CN204469271U - A kind of Extraction and isolation purification devices - Google Patents
A kind of Extraction and isolation purification devices Download PDFInfo
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- CN204469271U CN204469271U CN201520137112.1U CN201520137112U CN204469271U CN 204469271 U CN204469271 U CN 204469271U CN 201520137112 U CN201520137112 U CN 201520137112U CN 204469271 U CN204469271 U CN 204469271U
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- extraction
- tank
- evaporator
- condenser
- separator
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- 238000000605 extraction Methods 0.000 title claims abstract description 54
- 238000000746 purification Methods 0.000 title claims abstract description 12
- 238000002955 isolation Methods 0.000 title 1
- 238000000926 separation method Methods 0.000 claims abstract description 13
- 238000005485 electric heating Methods 0.000 claims abstract description 8
- 239000002904 solvent Substances 0.000 claims abstract description 6
- 238000002425 crystallisation Methods 0.000 claims abstract description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 5
- 230000008025 crystallization Effects 0.000 claims abstract description 4
- 239000007788 liquid Substances 0.000 claims description 11
- 239000004480 active ingredient Substances 0.000 abstract description 5
- 238000005265 energy consumption Methods 0.000 abstract description 3
- 238000000034 method Methods 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 2
- 238000002137 ultrasound extraction Methods 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 239000000741 silica gel Substances 0.000 description 1
- 229910002027 silica gel Inorganic materials 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
Landscapes
- Extraction Or Liquid Replacement (AREA)
Abstract
本实用新型涉及一种提取与分离纯化装置，主要解决现有技术中提取率低、能耗大，设备结构复杂的问题，其包括提取罐，蒸发器，分离器，冷凝器，超声波换能器，提取罐上部有进料口，溶剂入口，以及进水管，提取罐的中部设置超声波换能器，提取罐中下部设置有过滤筛，提取罐底部设置常闭提取口，提取罐的底部设置出料口并通过管路和蒸发器相连接，蒸发器为双层罐体结构，内外层中间设置电加热装置，电加热装置通过控制器来控制温度，蒸发器通过管路与分离器相连，分离器通过管路与冷凝器相连，冷凝器通过管路与提取罐上部相连，从而形成一个闭合回路，所有管路上均设置至少一个阀门，常闭提取口下部连接浓缩结晶罐。本装置结构紧凑，性能稳定，能有效的提升有效成份的提取率和分离纯化率，有广泛的应用前景。
The utility model relates to an extraction, separation and purification device, which mainly solves the problems of low extraction rate, high energy consumption and complicated equipment structure in the prior art, which includes an extraction tank, an evaporator, a separator, a condenser and an ultrasonic transducer , the upper part of the extraction tank has a feed inlet, a solvent inlet, and a water inlet pipe. The middle part of the extraction tank is equipped with an ultrasonic transducer. The feed port is connected to the evaporator through the pipeline. The evaporator is a double-layer tank structure. An electric heating device is installed in the middle of the inner and outer layers. The electric heating device controls the temperature through the controller. The evaporator is connected to the separator through the pipeline. The condenser is connected to the condenser through pipelines, and the condenser is connected to the upper part of the extraction tank through pipelines, thereby forming a closed circuit. At least one valve is arranged on all pipelines, and the lower part of the normally closed extraction port is connected to the concentration crystallization tank. The device has compact structure and stable performance, can effectively improve the extraction rate and separation and purification rate of active ingredients, and has wide application prospects.
Description
技术领域 technical field
本实用新型涉及一种提取与分离纯化装置。 The utility model relates to an extraction, separation and purification device.
背景技术 Background technique
从药材或有机物中提取有效成份用于专门的治疗效果是目前常用的一种研制方法，目前的一些提取设备和分离设备采用溶剂提取，硅胶柱分离，多次浓缩、结晶的方法进行，但该方法提取率低，能耗大，设备结构复杂，难以大规模产业化。 Extracting active ingredients from medicinal materials or organic matter for special therapeutic effects is a common development method at present. Some current extraction equipment and separation equipment use solvent extraction, silica gel column separation, multiple concentration and crystallization methods, but this The extraction rate of the method is low, the energy consumption is large, the equipment structure is complicated, and it is difficult to be industrialized on a large scale.
实用新型内容 Utility model content
本实用新型的目的就在于提供一种提取与分离纯化装置，解决现有技术中提取率低、能耗大，设备结构复杂的问题。 The purpose of the utility model is to provide an extraction, separation and purification device to solve the problems of low extraction rate, high energy consumption and complex equipment structure in the prior art.
为了实现上述目的，本实用新型采用如下技术方案：一种提取与分离纯化装置，包括提取罐，蒸发器，分离器，冷凝器，超声波换能器，提取罐上部有进料口，溶剂入口，以及进水管，提取罐的中部设置超声波换能器，提取罐中下部设置有过滤筛，提取罐底部设置常闭提取口，提取罐的底部设置出料口并通过管路和蒸发器相连接，蒸发器为双层罐体结构，内外层中间设置电加热装置，电加热装置通过控制器来控制温度，蒸发器通过管路与分离器相连，分离器通过管路与冷凝器相连，冷凝器通过管路与提取罐上部相连，从而形成一个闭合回路，所有管路上均设置至少一个阀门，常闭提取口下部连接浓缩结晶罐。 In order to achieve the above object, the utility model adopts the following technical scheme: an extraction and separation and purification device, including an extraction tank, an evaporator, a separator, a condenser, an ultrasonic transducer, and an upper part of the extraction tank with a feed port and a solvent inlet, And the water inlet pipe, the middle part of the extraction tank is provided with an ultrasonic transducer, the middle and lower part of the extraction tank is provided with a filter screen, the bottom of the extraction tank is provided with a normally closed extraction port, the bottom of the extraction tank is provided with a discharge port and connected to the evaporator through a pipeline, The evaporator is a double-layer tank structure, and an electric heating device is installed in the middle of the inner and outer layers. The electric heating device controls the temperature through a controller. The evaporator is connected to the separator through a pipeline, and the separator is connected to the condenser through a pipeline. The pipelines are connected to the upper part of the extraction tank to form a closed circuit, and at least one valve is arranged on all the pipelines, and the lower part of the normally closed extraction port is connected to the concentration crystallization tank.
分离器可以是油液分离器，或者固液分离器，或气液分离器。 The separator can be an oil-liquid separator, or a solid-liquid separator, or a gas-liquid separator.
与现有技术相比，本实用新型的优点在于： Compared with the prior art, the utility model has the advantages of:
本实用新型在传统的提热工艺当中加入超声波换能器，增加超声提取工艺，有效的提升了提取和纯化效果，同时，整个装置形成闭路，溶剂添加量少，采用控制器来控制加热温度，能根据不同的提取要求控制蒸发器的加热温度。本产品结构紧凑，性能稳定，能有效的提升有效成份的提取率和分离纯化率。 The utility model adds an ultrasonic transducer to the traditional heating process, increases the ultrasonic extraction process, and effectively improves the extraction and purification effects. At the same time, the entire device forms a closed circuit, and the amount of solvent added is small. The controller is used to control the heating temperature. The heating temperature of the evaporator can be controlled according to different extraction requirements. This product has compact structure and stable performance, which can effectively improve the extraction rate and separation and purification rate of active ingredients.
附图说明 Description of drawings
图1为本实用新型的结构示意图。 Fig. 1 is the structural representation of the utility model.
具体实施方式 Detailed ways
下面将结合附图和具体实施对本实用新型作进一步说明； The utility model will be further described below in conjunction with accompanying drawing and specific implementation;
参见图1：一种提取与分离纯化装置，包括提取罐1，蒸发器7，分离器8，冷凝器9，超声波换能器4，提取罐1上部有进料口2，溶剂入口3，以及进水管10，提取罐1的中部设置超声波换能器4，提取罐1中下部设置有过滤筛5，提取罐底部设置常闭提取口，提取罐1的底部设置出料口并通过管路和蒸发器7相连接，蒸发器7为双层罐体结构，内外层中间设置电加热装置，电加热装置通过控制器来控制温度，蒸发器7通过管路与分离器8相连，分离器8通过管路与冷凝器9相连，冷凝器9通过管路与提取罐1上部相连，从而形成一个闭合回路，所有管路上均设置至少一个阀门，常闭提取口下部连接浓缩结晶罐11。 Referring to Fig. 1: a kind of extraction and separation and purification device comprises extraction tank 1, evaporator 7, separator 8, condenser 9, ultrasonic transducer 4, and extraction tank 1 top has feed inlet 2, solvent inlet 3, and The water inlet pipe 10, the ultrasonic transducer 4 is arranged in the middle part of the extraction tank 1, the filter screen 5 is arranged in the middle and lower part of the extraction tank 1, the normally closed extraction port is arranged at the bottom of the extraction tank, the discharge port is arranged at the bottom of the extraction tank 1 and passes through the pipeline and The evaporator 7 is connected to each other, the evaporator 7 is a double-layer tank structure, an electric heating device is installed in the middle of the inner and outer layers, the electric heating device controls the temperature through a controller, the evaporator 7 is connected to the separator 8 through a pipeline, and the separator 8 passes The pipeline is connected to the condenser 9, and the condenser 9 is connected to the upper part of the extraction tank 1 through the pipeline to form a closed loop. At least one valve is arranged on all the pipelines, and the bottom of the normally closed extraction port is connected to the concentration crystallization tank 11.
分离器8可以是油液分离器，或者固液分离器，或气液分离器。 The separator 8 may be an oil-liquid separator, or a solid-liquid separator, or a gas-liquid separator.
物料从进料口进入提取罐，加入溶剂和水首先要经过超声波换能器进行超声提取，之后经过过滤筛之后进入蒸发器进行加热，通过该工艺之后，产生的高温蒸汽进入分离器进行分离，分离之后的气体或液体进入冷凝器冷凝，之后收集到的冷凝液体回流到提取罐进行下次的提取过程，如此往复，经过实验证明，通过该提取装置进行药物有效成份的提取，能够有效分离和纯化提取物，本装置性能稳定，能够有效的提升有效成份的提取率和分离纯化率。 The material enters the extraction tank from the feed port. After adding solvent and water, it first passes through the ultrasonic transducer for ultrasonic extraction, and then passes through the filter screen and then enters the evaporator for heating. After passing through this process, the high-temperature steam generated enters the separator for separation. The separated gas or liquid enters the condenser to condense, and then the collected condensed liquid returns to the extraction tank for the next extraction process, and so on. Experiments have proved that the extraction of the active ingredients of the drug through the extraction device can effectively separate and extract To purify the extract, this device has stable performance and can effectively improve the extraction rate and separation and purification rate of active ingredients.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520137112.1U CN204469271U (en) | 2015-03-11 | 2015-03-11 | A kind of Extraction and isolation purification devices |
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| CN201520137112.1U CN204469271U (en) | 2015-03-11 | 2015-03-11 | A kind of Extraction and isolation purification devices |
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| CN204469271U true CN204469271U (en) | 2015-07-15 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113018897A (en) * | 2021-03-05 | 2021-06-25 | 安徽工业大学 | Ultrasonic multi-solvent fractional extraction recycling device |
| CN114159832A (en) * | 2021-12-23 | 2022-03-11 | 上海信谊百路达药业有限公司 | Bilobalide B extraction element |
| CN114653093A (en) * | 2022-04-19 | 2022-06-24 | 河南农业大学 | Extraction and purification device of polysaccharide |
-
2015
- 2015-03-11 CN CN201520137112.1U patent/CN204469271U/en not_active Expired - Lifetime
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113018897A (en) * | 2021-03-05 | 2021-06-25 | 安徽工业大学 | Ultrasonic multi-solvent fractional extraction recycling device |
| CN114159832A (en) * | 2021-12-23 | 2022-03-11 | 上海信谊百路达药业有限公司 | Bilobalide B extraction element |
| CN114653093A (en) * | 2022-04-19 | 2022-06-24 | 河南农业大学 | Extraction and purification device of polysaccharide |
| CN114653093B (en) * | 2022-04-19 | 2023-02-28 | 河南农业大学 | A polysaccharide extraction and purification device |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20151203 Address after: 330046, Jiangxi, Nanchang province East Lake district government compound west two road newspaper building, 13 floor Patentee after: NANCHANG XINXUAN TECHNOLOGY Co.,Ltd. Address before: 330201 Jiangxi city of Nanchang province to Nanchang County Tang Zhen Nan Dian Cun backroom team Patentee before: Deng Ganping |
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| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20160214 Address after: 330033 Jiangxi province Nanchang City Meiling Changbei Development Zone foot Patentee after: JIANGXI TENGWANGGE PHARMACEUTICAL CO.,LTD. Address before: 330046, Jiangxi, Nanchang province East Lake district government compound west two road newspaper building, 13 floor Patentee before: NANCHANG XINXUAN TECHNOLOGY Co.,Ltd. |
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| CX01 | Expiry of patent term |
Granted publication date: 20150715 |