CN115148568A - Sample stage and system and method for modifying samples - Google Patents
Sample stage and system and method for modifying samples Download PDFInfo
- Publication number
- CN115148568A CN115148568A CN202110339352.XA CN202110339352A CN115148568A CN 115148568 A CN115148568 A CN 115148568A CN 202110339352 A CN202110339352 A CN 202110339352A CN 115148568 A CN115148568 A CN 115148568A
- Authority
- CN
- China
- Prior art keywords
- sample
- electron beam
- sample stage
- stage
- top surface
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims abstract description 30
- 238000010894 electron beam technology Methods 0.000 claims description 56
- 230000007547 defect Effects 0.000 claims description 41
- 239000004065 semiconductor Substances 0.000 claims description 36
- 238000010884 ion-beam technique Methods 0.000 claims description 31
- 238000005520 cutting process Methods 0.000 claims description 14
- 239000000463 material Substances 0.000 claims description 10
- 229910052710 silicon Inorganic materials 0.000 claims description 7
- 239000010703 silicon Substances 0.000 claims description 7
- 239000000084 colloidal system Substances 0.000 claims description 3
- 230000008859 change Effects 0.000 claims description 2
- 238000012986 modification Methods 0.000 abstract description 4
- 230000004048 modification Effects 0.000 abstract description 4
- 239000000523 sample Substances 0.000 description 217
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 10
- 230000008569 process Effects 0.000 description 9
- 239000010410 layer Substances 0.000 description 8
- GYHNNYVSQQEPJS-UHFFFAOYSA-N Gallium Chemical compound [Ga] GYHNNYVSQQEPJS-UHFFFAOYSA-N 0.000 description 7
- 238000010586 diagram Methods 0.000 description 7
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 6
- 229910052733 gallium Inorganic materials 0.000 description 6
- 239000003550 marker Substances 0.000 description 6
- 229910052751 metal Inorganic materials 0.000 description 6
- 239000002184 metal Substances 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- 230000005856 abnormality Effects 0.000 description 5
- 238000005259 measurement Methods 0.000 description 5
- 238000012545 processing Methods 0.000 description 5
- 238000004458 analytical method Methods 0.000 description 4
- 230000005540 biological transmission Effects 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 229910052697 platinum Inorganic materials 0.000 description 4
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 3
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 3
- 229910052802 copper Inorganic materials 0.000 description 3
- 239000010949 copper Substances 0.000 description 3
- 238000000921 elemental analysis Methods 0.000 description 3
- 230000000149 penetrating effect Effects 0.000 description 3
- 239000002243 precursor Substances 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 239000011241 protective layer Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 238000003325 tomography Methods 0.000 description 3
- 230000000903 blocking effect Effects 0.000 description 2
- 238000000151 deposition Methods 0.000 description 2
- 230000008021 deposition Effects 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 238000000313 electron-beam-induced deposition Methods 0.000 description 2
- CKHJYUSOUQDYEN-UHFFFAOYSA-N gallium(3+) Chemical compound [Ga+3] CKHJYUSOUQDYEN-UHFFFAOYSA-N 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- NJPPVKZQTLUDBO-UHFFFAOYSA-N novaluron Chemical compound C1=C(Cl)C(OC(F)(F)C(OC(F)(F)F)F)=CC=C1NC(=O)NC(=O)C1=C(F)C=CC=C1F NJPPVKZQTLUDBO-UHFFFAOYSA-N 0.000 description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003575 carbonaceous material Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 230000005684 electric field Effects 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000003384 imaging method Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000007737 ion beam deposition Methods 0.000 description 1
- 238000001888 ion beam-induced deposition Methods 0.000 description 1
- 230000000670 limiting effect Effects 0.000 description 1
- 238000004949 mass spectrometry Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 230000036961 partial effect Effects 0.000 description 1
- 230000002829 reductive effect Effects 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 239000002210 silicon-based material Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 230000007847 structural defect Effects 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 238000012876 topography Methods 0.000 description 1
- 238000004627 transmission electron microscopy Methods 0.000 description 1
Images
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/02—Details
- H01J37/20—Means for supporting or positioning the object or the material; Means for adjusting diaphragms or lenses associated with the support
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/02—Details
- H01J37/04—Arrangements of electrodes and associated parts for generating or controlling the discharge, e.g. electron-optical arrangement or ion-optical arrangement
- H01J37/06—Electron sources; Electron guns
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/02—Details
- H01J37/04—Arrangements of electrodes and associated parts for generating or controlling the discharge, e.g. electron-optical arrangement or ion-optical arrangement
- H01J37/08—Ion sources; Ion guns
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/02—Details
- H01J37/244—Detectors; Associated components or circuits therefor
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
- H01J37/00—Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
- H01J37/26—Electron or ion microscopes; Electron or ion diffraction tubes
Landscapes
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
本发明实施例涉及样品载台及修饰样品的系统及方法。本揭露提供一种样品载台,其包含基座及第一样品支柱。所述基座具有第一表面。所述第一样品支柱设置于所述基座的所述第一表面,所述第一样品支柱的顶面具有沟槽用以放置样品。本揭露还包含使用所述样品载台的样品修饰系统及方法。
Embodiments of the present invention relate to sample stages and systems and methods for modifying samples. The present disclosure provides a sample stage, which includes a base and a first sample support. The base has a first surface. The first sample support column is disposed on the first surface of the base, and the top surface of the first sample support column has a groove for placing the sample. The present disclosure also includes sample modification systems and methods using the sample stage.
Description
技术领域technical field
本发明实施例涉及一种样品载台、修饰样品的系统及方法,特别是关于一种使用加工后的样品载台进行样品修饰的系统及方法。Embodiments of the present invention relate to a sample stage, a system and method for modifying samples, and in particular, to a system and method for sample modification using a processed sample stage.
背景技术Background technique
在半导体工艺中,测量设备的性能直接影响到工艺调制的能力和产量的提升。半导体厂和设备供应商必须确保其测量的结果必须在公差范围内,并符合ISO和质量系统的认证。当元件的尺寸与公差不断地缩小,测量工作的困难性也随着提高。随着半导体工业不断地寻求各种方法以满足日趋严苛的测量需求,目前已有许多测量工具被开发以满足测量需求,例如测量半导体元件的CD(Critical Dimension)值、厚度、表面形貌(morphology)、掺杂浓度(doping concentration),以及缺陷分析等等。In the semiconductor process, the performance of measurement equipment directly affects the ability of process modulation and the improvement of yield. Semiconductor fabs and equipment suppliers must ensure that their measurements must be within tolerance and certified to ISO and quality systems. As the dimensions and tolerances of components continue to shrink, so does the difficulty of measuring. As the semiconductor industry continues to seek various methods to meet the increasingly stringent measurement needs, many measurement tools have been developed to meet the measurement needs, such as measuring the CD (Critical Dimension) value, thickness, surface topography ( morphology), doping concentration, and defect analysis, etc.
传统上,半导体元件的缺陷检测是透过穿透式电子显微镜(TransmissionElectron Microscopy,TEM)或扫描穿透式电子显微镜(Scanning Transmission ElectronMicroscope,STEM)所完成的。以TEM为例,其使用高能量电子束照射到超薄的TEM试片,再经放大成像而取得样品2D图像的技术,其图像分辨率可达0.1纳米的原子等级,用以观察材料微结构或晶格缺陷。由于TEM是通过穿透电子束打到TEM试片,因此TEM试片所要观察的区域厚度,必需达到电子束能穿透的等级,例如厚度约在2埃以下,这也使得TEM的应用容易受到样品置备的局限性所影响。举例来说,是否所要观察的半导体元件的结构缺陷确实有位于超薄的TEM试片上,或是所置备的TEM试片是否能呈现出感兴趣区域(Region of Interest,ROI),就是使用TEM在检测应用上所实际反映出的技术瓶颈。Traditionally, defect detection of semiconductor components is accomplished by transmission electron microscope (Transmission Electron Microscopy, TEM) or scanning transmission electron microscope (Scanning Transmission Electron Microscope, STEM). Taking TEM as an example, it uses a high-energy electron beam to irradiate an ultra-thin TEM specimen, and then magnifies the imaging technology to obtain a 2D image of the sample. The image resolution can reach the atomic level of 0.1 nanometers. or lattice defects. Since TEM hits the TEM specimen by penetrating the electron beam, the thickness of the area to be observed on the TEM specimen must reach the level that the electron beam can penetrate, for example, the thickness is about 2 angstroms or less, which also makes the application of TEM easy to be affected. affected by limitations in sample preparation. For example, whether the structural defects of the semiconductor element to be observed are indeed located on the ultra-thin TEM test piece, or whether the prepared TEM test piece can show a region of interest (ROI), that is, using TEM in the Detect technical bottlenecks that are actually reflected in the application.
发明内容SUMMARY OF THE INVENTION
本发明的一实施例涉及一种样品载台,其包含基座及第一样品支柱。所述基座具有第一表面。所述第一样品支柱设置于所述基座的所述第一表面,所述第一样品支柱的顶面具有沟槽用以放置样品。One embodiment of the present invention relates to a sample stage including a base and a first sample support. The base has a first surface. The first sample support column is disposed on the first surface of the base, and the top surface of the first sample support column has a groove for placing the sample.
本发明的另一实施例涉及一种修饰样品的系统,其包含电子束源、样品载台、离子束源及检测器。所述电子束源用以产生电子束。所述样品载台设置于所述电子束源下,其具有样品支柱,所述样品支柱的顶面具有沟槽用以放置样品。所述离子束源用以产生离子束而切削放置于所述样品载台的所述样品。所述检测器设置于所述样品载台下。其中,所述样品载台可经调整而改变其相对于所述电子束源的角度,使所述电子束源所产生的电子束可穿透所述样品并被所述检测器所检测。Another embodiment of the present invention is directed to a system for modifying a sample that includes an electron beam source, a sample stage, an ion beam source, and a detector. The electron beam source is used to generate electron beams. The sample stage is disposed under the electron beam source, and has a sample support, and the top surface of the sample support has a groove for placing the sample. The ion beam source is used to generate an ion beam to cut the sample placed on the sample stage. The detector is arranged under the sample stage. Wherein, the sample stage can be adjusted to change its angle relative to the electron beam source, so that the electron beam generated by the electron beam source can penetrate the sample and be detected by the detector.
本发明的再一实施例涉及一种修饰样品的方法,其包含以下步骤:放置样品于样品载台的样品支柱,所述样品支柱的顶面具有沟槽,所述沟槽延伸到所述顶面的相对的两边缘而使所述样品的两侧大致不受所述样品支柱遮蔽;及使用离子束切削所述样品,使所述样品具有锥状轮廓。Yet another embodiment of the present invention relates to a method of modifying a sample, comprising the steps of: placing a sample on a sample support of a sample stage, the sample support having a groove on its top surface, the groove extending to the top Opposite edges of the face such that the two sides of the sample are substantially unobstructed by the sample support; and an ion beam is used to ablate the sample so that the sample has a tapered profile.
附图说明Description of drawings
当结合附图阅读时,从以下详细描述最佳理解本揭露的方面。应注意,根据产业中的标准实践,各种结构未按比例绘制。事实上,为了清楚论述可任意增大或减小各种结构的尺寸。Aspects of the present disclosure are best understood from the following detailed description when read in conjunction with the accompanying drawings. It should be noted that in accordance with standard practice in the industry, the various structures are not drawn to scale. In fact, the dimensions of the various structures may be arbitrarily increased or decreased for clarity of discussion.
图1A是根据本揭露的一些实施例的样品载台俯视图。1A is a top view of a sample stage according to some embodiments of the present disclosure.
图1B是根据本揭露的一些实施例的样品载台侧视图。Figure IB is a side view of a sample stage according to some embodiments of the present disclosure.
图2A是根据本揭露的一些实施例的修饰样品的系统结构示意图。FIG. 2A is a schematic structural diagram of a system for modifying a sample according to some embodiments of the present disclosure.
图2B是根据本揭露的一些实施例的样品载台俯视图。2B is a top view of a sample stage according to some embodiments of the present disclosure.
图2C是根据本揭露的一些实施例的样品支柱及样品示意图。2C is a schematic diagram of a sample support and a sample according to some embodiments of the present disclosure.
图3A及图3B是根据本揭露的一些实施例的样品载台俯视图。3A and 3B are top views of a sample stage according to some embodiments of the present disclosure.
图4A及图4B是根据本揭露的一些实施例的半导体元件俯视图。4A and 4B are top views of semiconductor devices according to some embodiments of the present disclosure.
图4C是根据本揭露的一些实施例的半导体元件侧视图。4C is a side view of a semiconductor device according to some embodiments of the present disclosure.
图5A是根据本揭露的一些实施例的半导体元件俯视图。5A is a top view of a semiconductor device according to some embodiments of the present disclosure.
图5B及图5C是根据本揭露的一些实施例的样品示意图。5B and 5C are schematic diagrams of samples according to some embodiments of the present disclosure.
图6A及图6B是根据本揭露的一些实施例的样品支柱及样品示意图。6A and 6B are schematic diagrams of sample supports and samples according to some embodiments of the present disclosure.
图7是根据本揭露的一些实施例的步骤流程图。7 is a flow diagram of steps according to some embodiments of the present disclosure.
具体实施方式Detailed ways
以下揭露提供用于实施所提供的标的的不同构件的许多不同实施例或实例。下文描述元件及布置的特定实例以简化本揭露。当然,此些仅为实例且非旨在限制。举例来说,在以下描述中的第一构件形成于第二构件上方或上可包含其中所述第一构件及所述第二构件经形成为直接接触的实施例,且还可包含其中额外构件可形成在所述第一构件与所述第二构件之间,使得所述第一构件及所述第二构件可不直接接触的实施例。另外,本揭露可在各个实例中重复元件符号及/或字母。此重复出于简化及清楚的目的且本身不指示所论述的各个实施例及/或配置之间的关系。The following disclosure provides many different embodiments or examples of different means for implementing the provided subject matter. Specific examples of elements and arrangements are described below to simplify the present disclosure. Of course, these are merely examples and are not intended to be limiting. For example, the formation of a first member over or on a second member in the following description may include embodiments in which the first member and the second member are formed in direct contact, and may also include additional members An embodiment may be formed between the first member and the second member such that the first member and the second member may not be in direct contact. Additionally, the present disclosure may repeat reference numerals and/or letters in various instances. This repetition is for the purpose of simplicity and clarity and does not in itself indicate a relationship between the various embodiments and/or configurations discussed.
此外,为便于描述,例如“在…下面”、“在…下方”、“下”、“在…上方”、“上”、“在…上”及类似者的空间相对术语可在本文中用于描述一个元件或构件与另一(些)元件或构件的关系,如图中图解说明。空间相对术语打算涵盖除在图中描绘的定向以外的使用或操作中的装置的不同定向。设备可以其它方式定向(旋转90度或按其它定向)且因此可同样解释本文中使用的空间相对描述词。Furthermore, for ease of description, spatially relative terms such as "below", "below", "under", "above", "on", "on" and the like may be used herein Used to describe the relationship of one element or component to another element or component(s), as illustrated in the figures. The spatially relative terms are intended to encompass different orientations of the device in use or operation other than the orientation depicted in the figures. The device may be otherwise oriented (rotated 90 degrees or at other orientations) and thus the spatially relative descriptors used herein may be similarly interpreted.
如本文中使用,例如“第一”、“第二”及“第三”的术语描述各种元件、组件、区、层及/或区段,此些元件、组件、区、层及/或区段不应受此些术语限制。此些术语可仅用来区分一个元件、组件、区、层或区段与另一元件、组件、区、层或区段。除非由上下文清楚指示,否则例如“第一”、“第二”及“第三”的术语当在本文中使用时并不暗示一序列或顺序。As used herein, terms such as "first", "second" and "third" describe various elements, components, regions, layers and/or sections, such elements, components, regions, layers and/or Sections should not be limited by these terms. These terms may only be used to distinguish one element, component, region, layer or section from another element, component, region, layer or section. Terms such as "first," "second," and "third," when used herein do not imply a sequence or order unless clearly indicated by the context.
本揭露一些实施例中,对半导体元件的缺陷点进行定位、定点的三维结构观察,其中包含提供一种样品载台,此样品载台的结构便于使样品得以使用修饰样品系统,例如STEM,进行二维的观察,以及将样品加工削尖而修饰为可进一步使用原子探针断层扫描(Atom Probe Tomography)对缺陷点的三维结构和元素成分进行分析。In some embodiments of the present disclosure, the three-dimensional structure observation of the positioning and the fixed point of the defect point of the semiconductor element includes providing a sample stage, and the structure of the sample stage is convenient for the sample to be modified using a sample system, such as STEM. Two-dimensional observation, as well as processing and sharpening the sample to modify it, can further use Atom Probe Tomography to analyze the three-dimensional structure and elemental composition of defect points.
如图1A的俯视角度以及图1B的侧视角度所示,在一些实施例中,样品载台10包含基座11及第一样品支柱12。基座11具有第一表面11A。第一样品支柱12则是设至于基座11的第一表面11A。在一些实施例中,第一样品支柱12的顶面12A具有沟槽13用以放置样品14。As shown in the top view of FIG. 1A and the side view of FIG. 1B , in some embodiments, the
第一样品支柱12的用途之一在于定位样品14,由于样品14的尺寸约为100nm,而基座11的尺寸则可达数微米到数毫米之谱,因此在样品14远小于基座11的情况下,需要将样品14设置于特定的样品支柱上,以正确辨识样品14在样品载台10的位置,而非直接将样品14放置于基座11的第一表面11A上。进一步地,在一些实施例中,第一样品支柱12的沟槽13进一步提供样品14的定位,例如将样品14放置于沟槽13的中心,从而可透过沟槽13的位置而观察到样品14。One of the purposes of the
不过,考虑到当样品被放置于一般非本发明实施例的沟槽时,会因为沟槽具有深度而使样品大体上是隐没于沟槽当中,即,仅能透过俯视角度观察到样品,这使得电子束在任何角度照射样品时,即便是电子束穿透样品,电子束也会被样品支柱的结构所阻挡而无法到达检测器,严重影响到样品图像的分辨率。本发明实施例的沟槽设计可避免上述阻挡电子束而无法到达检测器的情形发生。However, considering that when the sample is placed in a groove that is not generally an embodiment of the present invention, the sample is substantially submerged in the groove due to the depth of the groove, that is, the sample can only be observed through a top view, This makes the electron beam irradiate the sample at any angle, even if the electron beam penetrates the sample, the electron beam will be blocked by the structure of the sample support and cannot reach the detector, which seriously affects the resolution of the sample image. The trench design of the embodiment of the present invention can avoid the above situation of blocking the electron beam from reaching the detector.
关于电子束与样品载台之间的位置关系,例如在图2A所示的修饰样品的系统,例如STEM,结构示意图,电子束源21是位于样品载台10的上方,其用以产生电子束照射样品。在一些实施例中,电子束源21可包含高电压系统、电子枪、聚光镜等元件(未示于图中),例如可由高电压系统产生100keV到1MeV的加速电压,送入镜筒上端的电子枪,让场发射式电子枪加温发射出的高亮度的电子束,经过聚光镜后到达并穿透样品14。Regarding the positional relationship between the electron beam and the sample stage, for example, as shown in FIG. 2A , a system for modifying a sample, such as STEM, is a schematic structural diagram. The
位于电子束源21下方的样品载台10除了其第一表面11A(见前图1B)具有第一样品支柱12之外,在一些实施例中,样品载台10的基座11相对于其第一表面11A的第二表面11B可与夹具31相连接(如图2A右侧所展示的侧视角度所示意),夹具31用以移动或转动样品载台10而调整样品载台10相对于电子束源21的角度,例如使电子束源21所产生的电子束与第一表面11A之间具有小于或等于90度的夹角,从而容许透过沟槽13而部分暴露于第一样品支柱12之外的样品14得以被电子束源21所产生的电子束所穿透。在一些实施例中,样品载台10仅具有单一第一样品支柱12,或是多个第一样品支柱12排列为单排的形式,且在电子束照射到第一样品支柱12上的样品14时,所述第一样品支柱12的排列方向大致正交于电子束的照射方向。换句话说,电子束在穿过任一个第一样品支柱12上的样品14之后,电子束于行径路径上并不会被其它的第一样品支柱12所阻挡。In addition to having a
再进一步参考图2B、图2C,其分别为经夹具调整倾斜角度的样品载台10的俯视图,以及针对第一样品支柱12的立体示意图。如图所示,前述电子束源21所产生的电子束具有行进路径DE,其可在高于第一样品支柱12的顶面12A的位置照射到样品14而无须顾虑受第一样品支柱12的结构所阻挡的问题;而在低于第一样品支柱12的顶面12A的位置照射样品14时,就需要透过沟槽位于第一样品支柱12的顶面12A的两边缘的开口,例如使电子束的行进路径DE与沟槽13的走向平行,使得电子束能经由电子束入口13A及电子束出口13B而可直接照射于样品14,并且在穿透样品14后不受阻挡地通过样品载台10。Referring further to FIGS. 2B and 2C , they are a top view of the
本揭露在一些实施例中,开设于第一样品支柱12的顶面12A的沟槽13可于结构上进一步区分为多个沟槽,例如以图2B最左侧所示的第一样品支柱12为例,其顶面具有第一沟槽131以及正交于第一沟槽131的第二沟槽132,而呈现十字型凹陷,样品14即放置于第一沟槽131与第二沟槽132交错的位置。在一些实施例中,第一样品支柱12的顶面12A开设有多个沟槽13,其中至少有一沟槽延伸到顶面12A的相对的两边缘而形成前述的电子束入口13A及电子束出口13B。In some embodiments of the present disclosure, the
在一些实施例中,穿过样品14的电子束接着可再通过物镜、中间镜和投影镜等多级放大元件(未示于图中),到达位于样品载台10下的检测器22。位于样品载台10下的检测器22可为明场扫描穿透式显微镜检测器(Bright Field STEM Detector)。当电子束源21产生的电子束穿过样品14时,电子束会与样品14的晶体发生交互作用而于样品载台10下方,产生各种散射电子,其中散射角度较小的电子会进入检测器22形成透射明场图像,以对样品14的二维结构进行观察。在一些实施例中,穿透样品14的电子会进一步穿过一或多个孔径光栏(Aperture Diaphragm)。在一些实施例中,检测器22可包含荧光板、相机或感光耦合元件(Charge Coupled Device,CCD)。In some embodiments, the electron beam passing through the
除了设置有单一第一样品支柱12或是单排的第一样品支柱12,如图3A所示,在一些实施例中,样品载台10可进一步包含一个或多个第二样品支柱15。第二样品支柱15也是设置于样品载台10的基座11的第一表面11A,其不与第一样品支柱12位于同一列,而是使样品载台10整体具有多排的样品支柱结构。由于穿透样品的电子束尚需行进到检测器22,因此第二样品支柱15是在电子束的行进方向上与第一样品支柱12错开,避免阻挡电子束的行进。在一些实施例中,如图3A、图3B所示,第二样品支柱15可为单一或多排的方式设置,使样品载台整体具有二排、三排或更多的样品支柱,惟在设置第二样品支柱15时,须避免其与第一样品支柱或其它第二样品支柱15在电子束的行进方向上存在重叠的情况。In addition to being provided with a single
传统上,STEM的样品载台的材料包含铜,并且是透过计算机数值控制(ComputerNumerical Control,CNC)工艺对铜基材料进行加工而形成。然而,考虑到铜元素可能会对样品的元素分析产生干扰,例如在质谱分析时产生过多的背景噪声而影响到对样品成分的判断,因此本揭露在一些实施例中,所使用的样品载台10的材料包含硅。在一些实施例中,样品载台10的基座11和第一、第二样品支柱12、15都是由硅所构成,例如透过激光对硅晶片进行加工,于硅晶片的一面雕刻出样品支柱的结构,并于样品支柱的顶面开设沟槽,在此实施例中,样品载台10的基座11和第一、第二样品支柱12、15也可谓是一体成形。在针对硅晶片加工的例子中,可于形成样品支柱后对硅晶片进行切割,以取得所需要的基座面积尺寸。Traditionally, the material of the STEM sample stage contains copper, and is formed by processing the copper-based material through a Computer Numerical Control (CNC) process. However, considering that copper may interfere with the elemental analysis of the sample, such as excessive background noise during mass spectrometry analysis, which affects the determination of sample components, in some embodiments of the present disclosure, the sample carrier used The material of table 10 contains silicon. In some embodiments, the
如果仅使用STEM对样品进行二维结构的观察,样品并不需要加工为具有锥状轮廓。不过,本揭露的目的之一在于使样品载台10及其上的样品14得以被一并使用原子探针断层扫描(Atom Probe Tomography,APT)技术进行三维结构的观察和定量化学成分鉴定,因此在一些实施例中,复如图2A所示,进一步使用离子束源23对样品14进行加工修饰,即利用离子束源23所产生的离子束对样品载台10上的样品14进行切削,使样品14具有锥状轮廓。在一些实施例中,离子束源23设置于样品载台10上方,且其与电子束源21之间具有角度,所述角度可约为52度。If only STEM is used to observe the two-dimensional structure of the sample, the sample does not need to be processed to have a tapered profile. However, one of the objectives of the present disclosure is to enable the
详细来说,APT是一种可以提供三维度图像及定量化学成分鉴定的原子级材料分析的技术,具有高灵敏度。所述技术依赖于样品表面上单个原子/原子团簇的电离和随后的场蒸发(Field Evaporation)。其样品是以圆锥形尖端的形式制备,一般来说,为了维持分析质量,其样品必须符合数项需求:(1)样品为圆锥状并具有顶点半径小于100nm;(2)样品形状必须对称,避免形成椭圆锥状;(3)样品的椎角(Shape Angle)不能太大;及(4)样品的圆锥柱身须避免微裂缝出现。而就样品制作技术,目前主要是透过聚焦离子束(FocusedIon Beam,FIB)的运用,例如针对半导体元件的目标分析区域先以铂(Pt)、镍(Ni)或者其它材料镀上保护层,接着切出一个楔形长条样品,其宽度约为1~2μm,而长度则约为15~20μm。然后先切断样品的一端进行镀接于操纵臂(Manipulator),再切断另一端后将样品从半导体元件的主体取出。接着将样品镀接到样品载台上。之后,以环状减薄法(AnnularMilling)将样品半径减到小于约100nm,最后再以较低的电压进行清洁,以清除例如镓(Ga)离子所造成的损伤层。In detail, APT is a technique for atomic-level material analysis that can provide three-dimensional images and quantitative chemical composition identification with high sensitivity. The technique relies on the ionization of individual atoms/clusters of atoms on the sample surface and subsequent Field Evaporation. Its samples are prepared in the form of conical tips. In general, in order to maintain analytical quality, the samples must meet several requirements: (1) the sample is conical and has an apex radius less than 100 nm; (2) the sample shape must be symmetrical, Avoid forming an elliptical cone; (3) the shape angle of the sample should not be too large; and (4) the conical cylinder of the sample must avoid micro-cracks. As for the sample preparation technology, currently it is mainly through the application of Focused Ion Beam (FIB), for example, the target analysis area of the semiconductor element is first plated with a protective layer of platinum (Pt), nickel (Ni) or other materials. Next, a wedge-shaped strip sample was cut out with a width of about 1-2 μm and a length of about 15-20 μm. Then, one end of the sample is cut off to be plated on a manipulator, and the other end is cut off, and then the sample is taken out from the main body of the semiconductor element. The sample is then plated onto the sample stage. After that, the radius of the sample is reduced to less than about 100 nm by an annular thinning method (Annular Milling), and finally, a lower voltage is used for cleaning to remove the damaged layer caused by, for example, gallium (Ga) ions.
经由上述方法制作的样品,即可应用于原子探针断层扫描技术以进行样品的立体结构扫描,从而以三维的角度观察半导体元件的缺陷点,包含观察缺陷点的形貌以及分析缺陷点所在位置的元素成分。The samples prepared by the above method can be applied to the atom probe tomography technology to scan the three-dimensional structure of the sample, so as to observe the defect points of the semiconductor element from a three-dimensional angle, including observing the morphology of the defect points and analyzing the location of the defect points. elemental composition.
从而,本揭露一些实施例中,离子束源23用以提供聚焦离子束,举例来说,离子束源23可使用镓做为离子源,此考虑到镓具有低熔点、低蒸气压及良好的抗氧化力等优点。离子束源23在使用时,外加电场而使液态镓形成细小尖端,例如使液态镓,将之拉成曲率半径小于阈值半径的圆锥体(Taylor cone),导致镓被游离而喷出,形成镓离子束。导出的镓离子束可以利用电透镜聚焦,经过一系列变化孔径而决定离子束的大小,再经过二次聚焦到样品表面,利用物理碰撞来达到切割的目的。一般来说,此方法所形成的离子束的尺寸小于10nm,可做为精确的纳米结构加工的工具。Therefore, in some embodiments of the present disclosure, the
进一步来说,本揭露所使用的样品也可以一并使用离子束源23进行半导体元件缺陷点的标记。为了降低半导体元件的功耗、提升性能以及增加晶体管密度等等实务需求,半导体元件的外观已微缩到纳米尺度,不但其缺陷难以直接被肉眼观察,实际上也仅能透过探针进行电性测试的方式,来精确判断电性异常的区域,例如测试出特定坐标位置的电子构件有异常。然而,即便是透过探针测试出电性异常,也已知发生异常的位置,然而如果要进行缺陷的观察,那么不如寻找电性异常来得直接。传统上的TEM或STEM需要将样品切薄进行观察,但所切薄的位置却不一定准确地对应到缺陷所在位置,迫使在操作者测得半导体元件电性异常的情况下,仍得有如大海捞针般地寻找缺陷结构在显微镜下的位置。Further, the samples used in the present disclosure can also use the
本揭露在一些实施例中,可利用离子束源23制做标记,例如使用聚焦离子束沉积金属线于样品的表面。如图4A所示的半导体元件俯视图,可透过电性测试而发现一半导体元件40存在电性异常,也就是经过电性测试而精确地判断存在缺陷点41的位置,然而,在STEM上以二维角度观察的样品却可能是切到半导体元件40的其它位置,例如非属缺陷点41所在之处的区域A、区域B、区域C等。因此本揭露在一些实施例中,如图4B所示,透过聚焦离子束沉积技术而在电性测试后,直接在缺陷点41的周边沉积多个金属线段作为定位标记42。传统上,运用聚焦离子束来沉积金属线,其用途之一是作为电路修改时的重新接线,或借此调整元件的电阻率,而本揭露在此实施例则是将此定位标记线42作为缺陷点41的标记之用。在一些实施例中,定位标记42的材料包含铂(Pt),其相较于碳基材料,可在观察时呈现更好的对比,进而较容易地被观察到。而运用FIB沉积的原理是利用金属管供应微量的含金属基前体(precursor)气体到半导体元件40的表面,利用离子束轰击作用将前体分解而沉积金属,其可归类为离子束诱导沉积(Ion beam-induced deposition,IBID)的一种。在一些实施例中,也可使用类似的电子束诱导沉积(Electron beam-induced deposition,EBID)来沉积形成定位标记42。In some embodiments of the present disclosure, the
如图4B所示的设置有定位标记的半导体元件俯视图,在一些实施例中,定位标记42可具有多个标记线42a、42b、42c、42d指向缺陷点41。在一些实施例中,定位标记41内的标记线42(a-d)是排列为十字型,而十字型的中心则为缺陷点41的所在之处。在一些实施例中,标记线42(a-d)并不相互接触,而是保留缺陷点41不被标记线42(a-d)所覆盖。举例来说,于同一方向上的标记线,例如标记线42a、42c或是标记线42b、42d的组合,其间距小于约30nm,因此在一些实施例中,缺陷点41是位于约30nm x 30nm的范围内,并被定位标记42所环绕。As shown in FIG. 4B , the top view of the semiconductor device provided with the positioning mark, in some embodiments, the
如图4C所示的半导体元件剖视图,其沿着图4B的线段FF'为剖面展示,在一些实施中,标记线42b(其它标记线亦同)可具有大致呈现方型或矩形的剖面结构。在一些实施例中,标记线的宽高比为约1:1到约1:3。在一些实施例中,可在透过FIB制做定位标记42后,进一步涂布有机胶体(未示于图中)覆盖定位标记42的标记线42(a-d),作为定位标记的保护层,可维持前述标记线42(a-d)的宽高比而不坍倒为扁平的形状。The cross-sectional view of the semiconductor device shown in FIG. 4C is shown in cross-section along the line segment FF' of FIG. 4B . In some implementations, the marking
本揭露一些实施例中,半导体元件40经电性测试而确认存在缺陷点41后,可先行沉积定位标记42以完成对缺陷点41的定位,而后为了进一步以定点的形式进行缺陷点41的立体结构观察,可接着如前述关于APT样品的制备方式,于半导体元件40进行切割而取得长条样品,而后镀接到样品载台10的样品支柱(例如:第一样品支柱12)上。In some embodiments of the present disclosure, after the
如图5A的设置有定位标记的半导体元件俯视图以及图5B的样品立体示意图,在本揭露一些实施例中,于样品区域50进行切割后所取得的样品51至少包含部分的定位标记42,其可被镀接于样品载台的样品支柱上。在一些实施例中,半导体元件40在形成定位标记42于其表面后,除了前述的有机胶体之外,可另形成其它结构于所述表面上,例如形成盖层或牺牲层43(后见于图6)保护下方的感兴趣区域(Region of Interest,ROI),例如包含缺陷点41的结构不受到镓的破坏。在此实施例中,虽然定位标记42被覆盖,定位标记42仍可在制备APT样品的过程中实现对缺陷点41的定位。As shown in FIG. 5A , the top view of the semiconductor device provided with the positioning marks, and the three-dimensional schematic view of the sample in FIG. 5B , in some embodiments of the present disclosure, the
如图5B所示,无论位于样品51的定位标记42是否有在被其它结构所覆盖,定位标记42的侧面420都可被观察到,因此在如图5C、图6A及图6B所示将样品半径减小而逐步切削为具锥状轮廓的过程中,可持续通过从样品51的侧面观察、跟踪定位标记42的侧面420,而得知样品51在切削为具锥状轮廓的过程中仍然是逐渐往缺陷点41的所在位置靠近。如前所述,定位标记42的材料包含铂,而其相对于周边其它材料可表现出较好的对比(如图6A的示意),因此可较为清楚地以定位标记42的标记线42(a-d)的剖面为定位标的。另外,由于标记线42(a-d)的一端都是指向缺陷点41但不覆盖缺陷点41的位置,因此在样品51切削为具锥状轮廓的过程中,观察到圆锥的侧面已从有标记线42(a-d)转变到不再有标记线,例如图6A及图6B的示意,那么表示切削、修饰后的样品51已相当到达或接近缺陷点41,而可将样品51连同样品载台10移到进行APT技术分析,也就是对缺陷点进行三维度图像观察以及定量化学成分鉴定。在一些实施例中,修饰后的样品51高度约为40nm,底部宽度约为20到30nm,顶部宽度约为10nm。As shown in FIG. 5B , no matter whether the
具上所述,如图7所示,本揭露一些实施中,揭露一种修饰样品的方法,其至少包含步骤601:放置样品于样品载台的样品支柱,所述样品支柱的顶面具有沟槽,所述沟槽延伸到所述顶面的相对的两边缘而使所述样品的两侧大致不受所述样品支柱遮蔽;以及步骤602:使用离子束切削所述样品,使所述样品具有锥状轮廓。并且,在一些实施例中,本揭露于放置样品于样品载台前,可在从半导体元件切割取得样品之前,先测量半导体元件的电性,以判断缺陷点,并形成定位标记位于半导体元件而利用定位标记的多个标记线指向缺陷点,接着再切割所述半导体元件以取得样品,此时样品是至少包含部分的定位标记。而后,即可在使用离子束切削样品的步骤中,切削定位标记的标记线的部分,使标记线分别暴露其剖面,并使用所述剖面辨识所述缺陷点的位置。With the above, as shown in FIG. 7 , in some implementations of the present disclosure, a method for modifying a sample is disclosed, which at least includes step 601 : placing a sample on a sample support of a sample stage, the top surface of the sample support having grooves grooves extending to opposite edges of the top surface such that both sides of the sample are substantially unobstructed by the sample support; and step 602 : cutting the sample using an ion beam such that the sample Has a tapered profile. In addition, in some embodiments, before placing the sample on the sample stage, the present disclosure can measure the electrical properties of the semiconductor element to determine the defect point, and form positioning marks on the semiconductor element before the sample is cut and obtained from the semiconductor element. Using a plurality of marking lines of the positioning mark to point to the defect point, and then cutting the semiconductor element to obtain a sample, at this time, the sample contains at least part of the positioning mark. Then, in the step of using the ion beam to cut the sample, the part of the marking line of the positioning mark can be cut, so that the marking lines respectively expose their cross-sections, and the positions of the defect points can be identified by using the cross-sections.
综上所述,本揭露在一些实施例中,提供一种兼具对半导体元件的缺陷点进行定位、定点的三维结构观察方式。此方法可结合新颖的样品载台结构,使样品载台上的样品不但可以被电子束和检测器进行二维结构的观察,也可以被离子束加工而切削、修饰为具有锥状轮廓而另为APT的三维观察和元素分析。而为了改善元素分析的准确性,本揭露使用硅材料制做样品载台。以及为了能够使得缺陷点被正确定位及定点观察,本揭露使用包含铂材料的定位标记,让样品被切削为具有锥状轮廓的过程可以透过定位标记而确认缺陷点的位置。To sum up, in some embodiments, the present disclosure provides a three-dimensional structure observation method for locating and locating defect points of a semiconductor device. This method can be combined with the novel sample stage structure, so that the sample on the sample stage can not only be observed by the electron beam and the detector for two-dimensional structure, but also can be cut and modified by the ion beam processing to have a conical profile and another 3D observation and elemental analysis for APT. In order to improve the accuracy of elemental analysis, the present disclosure uses silicon material to make the sample stage. And in order to enable the defect points to be correctly positioned and observed, the present disclosure uses a positioning mark containing platinum material, so that the process of cutting the sample into a tapered profile can confirm the position of the defect point through the positioning mark.
前述内容概述数项实施例的结构,使得所属领域的技术人员可更佳地理解本揭露的方面。所属领域的技术人员应了解,其可容易地使用本揭露作为用于设计或修改其它工艺及结构的基础以实行本文中介绍的实施例的相同目的及/或达成相同优点。所属领域的技术人员还应了解,此些等效构造不背离本揭露的精神及范围,且其可在不背离本揭露的精神及范围的情况下在本文中作出各种改变、置换及更改。The foregoing outlines the structure of several embodiments so that those skilled in the art may better understand aspects of the present disclosure. Those skilled in the art should appreciate that they may readily use the present disclosure as a basis for designing or modifying other processes and structures for carrying out the same purposes and/or achieving the same advantages of the embodiments described herein. Those skilled in the art should also realize that such equivalent constructions do not depart from the spirit and scope of the present disclosure, and that they can make various changes, substitutions, and alterations herein without departing from the spirit and scope of the present disclosure.
符号说明Symbol Description
10:样品载台10: Sample stage
11:基座11: Pedestal
11A:第一表面11A: First surface
11B:第二表面11B: Second Surface
12:第一样品支柱12: First Sample Pillar
12A:顶面12A: Top surface
13:沟槽13: Groove
13A:电子束入口13A: Electron beam entrance
13B:电子束出口13B: Electron beam exit
131:第一沟槽131: First groove
132:第二沟槽132: Second groove
14:样品14: Sample
15:第二样品支柱15: Second Sample Pillar
21:电子束源21: Electron beam source
22:检测器22: Detector
23:离子束源23: Ion beam source
31:夹具31: Fixtures
40:半导体元件40: Semiconductor components
41:缺陷点41: Defect point
42:定位标记42: Orientation Marker
42a:标记线42a: Marker line
42b:标记线42b: Marker line
42c:标记线42c: Marker line
42d:标记线42d: Marker line
420:侧面420: Side
43:牺牲层43: Sacrificial Layer
50:样品区域50: Sample area
51:样品51: Sample
601:步骤601: Steps
602:步骤602: Step
A:区域A: area
B:区域B: area
C:区域C: area
DE:行进路径D E : travel path
FF':线段。FF': Line segment.
Claims (10)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202110339352.XA CN115148568A (en) | 2021-03-30 | 2021-03-30 | Sample stage and system and method for modifying samples |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202110339352.XA CN115148568A (en) | 2021-03-30 | 2021-03-30 | Sample stage and system and method for modifying samples |
Publications (1)
Publication Number | Publication Date |
---|---|
CN115148568A true CN115148568A (en) | 2022-10-04 |
Family
ID=83404536
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN202110339352.XA Pending CN115148568A (en) | 2021-03-30 | 2021-03-30 | Sample stage and system and method for modifying samples |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN115148568A (en) |
Citations (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20040129878A1 (en) * | 2003-01-08 | 2004-07-08 | Satoshi Tomimatsu | Apparatus for specimen fabrication and method for specimen fabrication |
CN1766592A (en) * | 2004-07-14 | 2006-05-03 | 应用材料以色列公司 | Method and apparatus for sample formation and microanalysis in a vacuum chamber |
JP2008204959A (en) * | 2008-05-16 | 2008-09-04 | Hitachi Ltd | Sample analysis method and sample preparation method |
JP2008261891A (en) * | 2008-08-08 | 2008-10-30 | Hitachi Ltd | Sample preparation method |
CN103646839A (en) * | 2013-11-08 | 2014-03-19 | 上海华力微电子有限公司 | Metal net for bearing and fixing TEM sample |
CN104251795A (en) * | 2013-06-28 | 2014-12-31 | Fei公司 | Plan view sample preparation |
CN104880340A (en) * | 2014-02-28 | 2015-09-02 | 中芯国际集成电路制造(上海)有限公司 | Preparation method of transmission electron microscopic sample |
CN104979151A (en) * | 2014-04-14 | 2015-10-14 | Fei公司 | High Capacity TEM Grid |
TW201546865A (en) * | 2014-03-24 | 2015-12-16 | Hitachi High Tech Science Corp | Focused ion beam apparatus |
CN205911282U (en) * | 2016-08-08 | 2017-01-25 | 中芯国际集成电路制造(北京)有限公司 | TEM sample grid and TEM sample placer |
CN106449340A (en) * | 2016-08-26 | 2017-02-22 | 深圳市华星光电技术有限公司 | Sample bearing table and dual-beam system electron microscope |
KR101798473B1 (en) * | 2016-05-30 | 2017-11-17 | (주)코셈 | High-resolution scanning electron microscope |
CN108666193A (en) * | 2017-03-27 | 2018-10-16 | 日本株式会社日立高新技术科学 | charged particle beam device |
CN110987995A (en) * | 2019-12-26 | 2020-04-10 | 重庆大学 | Universal sample holder for scanning electron microscope, in-situ mechanical test and three-dimensional atom probe equipment |
WO2020084729A1 (en) * | 2018-10-25 | 2020-04-30 | 株式会社日立ハイテクノロジーズ | Charged particle beam device, autofocus processing method for charged particle beam device, and detector |
CN111220819A (en) * | 2020-01-19 | 2020-06-02 | 中国科学院上海微系统与信息技术研究所 | A kind of focused ion beam cutting sample preparation method |
CN111381355A (en) * | 2018-12-29 | 2020-07-07 | 南京培轩雅谱光电科技有限公司 | Optical imaging apparatus and method |
CN111474197A (en) * | 2020-04-16 | 2020-07-31 | 宸鸿科技(厦门)有限公司 | Method for controlling contamination resulting from transmission electron microscope sample preparation |
US20200402760A1 (en) * | 2016-03-04 | 2020-12-24 | Phenom-World Holding B.V. | Scanning electron microscope |
-
2021
- 2021-03-30 CN CN202110339352.XA patent/CN115148568A/en active Pending
Patent Citations (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20040129878A1 (en) * | 2003-01-08 | 2004-07-08 | Satoshi Tomimatsu | Apparatus for specimen fabrication and method for specimen fabrication |
CN1766592A (en) * | 2004-07-14 | 2006-05-03 | 应用材料以色列公司 | Method and apparatus for sample formation and microanalysis in a vacuum chamber |
JP2008204959A (en) * | 2008-05-16 | 2008-09-04 | Hitachi Ltd | Sample analysis method and sample preparation method |
JP2008261891A (en) * | 2008-08-08 | 2008-10-30 | Hitachi Ltd | Sample preparation method |
CN104251795A (en) * | 2013-06-28 | 2014-12-31 | Fei公司 | Plan view sample preparation |
CN103646839A (en) * | 2013-11-08 | 2014-03-19 | 上海华力微电子有限公司 | Metal net for bearing and fixing TEM sample |
CN104880340A (en) * | 2014-02-28 | 2015-09-02 | 中芯国际集成电路制造(上海)有限公司 | Preparation method of transmission electron microscopic sample |
TW201546865A (en) * | 2014-03-24 | 2015-12-16 | Hitachi High Tech Science Corp | Focused ion beam apparatus |
CN104979151A (en) * | 2014-04-14 | 2015-10-14 | Fei公司 | High Capacity TEM Grid |
US20200402760A1 (en) * | 2016-03-04 | 2020-12-24 | Phenom-World Holding B.V. | Scanning electron microscope |
KR101798473B1 (en) * | 2016-05-30 | 2017-11-17 | (주)코셈 | High-resolution scanning electron microscope |
CN205911282U (en) * | 2016-08-08 | 2017-01-25 | 中芯国际集成电路制造(北京)有限公司 | TEM sample grid and TEM sample placer |
CN106449340A (en) * | 2016-08-26 | 2017-02-22 | 深圳市华星光电技术有限公司 | Sample bearing table and dual-beam system electron microscope |
CN108666193A (en) * | 2017-03-27 | 2018-10-16 | 日本株式会社日立高新技术科学 | charged particle beam device |
WO2020084729A1 (en) * | 2018-10-25 | 2020-04-30 | 株式会社日立ハイテクノロジーズ | Charged particle beam device, autofocus processing method for charged particle beam device, and detector |
CN111381355A (en) * | 2018-12-29 | 2020-07-07 | 南京培轩雅谱光电科技有限公司 | Optical imaging apparatus and method |
CN110987995A (en) * | 2019-12-26 | 2020-04-10 | 重庆大学 | Universal sample holder for scanning electron microscope, in-situ mechanical test and three-dimensional atom probe equipment |
CN111220819A (en) * | 2020-01-19 | 2020-06-02 | 中国科学院上海微系统与信息技术研究所 | A kind of focused ion beam cutting sample preparation method |
CN111474197A (en) * | 2020-04-16 | 2020-07-31 | 宸鸿科技(厦门)有限公司 | Method for controlling contamination resulting from transmission electron microscope sample preparation |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
US11315756B2 (en) | Fiducial design for tilted or glancing mill operations with a charged particle beam | |
TWI767385B (en) | Semiconductor inspection device and method of analyzing a set of har structures within an integrated semiconductor device | |
KR102144555B1 (en) | Method and system for reducing curtaining in charged particle beam sample preparation | |
US20160020065A1 (en) | Tem sample mounting geometry | |
CN114121580A (en) | Radiation device and method of operation, computer program product and object holder | |
TWI731467B (en) | Image forming method, image forming system and ion milling device | |
TW201822242A (en) | Apparatus for combined STEM and EDS tomography | |
JP2023547856A (en) | Measurement of hole inclination angle using FIB diagonal cutting | |
TWI811653B (en) | Sample holder and system and method for sample modification | |
CN115148568A (en) | Sample stage and system and method for modifying samples | |
JP3266995B2 (en) | Method and apparatus for observing and measuring conductive members | |
US9734985B2 (en) | Analytical apparatus, sample holder and analytical method | |
US20210366687A1 (en) | Detection systems in semiconductor metrology tools | |
JP2024540808A (en) | Energy bandpass filtering to improve image resolution of backscattered charged particles with high landing energies. | |
JP2006119133A (en) | Semiconductor device tester | |
JP2004170395A (en) | Charged particle beam equipment | |
CN101233609B (en) | Method for manufacturing semiconductor device | |
Stegmann | Basics and Current Aspects of Scanning Electron Microscopy | |
CN116930232A (en) | Method and system for analyzing three-dimensional features | |
Park et al. | FIB overview | |
KR20090059237A (en) | Silicon Wafer Internal Defect Analysis Method | |
CN116718602A (en) | Failure positioning and failure analysis method | |
Srinivasan | MATERIAL CHARACTERIZATION BY ENERGY FILTERED SECONDARY ELECTRON SIGNALS INSIDE THE SCANNING ELECTRON MICROSCOPE | |
Altmann | Using High Resolution S/TEM to Analyze Smartphone Displays |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination |