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CN113797150A - Formula of hyaluronic acid collagen facial mask and preparation method thereof - Google Patents

Formula of hyaluronic acid collagen facial mask and preparation method thereof Download PDF

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CN113797150A
CN113797150A CN202111072180.0A CN202111072180A CN113797150A CN 113797150 A CN113797150 A CN 113797150A CN 202111072180 A CN202111072180 A CN 202111072180A CN 113797150 A CN113797150 A CN 113797150A
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extract
facial mask
hyaluronic acid
skin
formula
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马魁
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Shaanxi Aomeiya Biotechnology Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/99Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/65Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9706Algae
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/981Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
    • A61K8/986Milk; Derivatives thereof, e.g. butter
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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  • Cosmetics (AREA)

Abstract

本发明涉及面膜领域,具体地说,涉及一种透明质酸胶原蛋白面膜的配方及其制作方法。其包括皮肤调理剂、保湿剂、防腐剂、芳香剂和去离子水组成,该透明质酸胶原蛋白面膜的配方及其制作方法中,加入的海藻提取物,它内含有藻胶酸,粗蛋白,多种维生素,酶和微量元素,此类营养经皮肤吸收后,能降低表面血脂,增进表面皮肤造血功能,促进皮肤的新陈代谢,抗皱,抗衰老,加入的牛奶蛋白提取物有助于维持皮肤水分平衡,柔和净化肌肤,同时滋养肌肤,加入的蜗牛提取物对人的皮肤具有很好的美白保湿效果,而且长期使用可以改善皮肤的松弛、皱纹,且能有效修补伤疤,对于受损皮肤有着不错的修复和愈合作用。

Figure 202111072180

The invention relates to the field of facial masks, in particular to a formulation of a hyaluronic acid collagen facial mask and a preparation method thereof. It comprises skin conditioning agent, moisturizing agent, preservative, fragrance and deionized water. In the formula of the hyaluronic acid collagen mask and the preparation method thereof, the added seaweed extract contains alginic acid, crude protein , a variety of vitamins, enzymes and trace elements, after such nutrients are absorbed by the skin, can reduce the surface blood lipids, improve the hematopoietic function of the surface skin, promote skin metabolism, anti-wrinkle, anti-aging, the added milk protein extract helps to maintain the skin Moisture balance, softly purifies the skin, and nourishes the skin at the same time. The added snail extract has a good whitening and moisturizing effect on human skin, and long-term use can improve skin relaxation and wrinkles, and can effectively repair scars. It has a good effect on damaged skin. Nice repair and healing effect.

Figure 202111072180

Description

Formula of hyaluronic acid collagen facial mask and preparation method thereof
Technical Field
The invention relates to the field of facial masks, in particular to a formula of a hyaluronic acid collagen facial mask and a preparation method thereof.
Background
The facial mask is a carrier containing beauty and care products, can be cleaned or removed after nutrients of the beauty and care products are slowly absorbed by skin after being coated or applied on the face for a certain time, and is the most important purpose of making up the cleaning work that makeup removal and face washing are still insufficient, and realizes various different care functions such as moisturizing, whitening, wrinkle resistance, grease balancing, skin tightening and the like by matching with other essential components on the basis;
the existing facial mask essence has complex components, so the preparation process and the cost are high, the existing facial mask essence contains a large amount of chemical substances such as fluorescent whitening agents, titanium dioxide, phenol and the like, the effect can be achieved by using the facial mask, the visual whiteness is only false white after the facial mask is used, and the facial mask essence is not beneficial to long-term skin maintenance once the existing facial mask essence is stopped to restore the original appearance.
Disclosure of Invention
The invention aims to provide a formula of a hyaluronic acid collagen facial mask and a preparation method thereof, and aims to solve the problems in the background technology.
In order to achieve the above object, in one aspect, the present invention provides a formula of a hyaluronic acid collagen facial mask, comprising the following raw materials: skin conditioner, humectant, antiseptic and aromatic, and the balance of deionized water;
the skin conditioner comprises 0.03-0.6% of seaweed extract, 0.3-0.7% of milk extract and 0.5-2.5% of snail extract, the milk protein extract is helpful for maintaining the moisture balance of the skin, softly purifying the skin and simultaneously nourishing the skin, the snail extract has good whitening and moisturizing effects on the skin of people, can improve the relaxation and wrinkles of the skin after long-term use and effectively repair scars, has good repairing and healing effects on the damaged skin, accelerates the growth of cells and reduces scars;
the humectant comprises 0.001-0.02% of chondroitin sodium sulfate, 0.5-2.5% of hydrolyzed collagen and 0.01-0.2% of sodium hyaluronate, the chondroitin sodium sulfate is added into cosmetics, because of the polysaccharide structure, the collagen gel has good moisturizing property, can inhibit various bacteria, has anti-inflammatory effect, can promote the growth of cells, plays a role in resisting aging, has rich amino acid in hydrolyzed collagen, can improve the moisture supply of skin, supplement cell nutrition, relieve skin, tighten skin elasticity, promote metabolism and inhibit the generation of wrinkles, has strong viscoelasticity and lubricity, is coated on the surface of the skin, can form a layer of moisturizing breathable film to keep skin moist and bright, and the micromolecular hyaluronic acid can permeate into the dermis layer to promote blood microcirculation, be beneficial to the absorption of skin on nutrient substances and play a role in beautifying and anti-wrinkle health care.
As a further improvement of the technical scheme, the preservative is phenoxyethanol, the dosage of the phenoxyethanol is 0.05-0.25%, and the phenoxyethanol has the main function of being added into the application to play an antibacterial and antiseptic role and possibly has a certain emulsification effect to influence the viscosity of the skin care product.
As a further improvement of the technical scheme, the aromatic is essence, the using amount of the essence is 0.001-0.005%, and the essence can provide pleasant smell in cosmetics, cover the smell of a product matrix, help the product to establish a brand-new image and enhance the attraction of the product to customers.
As a further improvement of the technical scheme, the seaweed extract comprises a giant kelp extract, an austenitic seaweed extract and a bonadt spirulina extract, and the dosage ratio of the giant kelp extract to the austenitic seaweed extract to the bonadt spirulina extract is 1: 1: the seaweed extract is a pure natural marine organism product, all the characteristics come from the special seaweed, the seaweed contains alginic acid, crude protein, various vitamins, enzymes and trace elements, the nutrition can reduce surface blood fat and improve the surface skin hematopoiesis function after being absorbed by the skin, and the seaweed extract has a large amount of anions and can stimulate fiber cells to generate collagen and elastin so as to promote the metabolism of the skin, resist wrinkles and resist aging.
As a further improvement of the technical scheme, the extraction step of the seaweed extract comprises the following operations:
s1.1, repeatedly cleaning the seaweed, removing surface impurities, naturally drying and crushing to obtain crushed materials;
s1.2, adding the crushed material into an extraction kettle, and heating at the temperature of 110-;
and S1.3, repeatedly filtering the separation liquid to obtain a seaweed extract.
As a further improvement of the technical scheme, the extraction step of the milk extract comprises the following operations:
s2.1, placing milk in an extraction furnace, adding the milk under stirring, preheating to 40 ℃, adding an acetic acid-sodium acetate buffer solution, adjusting the pH to 4.7, observing that flocculent precipitates appear in the milk and forming a suspension, and keeping the temperature until the precipitates are completely precipitated;
s2.2, cooling the suspension to room temperature, and centrifugally separating at the rotation speed of 2000-;
s2.3, repeatedly washing the precipitate with distilled water, centrifugally separating for 5-10min at the rotating speed of 3000-12000r/min, and discarding the supernatant;
s2.4, adding ethanol into the precipitate, stirring, filtering the whole suspension, washing the precipitate with an ethanol-ether mixed solution, finally washing the precipitate with ether, draining, spreading the precipitate on a watch glass, and air-drying to obtain the milk extract.
In another aspect, the present invention provides a method for preparing a formulation of a hyaluronic acid collagen mask, comprising the formulation of a hyaluronic acid collagen mask according to any one of claims 1 to 6, comprising the following steps:
s3.1, preparing a seaweed extract, a milk extract and a snail extract for later use;
s3.2, adding the giant kelp extract, the austenitic seaweed extract, the bonadt spirulina extract, the milk extract and the snail extract into deionized water, and stirring and mixing to prepare an initial solution;
s3.3, adding chondroitin sodium sulfate, hydrolyzed collagen and sodium hyaluronate into the initial solution, heating, stirring and mixing;
s3.4, adding an aromatic and a preservative into the initial solution, heating, stirring and mixing, and cooling to obtain a mask solution;
and S3.5, adding the facial mask paper into the facial mask liquid, and soaking for 1-2 hours at normal temperature to obtain the hyaluronic acid collagen facial mask.
Preferably, in S3.2, the processing temperature is 30-50 ℃, and the rotation speed is 900-1200r/min, and the stirring time is 50-80 min.
Preferably, in S3.3, firstly, the hydrolyzed collagen is put in, sodium chondroitin sulfate and sodium hyaluronate are slowly added during stirring to ensure that each humectant can be fully mixed with the initial solution, wherein the temperature is raised to 50-70 ℃, and the stirring is carried out for 1-1.5 hours under the condition that the rotating speed is 600-900 r/min.
Preferably, in S3.4, the temperature is raised to 80-100 ℃, and the stirring is carried out for 30-60min under the condition that the rotating speed is 700-900 r/min.
Compared with the prior art, the invention has the beneficial effects that:
1. in the formula and the preparation method of the hyaluronic acid collagen facial mask, the added seaweed extract is a pure natural marine organism product, and contains alginic acid, crude protein, multiple vitamins, enzymes and trace elements, and after the nutrition is absorbed by skin, the hyaluronic acid collagen facial mask can reduce surface blood fat and enhance the hemopoiesis function of the surface skin, has a large amount of anions, and can stimulate fiber cells to generate collagen and elastin so as to promote the metabolism of the skin, resist wrinkles and resist aging.
2. In the formula and the preparation method of the hyaluronic acid collagen facial mask, the added milk protein extract is helpful for maintaining the moisture balance of skin, softly purifying the skin and nourishing the skin, the added snail extract has good whitening and moisturizing effects on the skin of a human, can improve the relaxation and wrinkles of the skin after long-term use, can effectively repair scars, has good repairing and healing effects on the damaged skin, accelerates the growth of cells and reduces scars.
Drawings
FIG. 1 is an overall flow diagram of the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Embodiment 1 a formula of a hyaluronic acid collagen facial mask and a preparation method thereof, comprising:
preparation method of seaweed extract
Repeatedly cleaning giant black seaweed, austenitic seaweed and Bonatt spirulina to remove surface impurities, naturally drying, and pulverizing to obtain three pulverized materials; adding the three crushed materials into different extraction kettles respectively, and heating at the temperature of 110-; filtering the three separated solutions repeatedly to obtain black giant seaweed extract, Austenitic seaweed extract and Bonatt Spirulina extract.
Second, preparation of milk extract
Placing milk in an extraction furnace, adding the milk under stirring, preheating to 40 ℃, adding an acetic acid-sodium acetate buffer solution, adjusting the pH value to 4.7, observing that the milk begins to have flocculent precipitates, keeping the temperature until the precipitates are completely precipitated, cooling the suspension to room temperature, carrying out centrifugal separation at the rotation speed of 2000-8000r/min for 8-15min to obtain a crude casein product, repeatedly washing the precipitates with distilled water, carrying out centrifugal separation at the rotation speed of 3000-12000r/min for 5-10min, and discarding the supernatant. Adding ethanol into the precipitate, stirring, filtering the suspension, washing the precipitate with ethanol-diethyl ether mixture, washing the precipitate with diethyl ether, draining, spreading the precipitate on a watch glass, and air drying to obtain milk extract.
Third, preparation of facial mask liquid
Adding 0.01% of Megasphaera anomala extract, 0.01% of Austenitic seaweed extract, 0.01% of Bonatt spirulina extract, 0.3% of milk extract and 0.5% of snail extract into deionized water, stirring for 50-80min under the conditions that the temperature is 30-50 ℃ and the rotating speed is 900-1200r/min, and stirring and mixing to obtain an initial solution; adding 0.5% of hydrolyzed collagen into the initial solution, slowly adding 0.001% of chondroitin sodium sulfate and 0.01% of sodium hyaluronate during stirring to ensure that each humectant can be fully mixed with the initial solution, wherein stirring for 1-1.5h under the conditions that the temperature is raised to 50-70 ℃ and the rotating speed is 600-; adding 0.001% of aromatic and 0.05% of preservative into the initial solution, heating to 80-100 ℃, stirring for 30-60min under the condition that the rotating speed is 700-.
Embodiment 2 a formula of a hyaluronic acid collagen facial mask and a preparation method thereof, comprising:
preparation method of seaweed extract
Repeatedly cleaning giant black seaweed, austenitic seaweed and Bonatt spirulina to remove surface impurities, naturally drying, and pulverizing to obtain three pulverized materials; adding the three crushed materials into different extraction kettles respectively, and heating at the temperature of 110-; filtering the three separated solutions repeatedly to obtain black giant seaweed extract, Austenitic seaweed extract and Bonatt Spirulina extract.
Second, preparation of milk extract
Placing milk in an extraction furnace, adding the milk under stirring, preheating to 40 ℃, adding an acetic acid-sodium acetate buffer solution, adjusting the pH value to 4.7, observing that the milk begins to have flocculent precipitates, keeping the temperature until the precipitates are completely precipitated, cooling the suspension to room temperature, carrying out centrifugal separation at the rotation speed of 2000-8000r/min for 8-15min to obtain a crude casein product, repeatedly washing the precipitates with distilled water, carrying out centrifugal separation at the rotation speed of 3000-12000r/min for 5-10min, and discarding the supernatant. Adding ethanol into the precipitate, stirring, filtering the suspension, washing the precipitate with ethanol-diethyl ether mixture, washing the precipitate with diethyl ether, draining, spreading the precipitate on a watch glass, and air drying to obtain milk extract.
Third, preparation of facial mask liquid
Adding 0.2% of Megasphaera anomala extract, 0.2% of Austenitic seaweed extract, 0.2% of Bonatt spirulina extract, 0.7% of milk extract and 2.5% of snail extract into deionized water, stirring for 50-80min under the conditions that the temperature is 30-50 ℃ and the rotating speed is 900-1200r/min, and stirring and mixing to obtain an initial solution; putting 2.5% of hydrolyzed collagen into the initial solution, slowly adding 0.02% of chondroitin sodium sulfate and 0.2% of sodium hyaluronate during stirring to ensure that each humectant can be fully mixed with the initial solution, wherein stirring for 1-1.5h under the conditions that the temperature is raised to 50-70 ℃ and the rotating speed is 600-; adding 0.005% of aromatic and 0.25% of preservative into the initial solution, heating to 80-100 ℃, stirring for 30-60min under the condition that the rotating speed is 700-.
Embodiment 3 a formula of a hyaluronic acid collagen facial mask and a preparation method thereof, comprising:
preparation method of seaweed extract
Repeatedly cleaning giant black seaweed, austenitic seaweed and Bonatt spirulina to remove surface impurities, naturally drying, and pulverizing to obtain three pulverized materials; adding the three crushed materials into different extraction kettles respectively, and heating at the temperature of 110-; filtering the three separated solutions repeatedly to obtain black giant seaweed extract, Austenitic seaweed extract and Bonatt Spirulina extract.
Second, preparation of milk extract
Placing milk in an extraction furnace, adding the milk under stirring, preheating to 40 ℃, adding an acetic acid-sodium acetate buffer solution, adjusting the pH value to 4.7, observing that the milk begins to have flocculent precipitates, keeping the temperature until the precipitates are completely precipitated, cooling the suspension to room temperature, carrying out centrifugal separation at the rotation speed of 2000-8000r/min for 8-15min to obtain a crude casein product, repeatedly washing the precipitates with distilled water, carrying out centrifugal separation at the rotation speed of 3000-12000r/min for 5-10min, and discarding the supernatant. Adding ethanol into the precipitate, stirring, filtering the suspension, washing the precipitate with ethanol-diethyl ether mixture, washing the precipitate with diethyl ether, draining, spreading the precipitate on a watch glass, and air drying to obtain milk extract.
Third, preparation of facial mask liquid
Adding 0.1% of Megasphaera anomala extract, 0.1% of Austenitic seaweed extract, 0.1% of Bonatt spirulina extract, 0.5% of milk extract and 1.5% of snail extract into deionized water, stirring for 50-80min under the conditions that the temperature is 30-50 ℃ and the rotating speed is 900-1200r/min, stirring and mixing to obtain an initial solution; putting 1.5% of hydrolyzed collagen into the initial solution, slowly adding 0.01% of chondroitin sodium sulfate and 0.1% of sodium hyaluronate during stirring to ensure that each humectant can be fully mixed with the initial solution, wherein stirring for 1-1.5h under the conditions that the temperature is raised to 50-70 ℃ and the rotating speed is 600-; adding 0.003% of aromatic and 0.15% of preservative into the initial solution, heating to 80-100 ℃, stirring for 30-60min under the condition that the rotation speed is 700-900r/min, cooling to obtain facial mask solution, adding facial mask paper into the facial mask solution, and soaking for 1-2h at normal temperature to obtain the hyaluronic acid collagen facial mask.
In the above examples 1-3, the seaweed extract is a pure natural marine product, all the characteristics are derived from the special seaweed itself, which contains alginic acid, crude protein, vitamins, enzymes and trace elements, and after being absorbed by skin, the nutrition can reduce surface blood fat and enhance surface skin hematopoiesis, has a large amount of anions, and can stimulate fiber cells to generate collagen and elastin, promote skin metabolism, resist wrinkles and resist aging;
the milk protein extract is helpful for maintaining the moisture balance of the skin, softly purifying the skin and simultaneously nourishing the skin, the snail extract has good whitening and moisturizing effects on the skin of a human, can improve the looseness and wrinkles of the skin after long-term use, can effectively repair scars, has good repairing and healing effects on the damaged skin, accelerates the growth of cells and reduces scars;
in cosmetics, the chondroitin sodium sulfate has a polysaccharide structure, has a good moisturizing type, can inhibit various bacteria, has an anti-inflammatory effect, can promote the growth of cells and plays a role in resisting aging, hydrolyzed collagen has rich amino acids, can improve the water supply of skin, supplement cell nutrition, relieve the skin, tighten the elasticity of the skin, promote metabolism and inhibit the generation of wrinkles, and a sodium hyaluronate aqueous solution has strong viscoelasticity and lubricity and can form a moisturizing and breathable film when being coated on the surface of the skin to keep the skin moist and bright, so that small-molecule hyaluronic acid can permeate into a dermis layer to promote blood microcirculation, thereby being beneficial to the absorption of nutrients by the skin and playing a role in beautifying, anti-wrinkle and health care;
the preservative is phenoxyethanol, the dosage of the phenoxyethanol is 0.05-0.25%, the phenoxyethanol has the main function of playing the role of antibiosis and antisepsis when being added into the application, and simultaneously has a certain emulsification effect, thus influencing the viscosity of the skin care product;
the aromatic is essence, the dosage of the essence is 0.001-0.005%, the essence can provide pleasant smell in cosmetics, cover the smell of the product matrix, help the product to establish brand-new image, and enhance the attraction of the product to customers.
Comparative example 1
The comparative example provides a facial mask formula, comprising, by percent: 0.1% of austenitic seaweed extract, 0.1% of bonadt spirulina extract, 0.5% of milk extract, 1.5% of snail extract, 1.5% of hydrolyzed collagen, 0.01% of chondroitin sodium sulfate, 0.1% of sodium hyaluronate, 0.003% of aromatic, 0.15% of preservative and the balance of deionized water.
In contrast to example 3, the Megasphaera blankoensis extract was absent.
Comparative example 2
The comparative example provides a facial mask formula, comprising, by percent: 0.1% of Megasphaera anomala extract, 0.1% of Austenitic seaweed extract, 0.5% of milk extract, 1.5% of snail extract, 1.5% of hydrolyzed collagen, 0.01% of sodium chondroitin sulfate, 0.1% of sodium hyaluronate, 0.003% of aromatic, 0.15% of preservative and the balance of deionized water.
In contrast to example 3, there was a lack of B.borna extract.
Comparative example 3
The comparative example provides a facial mask formula, comprising, by percent: 0.5% of milk extract, 1.5% of snail extract, 1.5% of hydrolyzed collagen, 0.01% of chondroitin sodium sulfate, 0.1% of sodium hyaluronate, 0.003% of aromatic, 0.15% of preservative and the balance of deionized water.
In comparison to example 3, there was a lack of borna spirulina extract, borna spirulina extract and seaweeds extract.
Comparative example 4
The comparative example provides a facial mask formula, comprising, by percent: 0.1% of Megasphaera nigroca extract, 0.1% of Austenitic seaweed extract, 0.1% of Bonatt spirulina extract, 1.5% of snail extract, 1.5% of hydrolyzed collagen, 0.01% of chondroitin sodium sulfate, 0.1% of sodium hyaluronate, 0.003% of aromatic, 0.15% of preservative and the balance of deionized water.
In contrast to example 3, milk extract was absent.
Comparative example 5
The comparative example provides a facial mask formula, comprising, by percent: 0.1% of Megasphaera nigroca extract, 0.1% of Austenitic seaweed extract, 0.1% of Bonatt spirulina extract, 0.5% of milk extract, 1.5% of hydrolyzed collagen, 0.01% of sodium chondroitin sulfate, 0.1% of sodium hyaluronate, 0.003% of aromatic, 0.15% of preservative and the balance of deionized water.
In contrast to example 3, snail extract was absent.
Comparative example 6
The comparative example provides a facial mask formula, comprising, by percent: 0.1% of Megasphaera nigroca extract, 0.1% of Austenitic seaweed extract, 0.1% of Bonatt spirulina extract, 1.5% of hydrolyzed collagen, 0.01% of sodium chondroitin sulfate, 0.1% of sodium hyaluronate, 0.003% of aromatic, 0.15% of preservative and the balance of deionized water.
Milk extract and snail extract were absent compared to example 3.
Comparative examples 1-6 provide facial mask formulations prepared in the same manner as example 3, wherein the missing materials were not added directly, and other steps were not changed, and thus are not described herein again.
Test example 1
The mask prepared from the mask formulations provided in examples 1-3 and comparative examples 1-6 above was tested by randomly inviting 45 women between ages 22-25 and divided into 9 groups. 5 persons were randomly assigned to each group, and the corresponding masks prepared according to the formulations in examples and comparative examples were tried, and the skin condition of the user was observed after 14 days of trial, and the test results are shown in table 1:
TABLE 1
Figure BDA0003260815480000091
As can be seen from table 1, compared with comparative examples 1 to 6, the improved facial mask formulations in examples 1 to 3 of the present invention have more significant color difference, which indicates that the skin whitening effect is better, the moisture content of the skin after application is higher, and the moisturizing effect is better, which indicates that the formula components and the mixture ratio of the hyaluronic acid collagen facial mask provided by the present invention are more reasonable, and the prepared facial mask has a better effect.
The foregoing shows and describes the general principles, essential features, and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, and the preferred embodiments of the present invention are described in the above embodiments and the description, and are not intended to limit the present invention. The scope of the invention is defined by the appended claims and equivalents thereof.

Claims (10)

1.一种透明质酸胶原蛋白面膜的配方,包括以下原料组成:皮肤调理剂、保湿剂、防腐剂和芳香剂,其余为去离子水;1. A formulation of a hyaluronic acid collagen facial mask, comprising the following raw materials: skin conditioning agent, moisturizing agent, preservative and fragrance, and the rest are deionized water; 所述皮肤调理剂包括淡海藻提取物0.03-0.6%、牛奶提取物0.3-0.7%和蜗牛提取物0.5-2.5%;The skin conditioning agent includes 0.03-0.6% of seaweed extract, 0.3-0.7% of milk extract and 0.5-2.5% of snail extract; 所述保湿剂包括软骨素硫酸钠0.001-0.02%、水解胶原0.5-2.5%和透明质酸钠0.01-0.2%。The moisturizing agent includes 0.001-0.02% of sodium chondroitin sulfate, 0.5-2.5% of hydrolyzed collagen and 0.01-0.2% of sodium hyaluronate. 2.根据权利要求1所述的透明质酸胶原蛋白面膜的配方,其特征在于:所述防腐剂为苯氧乙醇,所述苯氧乙醇的用量为0.05-0.25%。2. The formula of the hyaluronic acid collagen facial mask according to claim 1, wherein the preservative is phenoxyethanol, and the consumption of the phenoxyethanol is 0.05-0.25%. 3.根据权利要求1所述的透明质酸胶原蛋白面膜的配方,其特征在于:所述芳香剂为香精,所述香精的用量为0.001-0.005%。3. The formula of the hyaluronic acid collagen facial mask according to claim 1, wherein the fragrance is an essence, and the consumption of the essence is 0.001-0.005%. 4.根据权利要求1所述的透明质酸胶原蛋白面膜的配方,其特征在于:所述海藻提取物包括淡黑巨海藻提取物、奥氏海藻提取物和勃纳特螺旋藻提取物,所述黑巨海藻提取物、所述奥氏海藻提取物和所述勃纳特螺旋藻提取物的用量比例为1:1:1。4. the formula of hyaluronic acid collagen facial mask according to claim 1, is characterized in that: described seaweed extract comprises light black giant seaweed extract, Ostrich seaweed extract and Bonnett spirulina extract, so The dosage ratio of the black giant seaweed extract, the australian seaweed extract and the bonnett spirulina extract is 1:1:1. 5.根据权利要求1所述的透明质酸胶原蛋白面膜的配方,其特征在于:所述海藻提取物的提取步骤如以下操作:5. the formula of hyaluronic acid collagen facial mask according to claim 1, is characterized in that: the extraction step of described seaweed extract is as follows: S1.1、将海藻反复进行清洗,去除表面杂质,自然干燥后粉碎,制得粉碎料;S1.1. Wash the seaweed repeatedly to remove surface impurities, and pulverize after natural drying to obtain pulverized material; S1.2、将粉碎料加入至提取釜中,温度110-130℃下加热30-60min后,得到分离液;S1.2, adding the pulverized material to the extraction kettle, and heating at a temperature of 110-130 ° C for 30-60 min to obtain a separation liquid; S1.3、将分离液经反复过滤,得到海藻提取液。S1.3, the separation liquid is repeatedly filtered to obtain the seaweed extract. 6.根据权利要求1所述的透明质酸胶原蛋白面膜的配方,其特征在于:所述牛奶提取物的提取步骤如以下操作:6. the formula of hyaluronic acid collagen facial mask according to claim 1, is characterized in that: the extraction step of described milk extract is as follows: S2.1、将牛奶放置在提取炉中,在搅拌下加入预热至40℃,加入醋酸-醋酸钠缓冲液,调节pH至4.7,观察牛奶开始有絮状沉淀出现,并形成悬浮液,保温至沉淀完全;S2.1. Place the milk in the extraction furnace, add it under stirring and preheat to 40°C, add acetic acid-sodium acetate buffer, adjust the pH to 4.7, observe that the milk begins to have flocculent precipitation and form a suspension, keep warm until the precipitation is complete; S2.2将上述悬浮液冷却至室温,转速为2000-8000r/min离心分离8-15min,制得酪蛋白粗制品;S2.2 the above suspension is cooled to room temperature, and the rotating speed is 2000-8000r/min for centrifugal separation for 8-15min to obtain a crude casein product; S2.3、用蒸馏水反复洗涤沉淀,转速为3000-12000r/min下离心分离5-10min,弃去上清液;S2.3. Repeatedly washing the precipitate with distilled water, centrifuging for 5-10 min at a rotational speed of 3000-12000 r/min, and discarding the supernatant; S2.4、在沉淀中加入乙醇,搅拌,将全部悬浊液过滤,用乙醇-乙醚混合液洗涤沉淀,最后用乙醚洗涤沉淀,抽干后,将沉淀摊开在表面皿上,风干,制得牛奶提取物。S2.4. Add ethanol to the precipitation, stir, filter the entire suspension, wash the precipitation with ethanol-diethyl ether mixture, and finally wash the precipitation with diethyl ether. Get milk extract. 7.一种透明质酸胶原蛋白面膜的配方的制作方法,包括权利要求1-6中任意一项所述的一种透明质酸胶原蛋白面膜的配方,其操作步骤如下:7. a preparation method of the formula of a hyaluronic acid collagen facial mask, comprising the formula of a hyaluronic acid collagen facial mask described in any one of claim 1-6, and its operation steps are as follows: S3.1、制备海藻提取物、牛奶提取物和蜗牛提取物,备用;S3.1, prepare seaweed extract, milk extract and snail extract for use; S3.2、将淡黑巨海藻提取物、奥氏海藻提取物、勃纳特螺旋藻提取物、牛奶提取物和蜗牛提取物加入至去离子水中,搅拌混合,制得初始溶液;S3.2, adding the kelp extract, algae extract, spirulina bonnet extract, milk extract and snail extract to deionized water, stirring and mixing to obtain an initial solution; S3.3、加入软骨素硫酸钠、水解胶原和透明质酸钠至初始溶液中,升温,搅拌混合;S3.3, adding sodium chondroitin sulfate, hydrolyzed collagen and sodium hyaluronate to the initial solution, heating up, stirring and mixing; S3.4、再加入芳香剂和防腐剂至初始溶液,升温,搅拌混合后,冷却,制得面膜液;S3.4. Add aromatics and preservatives to the initial solution, raise the temperature, stir and mix, and cool to obtain a facial mask solution; S3.5、将面膜纸加入至面膜液中,常温下浸泡1-2h,即可制得透明质酸胶原蛋白面膜。S3.5. Add the facial mask paper to the facial mask solution, soak it for 1-2 hours at room temperature, and then prepare the hyaluronic acid collagen facial mask. 8.根据权利要求7所述的透明质酸胶原蛋白面膜的配方的制作方法,其特征在于:所述S3.2中,加工温度为30-50℃,转速为900-1200r/min的条件下,搅拌50-80min。8. The preparation method of the formula of the hyaluronic acid collagen facial mask according to claim 7, characterized in that: in the S3.2, the processing temperature is 30-50 DEG C, and the rotating speed is under the condition of 900-1200r/min , stir for 50-80min. 9.根据权利要求7所述的透明质酸胶原蛋白面膜的配方的制作方法,其特征在于:所述S3.3中,首先投放水解胶原,搅拌时缓缓加入软骨素硫酸钠和透明质酸钠,其中升温至温度为50-70℃,转速为600-900r/min的条件下,搅拌1-1.5h。9. The preparation method of the formula of the hyaluronic acid collagen facial mask according to claim 7, it is characterized in that: in described S3.3, first put in hydrolyzed collagen, slowly add chondroitin sulfate sodium and hyaluronic acid during stirring Sodium, which is heated to a temperature of 50-70 ° C and a rotating speed of 600-900 r/min, and stirred for 1-1.5 h. 10.根据权利要求7所述的透明质酸胶原蛋白面膜的配方的制作方法,其特征在于:所述S3.4中,升温至温度为80-100℃,转速为700-900r/min的条件下,搅拌30-60min。10. The preparation method of the formula of the hyaluronic acid collagen facial mask according to claim 7, characterized in that: in the S3.4, the temperature is raised to a temperature of 80-100°C, and the rotational speed is a condition of 700-900r/min under, stirring for 30-60min.
CN202111072180.0A 2021-09-14 2021-09-14 Formula of hyaluronic acid collagen facial mask and preparation method thereof Pending CN113797150A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115634171A (en) * 2022-10-27 2023-01-24 华熙生物科技股份有限公司 Cosmetic composition and application thereof, and method for improving skin barrier function or repairing skin barrier function

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115634171A (en) * 2022-10-27 2023-01-24 华熙生物科技股份有限公司 Cosmetic composition and application thereof, and method for improving skin barrier function or repairing skin barrier function

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