publication Critical patent/DE69508859D1/de
Application granted granted Critical
Publication of DE69508859T2 publication Critical patent/DE69508859T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • C11B9/022—Refining
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/78—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by condensation or crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C35/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring
    • C07C35/02—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring monocyclic
    • C07C35/08—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring monocyclic containing a six-membered rings
    • C07C35/18—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring monocyclic containing a six-membered rings with unsaturation at least in the ring
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
    • C11B9/0034—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing six carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/07—Optical isomers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Fats And Perfumes (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Cosmetics (AREA)
  • Seasonings (AREA)
DE69508859T 1994-07-29 1995-07-27 Verfahren zur Reinigung von (-)-n-Isopulegol sowie gereinigtes (-)-n-Isopulegol enthaltende Zitrusparfümzusammensetzungen Expired - Lifetime DE69508859T2 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP19628294A JP3241542B2 (ja) 1994-07-29 1994-07-29 （−）−ｎ−イソプレゴールの精製方法及びその方法で得られた（−）−ｎ−イソプレゴールを含有するシトラス系香料組成物

Publications (2)

Publication Number Publication Date
DE69508859D1 true DE69508859D1 (de) 1999-05-12
DE69508859T2 DE69508859T2 (de) 1999-10-07

Family

ID=16355215

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69508859T Expired - Lifetime DE69508859T2 (de) 1994-07-29 1995-07-27 Verfahren zur Reinigung von (-)-n-Isopulegol sowie gereinigtes (-)-n-Isopulegol enthaltende Zitrusparfümzusammensetzungen

Country Status (5)

Country Link
US (1) US5773410A (de)
EP (1) EP0694514B1 (de)
JP (1) JP3241542B2 (de)
DE (1) DE69508859T2 (de)
ES (1) ES2131273T3 (de)

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US7470244B2 (en) * 1996-01-26 2008-12-30 Harrison Jr Shelton E Flexion-discouraging splint system, method and device
US8512718B2 (en) 2000-07-03 2013-08-20 Foamix Ltd. Pharmaceutical composition for topical application
PT1336345E (pt) 2000-11-06 2009-11-16 Japan Tobacco Inc Composições de perfume para desodorizar tabaco, agentes desodorizantes contra tabaco e embalagens de cigarros e tabaco com emissão de pequeno caudal de cheiro a fumo
DE10112362B4 (de) * 2001-03-15 2004-09-30 Bayerische Motoren Werke Ag Montagevorrichtung
IL152486A0 (en) 2002-10-25 2003-05-29 Meir Eini Alcohol-free cosmetic and pharmaceutical foam carrier
WO2004037225A2 (en) 2002-10-25 2004-05-06 Foamix Ltd. Cosmetic and pharmaceutical foam
US20080138296A1 (en) 2002-10-25 2008-06-12 Foamix Ltd. Foam prepared from nanoemulsions and uses
US7704518B2 (en) 2003-08-04 2010-04-27 Foamix, Ltd. Foamable vehicle and pharmaceutical compositions thereof
US7820145B2 (en) 2003-08-04 2010-10-26 Foamix Ltd. Oleaginous pharmaceutical and cosmetic foam
US7700076B2 (en) 2002-10-25 2010-04-20 Foamix, Ltd. Penetrating pharmaceutical foam
US9265725B2 (en) 2002-10-25 2016-02-23 Foamix Pharmaceuticals Ltd. Dicarboxylic acid foamable vehicle and pharmaceutical compositions thereof
US10117812B2 (en) 2002-10-25 2018-11-06 Foamix Pharmaceuticals Ltd. Foamable composition combining a polar solvent and a hydrophobic carrier
US8486376B2 (en) 2002-10-25 2013-07-16 Foamix Ltd. Moisturizing foam containing lanolin
US9668972B2 (en) 2002-10-25 2017-06-06 Foamix Pharmaceuticals Ltd. Nonsteroidal immunomodulating kit and composition and uses thereof
US8900554B2 (en) 2002-10-25 2014-12-02 Foamix Pharmaceuticals Ltd. Foamable composition and uses thereof
US9211259B2 (en) 2002-11-29 2015-12-15 Foamix Pharmaceuticals Ltd. Antibiotic kit and composition and uses thereof
US7575739B2 (en) 2003-04-28 2009-08-18 Foamix Ltd. Foamable iodine composition
US8486374B2 (en) 2003-08-04 2013-07-16 Foamix Ltd. Hydrophilic, non-aqueous pharmaceutical carriers and compositions and uses
US8795693B2 (en) 2003-08-04 2014-08-05 Foamix Ltd. Compositions with modulating agents
SI1833443T1 (sl) * 2005-01-04 2012-03-30 Teikoku Pharma Usa Inc Hladilni pripravek v obliki topičnega obliža
DE102005040655A1 (de) * 2005-08-26 2007-03-01 Basf Ag Verfahren zur Herstellung von angereichertem Isopulegol
RU2407522C2 (ru) 2005-10-24 2010-12-27 ТЕЙКОКУ ФАРМА ЮЭсЭй, ИНК. Болеутоляющие композиции n,2,3-триметил-2-изопропилбутамида местного действия и способы их применения
US20080260655A1 (en) 2006-11-14 2008-10-23 Dov Tamarkin Substantially non-aqueous foamable petrolatum based pharmaceutical and cosmetic compositions and their uses
US8636982B2 (en) 2007-08-07 2014-01-28 Foamix Ltd. Wax foamable vehicle and pharmaceutical compositions thereof
EP2036875A1 (de) * 2007-09-11 2009-03-18 Basf Se Kontinuierliches Verfahren zur Herstellung von Menthol in reiner oder angereicherter Form
CN101932543B (zh) * 2007-11-30 2014-07-30 巴斯夫欧洲公司 生产光学活性、外消旋薄荷醇的方法
US9439857B2 (en) 2007-11-30 2016-09-13 Foamix Pharmaceuticals Ltd. Foam containing benzoyl peroxide
US8518376B2 (en) 2007-12-07 2013-08-27 Foamix Ltd. Oil-based foamable carriers and formulations
WO2009090495A2 (en) 2007-12-07 2009-07-23 Foamix Ltd. Oil and liquid silicone foamable carriers and formulations
CA2712120A1 (en) 2008-01-14 2009-07-23 Foamix Ltd. Poloxamer foamable pharmaceutical compositions with active agents and/or therapeutic cells and uses
EP2334620B1 (de) 2008-09-05 2018-09-05 Max-Planck-Gesellschaft zur Förderung der Wissenschaften e.V. Verfahren zur enantioselektiven trennung chiraler systeme mit verbindungsbildung unter anwendung von zwei aufeinanderfolgenden kristallisationsschritten
JP5603884B2 (ja) 2009-02-17 2014-10-08 長岡実業株式会社 天然ｌ−メントールを生成するための方法及び装置
CA2760186C (en) 2009-04-28 2019-10-29 Foamix Ltd. Foamable vehicle and pharmaceutical compositions comprising aprotic polar solvents and uses thereof
WO2011013008A2 (en) 2009-07-29 2011-02-03 Foamix Ltd. Non surface active agent non polymeric agent hydro-alcoholic foamable compositions, breakable foams and their uses
WO2011013009A2 (en) 2009-07-29 2011-02-03 Foamix Ltd. Non surfactant hydro-alcoholic foamable compositions, breakable foams and their uses
BR112012007473A2 (pt) 2009-10-02 2019-05-07 Foamix Ltd composições tópicas de tetraciclina e respectivo método de uso
US9849142B2 (en) 2009-10-02 2017-12-26 Foamix Pharmaceuticals Ltd. Methods for accelerated return of skin integrity and for the treatment of impetigo
JP5780933B2 (ja) * 2010-12-01 2015-09-16 高砂香料工業株式会社 光学活性メントールの製造方法
EP3262955A3 (de) 2011-09-01 2018-03-14 Takasago International Corporation (USA) Neuartige substituierte cyclohexanverbindungen
EP2921228A1 (de) * 2012-11-15 2015-09-23 Takasago International Corporation Verfahren zur herstellung von optisch aktivem isopulegol und optisch aktivem menthol
EP3984599A1 (de) 2015-02-24 2022-04-20 Takasago International Corporation Verbesserte parfümzusammensetzungen
WO2017146183A1 (en) 2016-02-24 2017-08-31 Takasago International Corporation Stimulating agent
US20190054200A1 (en) 2016-02-24 2019-02-21 Takasago International Corporation Household product delivering warming and/or tingling sensations
WO2017146181A2 (en) 2016-02-24 2017-08-31 Takasago International Corporation Household product delivering cooling sensations
WO2018027202A1 (en) 2016-08-04 2018-02-08 Takasago International Corporation (Usa) Warming sensation compounds
MX2020012139A (es) 2016-09-08 2021-01-29 Vyne Pharmaceuticals Inc Composiciones y metodos para tratar rosacea y acne.
EP3388411A1 (de) * 2017-04-13 2018-10-17 Sulzer Chemtech AG Verfahren zur reinigung einer rohzusammensetzung mit einer monoterpenverbindung, wie monocyclischer monoterpenalkohol, alkohol durch schichtschmelzkristallisation
ES2948614T3 (es) 2020-04-21 2023-09-14 Takasago Perfumery Co Ltd Composición de fragancia encapsulada
EP3900697B1 (de) 2020-04-21 2023-03-15 Takasago International Corporation Duftstoffzusammensetzung

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3218361A (en) * 1960-06-08 1965-11-16 Glidden Co Process for recovering specific isopulegols
US4217371A (en) * 1978-10-20 1980-08-12 International Flavors & Fragrances Inc. Flavoring with cyclohexene methanol lower alkyl esters
US5545424A (en) * 1994-10-12 1996-08-13 Takasago International Corporation 4-(1-menthoxymethyl)-2-phenyl-1,3-dioxolane or its derivatives and flavor composition containing the same

Also Published As

Publication number Publication date
EP0694514A2 (de) 1996-01-31
EP0694514A3 (de) 1996-03-27
US5773410A (en) 1998-06-30
EP0694514B1 (de) 1999-04-07
JPH0840959A (ja) 1996-02-13
ES2131273T3 (es) 1999-07-16
JP3241542B2 (ja) 2001-12-25
DE69508859T2 (de) 1999-10-07

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Legal Events

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8364 No opposition during term of opposition