CN1312238A - Amino acid chelate fertilizer producing process - Google Patents
Amino acid chelate fertilizer producing process Download PDFInfo
- Publication number
- CN1312238A CN1312238A CN00104213A CN00104213A CN1312238A CN 1312238 A CN1312238 A CN 1312238A CN 00104213 A CN00104213 A CN 00104213A CN 00104213 A CN00104213 A CN 00104213A CN 1312238 A CN1312238 A CN 1312238A
- Authority
- CN
- China
- Prior art keywords
- amino acid
- acid chelate
- chelate fertilizer
- hydrolysis
- fertilizer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 150000001413 amino acids Chemical class 0.000 title claims abstract description 25
- 239000003337 fertilizer Substances 0.000 title claims abstract description 19
- 239000013522 chelant Substances 0.000 title claims abstract description 15
- 238000000034 method Methods 0.000 title abstract description 10
- 238000004519 manufacturing process Methods 0.000 claims abstract description 14
- 230000007062 hydrolysis Effects 0.000 claims abstract description 12
- 238000006460 hydrolysis reaction Methods 0.000 claims abstract description 12
- 238000001914 filtration Methods 0.000 claims abstract description 11
- 240000004808 Saccharomyces cerevisiae Species 0.000 claims abstract description 10
- 208000035404 Autolysis Diseases 0.000 claims abstract description 5
- 206010057248 Cell death Diseases 0.000 claims abstract description 5
- 150000001875 compounds Chemical class 0.000 claims abstract description 5
- 230000028043 self proteolysis Effects 0.000 claims abstract description 5
- 238000001816 cooling Methods 0.000 claims abstract description 3
- 239000002002 slurry Substances 0.000 claims description 6
- 108091005804 Peptidases Proteins 0.000 claims description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 4
- 239000004365 Protease Substances 0.000 claims description 4
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 claims description 4
- 239000002131 composite material Substances 0.000 claims description 3
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 2
- 238000012856 packing Methods 0.000 claims description 2
- 238000012545 processing Methods 0.000 claims description 2
- 238000012546 transfer Methods 0.000 claims description 2
- 235000013619 trace mineral Nutrition 0.000 abstract description 7
- 239000011573 trace mineral Substances 0.000 abstract description 7
- 102000004190 Enzymes Human genes 0.000 abstract description 4
- 108090000790 Enzymes Proteins 0.000 abstract description 4
- 239000002994 raw material Substances 0.000 abstract description 4
- 235000013405 beer Nutrition 0.000 abstract description 3
- 230000008635 plant growth Effects 0.000 abstract description 2
- 239000010802 sludge Substances 0.000 abstract 2
- 238000013329 compounding Methods 0.000 abstract 1
- 238000004806 packaging method and process Methods 0.000 abstract 1
- 235000001014 amino acid Nutrition 0.000 description 16
- 239000002253 acid Substances 0.000 description 4
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 3
- 235000018102 proteins Nutrition 0.000 description 3
- 102000004169 proteins and genes Human genes 0.000 description 3
- 108090000623 proteins and genes Proteins 0.000 description 3
- 241000208125 Nicotiana Species 0.000 description 2
- -1 high temperature Substances 0.000 description 2
- 239000002366 mineral element Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 235000013311 vegetables Nutrition 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- QIVBCDIJIAJPQS-VIFPVBQESA-N L-tryptophane Chemical compound C1=CC=C2C(C[C@H](N)C(O)=O)=CNC2=C1 QIVBCDIJIAJPQS-VIFPVBQESA-N 0.000 description 1
- 244000061176 Nicotiana tabacum Species 0.000 description 1
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- QIVBCDIJIAJPQS-UHFFFAOYSA-N Tryptophan Natural products C1=CC=C2C(CC(N)C(O)=O)=CNC2=C1 QIVBCDIJIAJPQS-UHFFFAOYSA-N 0.000 description 1
- 238000005842 biochemical reaction Methods 0.000 description 1
- 229910052796 boron Inorganic materials 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000020776 essential amino acid Nutrition 0.000 description 1
- 239000003797 essential amino acid Substances 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 239000012065 filter cake Substances 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 230000012010 growth Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- 239000003895 organic fertilizer Substances 0.000 description 1
- 230000029553 photosynthesis Effects 0.000 description 1
- 238000010672 photosynthesis Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
- Y02A40/20—Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses
Landscapes
- Fertilizers (AREA)
Abstract
The production process of amino acid chelate fertilizer is characterized by that the chelate fertilizer is prepared by using the sludge from production of brewing beer as raw material, and the combination of yeast autolysis with compound enzyme hydrolysis to prepare amino acid liquor, then chelating the amino acid liquor with trace elements, and its process flow is as follows: enzyme mother sludge, press filtering, autolysis, hydrolysis by adding enzyme, filtering, batching, chelating, cooling, filtering, compounding and packaging finished product. It contains 18 amino acids and several trace elements necessary for growth of plant, can be used as high-efficiency foliage fertilizer, and can raise the yield of crops.
Description
The present invention relates to a kind of production method of amino acid chelate fertilizer, it belongs to the mixture class and the production method thereof of organic fertilizer and various trace elements.
The production of amino acids fertilizer normally adopts the protein raw material hydrolysis to make the mixed amino acid solution, makes through composite again.The preparation of aminoacids solution has acid hydrolyzation and enzymolysis process, and the amino acid fertilizer of domestic production at present all is to adopt acid hydrolyzation production.Though the acid hydrolyzation cost is low, this method needs strong acid, high temperature, and essential amino acids tryptophan is destroyed.And the enzymolysis process mild condition, amino acid is not destroyed, and configuration does not change.But enzymolysis process production generally exists hydrolysis thorough inadequately, the problem that percent hydrolysis is not high.
In order to improve the deficiency of enzymolysis process, purpose of the present invention is the enzymolysis novel process that provides a kind of percent hydrolysis high, is raw material with beer mud, adopts yeast autolysis to combine with combinative enzyme hydrolysis, again with the trace element chelated amino acid chelate fertilizer that makes.
Raw material and weight percent content thereof that amino acid chelate fertilizer of the present invention is required are respectively: yeast slurry (in butt) 50-60%, and proteinase-10 .1-0.2%, mineral element 1-3%, water 30-40%, mineral element can adopt Cu, Fe, Mn, Zn, B, Mo etc.
The producing and manufacturing technique of amino acid chelate fertilizer of the present invention is:
Yeast slurry → press filtration → self-dissolving → add enzymic hydrolysis → filtration → batching → chelating → cooling → filtration → composite → finished product packing.Now processing method is specified as follows:
1. yeast slurry press filtration: beer fermentation finishes, and discharges yeast slurry through the plate-and-frame filter press press filtration from pot bottom, gets filter cake and is used for hydrolysis.
2. self-dissolving is handled: will filter the yeast slurry of doing and add in the biochemical reaction pot, 1: 0.8 water is added in metering, adds 5% MgCL
2Make autolysis promoter, start agitator, and feed steam and slowly heat up, be raised to 48 ℃, be incubated 6 hours through 2 hours.
3. enzymolysis processing: transfer PH=7 with phosphoric acid, slowly be warmed up to 50-60 ℃, the compound protease that adds distiller's yeast mud amount (in butt) 0.1%-0.2%, in initial 6 hours, stirred 5 minutes every 2 hours, static then, allow it clarify naturally, the reaction times is 20 hours altogether, filter, get filtrate for later use.Above-mentioned used compound protease is to be cooperated in 1: 1 ratio by inscribe peptase and circumscribed peptase to form.
4. prepare burden: hydrolyzed solution is put in the ingredients pot, be warming up to 50 ℃-60 ℃, add trace element fertilizer, carried out chelatropic reaction 30 minutes, cooled and filtered, the alkylphenol polyoxyethylene that adds gross weight 1% is re-dubbed emulsion, and metering filling gets product.Adopt this technology, protein degree is more than 90%, and protein recovery is more than 85%.
Amino acid chelate fertilizer of the present invention can be used as efficient foliage spray.It contains needed 18 seed amino acids of plant-growth and various trace elements.Amino acid whose total content is about 15%, is about 10% with trace element chelated amino acid wherein.Crop sprays amino acid chelate fertilizer and can enhance metabolism, and improves the photosynthesis ability of farm crop, strengthens growth potential, improves output, improves quality.
Amino acid chelate fertilizer of the present invention has carried out the multiple spot field test on vegetables, tealeaves, tobacco, all obtain good effect, vegetables volume increase 20-30%; Tealeaves volume increase 15-20% improves tea leaf quality; Tobacco leaf volume increase 15-25%, and the grade of raising tobacco leaf.
Claims (4)
1. the production method of an amino acid chelate fertilizer is characterized in that, production process is: yeast slurry → press filtration → self-dissolving → add enzymic hydrolysis → filtration → batching → chelating → cooling → filtration → composite → finished product packing.
2. the production method of amino acid chelate fertilizer as claimed in claim 1 is characterized in that, when hydrolysis treatment, adds 5% MgCL
2Make autolysis promoter, and under 48 ℃ of conditions, be incubated 6 hours.
3. the production method of amino acid chelate fertilizer as claimed in claim 1 is characterized in that, during enzymolysis processing, transfers PH=7 with phosphoric acid, adds 0.1%～0.2% compound protease of mashed yeast butt amount, and hydrolysis is 20 hours under 50-60 ℃ of condition.
4. the production method of amino acid chelate fertilizer as claimed in claim 3 is characterized in that used compound protease is to be cooperated in 1: 1 ratio by inscribe peptase and circumscribed peptase to form.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN00104213A CN1312238A (en) | 2000-03-08 | 2000-03-08 | Amino acid chelate fertilizer producing process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN00104213A CN1312238A (en) | 2000-03-08 | 2000-03-08 | Amino acid chelate fertilizer producing process |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1312238A true CN1312238A (en) | 2001-09-12 |
Family
ID=4577217
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN00104213A Pending CN1312238A (en) | 2000-03-08 | 2000-03-08 | Amino acid chelate fertilizer producing process |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1312238A (en) |
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100369867C (en) * | 2006-09-01 | 2008-02-20 | 陈景华 | Highly effective ecology animal and plant nutriment, preparation method and application thereof |
| WO2010063195A1 (en) * | 2008-12-02 | 2010-06-10 | 安琪酵母股份有限公司 | Feed premix containing multiple trace elements and preparing method thereof |
| EP2128114A3 (en) * | 2008-05-28 | 2011-12-28 | Heineken España, S.A. | Procedure for obtaining a fertilizing product from beer production waste |
| EP2719289A1 (en) * | 2012-10-12 | 2014-04-16 | SC Medisan 2010 SRL | Process for obtainment of amino acids chelates with micro-elements |
| CN105198665A (en) * | 2014-06-06 | 2015-12-30 | 江苏植丰生物科技有限公司 | Amino acid water-soluble fertilizer and preparation method thereof |
| CN105272478A (en) * | 2015-11-17 | 2016-01-27 | 烟台泓源生物肥料有限公司 | Water-soluble protein peptide fertilizer |
| CN105819957A (en) * | 2016-03-17 | 2016-08-03 | 陕西先农生物科技有限公司 | Enzyme and amino acid containing aromatic liquid fertilizer prepared by inferior-quality fruit combined enzyme method and preparation method thereof |
| CN105967761A (en) * | 2016-05-26 | 2016-09-28 | 陈可夫 | Method for producing amino acid water-soluble fertilizer by utilizing Drawida Japonica Michelsen |
| CN106478271A (en) * | 2016-11-10 | 2017-03-08 | 云南农业大学 | A kind of water-soluble fertilizer of aminoacid containing enzymatic isolation method and preparation method thereof |
| CN110128213A (en) * | 2019-06-19 | 2019-08-16 | 乐斯福(明光)有限公司 | A method of liquid fertilizer is produced using beer waste yeast |
| CN112209784A (en) * | 2020-11-02 | 2021-01-12 | 中国科学院沈阳应用生态研究所 | A kind of synergistic and stable compound fertilizer fertilizer and preparation method thereof |
| CN112321361A (en) * | 2020-11-02 | 2021-02-05 | 中国科学院沈阳应用生态研究所 | Synergistic stable nitrogenous fertilizer and preparation method thereof |
-
2000
- 2000-03-08 CN CN00104213A patent/CN1312238A/en active Pending
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100369867C (en) * | 2006-09-01 | 2008-02-20 | 陈景华 | Highly effective ecology animal and plant nutriment, preparation method and application thereof |
| EP2128114A3 (en) * | 2008-05-28 | 2011-12-28 | Heineken España, S.A. | Procedure for obtaining a fertilizing product from beer production waste |
| WO2010063195A1 (en) * | 2008-12-02 | 2010-06-10 | 安琪酵母股份有限公司 | Feed premix containing multiple trace elements and preparing method thereof |
| EP2719289A1 (en) * | 2012-10-12 | 2014-04-16 | SC Medisan 2010 SRL | Process for obtainment of amino acids chelates with micro-elements |
| CN105198665A (en) * | 2014-06-06 | 2015-12-30 | 江苏植丰生物科技有限公司 | Amino acid water-soluble fertilizer and preparation method thereof |
| CN105272478A (en) * | 2015-11-17 | 2016-01-27 | 烟台泓源生物肥料有限公司 | Water-soluble protein peptide fertilizer |
| CN105819957A (en) * | 2016-03-17 | 2016-08-03 | 陕西先农生物科技有限公司 | Enzyme and amino acid containing aromatic liquid fertilizer prepared by inferior-quality fruit combined enzyme method and preparation method thereof |
| CN105967761A (en) * | 2016-05-26 | 2016-09-28 | 陈可夫 | Method for producing amino acid water-soluble fertilizer by utilizing Drawida Japonica Michelsen |
| CN106478271A (en) * | 2016-11-10 | 2017-03-08 | 云南农业大学 | A kind of water-soluble fertilizer of aminoacid containing enzymatic isolation method and preparation method thereof |
| CN110128213A (en) * | 2019-06-19 | 2019-08-16 | 乐斯福(明光)有限公司 | A method of liquid fertilizer is produced using beer waste yeast |
| CN112209784A (en) * | 2020-11-02 | 2021-01-12 | 中国科学院沈阳应用生态研究所 | A kind of synergistic and stable compound fertilizer fertilizer and preparation method thereof |
| CN112321361A (en) * | 2020-11-02 | 2021-02-05 | 中国科学院沈阳应用生态研究所 | Synergistic stable nitrogenous fertilizer and preparation method thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| ASS | Succession or assignment of patent right |
Owner name: KUMIN GUOZONG BIOLOGY ENGINEERING CO., LTD. Free format text: FORMER OWNER: AIDI BIOLOGICAL TECHN INST., YUNAN Effective date: 20020705 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20020705 Address after: 650011 Yunnan city of Kunming province Shu Lin Jie Shulin garden 5 Applicant after: Kunming Guozhong Biological Engineering Co. Ltd. Address before: 650021 Yunnan city in Kunming Province, the Provincial Association for science and Technology Road No. 22 Building 5 Applicant before: Aidi Bio-Technology Inst, Yunnan |
|
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |