CN116139050B - Essence water with microcapsule coated with sea buckthorn seed oil and grape seed oil and preparation method thereof - Google Patents
Essence water with microcapsule coated with sea buckthorn seed oil and grape seed oil and preparation method thereof Download PDFInfo
- Publication number
- CN116139050B CN116139050B CN202310381571.3A CN202310381571A CN116139050B CN 116139050 B CN116139050 B CN 116139050B CN 202310381571 A CN202310381571 A CN 202310381571A CN 116139050 B CN116139050 B CN 116139050B
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- water
- seed oil
- microcapsule
- solution
- skin care
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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Abstract
The application provides essence water coated with sea buckthorn seed oil and grape seed oil by microcapsules and a preparation method thereof, and relates to the technical field of skin care products. A microcapsule-coated essence water containing oleum Hippophae and grapeseed oil comprises skin care liquid and microcapsule beads. According to the application, the microcapsule beads are mixed with the skin care liquid, and the water and the oil are mixed, so that the oil phase substances can be uniformly distributed in the water phase substances, on one hand, the substance distribution in the essence water can be ensured to be balanced, and the essence water can promote the water-oil balance of facial skin when in use; on the other hand, the skin care product can also ensure good skin feel, and has excellent moisturizing effect while ensuring fresh and comfortable skin feel; in yet another aspect, the microcapsule beads are suspended in the skin care lotion, so that the microcapsule beads are uniformly distributed in the essence water, oil phase substances can be prevented from contacting with air, the microcapsule beads are not easy to deactivate, and the excellent efficacy of the essence water can be ensured.
Description
Technical Field
The application relates to the technical field of skin care products, in particular to essence water with microcapsule coated sea buckthorn seed oil and grape seed oil and a preparation method thereof.
Background
Water and oil are important elements for skin care, and the skin with balanced water and oil is full and elastic; skin with more water and less oil is ideal skin in theory, but the skin can not hold water due to the lack of oil, and fine lines and dry peeling are easy to occur when the water of the skin is lost; although the skin with less water and more oil is easy to retain water, the ability of the oil to acquire water from the inside and outside is low because the oil wraps the skin, so that the pores are enlarged, the horny layer is blackened, and skin problems such as blackheads, acnes and the like are easily generated. Therefore, it is important to maintain the water-oil balance of the skin. With the continuous progress of society and economy and the abundance of material life, skin care products become one of the daily necessities indispensable for modern people. It is well known that skin care products are various in variety and function, for example, have the effects of moisturizing, whitening, moisturizing, controlling oil, resisting aging, moisturizing skin, shrinking pores, removing blackheads, removing freckles, reducing fat and the like, and the effects of skin care essence are particularly remarkable. Moisturizing and moisturizing are the most basic and important links for skin care, and are also important means for keeping skin water-oil balance, whether skin moisture is full or not directly influences the external complexion of a person, and even causes a series of skin problems such as skin chapping, wrinkling, molting and allergy, so that the moisturizing essence water not only meets the mind requirements of high-end consumption to a great extent, but also is an effective way for consumers to moisturize the skin and supplement skin nutrition.
The essence water on the market at present is mostly in the form of water, O/W emulsion and water-oil layering, and although the essence water in the form of water can be used for moisturizing skin, the essence water cannot lock water and has poor moisturizing effect; the oil phase component in the O/W emulsified essence water is easy to separate from water, so that the property of the essence water is unstable, the oil phase component is easy to be exposed in the air for inactivation, and the action and effect of the essence water are affected; the oil phase component in the water-oil-layer essence water is suspended on the upper layer, so that the skin feel is poor when the essence water is used, and the oily position is exposed to the air for a long time, so that the risk of oxidation and inactivation exists, and the oil phase component has poor effect. The microcapsule beads are uniformly suspended in the aqueous system, and few products with natural active grease formulation are coated in the microcapsule beads. Therefore, the development of the essence product which is rich in microcapsule natural oil and has the effects of moisturizing and controlling oil has wide market prospect.
Disclosure of Invention
The application aims to provide essence water with micro-capsules coated with sea buckthorn seed oil and grape seed oil, which has the advantages of being capable of effectively maintaining the activity of natural vegetable oil and having moisturizing and oil controlling effects.
The application further aims to provide a preparation method of the essence water with the microcapsule coated with the sea buckthorn seed oil and the grape seed oil, so that the essence water can be produced with high efficiency.
The application solves the technical problems by adopting the following technical scheme.
In one aspect, the embodiment of the application provides essence water with micro-capsules coated with sea buckthorn seed oil and grape seed oil, which comprises skin care liquid and micro-capsule beads;
the skin care liquid comprises the following raw materials in percentage by weight: 2-4% of glycerin, 2-4% of butanediol, 0.05-0.1% of sodium hyaluronate, 1-2% of ectoin, 1-3% of lactobacillus fermentation lysate, 1-3% of Opuntia ficus-indica flower extract, 0.3-0.8% of chitosan, 0.5-1.5% of dipotassium glycyrrhizinate, 0.1-0.2% of polyacrylate crosslinked polymer, 0.01-0.03% of disodium edetate, 0.3-0.6% of p-hydroxyacetophenone, 0.6-1.0% of 1, 2-hexanediol and the balance of water;
the microcapsule beads comprise the following raw materials in percentage by weight: acrylic acid (esters)/C10-30 alkanol acrylate cross-linked polymer 0.01-0.2%, glycerin 1-2%, hydroxyethyl cellulose 0.1-0.5%, 1, 2-hexanediol 0.25-0.5%, octanediol 0.25-0.5%, butanediol 1-2%, triglyceride (ethyl caproic acid) 33-37%, sea buckthorn seed oil 0.4-1.2%, vitamin E0.5-1.5%, grape seed oil 0.2-0.8%, and water balance.
On the other hand, the embodiment of the application provides a preparation method of essence water with microcapsule coated sea buckthorn seed oil and grape seed oil, which comprises the following steps:
dissolving glycerin, butanediol and p-hydroxyacetophenone in skin care liquid raw materials in water, mixing, heating, stirring and mixing uniformly to obtain a solution 1;
adding water into sodium hyaluronate in skin care lotion raw materials to prepare a solution 2 with the concentration of 1%;
dissolving polyacrylate crosslinked polymer-6 in skin care lotion raw material in water to obtain solution 3;
uniformly mixing the ectoin, lactobacillus fermentation lysate, opuntia Dillenii flower extract, chitosan, dipotassium glycyrrhizinate, disodium edetate and 1, 2-hexanediol in the skin care lotion raw material to obtain a solution 4;
mixing the solution 1, the solution 2, the solution 3 and the solution 4, and heating to obtain skin care liquid;
mixing water, acrylic acid (esters) or C10-30 alkanol acrylate cross-linked polymer, glycerol, hydroxyethyl cellulose, 1, 2-hexanediol, octanediol and butanediol in the microcapsule bead raw material, heating, stirring and dissolving to obtain a solution 5;
mixing sea buckthorn seed oil, vitamin E and grape seed oil in the microcapsule bead raw material, heating, stirring and dissolving to obtain a solution 6;
heating the triglyceride (ethyl caproic acid) ester in the microcapsule bead raw material to obtain a solution 7;
adding the solution 6 into the solution 7, and uniformly stirring to obtain an oil phase;
mixing the oil phase and the water phase, stirring and cooling until microcapsule beads appear;
mixing the microcapsule beads with skin care liquid, and stirring to obtain the final product of essence water.
Compared with the prior art, the embodiment of the application has at least the following advantages or beneficial effects:
according to the application, the microcapsule beads are mixed with the skin care liquid, and the water and the oil are mixed, so that the oil phase substances can be uniformly distributed in the water phase substances, on one hand, the substance distribution in the essence water can be ensured to be balanced, and the essence water can promote the water-oil balance of facial skin when in use; on the other hand, the skin care product can also ensure good skin feel, and has excellent moisturizing effect while ensuring fresh and comfortable skin feel; in yet another aspect, the microcapsule beads are suspended in the skin care lotion, so that the microcapsule beads are uniformly distributed in the essence water, oil phase substances can be prevented from contacting with air, the microcapsule beads are not easy to deactivate, and the excellent efficacy of the essence water can be ensured.
The preparation method is simple and convenient, firstly, after a plurality of substances of the skin care liquid are respectively dissolved and mixed, the water phase and the oil phase of the microcapsule beads are mixed to prepare the microcapsule bead particles, and finally, the microcapsule beads are added into the skin care liquid and uniformly mixed, so that the active ingredients and beneficial substances in the essence water can be wrapped and remain active, the active ingredients and beneficial substances are uniformly distributed in the water phase, and meanwhile, the comfortable use experience and excellent use effect of the essence water are ensured.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present application more clear, the technical solutions of the embodiments of the present application will be clearly and completely described below. The specific conditions are not noted in the examples and are carried out according to conventional conditions or conditions recommended by the manufacturer. The reagents or apparatus used were conventional products commercially available without the manufacturer's attention.
It should be noted that, without conflict, the embodiments of the present application and features of the embodiments may be combined with each other. The present application will be described in detail with reference to specific examples.
The embodiment provides essence water with micro-capsules coated with sea buckthorn seed oil and grape seed oil,
including skin lotions and microencapsulated beads;
the skin care liquid comprises the following raw materials in percentage by weight: 2-4% of glycerin, 2-4% of butanediol, 0.05-0.1% of sodium hyaluronate, 1-2% of ectoin, 1-3% of lactobacillus fermentation lysate, 1-3% of Opuntia ficus-indica flower extract, 0.3-0.8% of chitosan, 0.5-1.5% of dipotassium glycyrrhizinate, 0.1-0.2% of polyacrylate crosslinked polymer, 0.01-0.03% of disodium edetate, 0.3-0.6% of p-hydroxyacetophenone, 0.6-1.0% of 1, 2-hexanediol and the balance of water;
the microcapsule beads comprise the following raw materials in percentage by weight: acrylic acid (esters)/C10-30 alkanol acrylate cross-linked polymer 0.01-0.2%, glycerin 1-2%, hydroxyethyl cellulose 0.1-0.5%, 1, 2-hexanediol 0.25-0.5%, octanediol 0.25-0.5%, butanediol 1-2%, triglyceride (ethyl caproic acid) 33-37%, sea buckthorn seed oil 0.4-1.2%, vitamin E0.5-1.5%, grape seed oil 0.2-0.8%, and water balance.
According to the application, the microcapsule beads are mixed with the skin care liquid, and the water and the oil are mixed, so that the oil phase substances can be uniformly distributed in the water phase substances, on one hand, the substance distribution in the essence water can be ensured to be balanced, and the essence water can promote the water-oil balance of facial skin when in use; on the other hand, the skin care product can also ensure good skin feel, and has excellent moisturizing effect while ensuring fresh and comfortable skin feel; in yet another aspect, the microcapsule beads are suspended in the skin care lotion, so that the microcapsule beads are uniformly distributed in the essence water, oil phase substances can be prevented from contacting with air, the microcapsule beads are not easy to deactivate, and the excellent efficacy of the essence water can be ensured. Glycerol: has good moisturizing effect and can effectively keep skin moist.
Butanediol: butanediol is a polyol with mild texture, can increase the smoothness of the product, and has good moisturizing effect.
Sodium hyaluronate: the hydrolyzed sodium hyaluronate is acidic mucopolysaccharide, naturally exists in cornea skin, can absorb 1000 times of water by weight, can prevent water from losing through epidermis, can repair skin barrier, can improve skin nutrition metabolism, and can make skin soft, smooth and elastic.
Rickettsial: can have good protection effect on cells under the conditions of high temperature, severe plugging, drought, extreme pH value, high pressure, high salt, high radiation and the like. The ectoin has the effects of enhancing skin immunity, repairing ultraviolet injury, maintaining skin water locking capacity, resisting aging and wrinkle, and can be used for treating diseases such as atopic dermatitis.
Lactic acid bacteria fermentation lysate: contains thalli and all active ingredients synthesized in the fermentation process, contains peptidoglycan, phospholipid, sterol, fatty acid, extracellular polysaccharide and the like, provides rich nutrition for skin, and has good anti-aging effect and anti-oxidation effect.
Opuntia ficus-indica flower extract: has good anti-inflammatory and antioxidant effects, high safety in skin use, no acne, antibacterial effect, and skin growth factor generation promoting effect.
Acetylchitosamine: the composition is safe, and has effects of accelerating wound healing, improving skin hydration degree, reducing skin fine lines, improving rough skin, inhibiting tyrosinase synthesis, reducing melanin generation, improving uneven skin color, and whitening skin.
Dipotassium glycyrrhizinate: the skin care cream has the effects of resisting inflammation and allergy, moisturizing skin, reducing skin irritation and sensitivity, reducing skin irritation caused by fruit acid, enhancing efficacy by accelerating the absorption of other active ingredients by skin, and can be used for preventing dermatitis, relieving itching, assisting whitening, regulating sebum, relieving skin dryness and the like.
Polyacrylate crosslinked polymer-6: can help the cosmetic to have auxiliary effects on the aspects of consistency, stability and the like.
Disodium edetate: it has stabilizing effect in cosmetics, and has synergistic effect on antiseptic system and antioxidant system.
P-hydroxyacetophenone: the preservative has the effects of clearing damp heat, is also a preservative promoter, has multiple effects of antioxidation, anti-irritation and the like, has antioxidation and bacteriostasis from hydroxyl groups, is an antioxidant (phenol and ketone characteristics), is effective to fungi, has strong capability of killing aspergillus niger, has a certain inhibition effect to pseudomonas aeruginosa, has excellent stability in high and low pH values and temperature ranges, can prolong the shelf life of other substance active ingredients under high temperature conditions, can promote the efficacy of various preservatives, and has good compatibility with various cosmetic ingredients and packaging materials.
1, 2-hexanediol: it is a colorless transparent viscous liquid, can be mixed with various organic compounds in any proportion, is easily dissolved in water, and has the effects of sterilization and moisture preservation.
Acrylic acid (esters)/C10-30 alkanol acrylate cross-linked polymer: the emulsion system can lock the absorbed free water, so that the polymer is expanded to increase viscosity, and has good suspension force, so that the emulsion system has better rheological property and excellent thickening stability.
Hydroxyethyl cellulose: the cellulose ether organic water-based synthetic polymer gel is a common cellulose ether organic water-based synthetic polymer gel, has good thickening ability to water, and can be used as a skin conditioner, a film forming agent and an antioxidant in cosmetics.
Octyl glycol: the water-based emulsion is a good humectant, has a preservative function, can replace a preservative, can prevent bacteria and yeast in a water-based formula from exceeding standards, is also beneficial to maintaining the stability of emulsion, and can regulate the viscosity of essence water.
Glycerol tris (ethylhexanoate): the emulsion is a low-polarity emollient, can reduce the greasy feel of an emulsion system, has good spreadability and low cloud point, and has good hydrolytic stability and silicone oil compatibility.
Sea buckthorn seed oil: the skin aging inhibitor has good inhibition effect on metalloprotease, activation of the metalloprotease is an index of skin aging, and the combination of the metalloprotease and the elimination of superoxide radicals shows that the skin aging inhibitor has an anti-aging function; meanwhile, the product has antibacterial and anti-inflammatory effects.
Grape seed oil: the grape seed oil has the characteristics of safety, no stimulation and good skin feel, contains squalene, VE and other components, has the effects of scavenging free radicals and resisting aging, and has a certain freckle removing effect on chloasma and mottle on skin. In addition, the grape seed oil has the function of astringing and controlling oil, can tighten skin, and has no sensitization.
Vitamin E: it is a fat-soluble vitamin and is also an excellent antioxidant, which is easy to be absorbed by skin, and can promote skin metabolism, prevent pigmentation, improve skin elasticity, moisten skin, and play a role in beautifying, protecting skin and resisting aging.
In some embodiments of the present application, the skin care liquid comprises the following raw materials in percentage by weight: 3% of glycerin, 3% of butanediol, 0.08% of sodium hyaluronate, 1.5% of ectoin, 2% of lactobacillus fermentation lysate, 2% of Opuntia ficus-indica flower extract, 0.6% of chitosan amine, 1% of dipotassium glycyrrhizinate, 0.15% of polyacrylate crosslinked polymer, 0.02% of disodium ethylenediamine tetraacetate, 0.5% of p-hydroxyacetophenone, 0.8% of 1, 2-hexanediol and the balance of water;
the microcapsule beads comprise the following raw materials in percentage by weight: acrylic acid (esters)/C10-30 alkanol acrylate cross-linked polymer 0.1%, glycerin 1.5%, hydroxyethyl cellulose 0.3%, 1, 2-hexanediol 0.3%, octanediol 3%, butanediol 1.5%, triglyceride (ethylhexanoic acid) ester 35%, sea buckthorn seed oil 0.8%, vitamin E1%, grape seed oil 0.5%, and water in balance.
The embodiment of the application also provides a preparation method of the essence water with the microcapsule coated with the sea buckthorn seed oil and the grape seed oil, which comprises the following steps:
dissolving glycerin, butanediol and p-hydroxyacetophenone in skin care liquid raw materials in water, mixing, heating, stirring and mixing uniformly to obtain a solution 1;
adding water into sodium hyaluronate in skin care lotion raw materials to prepare a solution 2 with the concentration of 1%;
dissolving polyacrylate crosslinked polymer-6 in skin care lotion raw material in water to obtain solution 3;
uniformly mixing the ectoin, lactobacillus fermentation lysate, opuntia Dillenii flower extract, chitosan, dipotassium glycyrrhizinate, disodium edetate and 1, 2-hexanediol in the skin care lotion raw material to obtain a solution 4;
mixing the solution 1, the solution 2, the solution 3 and the solution 4, and heating to obtain skin care liquid;
mixing water, acrylic acid (esters) or C10-30 alkanol acrylate cross-linked polymer, glycerol, hydroxyethyl cellulose, 1, 2-hexanediol, octanediol and butanediol in the microcapsule bead raw material, heating, stirring and dissolving to obtain a solution 5;
mixing sea buckthorn seed oil, vitamin E and grape seed oil in the microcapsule bead raw material, heating, stirring and dissolving to obtain a solution 6;
heating the triglyceride (ethyl caproic acid) ester in the microcapsule bead raw material to obtain a solution 7;
adding the solution 6 into the solution 7, and uniformly stirring to obtain an oil phase;
mixing the oil phase and the water phase, stirring and cooling until microcapsule beads appear;
mixing the microcapsule beads with skin care liquid, and stirring to obtain the final product of essence water.
The preparation method is simple and convenient, firstly, after a plurality of substances of the skin care liquid are respectively dissolved and mixed, the water phase and the oil phase of the microcapsule beads are mixed to prepare the microcapsule bead particles, and finally, the microcapsule beads are added into the skin care liquid and uniformly mixed, so that the active ingredients and beneficial substances in the essence water can be wrapped and remain active, the active ingredients and beneficial substances are uniformly distributed in the water phase, and meanwhile, the comfortable use experience and excellent use effect of the essence water are ensured. In some embodiments of the application, the heating temperature of the solution 1 is 58-63 ℃.
In some embodiments of the present application, the lotion is warmed to 65-80 ℃.
In some embodiments of the application, the solution 5 is warmed to 70-85 ℃.
In some embodiments of the application, the solution 6 is warmed to 60-80 ℃.
In some embodiments of the application, the solution 7 is warmed to 40-80 ℃.
In some embodiments of the application, the weight ratio of the microcapsule beads to the skin lotion is (1-5): 20.
the features and capabilities of the present application are described in further detail below in connection with the examples.
Example 1
A preparation method of essence water with microcapsule coated with sea buckthorn seed oil and grape seed oil comprises the following steps:
the skin care liquid comprises the following raw materials in percentage by weight: 2% of glycerin, 2% of butanediol, 0.05% of sodium hyaluronate, 1% of ectoin, 1% of lactobacillus fermentation lysate, 1% of Opuntia ficus-indica flower extract, 0.3% of chitosan amine, 0.5% of dipotassium glycyrrhizinate, 0.1% of polyacrylate crosslinked polymer-6, 0.01% of disodium edetate, 0.3% of p-hydroxyacetophenone, 0.6% of 1, 2-hexanediol and the balance of water;
the microcapsule beads comprise the following raw materials in percentage by weight: acrylic acid (esters) of C10-30 alkanol acrylate cross-linked polymer 0.01%, glycerin 1%, hydroxyethyl cellulose 0.1%, 1, 2-hexanediol 0.25%, octaethylene glycol 0.25%, butylene glycol 1%, triglyceride (ethyl hexanoate) 33%, sea buckthorn seed oil 0.4%, vitamin E0.5%, grape seed oil 0.2%, and the balance water.
Dissolving glycerin, butanediol and p-hydroxyacetophenone in skin care liquid raw materials in water, mixing, heating to 58 ℃, and stirring and mixing uniformly to obtain a solution 1;
adding water into sodium hyaluronate in skin care lotion raw materials to prepare a solution 2 with the concentration of 1%;
dissolving polyacrylate crosslinked polymer-6 in skin care lotion raw material in water to obtain solution 3;
uniformly mixing the ectoin, lactobacillus fermentation lysate, opuntia Dillenii flower extract, chitosan, dipotassium glycyrrhizinate, disodium edetate and 1, 2-hexanediol in the skin care lotion raw material to obtain a solution 4;
mixing the solution 1, the solution 2, the solution 3 and the solution 4, and heating to 65 ℃ to obtain skin care liquid;
mixing water, acrylic acid (esters) or C10-30 alkanol acrylate cross-linked polymer, glycerol, hydroxyethyl cellulose, 1, 2-hexanediol, octanediol and butanediol in the microcapsule bead raw material, heating to 70 ℃, stirring and dissolving to obtain a solution 5;
mixing sea buckthorn seed oil, vitamin E and grape seed oil in the microcapsule bead raw material, heating to 60 ℃, and stirring and dissolving to obtain a solution 6;
heating the triglyceride (ethyl caproic acid) ester in the microcapsule bead raw material to 40 ℃ to obtain a solution 7;
adding the solution 6 into the solution 7, and uniformly stirring to obtain an oil phase;
mixing the oil phase and the water phase, stirring and cooling until microcapsule beads appear;
the microcapsule beads and the skin lotion were mixed according to a 1:20 weight ratio, and uniformly stirring to obtain the essence water finished product.
Example 2
A preparation method of essence water with microcapsule coated with sea buckthorn seed oil and grape seed oil comprises the following steps:
the skin care liquid comprises the following raw materials in percentage by weight: 3% of glycerin, 3% of butanediol, 0.08% of sodium hyaluronate, 1.5% of ectoin, 2% of lactobacillus fermentation lysate, 2% of Opuntia ficus-indica flower extract, 0.6% of chitosan amine, 1% of dipotassium glycyrrhizinate, 0.15% of polyacrylate crosslinked polymer, 0.02% of disodium ethylenediamine tetraacetate, 0.5% of p-hydroxyacetophenone, 0.8% of 1, 2-hexanediol and the balance of water;
the microcapsule beads comprise the following raw materials in percentage by weight: acrylic acid (esters)/C10-30 alkanol acrylate cross-linked polymer 0.1%, glycerin 1.5%, hydroxyethyl cellulose 0.3%, 1, 2-hexanediol 0.3%, octanediol 3%, butanediol 1.5%, triglyceride (ethylhexanoic acid) ester 35%, sea buckthorn seed oil 0.8%, vitamin E1%, grape seed oil 0.5%, and water in balance.
Dissolving glycerin, butanediol and p-hydroxyacetophenone in skin care liquid raw materials in water, mixing, heating to 60 ℃, and stirring and mixing uniformly to obtain a solution 1;
adding water into sodium hyaluronate in skin care lotion raw materials to prepare a solution 2 with the concentration of 1%;
dissolving polyacrylate crosslinked polymer-6 in skin care lotion raw material in water to obtain solution 3;
uniformly mixing the ectoin, lactobacillus fermentation lysate, opuntia Dillenii flower extract, chitosan, dipotassium glycyrrhizinate, disodium edetate and 1, 2-hexanediol in the skin care lotion raw material to obtain a solution 4;
mixing the solution 1, the solution 2, the solution 3 and the solution 4, and heating to 75 ℃ to obtain skin care liquid;
mixing water, acrylic acid (esters) or C10-30 alkanol acrylate cross-linked polymer, glycerol, hydroxyethyl cellulose, 1, 2-hexanediol, octanediol and butanediol in the microcapsule bead raw material, heating to 78 ℃, stirring and dissolving to obtain a solution 5;
mixing sea buckthorn seed oil, vitamin E and grape seed oil in the microcapsule bead raw material, heating to 70 ℃, stirring and dissolving to obtain a solution 6;
heating the triglyceride (ethyl caproic acid) ester in the microcapsule bead raw material to 60 ℃ to obtain a solution 7;
adding the solution 6 into the solution 7, and uniformly stirring to obtain an oil phase;
mixing the oil phase and the water phase, stirring and cooling until microcapsule beads appear;
the microcapsule beads and the skin lotion were mixed according to 3:20 weight ratio, and uniformly stirring to obtain the essence water finished product.
Example 3
A preparation method of essence water with microcapsule coated with sea buckthorn seed oil and grape seed oil comprises the following steps:
the skin care liquid comprises the following raw materials in percentage by weight: 4% of glycerin, 4% of butanediol, 0.1% of sodium hyaluronate, 2% of ectoin, 3% of lactobacillus fermentation lysate, 3% of Opuntia ficus-indica flower extract, 0.8% of chitosan amine, 1.5% of dipotassium glycyrrhizinate, 0.2% of polyacrylate crosslinked polymer-6, 0.03% of disodium ethylenediamine tetraacetate, 0.6% of p-hydroxyacetophenone, 1, 2-hexanediol and the balance of water;
the microcapsule beads comprise the following raw materials in percentage by weight: acrylic acid (esters) of C10-30 alkanol acrylate cross-linked polymer 0.2%, glycerin 2%, hydroxyethyl cellulose 0.5%, 1, 2-hexanediol 0.5%, octaethylene glycol 0.5%, butanediol 2%, triglyceride (ethylhexanoic acid) 37%, sea buckthorn seed oil 1.2%, vitamin E1.5%, grape seed oil 0.8%, and the balance of water.
Dissolving glycerin, butanediol and p-hydroxyacetophenone in skin care liquid raw materials in water, mixing, heating to 63 ℃, and stirring and mixing uniformly to obtain a solution 1;
adding water into sodium hyaluronate in skin care lotion raw materials to prepare a solution 2 with the concentration of 1%;
dissolving polyacrylate crosslinked polymer-6 in skin care lotion raw material in water to obtain solution 3;
uniformly mixing the ectoin, lactobacillus fermentation lysate, opuntia Dillenii flower extract, chitosan, dipotassium glycyrrhizinate, disodium edetate and 1, 2-hexanediol in the skin care lotion raw material to obtain a solution 4;
mixing the solution 1, the solution 2, the solution 3 and the solution 4, and heating to 80 ℃ to obtain skin care liquid;
mixing water, acrylic acid (esters) or C10-30 alkanol acrylate cross-linked polymer, glycerol, hydroxyethyl cellulose, 1, 2-hexanediol, octanediol and butanediol in the microcapsule bead raw material, heating to 85 ℃, stirring and dissolving to obtain a solution 5;
mixing sea buckthorn seed oil, vitamin E and grape seed oil in the microcapsule bead raw material, heating to 80 ℃, and stirring and dissolving to obtain a solution 6;
heating the triglyceride (ethyl caproic acid) ester in the microcapsule bead raw material to 80 ℃ to obtain a solution 7;
adding the solution 6 into the solution 7, and uniformly stirring to obtain an oil phase;
mixing the oil phase and the water phase, stirring and cooling until microcapsule beads appear;
the microcapsule beads and the skin lotion were mixed according to a ratio of 5:20 weight ratio, and uniformly stirring to obtain the essence water finished product.
Comparative example 1
This comparative example is substantially identical to example 2, except that: only the sea buckthorn seed oil and the grape seed oil are reserved in the microcapsule bead raw material.
Comparative example 2
This comparative example is substantially identical to example 2, except that: no microcapsule beads were added.
Experimental example
(one), skin irritation test
The test was performed according to the skin irritation test method in cosmetic safety Specification (2015 edition).
15 white rabbits which are adult, healthy, skin-friendly and ungstented are taken and equally divided into 3 groups, the hairs on two sides of the back spine of an experimental animal are cut off about 24 hours before the test, the epidermis is not damaged, the left and right hair removing ranges are about 3cm multiplied by 3cm, 0.5mL of a test object (essence water prepared in the examples 1-3) is directly coated on the skin of the 3 groups of rabbits, then the rabbits are covered by two layers of gauze (2.5 cm multiplied by 2.5 cm) and one layer of cellophane, and then the rabbits are fixed by using a non-irritating adhesive tape and a bandage. The other side skin served as a control. The application time was 4h using the blocking test. No erythema or edema was observed in the white rabbits of group 3, which indicates that the essence prepared by the application is mild in water and has no irritation. (II) moisture test
100 healthy subjects who were in line with the inclusion standard were enrolled, aged 25 to 35 years, randomly divided into 5 groups, respectively, and applied to cheeks after washing the cheeks with the essence water prepared in examples 1 to 3 and comparative examples 1 to 2, respectively, the skin moisture content of the applied portion was measured using a skin moisture tester before and after use for 2 hours, 12 hours, 24 hours and 120 hours, and the average value calculated 3 times was measured as a test value, wherein more than 24 hours was recorded each morning and evening every day. And the skin moisture content change rate was calculated from the skin moisture content, and the results are shown in table 1.
Skin moisture content change rate = (moisture content after use-moisture content before use)/moisture content after use×100%
TABLE 1
Looking at Table 1, it can be seen that the essence water prepared in examples 1-3 of the present application has excellent moisturizing effect, and comparative examples 1-3 can be seen that the essence water prepared in example 2 has the best moisturizing effect; comparative example 2 and comparative examples 1-2 can intuitively show that the moisturizing effect of essence water is remarkably reduced whether the sea buckthorn seed oil and the grape seed oil are directly added into the skin care liquid or the microcapsule beads are not added, which shows that the inventor can improve the moisturizing effect of the essence water by mixing the skin care liquid and the microcapsule beads.
(III) skin oil secretion test
6 healthy subjects were invited to be divided into 2 groups, 1 group using the essence water prepared in example 2, and 2 groups using the essence water prepared in comparative example 1. The experimental method comprises the following steps: before testing, the face of the subject is cleaned, the subject sits still for 30min, the forehead of the subject is divided into left and right sides by using a skin grease tester to test the skin grease of the left and right forehead, each test area is tested for 3 times, an average value is obtained, and data are recorded. After the essence water was used for 8 hours, skin oil was recorded in the same manner. The results are shown in Table 2.
TABLE 2
By observing Table 2, it can be seen that the essence water prepared by the application has good oil control effect, and comparing group 1 with group 2, it can be seen that the oil control effect of group 1 is better. The moisture retention test and the skin grease test are combined, so that the essence water prepared by the application can maintain the skin water-oil balance.
In conclusion, the microcapsule beads are mixed with the skin care liquid, and the water and the oil are mixed, so that the oil phase substances can be uniformly distributed in the water phase substances, on one hand, the substance distribution in the essence water can be balanced, and the essence water can promote the water-oil balance of facial skin when in use; on the other hand, the skin care product can also ensure good skin feel, and has excellent moisturizing effect while ensuring fresh and comfortable skin feel; in yet another aspect, the microcapsule beads are suspended in the skin care lotion, so that the microcapsule beads are uniformly distributed in the essence water, oil phase substances can be prevented from contacting with air, the microcapsule beads are not easy to deactivate, and the excellent efficacy of the essence water can be ensured.
The preparation method is simple and convenient, firstly, after a plurality of substances of the skin care liquid are respectively dissolved and mixed, the water phase and the oil phase of the microcapsule beads are mixed to prepare the microcapsule bead particles, and finally, the microcapsule beads are added into the skin care liquid and uniformly mixed, so that the active ingredients and beneficial substances in the essence water can be wrapped and remain active, the active ingredients and beneficial substances are uniformly distributed in the water phase, and meanwhile, the comfortable use experience and excellent use effect of the essence water are ensured. The embodiments described above are some, but not all embodiments of the application. The detailed description of the embodiments of the application is not intended to limit the scope of the application, as claimed, but is merely representative of selected embodiments of the application. All other embodiments, which can be made by those skilled in the art based on the embodiments of the application without making any inventive effort, are intended to be within the scope of the application.
Claims (9)
1. The essence water with the microcapsule coated with the sea buckthorn seed oil and the grape seed oil is characterized by comprising skin care liquid and microcapsule beads;
the skin care liquid comprises the following raw materials in percentage by weight: 2-4% of glycerin, 2-4% of butanediol, 0.05-0.1% of sodium hyaluronate, 1-2% of ectoin, 1-3% of lactobacillus fermentation lysate, 1-3% of Opuntia ficus-indica flower extract, 0.3-0.8% of chitosan, 0.5-1.5% of dipotassium glycyrrhizinate, 0.1-0.2% of polyacrylate crosslinked polymer, 0.01-0.03% of disodium edetate, 0.3-0.6% of p-hydroxyacetophenone, 0.6-1.0% of 1, 2-hexanediol and the balance of water;
the microcapsule beads comprise the following raw materials in percentage by weight: acrylic acid (esters)/C10-30 alkanol acrylate cross-linked polymer 0.01-0.2%, glycerin 1-2%, hydroxyethyl cellulose 0.1-0.5%, 1, 2-hexanediol 0.25-0.5%, octanediol 0.25-0.5%, butanediol 1-2%, triglyceride (ethyl caproic acid) 33-37%, sea buckthorn seed oil 0.4-1.2%, vitamin E0.5-1.5%, grape seed oil 0.2-0.8%, and water balance.
2. The essence water with the microcapsule coating on the sea buckthorn seed oil and the grape seed oil according to claim 1, wherein the skin care liquid comprises the following raw materials in percentage by weight: 3% of glycerin, 3% of butanediol, 0.08% of sodium hyaluronate, 1.5% of ectoin, 2% of lactobacillus fermentation lysate, 2% of Opuntia ficus-indica flower extract, 0.6% of chitosan amine, 1% of dipotassium glycyrrhizinate, 0.15% of polyacrylate crosslinked polymer, 0.02% of disodium ethylenediamine tetraacetate, 0.5% of p-hydroxyacetophenone, 0.8% of 1, 2-hexanediol and the balance of water;
the microcapsule beads comprise the following raw materials in percentage by weight: acrylic acid (esters)/C10-30 alkanol acrylate cross-linked polymer 0.1%, glycerin 1.5%, hydroxyethyl cellulose 0.3%, 1, 2-hexanediol 0.3%, octanediol 3%, butanediol 1.5%, triglyceride (ethylhexanoic acid) ester 35%, sea buckthorn seed oil 0.8%, vitamin E1%, grape seed oil 0.5%, and water in balance.
3. The preparation method of the essence water with the microcapsule coated with the sea buckthorn seed oil and the grape seed oil according to any one of claims 1 to 2, which is characterized by comprising the following steps:
dissolving glycerin, butanediol and p-hydroxyacetophenone in skin care liquid raw materials in water, mixing, heating, stirring and mixing uniformly to obtain a solution 1;
adding water into sodium hyaluronate in skin care lotion raw materials to prepare a solution 2 with the concentration of 1%;
dissolving polyacrylate crosslinked polymer-6 in skin care lotion raw material in water to obtain solution 3;
uniformly mixing the ectoin, lactobacillus fermentation lysate, opuntia Dillenii flower extract, chitosan, dipotassium glycyrrhizinate, disodium edetate and 1, 2-hexanediol in the skin care lotion raw material to obtain a solution 4;
mixing the solution 1, the solution 2, the solution 3 and the solution 4, and heating to obtain skin care liquid;
mixing water, acrylic acid (esters) or C10-30 alkanol acrylate cross-linked polymer, glycerol, hydroxyethyl cellulose, 1, 2-hexanediol, octanediol and butanediol in the microcapsule bead raw material, heating, stirring and dissolving to obtain a solution 5;
mixing sea buckthorn seed oil, vitamin E and grape seed oil in the microcapsule bead raw material, heating, stirring and dissolving to obtain a solution 6;
heating the triglyceride (ethyl caproic acid) ester in the microcapsule bead raw material to obtain a solution 7;
adding the solution 6 into the solution 7, and uniformly stirring to obtain an oil phase;
mixing the oil phase and the water phase, stirring and cooling until microcapsule beads appear;
mixing the microcapsule beads with skin care liquid, and stirring to obtain the final product of essence water.
4. The method for preparing the essence water coated with the sea buckthorn seed oil and the grape seed oil by the microcapsules according to claim 3, wherein the heating temperature of the solution 1 is 58-63 ℃.
5. The method for preparing the essence water with the microcapsule coated with the sea buckthorn seed oil and the grape seed oil according to claim 3, wherein the skin care liquid is heated to 65-80 ℃.
6. The method for preparing the essence water coated with the sea buckthorn seed oil and the grape seed oil by the microcapsules according to claim 3, wherein the temperature of the solution 5 is raised to 70-85 ℃.
7. The method for preparing the essence water with the microcapsule coated with the sea buckthorn seed oil and the grape seed oil according to claim 3, wherein the temperature of the solution 6 is raised to 60-80 ℃.
8. The method for preparing the essence water with the microcapsule coated with the sea buckthorn seed oil and the grape seed oil according to claim 3, wherein the temperature of the solution 7 is raised to 40-80 ℃.
9. The preparation method of the essence water with the microcapsule coated with the sea buckthorn seed oil and the grape seed oil according to claim 3, wherein the weight ratio of the microcapsule beads to the skin care liquid is (1-5): 20.
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| KR20080029035A (en) * | 2006-09-28 | 2008-04-03 | 라호열 | Natural Cosmetic Composition Containing Palm Cactus Fermentation Solution and Grape Seed Extract |
| CN106265101A (en) * | 2016-09-05 | 2017-01-04 | 上海萧雅生物科技股份有限公司 | Microcapsule spraying elite with regulation water and oil balance and preparation method thereof |
| CN106924139A (en) * | 2017-03-23 | 2017-07-07 | 广州市帝臣日化科技有限公司 | A kind of moisturizing stoste and preparation method thereof |
| KR102325648B1 (en) * | 2021-07-13 | 2021-11-15 | (주)케이엠더블유코스메틱스 | Cosmetic composition for anti-aging and skin moisture and eye patch comprising same |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20080029035A (en) * | 2006-09-28 | 2008-04-03 | 라호열 | Natural Cosmetic Composition Containing Palm Cactus Fermentation Solution and Grape Seed Extract |
| CN106265101A (en) * | 2016-09-05 | 2017-01-04 | 上海萧雅生物科技股份有限公司 | Microcapsule spraying elite with regulation water and oil balance and preparation method thereof |
| CN106924139A (en) * | 2017-03-23 | 2017-07-07 | 广州市帝臣日化科技有限公司 | A kind of moisturizing stoste and preparation method thereof |
| KR102325648B1 (en) * | 2021-07-13 | 2021-11-15 | (주)케이엠더블유코스메틱스 | Cosmetic composition for anti-aging and skin moisture and eye patch comprising same |
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