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CN115138098A - Method for extracting flavonoid substances in orange peel based on ultrasonic component - Google Patents

Method for extracting flavonoid substances in orange peel based on ultrasonic component Download PDF

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CN115138098A
CN115138098A CN202210888817.1A CN202210888817A CN115138098A CN 115138098 A CN115138098 A CN 115138098A CN 202210888817 A CN202210888817 A CN 202210888817A CN 115138098 A CN115138098 A CN 115138098A
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extraction tank
extraction
measuring
measurement
telescopic rod
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邱锦玉
何英姿
王淑培
唐诗音
黎秋玲
钟雪梅
林春伶
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Nanning Normal University
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/0261Solvent extraction of solids comprising vibrating mechanisms, e.g. mechanical, acoustical
    • B01D11/0265Applying ultrasound
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/0215Solid material in other stationary receptacles
    • B01D11/0223Moving bed of solid material
    • B01D11/0234Moving bed of solid material using other slow rotating arms or elements, whereby the general transport direction of the solids is not parallel to the rotation axis, e.g. perpendicular

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Abstract

本发明公开了基于超声构件的柑橘皮中黄酮类物质提方法,涉及化合物提取装置技术领域,包括提取罐,所述提取罐的上侧设置有进料口,所述提取罐上侧设置有测量口,所述测量口内安装有测量机构,所述测量机构包括伸缩杆,所述伸缩杆的末端转动安装有测量摆杆,所述测量摆杆为空心设置,所述测量摆杆内穿插设置有测量绳,所述测量绳的末端连接有漂浮球,所述测量绳上设置有刻度线,所述测量机构还包括触底检测组件,所述提取罐内悬挂安装有超声波振荡器,本发明通过在提取罐上设置测量口,结合测量机构对提取罐内的萃取原料配比进行控制,同时可以便捷监控萃取进度,提升了柑橘中黄酮类物质的提取效率和提取量。

Figure 202210888817

The invention discloses a method for extracting flavonoids in citrus peels based on ultrasonic components, and relates to the technical field of compound extraction devices, including an extraction tank, an upper side of the extraction tank is provided with a feeding port, and a measurement A measurement mechanism is installed in the measurement port, the measurement mechanism includes a telescopic rod, and a measurement pendulum rod is installed at the end of the telescopic rod. The measurement pendulum rod is hollow, and the measurement pendulum rod is interspersed with a A measuring rope, the end of the measuring rope is connected with a floating ball, a scale line is arranged on the measuring rope, the measuring mechanism further includes a bottoming detection component, an ultrasonic oscillator is suspended in the extraction tank, and the present invention adopts A measuring port is set on the extraction tank, and the ratio of the extraction raw materials in the extraction tank is controlled in combination with the measuring mechanism. At the same time, the extraction progress can be easily monitored, and the extraction efficiency and extraction amount of flavonoids in citrus are improved.

Figure 202210888817

Description

基于超声构件的柑橘皮中黄酮类物质提取方法Extraction method of flavonoids from citrus peel based on ultrasonic components

技术领域technical field

本发明涉及柑橘皮提取技术领域,具体是基于超声构件的柑橘皮中黄酮类物质提取方法。The invention relates to the technical field of citrus peel extraction, in particular to a method for extracting flavonoids from citrus peel based on an ultrasonic component.

背景技术Background technique

超声波提取(也称为超声波萃取)以其提取温度低、提取率高、提取时间短的独特优势被具有创新意识者应用于中药材和各种动、植物有效含量的提取,是替代传统剪切工艺方法实现高效、节能、环保式提取的现代技术手段,超声波提取是利用超声波具有的机械效应,空化效应和热效应,通过增大介质分子的运动速度、增大介质的穿透力以提取生物有效成分。Ultrasonic extraction (also known as ultrasonic extraction) is used by innovative people to extract effective content of Chinese medicinal materials and various animals and plants due to its unique advantages of low extraction temperature, high extraction rate and short extraction time. It is an alternative to traditional shearing. The process method is a modern technical means to achieve high-efficiency, energy-saving and environmentally friendly extraction. Ultrasonic extraction is to use the mechanical effect, cavitation effect and thermal effect of ultrasonic waves to increase the moving speed of the medium molecules and increase the penetrating force of the medium to extract biological substances. Active ingredients.

柑橘皮为芸香科植物桔树成熟果实的果皮,在我国分布非常广泛,具有很好的药用价值。研究表明柑橘皮中黄酮类化合物的含量尤为丰富,从中分离鉴定出来的黄酮类化合物有60余种,主要为黄烷酮、黄酮、黄酮醇及花色苷,现有的柑橘皮提取黄酮类化合物的提取方法时间长提取率低、杂质含量高,造成大量黄酮类化合物浪费,且提取进度难以把握。Citrus peel is the peel of the ripe fruit of the rutaceae plant orange tree, which is widely distributed in my country and has good medicinal value. Studies have shown that the content of flavonoids in citrus peel is particularly rich. There are more than 60 kinds of flavonoids isolated and identified, mainly flavanones, flavonoids, flavonols and anthocyanins. The extraction time is long, the extraction rate is low, and the impurity content is high, resulting in a large amount of waste of flavonoids, and the extraction progress is difficult to grasp.

发明内容SUMMARY OF THE INVENTION

本发明的目的在于提供基于超声构件的柑橘皮中黄酮类物质提取方法,以解决上述背景技术中提出的问题。The purpose of the present invention is to provide a method for extracting flavonoids from citrus peels based on ultrasonic components, so as to solve the problems raised in the above background art.

为实现上述目的,本发明提供如下技术方案:To achieve the above object, the present invention provides the following technical solutions:

基于超声构件的柑橘皮中黄酮类物质提取方法,包括以下步骤:A method for extracting flavonoids from citrus peel based on ultrasonic components, comprising the following steps:

S1、首先将破碎完成的柑橘皮料通过提取装置的进料口送入提取罐内,结合第一加料管以及第二加料管向提取罐内注入萃取剂;S1. First, the crushed citrus peel is fed into the extraction tank through the feed port of the extraction device, and the extraction agent is injected into the extraction tank in combination with the first feeding pipe and the second feeding pipe;

S2、通过进料口和第一加料管以及第二加料管箱提取罐内加料时,控制测量摆杆将连接有漂浮球的测量绳送入提取罐内,利用测量摆杆端部的可视探头以及补光灯,对提取罐内的原料加注深度进行监控并计算数据,保证原料配比准确;S2. When the material is extracted from the tank through the feeding port, the first feeding pipe and the second feeding pipe box, the measuring pendulum is controlled to send the measuring rope connected with the floating ball into the extraction tank, and the visual inspection at the end of the measuring pendulum is used. Probe and fill light to monitor the filling depth of raw materials in the extraction tank and calculate the data to ensure the accurate ratio of raw materials;

S3、原料加注完成后,启动搅动电机带动搅动桨叶进行转动搅拌,搅拌十到十五分钟后,停止搅动电机,开启超声波振荡器,进行超声提取,加速提取效率,在提取的过程中结合测量摆杆末端的可视探头监控柑橘混料的颜色,当柑橘混料的颜色接近萃取完成时的颜色时停止超声萃取,打开排料管进行排出过滤,得到黄酮类化合物。S3. After the filling of the raw materials is completed, start the stirring motor to drive the stirring blades to rotate and stir, and after ten to fifteen minutes of stirring, stop the stirring motor, turn on the ultrasonic oscillator, perform ultrasonic extraction, and speed up the extraction efficiency. The visual probe at the end of the measuring pendulum monitors the color of the citrus mixture. When the color of the citrus mixture is close to the color when the extraction is completed, the ultrasonic extraction is stopped, and the discharge pipe is opened to discharge and filter to obtain flavonoids.

提取装置,包括提取罐,所述提取罐的上侧设置有进料口,所述提取罐的顶部设置有盖板,所述提取罐的底部设置有支撑腿以及底座,所述提取罐的顶部安装有第一加料管以及第二加料管,所述提取罐的底部设置有排料管,所述提取罐上侧还设置有测量口,所述测量口内安装有测量机构,所述测量机构包括伸缩杆,所述伸缩杆的末端转动安装有测量摆杆,所述测量摆杆为空心设置,所述测量摆杆内穿插设置有测量绳,所述测量绳的末端连接有漂浮球,所述测量绳上设置有刻度线,所述测量机构还包括触底检测组件,所述提取罐内悬挂安装有超声波振荡器,所述超声波振荡器安装在提取罐的中轴线上。The extraction device includes an extraction tank, the upper side of the extraction tank is provided with a feeding port, the top of the extraction tank is provided with a cover plate, the bottom of the extraction tank is provided with a support leg and a base, and the top of the extraction tank is provided with a cover plate. A first feeding pipe and a second feeding pipe are installed, the bottom of the extraction tank is provided with a discharge pipe, the upper side of the extraction tank is also provided with a measurement port, and a measurement mechanism is installed in the measurement port, and the measurement mechanism includes A telescopic rod, the end of the telescopic rod is rotatably installed with a measurement pendulum rod, the measurement pendulum rod is hollow, a measurement rope is interspersed in the measurement pendulum rod, and the end of the measurement rope is connected with a floating ball, the A scale line is arranged on the measuring rope, the measuring mechanism further includes a bottoming detection component, an ultrasonic oscillator is suspended in the extraction tank, and the ultrasonic oscillator is installed on the central axis of the extraction tank.

作为本发明进一步的方案:所述触底检测组件包括设置在伸缩杆上的固定架,所述固定架与伸缩杆之间垂直安装,所述固定架上安装有绕卷筒,所述绕卷筒上绕卷有测量绳,所述绕卷筒与固定架之间转动安装,所述绕卷筒上同轴安装有旋转把手,所述伸缩杆的末端设置有通孔,所述测量绳穿过通孔与测量摆杆相连,所述测量摆杆的端部设置有压力感应器,所述测量绳设置在压力感应器的上方,所述触底检测组件还包括可视单元。As a further solution of the present invention: the bottoming detection assembly includes a fixing frame arranged on the telescopic rod, the fixing frame and the telescopic rod are installed vertically, a winding drum is installed on the fixing frame, and the winding A measuring rope is wound on the drum, the winding drum and the fixing frame are rotatably installed, the rotating handle is coaxially installed on the winding drum, the end of the telescopic rod is provided with a through hole, and the measuring rope passes through The measuring pendulum is connected with the measuring pendulum through the through hole, the end of the measuring pendulum is provided with a pressure sensor, the measurement rope is arranged above the pressure sensor, and the bottoming detection assembly further includes a visual unit.

作为本发明再进一步的方案:所述可视单元包括设置在测量摆杆端部的可视探头,所述可视探头通过万向管与测量摆杆的端部相连,所述测量摆杆的端部还设置有补光灯,所述伸缩杆上设置有显示器,所述显示器与可视探头相连。As a further solution of the present invention: the visual unit includes a visual probe arranged at the end of the measurement pendulum rod, the visual probe is connected to the end of the measurement pendulum rod through a universal pipe, and the measurement pendulum rod is The end is also provided with a fill light, a display is arranged on the telescopic rod, and the display is connected with a visual probe.

作为本发明再进一步的方案:所述伸缩杆上安装有水平调节组件,所述水平调节组件包括设置在提取罐顶部的配合柱,所述配合柱对称设置,所述配合柱上配合安装有悬挂板,所述悬挂板的端部设置有配合块,所述配合块穿插配合在对称设置的配合柱之间,所述悬挂板的底部设置有调节滑轨,所述调节滑轨内设置有调节槽,所述伸缩杆的端部安装有套接环,所述套接环上侧固定安装有配合板,所述配合板的中间位置固定安装有伸缩柱,所述伸缩柱的末端与调节槽之间滑动安装。As a further solution of the present invention: a horizontal adjustment component is installed on the telescopic rod, and the horizontal adjustment component includes a matching column arranged on the top of the extraction tank, the matching column is symmetrically arranged, and a suspension is installed on the matching column. The end of the suspension plate is provided with a matching block, and the matching block is inserted and fitted between the symmetrically arranged matching columns. The bottom of the suspension plate is provided with an adjusting slide rail, and an adjusting slide rail is provided in the adjusting slide rail. A socket ring is installed at the end of the telescopic rod, a matching plate is fixedly installed on the upper side of the socket ring, a telescopic column is fixedly installed in the middle of the matching plate, and the end of the telescopic column is connected to the adjustment groove. Sliding installation between.

作为本发明再进一步的方案:所述提取罐的上侧设置有盖板,所述盖板通过密封螺栓与提取罐之间固定连接,所述盖板与提取罐之间设置有密封垫。As a further solution of the present invention, a cover plate is arranged on the upper side of the extraction tank, the cover plate is fixedly connected to the extraction tank through sealing bolts, and a sealing gasket is arranged between the cover plate and the extraction tank.

作为本发明再进一步的方案:所述提取罐的底部设置有搅动电机,所述提取罐的底部转动安装有搅动桨叶,所述搅动桨叶倾斜设置,所述搅动桨叶的底部边缘与提取罐的底部相切安装,所述搅动桨叶的回转中心与提取罐之间通过密封轴承安装。As a further solution of the present invention: the bottom of the extraction tank is provided with a stirring motor, the bottom of the extraction tank is rotatably installed with a stirring blade, the stirring blade is inclined, and the bottom edge of the stirring blade is connected to the extraction tank. The bottom of the tank is installed tangentially, and a sealed bearing is installed between the center of rotation of the stirring blade and the extraction tank.

作为本发明再进一步的方案:所述伸缩杆的末端与测量摆杆的端部之间设置有转动连接架,所述转动连接架与伸缩杆之间设置有固定把手,所述固定把手上设置有角度尺。As a further solution of the present invention, a rotating connecting frame is provided between the end of the telescopic rod and the end of the measuring pendulum rod, a fixed handle is set between the rotating connecting frame and the telescopic rod, and a fixed handle is provided on the fixed handle There is an angle ruler.

作为本发明再进一步的方案:所述进料口与测量口对称设置,所述测量口的边缘设置有圆角,所述压力感应器呈条状设置,所述压力感应器的中间部位向下凹陷,所述测量绳沿着凹陷部位进入测量摆杆。As a further solution of the present invention: the feeding port and the measuring port are arranged symmetrically, the edge of the measuring port is provided with rounded corners, the pressure sensor is arranged in a strip shape, and the middle part of the pressure sensor is downward A depression, the measurement rope enters the measurement pendulum along the depression.

作为本发明再进一步的方案:所述超声波振荡器与提取罐侧边距离等于超声波振荡器与提取罐底部距离。As a further solution of the present invention: the distance between the ultrasonic oscillator and the side of the extraction tank is equal to the distance between the ultrasonic oscillator and the bottom of the extraction tank.

与现有技术相比,本发明的有益效果是:Compared with the prior art, the beneficial effects of the present invention are:

(1)本发明通过在提取罐上设置测量口,利用测量口将测量摆杆深伸入提取罐内,结合测量绳以及漂浮球,对提取罐内的柑橘皮原料以及萃取剂进行控制,保证柑橘皮与萃取剂的配合吻合,确保黄酮类物质的提取效率和提取量,在提取罐的中间部位悬挂设置超声波振荡器,结合超声波振荡器进行超声提取,提升提取效率和提取量。(1) In the present invention, a measuring port is provided on the extraction tank, and the measuring pendulum is deeply extended into the extraction tank by using the measuring port, combined with the measuring rope and the floating ball, the citrus peel raw material and the extraction agent in the extraction tank are controlled to ensure that The combination of the citrus peel and the extractant is consistent to ensure the extraction efficiency and extraction volume of flavonoids. An ultrasonic oscillator is suspended in the middle of the extraction tank, and ultrasonic extraction is carried out in combination with the ultrasonic oscillator to improve the extraction efficiency and extraction volume.

(2)通过在测量摆杆的端部入口处设置压力感应器,压在压力感应器上的测量绳在没有到达提取罐内原料表面时,漂浮球自身重力使得测量绳张紧并对压力传感器施加压力,当测量绳不断下放并最终触底时,测量绳上的张力消失,压力传感器压力竖直瞬间消失,此时根据测量绳的下放高度得知提取罐内原料添加量。(2) By arranging a pressure sensor at the entrance of the end of the measuring pendulum rod, when the measuring rope pressed on the pressure sensor does not reach the surface of the raw material in the extraction tank, the gravity of the floating ball makes the measuring rope tension and the pressure sensor Apply pressure, when the measuring rope is lowered continuously and finally touches the bottom, the tension on the measuring rope disappears, and the pressure of the pressure sensor disappears instantly.

(3)为了便于观测提取罐内的提取进度,在测量摆杆的端部设置可视探头,同时设置补光灯,在萃取的过程中查看柑橘皮的颜色,从而判断萃取进度,相比以往打开提取罐观察,该观察手段安全高效。(3) In order to facilitate the observation of the extraction progress in the extraction tank, a visual probe is set at the end of the measuring pendulum rod, and a fill light is set at the same time to check the color of the citrus peel during the extraction process, so as to judge the extraction progress. Compared with the past Open the extraction tank and observe, the observation method is safe and efficient.

(4)通过配合柱以及配合块安装悬挂板,悬挂板水平设置,在悬挂板的底部设置调节滑轨以及调节槽,伸缩杆的端部利用套接环安装配合板,配合板通过伸缩柱与调剂槽之间滑动安装,从而在不影响伸缩杆高度调节的同时保证伸缩杆的水平度,确保伸缩杆为水平之后可以快速得出测量绳的高度,进而得出提取罐内物料的添加量。设置固定把手以及角度尺可以快速读出测量摆杆与伸缩杆之间角度,从而快速得出提取罐内物料的添加高度。(4) Install the suspension plate through the matching column and the matching block. The suspension plate is set horizontally, and the adjustment slide rail and the adjustment groove are arranged at the bottom of the suspension plate. The end of the telescopic rod is installed with a socket ring. Sliding installation between the adjustment tanks, so as to ensure the levelness of the telescopic rod without affecting the height adjustment of the telescopic rod. After ensuring that the telescopic rod is horizontal, the height of the measuring rope can be quickly obtained, and then the addition amount of the material in the extraction tank can be obtained. Setting the fixed handle and the angle ruler can quickly read the angle between the measuring pendulum and the telescopic rod, so as to quickly obtain the added height of the material in the extraction tank.

附图说明Description of drawings

图1为基于超声构件的柑橘皮中黄酮类物质提取方法的结构示意图。Figure 1 is a schematic structural diagram of a method for extracting flavonoids from citrus peels based on ultrasonic components.

图2为基于超声构件的柑橘皮中黄酮类物质提取装置的剖切结构示意图。FIG. 2 is a schematic view of the cut-away structure of an apparatus for extracting flavonoids from citrus peels based on ultrasonic components.

图3为基于超声构件的柑橘皮中黄酮类物质提取方法中测量机构的结构示意图。3 is a schematic structural diagram of a measuring mechanism in a method for extracting flavonoids from citrus peels based on ultrasonic components.

图4为图3中A处放大结构示意图。FIG. 4 is an enlarged schematic view of the structure at A in FIG. 3 .

图5为基于超声构件的柑橘皮中黄酮类物质提取方法中盖板与提取罐的配合示意图。5 is a schematic diagram of the cooperation between a cover plate and an extraction tank in the method for extracting flavonoids from citrus peels based on ultrasonic components.

图6为基于超声构件的柑橘皮中黄酮类物质提取方法中测量机构的安装示意图。FIG. 6 is a schematic diagram of the installation of the measuring mechanism in the method for extracting flavonoids from citrus peels based on ultrasonic components.

图7为基于超声构件的柑橘皮中黄酮类物质提取方法中可视探头的安装结构示意图。FIG. 7 is a schematic diagram of the installation structure of a visual probe in the method for extracting flavonoids from citrus peels based on ultrasonic components.

图8为基于超声构件的柑橘皮中黄酮类物质提取方法中悬挂板的安装结构示意图。FIG. 8 is a schematic diagram of the installation structure of the hanging plate in the method for extracting flavonoids from citrus peels based on ultrasonic components.

图中:1提取罐,100搅动电机,101搅动桨叶,2支撑腿,3底座,4进料口,5第一加料管,6第二加料管,7中间管,8连接器,80超声波振荡器,9悬挂板,10盖板,101密封螺栓,102密封垫,11测量机构,12测量绳,13漂浮球,14排料管,01固定架,02绕卷筒,03旋转把手,04通孔,05清洗管,06喷头,07压力感应器,08转动连接架,09固定把手,010显示器,90配合块,91配合柱,92调节滑轨,93调节槽,120测量摆杆,1201可视探头,1202补光灯,121测量口,122伸缩杆,1220套接环,1221配合板,1222伸缩柱。In the picture: 1 extraction tank, 100 stirring motor, 101 stirring paddle, 2 supporting legs, 3 base, 4 feeding port, 5 first feeding pipe, 6 second feeding pipe, 7 intermediate pipe, 8 connector, 80 ultrasonic Shaker, 9 Suspension Plate, 10 Cover, 101 Sealing Bolt, 102 Gasket, 11 Measuring Mechanism, 12 Measuring Rope, 13 Floating Ball, 14 Discharge Tube, 01 Fixing Frame, 02 Winding Reel, 03 Rotating Handle, 04 Through hole, 05 cleaning pipe, 06 spray head, 07 pressure sensor, 08 rotating connection frame, 09 fixed handle, 010 display, 90 matching block, 91 matching column, 92 adjusting slide rail, 93 adjusting groove, 120 measuring pendulum, 1201 Visual probe, 1202 fill light, 121 measurement port, 122 telescopic rod, 1220 socket ring, 1221 matching plate, 1222 telescopic column.

具体实施方式Detailed ways

在本发明的描述中,需要理解的是,术语“纵向”、“横向”、“上”、“下”、“顶”、“底”、“内”、“外”等指示的方位或位置关系为基于附图所示的方位或位置关系,仅是为了便于描述本发明和简化描述,而不是指示或暗示所指的装置或元件必须具有特定的方位、以特定的方位构造和操作,因此不能理解为对本发明的限制。In the description of the present invention, it should be understood that the terms "longitudinal", "transverse", "upper", "lower", "top", "bottom", "inner", "outer", etc. refer to the orientation or position The relationship is based on the orientation or positional relationship shown in the drawings, which is only for the convenience of describing the present invention and simplifying the description, rather than indicating or implying that the device or element referred to must have a particular orientation, be constructed and operated in a particular orientation, and therefore It should not be construed as a limitation of the present invention.

此外,术语“第一”、“第二”仅用于描述目的,而不能理解为指示或暗示相对重要性或者隐含指明所指示的技术特征的数量。由此,限定有“第一”、“第二”的特征可以明示或者隐含地包括一个或者更多个该特征。在本发明的描述中,“多个”的含义是两个或两个以上,除非另有明确具体的限定。In addition, the terms "first" and "second" are only used for descriptive purposes, and should not be construed as indicating or implying relative importance or implying the number of indicated technical features. Thus, a feature defined as "first" or "second" may expressly or implicitly include one or more of that feature. In the description of the present invention, "plurality" means two or more, unless otherwise expressly and specifically defined.

在本发明中,除非另有明确的规定和限定,术语“安装”、“相连”、“连接”、“固定”等术语应做广义理解,例如,可以是固定连接,也可以是可拆卸连接,或成一体;可以是机械连接,也可以是电连接;可以是直接相连,也可以通过中间媒介间接相连,可以是两个元件内部的连通或两个元件的相互作用关系。对于本领域的普通技术人员而言,可以根据具体情况理解上述术语在本发明中的具体含义。In the present invention, unless otherwise expressly specified and limited, the terms "installed", "connected", "connected", "fixed" and other terms should be understood in a broad sense, for example, it may be a fixed connection or a detachable connection , or integrated; it can be a mechanical connection or an electrical connection; it can be a direct connection or an indirect connection through an intermediate medium, and it can be the internal connection of the two elements or the interaction relationship between the two elements. For those of ordinary skill in the art, the specific meanings of the above terms in the present invention can be understood according to specific situations.

下面结合具体实施方式对本专利的技术方案作进一步详细地说明。The technical solution of the present patent will be described in further detail below in conjunction with specific embodiments.

实施例1:Example 1:

基于超声构件的柑橘皮中黄酮类物质提取方法,包括以下步骤:A method for extracting flavonoids from citrus peel based on ultrasonic components, comprising the following steps:

S1、首先将破碎完成的柑橘皮料通过提取装置的进料口4送入提取罐1内,结合第一加料管5以及第二加料管6向提取罐1内注入萃取剂;S1, at first the broken citrus peel material is sent into the extraction tank 1 through the feed port 4 of the extraction device, and the extraction agent is injected into the extraction tank 1 in combination with the first feeding pipe 5 and the second feeding pipe 6;

S2、通过进料口4和第一加料管5以及第二加料管6箱提取罐1内加料时,控制测量摆杆120将连接有漂浮球13的测量绳12送入提取罐1内,利用测量摆杆120端部的可视探头1201以及补光灯1202,对提取罐1内的原料加注深度进行监控并计算数据,保证原料配比准确;S2. When feeding into the extraction tank 1 through the feeding port 4, the first feeding pipe 5 and the second feeding pipe 6, control the measuring pendulum 120 to send the measuring rope 12 connected with the floating ball 13 into the extraction tank 1, and use the Measure the visual probe 1201 and the fill light 1202 at the end of the pendulum rod 120, monitor the filling depth of the raw materials in the extraction tank 1 and calculate the data to ensure the accurate ratio of raw materials;

S3、原料加注完成后,启动搅动电机100带动搅动桨叶101进行转动搅拌,搅拌十到十五分钟后,停止搅动电机100,开启超声波振荡器80,进行超声提取,加速提取效率,在提取的过程中结合测量摆杆120末端的可视探头1201监控柑橘混料的颜色,当柑橘混料的颜色接近萃取完成时的颜色时停止超声萃取,打开排料管14进行排出过滤,得到黄酮类化合物。S3. After the filling of the raw materials is completed, start the stirring motor 100 to drive the stirring blades 101 to rotate and stir, after ten to fifteen minutes of stirring, stop the stirring motor 100, turn on the ultrasonic oscillator 80, and perform ultrasonic extraction to accelerate the extraction efficiency. In the process of monitoring the color of the citrus mixture with the visual probe 1201 at the end of the measuring pendulum rod 120, the ultrasonic extraction is stopped when the color of the citrus mixture is close to the color when the extraction is completed, and the discharge pipe 14 is opened to discharge and filter to obtain flavonoids. compound.

如图1、图2、图3、图4、图7所示,提取装置包括提取罐1,所述提取罐1的上侧设置有进料口4,所述提取罐1的顶部设置有盖板10,所述提取罐1的底部设置有支撑腿2以及底座3,所述提取罐1的顶部安装有第一加料管5以及第二加料管6,所述提取罐1的底部设置有排料管14,所述提取罐1上侧还设置有测量口121,所述测量口121内安装有测量机构11,所述测量机构11包括伸缩杆122,所述伸缩杆122的末端转动安装有测量摆杆120,所述测量摆杆120为空心设置,所述测量摆杆120内穿插设置有测量绳12,所述测量绳12的末端连接有漂浮球13,所述测量绳12上设置有刻度线,所述测量机构11还包括触底检测组件,所述提取罐1内悬挂安装有超声波振荡器80,所述超声波振荡器80安装在提取罐1的中轴线上。As shown in Fig. 1, Fig. 2, Fig. 3, Fig. 4, Fig. 7, the extraction device includes an extraction tank 1, the upper side of the extraction tank 1 is provided with a feeding port 4, and the top of the extraction tank 1 is provided with a cover Plate 10, the bottom of the extraction tank 1 is provided with a support leg 2 and a base 3, the top of the extraction tank 1 is provided with a first feeding pipe 5 and a second feeding pipe 6, and the bottom of the extraction tank 1 is provided with a row The material pipe 14, the upper side of the extraction tank 1 is also provided with a measuring port 121, the measuring mechanism 11 is installed in the measuring port 121, and the measuring mechanism 11 includes a telescopic rod 122, and the end of the telescopic rod 122 is rotatably installed with The measurement pendulum rod 120 is hollow, the measurement pendulum rod 120 is interspersed with a measurement rope 12, the end of the measurement rope 12 is connected with a floating ball 13, and the measurement rope 12 is provided with The measuring mechanism 11 further includes a bottoming detection component, an ultrasonic oscillator 80 is suspended in the extraction tank 1 , and the ultrasonic oscillator 80 is installed on the central axis of the extraction tank 1 .

具体的,通过在提取罐1上设置测量口121,利用测量口121将测量摆杆120深伸入提取罐1内,结合测量绳12以及漂浮球13,对提取罐1内的柑橘皮原料以及萃取剂进行控制,保证柑橘皮与萃取剂的配合吻合,确保黄酮类物质的提取效率和提取量,在提取罐1的中间部位悬挂设置超声波振荡器80,结合超声波振荡器80进行超声提取,提升提取效率和提取量。Specifically, by setting the measurement port 121 on the extraction tank 1, the measurement pendulum 120 is deeply extended into the extraction tank 1 by using the measurement port 121, and combined with the measurement rope 12 and the floating ball 13, the citrus peel raw materials in the extraction tank 1 and The extraction agent is controlled to ensure that the citrus peel and the extraction agent are in good agreement, to ensure the extraction efficiency and extraction amount of flavonoids. An ultrasonic oscillator 80 is suspended in the middle of the extraction tank 1, and the ultrasonic oscillator 80 is used for ultrasonic extraction. Extraction efficiency and extraction volume.

如图2、图3所示,所述触底检测组件包括设置在伸缩杆122上的固定架01,所述固定架01与伸缩杆122之间垂直安装,所述固定架01上安装有绕卷筒02,所述绕卷筒02上绕卷有测量绳12,所述绕卷筒02与固定架01之间转动安装,所述绕卷筒02上同轴安装有旋转把手03,所述伸缩杆122的末端设置有通孔04,所述测量绳12穿过通孔04与测量摆杆120相连,所述测量摆杆120的端部设置有压力感应器07,所述测量绳12设置在压力感应器07的上方,所述触底检测组件还包括可视单元。As shown in FIG. 2 and FIG. 3 , the bottoming detection assembly includes a fixing frame 01 arranged on the telescopic rod 122 , the fixing frame 01 and the telescopic rod 122 are installed vertically, and the fixing frame 01 is mounted with a winding Reel 02, the measuring rope 12 is wound on the winding reel 02, the winding reel 02 and the fixing frame 01 are rotated and installed, the reel 02 is coaxially installed with a rotating handle 03, the The end of the telescopic rod 122 is provided with a through hole 04, the measurement rope 12 is connected to the measurement pendulum rod 120 through the through hole 04, the end of the measurement pendulum rod 120 is provided with a pressure sensor 07, and the measurement rope 12 is provided with Above the pressure sensor 07, the bottoming detection assembly further includes a visual unit.

具体的,通过在测量摆杆120的端部入口处设置压力感应器07,压在压力感应器07上的测量绳12在没有到达提取罐1内原料表面时,漂浮球13自身重力使得测量绳12张紧并对压力传感器施加压力,当测量绳12不断下放并最终触底时,测量绳12上的张力消失,压力传感器压力竖直瞬间消失,此时根据测量绳12的下放高度得知提取罐1内原料添加量。Specifically, by arranging the pressure sensor 07 at the entrance of the end of the measurement pendulum rod 120, when the measurement rope 12 pressed on the pressure sensor 07 does not reach the surface of the raw material in the extraction tank 1, the gravity of the floating ball 13 makes the measurement rope 12 tension and apply pressure to the pressure sensor, when the measuring rope 12 is lowered continuously and finally touches the bottom, the tension on the measuring rope 12 disappears, and the pressure of the pressure sensor disappears instantly. The amount of raw materials added in tank 1.

如图7所示,所述可视单元包括设置在测量摆杆120端部的可视探头1201,所述可视探头1201通过万向管与测量摆杆120的端部相连,所述测量摆杆120的端部还设置有补光灯1202,所述伸缩杆122上设置有显示器010,所述显示器010与可视探头1201相连。As shown in FIG. 7 , the visual unit includes a visual probe 1201 disposed at the end of the measurement pendulum 120, the visual probe 1201 is connected to the end of the measurement pendulum 120 through a universal tube, and the measurement pendulum The end of the rod 120 is also provided with a fill light 1202 , and a display 010 is provided on the telescopic rod 122 , and the display 010 is connected with the visual probe 1201 .

具体的,为了便于观测提取罐1内的提取进度,在测量摆杆120的端部设置可视探头1201,同时设置补光灯1202,在萃取的过程中查看柑橘皮的颜色,从而判断萃取进度,相比以往打开提取罐1观察,该观察手段安全高效。Specifically, in order to facilitate the observation of the extraction progress in the extraction tank 1, a visual probe 1201 is set at the end of the measuring pendulum rod 120, and a fill light 1202 is set at the same time to check the color of the citrus peel during the extraction process, so as to judge the extraction progress. , compared with the previous observation by opening the extraction tank 1, the observation method is safe and efficient.

实施例2:Example 2:

本实施例在实施例1的基础上,结合图6和图8给出,所述伸缩杆122上安装有水平调节组件,所述水平调节组件包括设置在提取罐1顶部的配合柱91,所述配合柱91对称设置,所述配合柱91上配合安装有悬挂板9,所述悬挂板9的端部设置有配合块90,所述配合块90穿插配合在对称设置的配合柱91之间,所述悬挂板9的底部设置有调节滑轨92,所述调节滑轨92内设置有调节槽93,所述伸缩杆122的端部安装有套接环1220,所述套接环1220上侧固定安装有配合板1221,所述配合板1221的中间位置固定安装有伸缩柱1222,所述伸缩柱1222的末端与调节槽93之间滑动安装。On the basis of Embodiment 1, this embodiment is given in conjunction with FIG. 6 and FIG. 8 , the telescopic rod 122 is provided with a horizontal adjustment component, and the horizontal adjustment component includes a matching column 91 arranged on the top of the extraction tank 1 , so The matching columns 91 are symmetrically arranged, a suspension plate 9 is fitted on the matching columns 91 , and a matching block 90 is arranged at the end of the suspension plate 9 , and the matching block 90 is inserted and fitted between the symmetrically arranged matching columns 91 . , the bottom of the suspension plate 9 is provided with an adjustment slide rail 92, the adjustment slide rail 92 is provided with an adjustment groove 93, the end of the telescopic rod 122 is installed with a sleeve ring 1220, and the sleeve ring 1220 is installed A matching plate 1221 is fixedly installed on the side, a telescopic column 1222 is fixedly installed in the middle position of the matching plate 1221 , and the end of the telescopic column 1222 is slidably installed between the adjustment groove 93 .

具体的,通过配合柱91以及配合块90安装悬挂板9,悬挂板9水平设置,在悬挂板9的底部设置调节滑轨92以及调节槽93,伸缩杆122的端部利用套接环1220安装配合板1221,配合板1221通过伸缩柱1222与调剂槽之间滑动安装,从而在不影响伸缩杆122高度调节的同时保证伸缩杆122的水平度,确保伸缩杆122为水平之后可以快速得出测量绳12的高度,进而得出提取罐1内物料的添加量。Specifically, the suspension plate 9 is installed through the matching column 91 and the matching block 90 , the suspension plate 9 is arranged horizontally, the adjustment slide rail 92 and the adjustment groove 93 are arranged at the bottom of the suspension plate 9 , and the end of the telescopic rod 122 is installed with a socket ring 1220 Matching plate 1221, the matching plate 1221 is slidably installed between the telescopic column 1222 and the adjusting groove, so as to ensure the levelness of the telescopic rod 122 without affecting the height adjustment of the telescopic rod 122, and to ensure that the telescopic rod 122 is horizontal, the measurement can be quickly obtained The height of the rope 12 is used to obtain the addition amount of the material in the extraction tank 1 .

结合三角函数知识,设定测量绳12的下方长度为s,测量摆杆120的长度为n,测量摆杆120与伸缩杆122之间的角度为a,提取罐1的深度为H,则提取罐1内的物料添加深度h=H-(s-sina*n),其中a为大于九十度的角。Combined with the knowledge of trigonometric functions, set the length of the lower part of the measuring rope 12 to be s, the length of the measurement pendulum rod 120 to be n, the angle between the measurement pendulum rod 120 and the telescopic rod 122 to be a, and the depth of the extraction tank 1 to be H, then extract the Material addition depth h=H-(s-sina*n) in tank 1, where a is an angle greater than ninety degrees.

如图5所示,所述提取罐1的上侧设置有盖板10,所述盖板10通过密封螺栓101与提取罐1之间固定连接,所述盖板10与提取罐1之间设置有密封垫102。As shown in FIG. 5 , a cover plate 10 is provided on the upper side of the extraction tank 1 , and the cover plate 10 is fixedly connected to the extraction tank 1 through sealing bolts 101 , and the cover plate 10 and the extraction tank 1 are arranged between the cover plate 10 and the extraction tank 1 . There is a gasket 102 .

如图2所示,所述提取罐1的底部设置有搅动电机100,所述提取罐1的底部转动安装有搅动桨叶101,所述搅动桨叶101倾斜设置,所述搅动桨叶101的底部边缘与提取罐1的底部相切安装,所述搅动桨叶101的回转中心与提取罐1之间通过密封轴承安装。As shown in FIG. 2 , the bottom of the extraction tank 1 is provided with a stirring motor 100, and the bottom of the extraction tank 1 is rotatably installed with a stirring paddle 101. The stirring paddle 101 is arranged obliquely. The bottom edge is installed tangentially to the bottom of the extraction tank 1 , and a sealed bearing is installed between the rotation center of the stirring paddle 101 and the extraction tank 1 .

具体的,搅动桨叶101倾斜设置,可以通过调整搅动电机100的转向,从而使得提取罐1内的物料向上搅动或者向下搅动。Specifically, the stirring paddles 101 are set obliquely, and the rotation of the stirring motor 100 can be adjusted, so that the material in the extraction tank 1 can be stirred upwards or downwards.

作为本发明再进一步的方案:所述伸缩杆122的末端与测量摆杆120的端部之间设置有转动连接架08,所述转动连接架08与伸缩杆122之间设置有固定把手09,所述固定把手09上设置有角度尺。As a further solution of the present invention, a rotating connecting frame 08 is provided between the end of the telescopic rod 122 and the end of the measuring pendulum rod 120, and a fixed handle 09 is set between the rotating connecting frame 08 and the telescopic rod 122, The fixed handle 09 is provided with an angle ruler.

具体的,设置固定把手09以及角度尺可以快速读出测量摆杆120与伸缩杆122之间角度,从而快速得出提取罐1内物料的添加高度。Specifically, setting the fixed handle 09 and the angle ruler can quickly read and measure the angle between the pendulum rod 120 and the telescopic rod 122 , so as to quickly obtain the added height of the material in the extraction tank 1 .

作为本发明再进一步的方案:所述进料口4与测量口121对称设置,所述测量口121的边缘设置有圆角,所述压力感应器07呈条状设置,所述压力感应器07的中间部位向下凹陷,所述测量绳12沿着凹陷部位进入测量摆杆120。As a further solution of the present invention: the feeding port 4 and the measuring port 121 are arranged symmetrically, the edge of the measuring port 121 is provided with rounded corners, the pressure sensor 07 is arranged in a strip shape, and the pressure sensor 07 The middle part of the measuring rope 12 is recessed downward, and the measuring rope 12 enters the measuring pendulum 120 along the recessed part.

作为本发明再进一步的方案:所述超声波振荡器80与提取罐1侧边距离等于超声波振荡器80与提取罐1底部距离。As a further solution of the present invention, the distance between the ultrasonic oscillator 80 and the side of the extraction tank 1 is equal to the distance between the ultrasonic oscillator 80 and the bottom of the extraction tank 1 .

本发明实施例的工作原理是:The working principle of the embodiment of the present invention is:

如图1-8所示,通过在提取罐1上设置测量口121,利用测量口121将测量摆杆120深伸入提取罐1内,结合测量绳12以及漂浮球13,对提取罐1内的柑橘皮原料以及萃取剂进行控制,保证柑橘皮与萃取剂的配合吻合,确保黄酮类物质的提取效率和提取量,在提取罐1的中间部位悬挂设置超声波振荡器80,结合超声波振荡器80进行超声提取,提升提取效率和提取量。通过在测量摆杆120的端部入口处设置压力感应器07,压在压力感应器07上的测量绳12在没有到达提取罐1内原料表面时,漂浮球13自身重力使得测量绳12张紧并对压力传感器施加压力,当测量绳12不断下放并最终触底时,测量绳12上的张力消失,压力传感器压力竖直瞬间消失,此时根据测量绳12的下放高度得知提取罐1内原料添加量。为了便于观测提取罐1内的提取进度,在测量摆杆120的端部设置可视探头1201,同时设置补光灯1202,在萃取的过程中查看柑橘皮的颜色,从而判断萃取进度,相比以往打开提取罐1观察,该观察手段安全高效。通过配合柱91以及配合块90安装悬挂板9,悬挂板9水平设置,在悬挂板9的底部设置调节滑轨92以及调节槽93,伸缩杆122的端部利用套接环1220安装配合板1221,配合板1221通过伸缩柱1222与调剂槽之间滑动安装,从而在不影响伸缩杆122高度调节的同时保证伸缩杆122的水平度,确保伸缩杆122为水平之后可以快速得出测量绳12的高度,进而得出提取罐1内物料的添加量。设置固定把手09以及角度尺可以快速读出测量摆杆120与伸缩杆122之间角度,从而快速得出提取罐1内物料的添加高度。As shown in Figures 1-8, by setting the measuring port 121 on the extraction tank 1, the measuring pendulum rod 120 is deeply extended into the extraction tank 1 through the measuring port 121, and combined with the measuring rope 12 and the floating ball 13, the inside of the extraction tank 1 is measured. The raw material of citrus peel and the extractant are controlled to ensure that the citrus peel and the extractant are matched to ensure the extraction efficiency and amount of flavonoids. An ultrasonic oscillator 80 is suspended in the middle of the extraction tank 1, combined with the ultrasonic oscillator 80 Ultrasonic extraction is performed to improve extraction efficiency and extraction volume. By arranging the pressure sensor 07 at the entrance of the end of the measuring pendulum rod 120, when the measuring rope 12 pressed on the pressure sensor 07 does not reach the surface of the raw material in the extraction tank 1, the gravity of the floating ball 13 makes the measuring rope 12 tensioned Apply pressure to the pressure sensor, when the measuring rope 12 is lowered continuously and finally touches the bottom, the tension on the measuring rope 12 disappears, and the pressure on the pressure sensor disappears instantly. The amount of raw materials added. In order to facilitate the observation of the extraction progress in the extraction tank 1, a visual probe 1201 is set at the end of the measuring pendulum rod 120, and a fill light 1202 is set at the same time to check the color of the citrus peel during the extraction process, so as to judge the extraction progress. In the past, the extraction tank 1 was opened for observation, and this observation method was safe and efficient. The suspension plate 9 is installed through the matching column 91 and the matching block 90 , the suspension plate 9 is arranged horizontally, the adjustment slide rail 92 and the adjustment groove 93 are arranged at the bottom of the suspension plate 9 , and the end of the telescopic rod 122 uses the socket ring 1220 to install the matching plate 1221 , the matching plate 1221 is slidably installed between the telescopic column 1222 and the adjusting groove, so as to ensure the levelness of the telescopic rod 122 without affecting the height adjustment of the telescopic rod 122, and to ensure that the telescopic rod 122 is horizontal, the measurement rope 12 can be quickly obtained. height, and then obtain the addition amount of the material in the extraction tank 1. Setting the fixed handle 09 and the angle ruler can quickly read and measure the angle between the pendulum rod 120 and the telescopic rod 122 , so as to quickly obtain the added height of the material in the extraction tank 1 .

以上所述仅为本发明的较佳实施例而已,并不用以限制本发明,凡在本发明的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。不应将权利要求中的任何附图标记视为限制所涉及的权利要求。The above descriptions are only preferred embodiments of the present invention, and are not intended to limit the present invention. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present invention shall be included in the scope of the present invention. within the scope of protection. Any reference signs in the claims shall not be construed as limiting the involved claim.

此外,应当理解,虽然本说明书按照实施方式加以描述,但并非每个实施方式仅包含一个独立的技术方案,说明书的这种叙述方式仅仅是为清楚起见,本领域技术人员应当将说明书作为一个整体,各实施例中的技术方案也可以经适当组合,形成本领域技术人员可以理解的其他实施方式。In addition, it should be understood that although this specification is described in terms of embodiments, not each embodiment only includes an independent technical solution, and this description in the specification is only for the sake of clarity, and those skilled in the art should take the specification as a whole , the technical solutions in each embodiment can also be appropriately combined to form other implementations that can be understood by those skilled in the art.

Claims (10)

1.基于超声构件的柑橘皮中黄酮类物质提取方法,其特征在于,包括以下步骤:1. a method for extracting flavonoids from citrus peel based on ultrasonic components, characterized in that, comprising the following steps: S1、首先将破碎完成的柑橘皮料通过提取装置的进料口(4)送入提取罐(1)内,结合第一加料管(5)以及第二加料管(6)向提取罐(1)内注入萃取剂;S1. First, the crushed citrus peel is fed into the extraction tank (1) through the feeding port (4) of the extraction device, and the first feeding pipe (5) and the second feeding pipe (6) are combined to the extraction tank (1). ) inject the extractant; S2、通过进料口(4)和第一加料管(5)以及第二加料管(6)箱提取罐(1)内加料时,控制测量摆杆(120)将连接有漂浮球(13)的测量绳(12)送入提取罐(1)内,利用测量摆杆(120)端部的可视探头(1201)以及补光灯(1202),对提取罐(1)内的原料加注深度进行监控并计算数据,保证原料配比准确;S2. When feeding material into the extraction tank (1) through the feeding port (4), the first feeding pipe (5) and the second feeding pipe (6), the control and measurement pendulum rod (120) will be connected with the floating ball (13) The measuring rope (12) is fed into the extraction tank (1), and the raw material in the extraction tank (1) is filled with the visual probe (1201) and the fill light (1202) at the end of the measuring pendulum rod (120). In-depth monitoring and calculation of data to ensure accurate raw material ratio; S3、原料加注完成后,启动搅动电机(100)带动搅动桨叶(101)进行转动搅拌,搅拌十到十五分钟后,停止搅动电机(100),开启超声波振荡器(80),进行超声提取,加速提取效率,在提取的过程中结合测量摆杆(120)末端的可视探头(1201)监控柑橘混料的颜色,当柑橘混料的颜色接近萃取完成时的颜色时停止超声萃取,打开排料管(14)进行排出过滤,得到黄酮类化合物。S3. After the filling of the raw materials is completed, start the stirring motor (100) to drive the stirring paddle (101) to rotate and stir, after ten to fifteen minutes of stirring, stop the stirring motor (100), turn on the ultrasonic oscillator (80), and carry out ultrasonication Extraction, to speed up the extraction efficiency, monitor the color of the citrus mixture in combination with the visual probe (1201) at the end of the measuring pendulum (120) during the extraction process, stop ultrasonic extraction when the color of the citrus mixture is close to the color when the extraction is completed, The discharge pipe (14) is opened to discharge and filter to obtain flavonoids. 2.根据权利要求1所述的基于超声构件的柑橘皮中黄酮类物质提取方法,其特征在于,所述提取装置包括提取罐(1),所述提取罐(1)的上侧设置有进料口(4),所述提取罐(1)的顶部设置有盖板(10),所述提取罐(1)的底部设置有支撑腿(2)以及底座(3),所述提取罐(1)的顶部安装有第一加料管(5)以及第二加料管(6),所述提取罐(1)的底部设置有排料管(14),所述提取罐(1)上侧还设置有测量口(121),所述测量口(121)内安装有测量机构(11),所述测量机构(11)包括伸缩杆(122),所述伸缩杆(122)的末端转动安装有测量摆杆(120),所述测量摆杆(120)为空心设置,所述测量摆杆(120)内穿插设置有测量绳(12),所述测量绳(12)的末端连接有漂浮球(13),所述测量绳(12)上设置有刻度线,所述测量机构(11)还包括触底检测组件,所述提取罐(1)内悬挂安装有超声波振荡器(80),所述超声波振荡器(80)安装在提取罐(1)的中轴线上。2 . The method for extracting flavonoids from citrus peels based on an ultrasonic component according to claim 1 , wherein the extraction device comprises an extraction tank (1), and an extraction tank (1) is provided on the upper side of the extraction tank (1). 3 . The material port (4), the top of the extraction tank (1) is provided with a cover plate (10), the bottom of the extraction tank (1) is provided with support legs (2) and a base (3), the extraction tank ( 1) A first feeding pipe (5) and a second feeding pipe (6) are installed at the top of the extraction tank (1), a discharge pipe (14) is arranged at the bottom of the extraction tank (1), and the upper side of the extraction tank (1) is also A measurement port (121) is provided, a measurement mechanism (11) is installed in the measurement port (121), the measurement mechanism (11) includes a telescopic rod (122), and the end of the telescopic rod (122) is rotatably installed with a A measurement pendulum rod (120), the measurement pendulum rod (120) is hollow, a measurement rope (12) is interspersed in the measurement pendulum rod (120), and the end of the measurement rope (12) is connected with a floating ball (13), the measuring rope (12) is provided with a scale line, the measuring mechanism (11) also includes a bottom detection component, and an ultrasonic oscillator (80) is suspended in the extraction tank (1), so The ultrasonic oscillator (80) is installed on the central axis of the extraction tank (1). 3.根据权利要求2所述的基于超声构件的柑橘皮中黄酮类物质提取方法,其特征在于,所述触底检测组件包括设置在伸缩杆(122)上的固定架(01),所述固定架(01)与伸缩杆(122)之间垂直安装,所述固定架(01)上安装有绕卷筒(02),所述绕卷筒(02)上绕卷有测量绳(12),所述绕卷筒(02)与固定架(01)之间转动安装,所述绕卷筒(02)上同轴安装有旋转把手(03),所述伸缩杆(122)的末端设置有通孔(04),所述测量绳(12)穿过通孔(04)与测量摆杆(120)相连,所述测量摆杆(120)的端部设置有压力感应器(07),所述测量绳(12)设置在压力感应器(07)的上方,所述触底检测组件还包括可视单元。3. The method for extracting flavonoids from citrus peels based on an ultrasonic component according to claim 2, wherein the bottoming detection component comprises a fixing frame (01) arranged on a telescopic rod (122), and the The fixing frame (01) and the telescopic rod (122) are installed vertically, a winding drum (02) is installed on the fixing frame (01), and a measuring rope (12) is wound on the winding drum (02). , the winding drum (02) and the fixing frame (01) are rotated and installed, a rotating handle (03) is coaxially installed on the winding drum (02), and the end of the telescopic rod (122) is provided with a a through hole (04) through which the measuring rope (12) is connected to a measuring pendulum (120), the end of the measuring pendulum (120) is provided with a pressure sensor (07), so The measuring rope (12) is arranged above the pressure sensor (07), and the bottoming detection assembly further includes a visual unit. 4.根据权利要求3所述的基于超声构件的柑橘皮中黄酮类物质提取方法,其特征在于,所述可视单元包括设置在测量摆杆(120)端部的可视探头(1201),所述可视探头(1201)通过万向管与测量摆杆(120)的端部相连,所述测量摆杆(120)的端部还设置有补光灯(1202),所述伸缩杆(122)上设置有显示器(010),所述显示器(010)与可视探头(1201)相连。4. The method for extracting flavonoids from citrus peels based on an ultrasonic component according to claim 3, wherein the visual unit comprises a visual probe (1201) arranged at the end of the measuring pendulum (120), The visible probe (1201) is connected to the end of the measurement pendulum rod (120) through a universal tube, and the end of the measurement pendulum rod (120) is further provided with a fill light (1202), and the telescopic rod ( 122) is provided with a display (010), and the display (010) is connected with the visual probe (1201). 5.根据权利要求3所述的基于超声构件的柑橘皮中黄酮类物质提取方法,其特征在于,所述伸缩杆(122)上安装有水平调节组件,所述水平调节组件包括设置在提取罐(1)顶部的配合柱(91),所述配合柱(91)对称设置,所述配合柱(91)上配合安装有悬挂板(9),所述悬挂板(9)的端部设置有配合块(90),所述配合块(90)穿插配合在对称设置的配合柱(91)之间,所述悬挂板(9)的底部设置有调节滑轨(92),所述调节滑轨(92)内设置有调节槽(93),所述伸缩杆(122)的端部安装有套接环(1220),所述套接环(1220)上侧固定安装有配合板(1221),所述配合板(1221)的中间位置固定安装有伸缩柱(1222),所述伸缩柱(1222)的末端与调节槽(93)之间滑动安装。5 . The method for extracting flavonoids from citrus peels based on an ultrasonic component according to claim 3 , wherein a level adjusting assembly is installed on the telescopic rod ( 122 ), and the level adjusting assembly comprises an extraction tank arranged in an extraction tank. 6 . (1) The matching column (91) at the top, the matching column (91) is symmetrically arranged, a suspension plate (9) is fitted on the matching column (91), and the end of the suspension plate (9) is provided with a A matching block (90), the matching block (90) is inserted and fitted between the symmetrically arranged matching columns (91), the bottom of the suspension plate (9) is provided with an adjusting slide rail (92), and the adjusting slide rail (92) is provided with an adjustment groove (93), the end of the telescopic rod (122) is installed with a sleeve ring (1220), and a matching plate (1221) is fixedly installed on the upper side of the sleeve ring (1220), A telescopic column (1222) is fixedly installed in the middle position of the matching plate (1221), and the end of the telescopic column (1222) is slidably installed between the adjustment groove (93). 6.根据权利要求2所述的基于超声构件的柑橘皮中黄酮类物质提取方法,其特征在于,所述盖板(10)通过密封螺栓(101)与提取罐(1)之间固定连接,所述盖板(10)与提取罐(1)之间设置有密封垫(102)。6. The method for extracting flavonoids from citrus peel based on an ultrasonic component according to claim 2, wherein the cover plate (10) is fixedly connected to the extraction tank (1) through a sealing bolt (101), A gasket (102) is arranged between the cover plate (10) and the extraction tank (1). 7.根据权利要求2所述的基于超声构件的柑橘皮中黄酮类物质提取方法,其特征在于,所述提取罐(1)的底部设置有搅动电机(100),所述提取罐(1)的底部转动安装有搅动桨叶(101),所述搅动桨叶(101)倾斜设置,所述搅动桨叶(101)的底部边缘与提取罐(1)的底部相切安装,所述搅动桨叶(101)的回转中心与提取罐(1)之间通过密封轴承安装。7. The method for extracting flavonoids from citrus peel based on an ultrasonic component according to claim 2, wherein a stirring motor (100) is provided at the bottom of the extraction tank (1), and the extraction tank (1) is provided with a stirring motor (100). A stirring paddle (101) is rotatably installed at the bottom of the stirring paddle, the stirring paddle (101) is inclined and the bottom edge of the stirring paddle (101) is installed tangentially to the bottom of the extraction tank (1). A sealed bearing is installed between the rotation center of the leaf (101) and the extraction tank (1). 8.根据权利要求2所述的基于超声构件的柑橘皮中黄酮类物质提取方法,其特征在于,所述伸缩杆(122)的末端与测量摆杆(120)的端部之间设置有转动连接架(08),所述转动连接架(08)与伸缩杆(122)之间设置有固定把手(09),所述固定把手(09)上设置有角度尺。8 . The method for extracting flavonoids from citrus peels based on an ultrasonic component according to claim 2 , wherein a rotation is provided between the end of the telescopic rod ( 122 ) and the end of the measuring pendulum rod ( 120 ). 9 . A connecting frame (08), a fixed handle (09) is arranged between the rotating connecting frame (08) and the telescopic rod (122), and an angle ruler is arranged on the fixed handle (09). 9.根据权利要求3所述的基于超声构件的柑橘皮中黄酮类物质提取方法,其特征在于,所述进料口(4)与测量口(121)对称设置,所述测量口(121)的边缘设置有圆角,所述压力感应器(07)呈条状设置,所述压力感应器(07)的中间部位向下凹陷,所述测量绳(12)沿着凹陷部位进入测量摆杆(120)。9 . The method for extracting flavonoids from citrus peel based on an ultrasonic component according to claim 3 , wherein the feeding port ( 4 ) and the measuring port ( 121 ) are symmetrically arranged, and the measuring port ( 121 ) The edge is provided with rounded corners, the pressure sensor (07) is arranged in a strip shape, the middle part of the pressure sensor (07) is concave downward, and the measuring rope (12) enters the measuring pendulum along the concave part. (120). 10.根据权利要求2所述的基于超声构件的柑橘皮中黄酮类物质提取方法,其特征在于,所述超声波振荡器(80)与提取罐(1)侧边距离等于超声波振荡器(80)与提取罐(1)底部距离。10. The method for extracting flavonoids from citrus peels based on an ultrasonic component according to claim 2, wherein the distance between the ultrasonic oscillator (80) and the side of the extraction tank (1) is equal to the ultrasonic oscillator (80) Distance from the bottom of the extraction tank (1).
CN202210888817.1A 2022-07-27 2022-07-27 Method for extracting flavonoid substances in orange peel based on ultrasonic component Pending CN115138098A (en)

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Application publication date: 20221004