CN203365188U - High-temperature fused salt sampling device - Google Patents
High-temperature fused salt sampling device Download PDFInfo
- Publication number
- CN203365188U CN203365188U CN 201320448432 CN201320448432U CN203365188U CN 203365188 U CN203365188 U CN 203365188U CN 201320448432 CN201320448432 CN 201320448432 CN 201320448432 U CN201320448432 U CN 201320448432U CN 203365188 U CN203365188 U CN 203365188U
- Authority
- CN
- China
- Prior art keywords
- molten salt
- piston
- temperature molten
- cylinder
- sampling
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Images
Landscapes
- Sampling And Sample Adjustment (AREA)
Abstract
本实用新型提供了一种高温熔盐取样装置。所述装置包括取样管、封堵构件、彼此配合的活塞和筒体，其中，筒体的一端设置有具有通孔的筒体封头，活塞通过筒体的另一端进入筒体内部，活塞外端连接有活塞手柄；取样管的一端结合在筒体封头上，并通过筒体封头的通孔与筒体的内腔连通，取样管的另一端具有用于获取高温熔盐的开口；封堵构件包括连接件和封堵头，连接件穿过取样管将封堵头与活塞连接，封堵头设置在取样管的所述另一端附近并能够随着活塞的运动打开和关闭所述取样管的开口。本实用新型广泛适用于高温熔盐取样过程，特别适用于电解镁过程中电解槽和镁精炼槽中下部熔盐的取样过程，并且取样快速、准确。
The utility model provides a high-temperature molten salt sampling device. The device includes a sampling tube, a blocking member, a piston and a cylinder that cooperate with each other, wherein one end of the cylinder is provided with a cylinder head with a through hole, the piston enters the interior of the cylinder through the other end of the cylinder, and the outside of the piston The end is connected with a piston handle; one end of the sampling tube is combined with the cylinder head, and communicates with the inner cavity of the cylinder through the through hole of the cylinder head, and the other end of the sampling tube has an opening for obtaining high-temperature molten salt; The blocking member includes a connecting piece and a blocking head, the connecting piece passes through the sampling tube and connects the blocking head with the piston, the blocking head is arranged near the other end of the sampling tube and can open and close the plugging head with the movement of the piston. The opening of the sampling tube. The utility model is widely applicable to the sampling process of high-temperature molten salt, and is especially suitable for the sampling process of the molten salt in the lower part of the electrolytic tank and the magnesium refining tank in the process of electrolyzing magnesium, and the sampling is fast and accurate.
Description
Technical field
The utility model relates to a kind of high-temperature molten salt sampling technique field, specifically, relates to and a kind ofly can be applied to the device that the high-temperature molten salt such as fields such as magnesium eletrolysis is sampled.
Background technology
At present, high-temperature molten salt has been widely used in the every field such as molten-salt electrolysis, fused salt chlorimation as the chemical reaction medium, but temperature of molten salt is high, corrosivity is large, so the accurate sampling of fused-salt medium is always comparatively thorny.Especially in the electrolytic magnesium production run, need constantly to detect the fused salt composition, to grasp the fused salt composition situation in electrolytic tank, and according to fused salt composition situation judgement electrolysis of magnesium chloride situation.In tank room, liquid magnesium metal density is less, covers on bath surface, the process from the sampling of bottom, molten bath, inevitably can mix the metal magnesium granule that has quantity not wait in the fused salt sample, causes the inaccurate of sampling result.
The utility model content
The purpose of this utility model is to solve at least one in the deficiencies in the prior art.
For example, the purpose of this utility model is to provide a kind of and can be applied to the device that the high-temperature molten salt such as fields such as magnesium eletrolysis is sampled.
The utility model provides a kind of high-temperature molten salt sampler.Described high-temperature molten salt sampler comprises stopple coupon, plug members, the piston be fitted to each other and cylindrical shell, wherein, one end of cylindrical shell is provided with the cylindrical shell end socket with through hole, and piston enters inner barrel by the other end of cylindrical shell, and the piston outer end is connected with the piston handle; One end of stopple coupon is combined on the cylindrical shell end socket, and is communicated with the inner chamber of cylindrical shell by the through hole of cylindrical shell end socket, and the other end of stopple coupon has for obtaining the opening of high-temperature molten salt; Plug members comprises web member and block head, and web member is connected block head through stopple coupon with piston, and block head is arranged on that the described other end of stopple coupon is neighbouring also can open and close along with the motion of piston the opening of described stopple coupon.
Compared with prior art, the utility model is widely used in the high-temperature molten salt sampling process, be specially adapted to the sampling process of electrolytic tank and magnesium refining groove middle and lower part fused salt in the electrolytic magnesium process, and can be fast from the sampling of molten salt system bottom, can also effectively reduce the interference of tramp metal magnesium to fused salt sample analysis result, guarantee the accurate and effective of sampling result, thereby effectively instruct and produce.
The accompanying drawing explanation
By the description of carrying out below in conjunction with accompanying drawing, above and other purpose of the present utility model and characteristics will become apparent, wherein:
Fig. 1 shows the structural representation according to an exemplary embodiment of the utility model high-temperature molten salt sampler.
Fig. 2 shows along the cut-open view of the A-A in Fig. 1.
Description of reference numerals is as follows:
1-piston handle, 2-piston, 3-cylindrical shell, 4-keeper, 5-connecting thread, 6-threaded coupling sleeve, 7-stopple coupon, 8-water chestnut cover, 9-pole, 10-cylindrical shell end socket, 11-atmospheric valve, 12-web member and 13-block head.
Embodiment
Hereinafter, describe the exemplary embodiment according to high-temperature molten salt sampler of the present utility model in detail in connection with accompanying drawing.
Fig. 1 shows the structural representation according to an exemplary embodiment of the utility model high-temperature molten salt sampler.Fig. 2 shows along the cut-open view of the A-A in Fig. 1.
As illustrated in fig. 1 and 2, in an exemplary embodiment of the present utility model, the high-temperature molten salt sampler comprises stopple coupon 7, plug members, the piston 2 be fitted to each other and cylindrical shell 3.
One end of cylindrical shell 3 is provided with the cylindrical shell end socket 10 with through hole, and piston 2 enters cylindrical shell 3 inside by the other end of cylindrical shell 3, and piston 2 outer ends are connected with piston handle 1.
One end of stopple coupon 7 is combined on cylindrical shell end socket 10, and is communicated with the inner chamber of cylindrical shell 3 by the through hole of cylindrical shell end socket 10, and the other end of stopple coupon 7 has for obtaining the opening of high-temperature molten salt.
Plug members comprises web member 12 and block head 13, and web member 12 is connected block head 13 through stopple coupon 7 with piston 2, and block head 13 is arranged near the described other end of stopple coupon 7 also can be along with the opening of the motion opening and closing stopple coupon 7 of piston 2.
In another exemplary embodiment of the present utility model, the high-temperature molten salt sampler can also comprise the atmospheric valve 11 be opened on cylindrical shell end socket 10 on the basis of above-mentioned exemplary embodiment.Further say, the high-temperature molten salt sampler also can comprise the piston fixed component, and described piston fixed component is connected with piston handle 1 and position that can fixed piston 2.For example, as shown in Figure 1, the piston fixed component comprises pole 9 and is arranged on a plurality of anchor points (as shown in Figure 2) on piston handle 1, wherein, one end of described pole 9 is fixed on cylindrical shell 3 outer walls, and the other end of described pole 9 can be removably mounted in any one anchor point in described a plurality of anchor point.
In another exemplary embodiment of the present utility model, for the ease of being fixed on sampler, the high-temperature molten salt sampler also can comprise keeper 4, and this keeper 4 is arranged on cylindrical shell 3 or cylindrical shell end socket 10 sampler is fixed on the sampling object.
In another exemplary embodiment of the present utility model, the stopple coupon 7 of high-temperature molten salt sampler can consist of a plurality of subsample pipe string connection according to sampling depth.Therefore, high-temperature molten salt sampler of the present utility model can adapt to the high-temperature molten salt sampling operation of the various degree of depth.
In another exemplary embodiment of the present utility model, the high-temperature molten salt sampler also can comprise the water chestnut cover 8 of the described opening part that is arranged on stopple coupon 7.Can effectively prevent that like this solid formation that may exist in high-temperature molten salt from entering in stopple coupon 7.Obviously, water chestnut cover 8 can arrange or remove according to whether containing solid formation in high-temperature molten salt.
In another exemplary embodiment of the present utility model, block head 13 can be dome head, but the utility model is not limited to this.In another exemplary embodiment of the present utility model, piston 2 can consist of heat-resisting fluorosioloxane rubber, and the steel cylinder that cylindrical shell 3 can have enamel by inwall forms.Yet other piston or cylindrical shell with heat-resisting function also can be used for the utility model.
In another exemplary embodiment of the present utility model, the high-temperature molten salt sampler can be made and obtain in the following ways.
On piston 2 tops, piston handle 1 is installed.The fluorosioloxane rubber that the material of piston 2 is fine heat-resisting performance.Piston handle 1 is the T-shaped structure be comprised of hand grip portion and connecting portion.The hand grip portion that piston handle 1 is and the material of connecting portion are wooden or rigid plastic, and the bottom of the hand grip portion of piston handle 1 offers some anchor points (for example, can be the diameter aperture that is 3mm).One end of pole 9 is rotatably mounted (for example, installing by hinge means) on cylindrical shell 3, and therefore, pole 9 take the joint portion of itself and cylindrical shell 3 outsides and rotated freely as fulcrum.The locating point position be connected with pole 9 by the depression distance of adjusting piston 2 is controlled sampling amount.
The steel cylinder that cylindrical shell 3 has enamel by inwall forms.One end of cylindrical shell 3 is provided with the cylindrical shell end socket 10 with through hole, and piston 2 enters cylindrical shell 3 inside by the other end of cylindrical shell 3.Offer atmospheric valve 11 on cylindrical shell end socket 10.For example, atmospheric valve 11 can be spiral sealing device, by it, screws or opens, and can regulate cylindrical shell 3 internal pressures, realizes different sampled functions.Keeper 4 for sampler is fixed on the sampling object, keeper 4 can by welding manner connects and cylindrical shell 3 on; Perforate inwall car on the end socket of cylindrical shell 3 bottoms has connecting thread 5, for connecting stopple coupon 7.
The alundum tube that stopple coupon 7 is 10mm by a plurality of diameters forms.The two ends of each alundum tube all are processed with external thread.Screw joint casing 6 is the common stainless steel pipe, and its two ends all are processed with the internal thread with stopple coupon 7 screw thread couplings.Adjacent alundum tube is threaded connection sleeve pipe 6 and couples together.In addition, the length of alundum tube can be processed as the equal length specification of 50mm, 100mm, 300mm and 500mm as required, then, according to the sampling on-site actual situations, selects collocation to use.The mode that stopple coupon 7 adopts multistage to connect, so its assembly operation is simple, flexible, and can for example,, according to actual conditions (, sampling depth), determine the length of stopple coupon 7.
Block head 13(for example, dome head) by web member 12, be connected on piston 2, drive the dome heads motion by piston 2 motion, thereby realize the folding of the sample tap of stopple coupon 7, prevent the situation that causes sample loss even can't sample because of device gas leakage.Water chestnut cover 8 enters sample (can dismantle as required) for preventing the solid formation in fused salt, and it is threaded connection on stopple coupon 7; Dome head 13, web member 12 and water chestnut cover 8 all can adopt the 1Cr18Ni9Ti alloy steel.
When the high-temperature molten salt sampler of this exemplary embodiment of assembling, at first, according to the on-the-spot molten bath of sampling situation, determine stopple coupon 7 length, utilize threaded coupling sleeve 6 that stopple coupon 7 and water chestnut cover 8 are installed; Before cylindrical shell 3 is used, at cylindrical shell 3 inwalls, smear the lubricity that suitable grease guarantees cylindrical shell 3 inwalls, then by piston 2(with piston handle 1) in the cylindrical shell 3 of packing into, and motion makes cylindrical shell 3 inwalls evenly adhere to a small amount of grease repeatedly; Then the stopple coupon 7 connected is connected in the connecting thread 5 of cylindrical shell 3 lower ends, completes the assembling of sampler.
The high-temperature molten salt sampler of this exemplary embodiment can be realized two kinds of sampled functions: the one, and the fixed position sampling; The 2nd, measure the sample of different pool depths.Be described in detail as follows:
Adopting the first kind of way sampling (, the fixed position sampling) time, close atmospheric valve 11(also installation of relief valve not certainly), suitably press piston handle 1 downwards according to sampling amount, discharge the interior gas of cylindrical shell 3, stopple coupon 7 bottom water chestnut covers 8 are inserted to sample location, lift piston handle 1 to dome head and seal bottom stopple coupon 7 fully, then pole 9 is moved to the appropriate position of piston handle 1, prevent that piston 2 is affected by gravity descending (certain, in the situation that piston fixed support fixed component is not set, also can prevent that piston 2 gravitates are descending by alternate manners such as manual control), finally take out sampler, press piston handle 1 or open atmospheric valve 11, emitting sample gets final product.
While adopting second way sampling (that is, measuring the sample of different pool depths), at first utilize pole 9 fixed piston handles 1, open atmospheric valve 11; Then, sampler is inserted in melt and sampled, sampling is closed atmospheric valve 11 after finishing, and takes out and cooling sampler, after temperature is reduced to room temperature, after stopple coupon 7 is taken apart, can take out the fused salt sample of different depth.
In addition, after each use high-temperature molten salt sampler sampling of the present utility model finishes, as do not used for a long time this sampler, need the sampler each several part is cleaned with clear water and dried, especially the positions such as stopple coupon 7, water chestnut cover 8, dome head and threaded coupling sleeve 6.
In sum, this uses novel high-temperature molten salt sampler to be fixed position sample and to measure the sample of different pool depths high-temperature molten salt, and compares with conventional art, and it has following advantage:
(1) mode that adopts bottom to suck samples, and has avoided being positioned at the interference of the metal (for example, the magnesium metal on fused salt top in magnesium eletrolysis) of fused salt top to sampling result, and sampling accurately;
(2) stopple coupon adopts the corundum material, and high temperature resistant, salt tolerant class corrosion effectively reduces the impact of sampling material on sample; The mode that stopple coupon adopts multistage to connect, can adjust stopple coupon length in time according to different pool depths, easy to operate, and can be according to actual conditions, and the fused salt of 11 pairs of molten salt layer diverse locations of operation atmospheric valve is sampled;
(3) be easy to dismounting, transportation and install.
Although the above has described the utility model with exemplary embodiment by reference to the accompanying drawings, those of ordinary skills should be clear, in the situation that do not break away from the spirit and scope of claim, can carry out various modifications to above-described embodiment.
Claims (10)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201320448432 CN203365188U (en) | 2013-07-25 | 2013-07-25 | High-temperature fused salt sampling device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201320448432 CN203365188U (en) | 2013-07-25 | 2013-07-25 | High-temperature fused salt sampling device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203365188U true CN203365188U (en) | 2013-12-25 |
Family
ID=49812934
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201320448432 Expired - Fee Related CN203365188U (en) | 2013-07-25 | 2013-07-25 | High-temperature fused salt sampling device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203365188U (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107748089A (en) * | 2017-12-07 | 2018-03-02 | 华东理工大学 | A kind of metal solubility test sampler, sampling method and application in fused salt |
| CN108489581A (en) * | 2018-03-23 | 2018-09-04 | 山东商业职业技术学院 | A kind of viscous samples sample injector and its application method |
| CN108760400A (en) * | 2018-07-24 | 2018-11-06 | 中国地质科学院 | A kind of underwater sediment sampler |
-
2013
- 2013-07-25 CN CN 201320448432 patent/CN203365188U/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107748089A (en) * | 2017-12-07 | 2018-03-02 | 华东理工大学 | A kind of metal solubility test sampler, sampling method and application in fused salt |
| CN108489581A (en) * | 2018-03-23 | 2018-09-04 | 山东商业职业技术学院 | A kind of viscous samples sample injector and its application method |
| CN108760400A (en) * | 2018-07-24 | 2018-11-06 | 中国地质科学院 | A kind of underwater sediment sampler |
| CN108760400B (en) * | 2018-07-24 | 2021-02-05 | 中国地质科学院 | An underwater sediment sampler |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN203365188U (en) | High-temperature fused salt sampling device | |
| GB2433122A (en) | Gas sampling probe | |
| CN201555791U (en) | A multi-layer flat model core holder | |
| CN201561883U (en) | A leak-free liquid sampler | |
| CN204241270U (en) | Liquid positioning sampler | |
| CN218349919U (en) | Sampling device | |
| CN202814756U (en) | Liquid sample sampler | |
| CN210774691U (en) | Simple test bench for stability of liquid flow of liquid valve | |
| CN107907369A (en) | A kind of deep-sea pressurize organic matter sampler | |
| RU167971U1 (en) | Sectional sampler for oil products | |
| CN207751735U (en) | A kind of sediment interstitial water sampler | |
| CN207899471U (en) | A kind of pipettor for medical inspection | |
| CN110589271B (en) | An oil tank with anti-corrosion function | |
| CN105413245B (en) | A kind of forward view apparatus for oil tank automatic dewatering device | |
| CN205745781U (en) | A kind of anticorrosive cooling tube | |
| CN208237263U (en) | A kind of transformer or reactor are with taking oily transit joint | |
| CN212440342U (en) | Pipeline filtering device | |
| CN211374228U (en) | Fast-assembling pipeline sampling device | |
| CN210751505U (en) | Water tank for xylene condensation recovery unit | |
| CN207393988U (en) | A kind of corrosion-resistant sampling valve | |
| CN204214663U (en) | High-temperature sampling probe | |
| CN209027854U (en) | A high-pressure and corrosion-resistant sampler | |
| CN208187765U (en) | A kind of reactor tank sampling cleaning device | |
| CN208074257U (en) | A kind of valve being convenient to clean tamper | |
| CN205691364U (en) | A kind of portable shallow water body former state column shaped deposit sampling apparatus |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20131225 Termination date: 20170725 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |