CN112194370A - Blue and white marbling glaze and preparation method thereof - Google Patents
Blue and white marbling glaze and preparation method thereof Download PDFInfo
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- CN112194370A CN112194370A CN202010946283.4A CN202010946283A CN112194370A CN 112194370 A CN112194370 A CN 112194370A CN 202010946283 A CN202010946283 A CN 202010946283A CN 112194370 A CN112194370 A CN 112194370A
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- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 239000005995 Aluminium silicate Substances 0.000 claims abstract description 16
- 235000012211 aluminium silicate Nutrition 0.000 claims abstract description 16
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims abstract description 16
- 235000019353 potassium silicate Nutrition 0.000 claims abstract description 16
- 239000010453 quartz Substances 0.000 claims abstract description 16
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 16
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000011521 glass Substances 0.000 claims abstract description 13
- 239000000843 powder Substances 0.000 claims abstract description 13
- 229910000428 cobalt oxide Inorganic materials 0.000 claims abstract description 10
- IVMYJDGYRUAWML-UHFFFAOYSA-N cobalt(ii) oxide Chemical compound [Co]=O IVMYJDGYRUAWML-UHFFFAOYSA-N 0.000 claims abstract description 10
- GFQYVLUOOAAOGM-UHFFFAOYSA-N zirconium(iv) silicate Chemical compound [Zr+4].[O-][Si]([O-])([O-])[O-] GFQYVLUOOAAOGM-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229910021538 borax Inorganic materials 0.000 claims abstract description 8
- 239000010459 dolomite Substances 0.000 claims abstract description 8
- 229910000514 dolomite Inorganic materials 0.000 claims abstract description 8
- 235000010339 sodium tetraborate Nutrition 0.000 claims abstract description 8
- 239000000454 talc Substances 0.000 claims abstract description 8
- 235000012222 talc Nutrition 0.000 claims abstract description 8
- 229910052623 talc Inorganic materials 0.000 claims abstract description 8
- BSVBQGMMJUBVOD-UHFFFAOYSA-N trisodium borate Chemical compound [Na+].[Na+].[Na+].[O-]B([O-])[O-] BSVBQGMMJUBVOD-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000010433 feldspar Substances 0.000 claims abstract description 7
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims abstract description 6
- 229940072033 potash Drugs 0.000 claims abstract description 6
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims abstract description 6
- 235000015320 potassium carbonate Nutrition 0.000 claims abstract description 6
- 239000002002 slurry Substances 0.000 claims description 22
- 238000000034 method Methods 0.000 claims description 10
- 238000000498 ball milling Methods 0.000 claims description 7
- 239000011248 coating agent Substances 0.000 claims description 7
- 238000000576 coating method Methods 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 230000000694 effects Effects 0.000 abstract description 11
- 239000004579 marble Substances 0.000 abstract description 11
- 230000016507 interphase Effects 0.000 abstract description 5
- 238000010304 firing Methods 0.000 description 10
- 238000001816 cooling Methods 0.000 description 5
- 238000005245 sintering Methods 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 4
- 239000002689 soil Substances 0.000 description 4
- 238000012986 modification Methods 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- DLHONNLASJQAHX-UHFFFAOYSA-N aluminum;potassium;oxygen(2-);silicon(4+) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Al+3].[Si+4].[Si+4].[Si+4].[K+] DLHONNLASJQAHX-UHFFFAOYSA-N 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 2
- 239000011505 plaster Substances 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 229910052793 cadmium Inorganic materials 0.000 description 1
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Structural Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Glass Compositions (AREA)
Abstract
The invention discloses a blue and white marbling glaze and a preparation method thereof, wherein the blue and white marbling glaze comprises white ground coat and blue overglaze which is smeared on the white ground coat to enable the glaze surface to form blue and white alternate stripes; wherein, the blue overglaze: 40-45% of potash feldspar, 4% of kaolin, 20-25% of quartz, 5-10% of dolomite, 15-20% of talcum, 5-10% of sodium borate, 1-2% of cobalt oxide and 0.1-0.15% of water glass; CMC: 0.2 percent; the total amount of the above is 100%; white ground coat: 45-50% of glass powder, 20-22% of kaolin, 25-30% of quartz, 3-5% of zirconium silicate and 0.1-0.15% of water glass; CMC: 0.1 percent. The above total is 100%. The glaze surface is bright and smooth, and the effect of clear and natural marble grains with blue and white interphase grains is presented.
Description
Technical Field
The invention relates to a blue and white marbled glaze and a preparation method thereof.
Background
At present, the traditional texturing treatment comprises a plurality of methods for forming marble grains, such as a color soil mud twisting method, wherein a plurality of color soils are mixed and molded in a rotary blank forming mode to form marble grains, and then transparent glaze is applied for sintering; or mixing several kinds of colored slurry, injecting into plaster mould, rotating plaster mould to form marble-like pattern, then applying transparent glaze and firing. The two methods can cause a large amount of colored waste soil, and the waste soil can not be recycled. The safety performance of the ceramic is studied in the ceramic industry, the lead and cadmium content is not over-standard, and the blue-white marbling glaze meets the regulation that the heavy metal standard is not over-standard.
Disclosure of Invention
The technical problem to be solved by the invention is to overcome the defects of the prior art and provide the blue-white marbling glaze which has bright and smooth glaze surface and presents the effect of clear and natural marbling of blue-white interphase grains.
In order to solve the technical problems, the technical scheme of the invention is as follows: a blue and white marbled glaze comprises a white ground glaze and a blue overglaze which is coated on the white ground glaze to form blue and white alternate stripes on the glaze surface; wherein,
blue overglaze: 40-45% of potash feldspar, 4% of kaolin, 20-25% of quartz, 5-10% of dolomite, 15-20% of talcum, 5-10% of sodium borate, 1-2% of cobalt oxide and 0.1-0.15% of water glass; CMC: 0.2 percent; the total amount of the above is 100%;
white ground coat: 45-50% of glass powder, 20-22% of kaolin, 25-30% of quartz, 3-5% of zirconium silicate and 0.1-0.15% of water glass; CMC: 0.1 percent. The above total is 100%.
The invention also provides a preparation method of the blue and white marbled glaze, which comprises the following steps:
preparing blue surface glaze slurry and white base glaze slurry;
applying white ground coat on the blank body by adopting white ground coat slip, and then coating blue overglaze on the white ground coat by adopting blue overglaze slip to form blue-white alternate stripes on the glaze surface;
putting the glazed green body into a kiln to be sintered at 1270 ℃; wherein,
the preparation process of the blue surface glaze slip and the white bottom glaze slip comprises the following steps:
preparing the materials according to the mass percent of each component;
wet ball milling is carried out for 20 hours according to the mass ratio of glaze to ball to water being 1 to 1.8 to 0.6, the ball milled glaze is sieved by a 250-mesh sieve, and the glaze slurry with Baume concentration of 50-52 is prepared for standby after the sieve residue is 0.1%.
After the technical scheme is adopted, the blue-white marbling glaze is bright and smooth in glaze surface, presents the marble line effect of clear and natural blue-white interphase lines, is coated with blue overglaze on white ground glaze, and forms the flow lines of the blue-white marble lines by the flowing of the blue glaze in the firing process. The sintering curve of quick sintering and natural cooling to room temperature is adopted.
Detailed Description
The invention provides a blue and white marble grain glaze and a preparation method thereof, and a person skilled in the art can use the contents for reference and appropriately improve the technological parameters to realize the blue and white marble grain glaze. It is expressly intended that all such similar substitutes and modifications apparent to those skilled in the art are deemed to be within the scope of the invention. While the methods and applications of this invention have been described in terms of preferred embodiments, it will be apparent to those of ordinary skill in the art that variations and modifications in the methods and applications described herein, as well as other suitable variations and combinations, may be made to implement and use the techniques of this invention without departing from the spirit and scope of the invention.
A blue and white marbled glaze comprises a white ground glaze and a blue overglaze which is coated on the white ground glaze to form blue and white alternate stripes on the glaze surface; wherein,
blue overglaze: 40-45% of potash feldspar, 4% of kaolin, 20-25% of quartz, 5-10% of dolomite, 15-20% of talcum, 5-10% of sodium borate, 1-2% of cobalt oxide and 0.1-0.15% of water glass; CMC: 0.2 percent; the total amount of the above is 100%;
white ground coat: 45-50% of glass powder, 20-22% of kaolin, 25-30% of quartz, 3-5% of zirconium silicate and 0.1-0.15% of water glass; CMC: 0.1 percent. The above total is 100%.
The preparation method of the blue and white marbled glaze comprises the following steps:
preparing blue surface glaze slurry and white base glaze slurry;
applying white ground coat on the blank body by adopting white ground coat slip, and then coating blue overglaze on the white ground coat by adopting blue overglaze slip to form blue-white alternate stripes on the glaze surface;
putting the glazed green body into a kiln to be sintered at 1270 ℃; wherein,
the preparation process of the blue surface glaze slip and the white bottom glaze slip comprises the following steps:
preparing the materials according to the mass percent of each component;
wet ball milling is carried out for 20 hours according to the mass ratio of glaze to ball to water being 1 to 1.8 to 0.6, the ball milled glaze is sieved by a 250-mesh sieve, and the glaze slurry with Baume concentration of 50-52 is prepared for standby after the sieve residue is 0.1%.
After the technical scheme is adopted, the blue-white marbling glaze is bright and smooth in glaze surface, presents the marble line effect of clear and natural blue-white interphase lines, is coated with blue overglaze on white ground glaze, and forms the flow lines of the blue-white marble lines by the flowing of the blue glaze in the firing process. The sintering curve of quick sintering and natural cooling to room temperature is adopted.
In order that the present invention may be more clearly understood, the following detailed description of the present invention is given with reference to specific examples.
Comparative example 1
A blue and white marbled glaze comprises a white ground glaze and a blue overglaze which is coated on the white ground glaze to form blue and white alternate stripes on the glaze surface; wherein,
blue overglaze: 40% of potash feldspar, 4% of kaolin, 29.7% of quartz, 5% of dolomite, 15% of talc, 5% of sodium borate, 1% of cobalt oxide and 0.1% of water glass; CMC: 0.2 percent;
white ground coat: 47% of glass powder, 20% of kaolin, 29.8% of quartz, 3% of zirconium silicate and 0.1% of water glass; CMC: 0.1 percent.
The preparation method of the blue and white marbled glaze comprises the following steps:
preparing blue surface glaze slurry and white base glaze slurry;
applying white ground coat on the blank body by adopting white ground coat slip, and then coating blue overglaze on the white ground coat by adopting blue overglaze slip to form blue-white alternate stripes on the glaze surface;
putting the glazed green body into a kiln to be sintered at 1250 ℃; wherein,
the preparation process of the blue surface glaze slip and the white bottom glaze slip comprises the following steps:
preparing the materials according to the mass percent of each component;
wet ball milling is carried out for 20 hours according to the mass ratio of glaze to ball to water being 1 to 1.8 to 0.6, the ball milled glaze is sieved by a 250-mesh sieve, and the glaze slurry with Baume concentration of 50-52 is prepared for standby after the sieve residue is 0.1%.
The specific firing data for this comparative example is as follows:
| 0～420℃ | 420～720℃ | 720～980℃ | 980～1250℃ | 1250℃ | 1250 to room temperature DEG C |
| 90 minutes | 90 minutes | 30 minutes | 200 minutes | 20 minutes | Natural cooling |
And (3) firing result: the glaze is matt, blue is not obvious, the texture effect is relatively rigid, and the design requirement is not met.
Comparative example No. two
A blue and white marbled glaze comprises a white ground glaze and a blue overglaze which is coated on the white ground glaze to form blue and white alternate stripes on the glaze surface; wherein,
blue overglaze: 44% of potassium feldspar, 4% of kaolin, 24.65% of quartz, 5% of dolomite, 15% of talc, 5% of sodium borate, 2% of cobalt oxide and 0.15% of water glass; CMC: 0.2 percent;
white ground coat: 46% of glass powder, 21% of kaolin, 27.75% of quartz, 5% of zirconium silicate and 0.15% of water glass; CMC: 0.1 percent.
The preparation method of the blue and white marbled glaze comprises the following steps:
preparing blue surface glaze slurry and white base glaze slurry;
applying white ground coat on the blank body by adopting white ground coat slip, and then coating blue overglaze on the white ground coat by adopting blue overglaze slip to form blue-white alternate stripes on the glaze surface;
putting the glazed green body into a kiln to be sintered at 1260 ℃; wherein,
the preparation process of the blue surface glaze slip and the white bottom glaze slip comprises the following steps:
preparing the materials according to the mass percent of each component;
wet ball milling is carried out for 20 hours according to the mass ratio of glaze to ball to water being 1 to 1.8 to 0.6, the ball milled glaze is sieved by a 250-mesh sieve, and the glaze slurry with Baume concentration of 50-52 is prepared for standby after the sieve residue is 0.1%.
The specific firing data for this comparative example is as follows:
| 0～420℃ | 420～720℃ | 720～980℃ | 980～1260℃ | 1260℃ | 1260-room temperature DEG C |
| 90 minutes | 90 minutes | 30 minutes | 200 minutes | 20 minutes | Natural cooling |
And (3) firing result: the glaze is bright, the blue and white effect is deepened, but the glaze is not clear and natural enough, has glaze color flowing texture and does not meet the design requirement.
Example one
A blue and white marbled glaze comprises a white ground glaze and a blue overglaze which is coated on the white ground glaze to form blue and white alternate stripes on the glaze surface; wherein,
blue overglaze: 40% of potash feldspar, 4% of kaolin, 29.7% of quartz, 5% of dolomite, 15% of talc, 5% of sodium borate, 1% of cobalt oxide and 0.1% of water glass; CMC: 0.2 percent;
white ground coat: 47% of glass powder, 20% of kaolin, 29.8% of quartz, 3% of zirconium silicate and 0.1% of water glass; CMC: 0.1 percent.
The preparation method of the blue and white marbled glaze comprises the following steps:
preparing blue surface glaze slurry and white base glaze slurry;
applying white ground coat on the blank body by adopting white ground coat slip, and then coating blue overglaze on the white ground coat by adopting blue overglaze slip to form blue-white alternate stripes on the glaze surface;
putting the glazed green body into a kiln to be sintered at 1270 ℃; wherein,
the preparation process of the blue surface glaze slip and the white bottom glaze slip comprises the following steps:
preparing the materials according to the mass percent of each component;
wet ball milling is carried out for 20 hours according to the mass ratio of glaze to ball to water being 1 to 1.8 to 0.6, the ball milled glaze is sieved by a 250-mesh sieve, and the glaze slurry with Baume concentration of 50-52 is prepared for standby after the sieve residue is 0.1%.
Example two
A blue and white marbled glaze comprises a white ground glaze and a blue overglaze which is coated on the white ground glaze to form blue and white alternate stripes on the glaze surface; wherein,
blue overglaze: 44% of potassium feldspar, 4% of kaolin, 24.65% of quartz, 5% of dolomite, 15% of talc, 5% of sodium borate, 2% of cobalt oxide and 0.15% of water glass; CMC: 0.2 percent;
white ground coat: 46% of glass powder, 21% of kaolin, 27.75% of quartz, 5% of zirconium silicate and 0.15% of water glass; CMC: 0.1 percent.
The preparation method of the blue and white marbled glaze comprises the following steps:
preparing blue surface glaze slurry and white base glaze slurry;
applying white ground coat on the blank body by adopting white ground coat slip, and then coating blue overglaze on the white ground coat by adopting blue overglaze slip to form blue-white alternate stripes on the glaze surface;
putting the glazed green body into a kiln to be sintered at 1270 ℃; wherein,
the preparation process of the blue surface glaze slip and the white bottom glaze slip comprises the following steps:
preparing the materials according to the mass percent of each component;
wet ball milling is carried out for 20 hours according to the mass ratio of glaze to ball to water being 1 to 1.8 to 0.6, the ball milled glaze is sieved by a 250-mesh sieve, and the glaze slurry with Baume concentration of 50-52 is prepared for standby after the sieve residue is 0.1%.
The specific firing data for examples one and two are shown in the following table:
| 0～420℃ | 420～720℃ | 720～980℃ | 980～1270℃ | 1270℃ | 1270-room temperature DEG C |
| 90 minutes | 90 minutes | 30 minutes | 200 minutes | 20 minutes | Natural cooling |
Firing results for examples one and two: the glaze surface is bright and smooth, presents the effect of clear and natural marble grains of blue and white interphase grains, and meets the design requirement.
The blue glaze is colored by adding cobalt oxide into common feldspar base glaze, and the glaze color firing is more stable. The white glaze has fluidity and is adjusted by adding 35-39%, 45-50% and 51-55% of strong flux glass powder, 35-39% of glass powder has no flowing effect, 51-55% of glass powder has too much glass powder, the flowing effect is too strong, the marble grain effect with clear and natural grains can not be obtained, and 45-50% of glass powder just obtains the best effect in a slight flowing state; in addition, the depth of blue and white is controlled by adjusting the amount of cobalt oxide and zirconium silicate.
The above embodiments are described in further detail to solve the technical problems, technical solutions and advantages of the present invention, and it should be understood that the above embodiments are only examples of the present invention and are not intended to limit the present invention, and any modifications, equivalent substitutions, improvements and the like made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (2)
1. The blue-white marbled glaze is characterized by comprising a white base glaze and a blue overglaze which is coated on the white base glaze to enable glaze surfaces to form blue-white alternate stripes; wherein,
blue overglaze: 40-45% of potash feldspar, 4% of kaolin, 20-25% of quartz, 5-10% of dolomite, 15-20% of talcum, 5-10% of sodium borate, 1-2% of cobalt oxide and 0.1-0.15% of water glass; CMC: 0.2 percent; the total amount of the above is 100%;
white ground coat: 45-50% of glass powder, 20-22% of kaolin, 25-30% of quartz, 3-5% of zirconium silicate and 0.1-0.15% of water glass; CMC: 0.1 percent; the above total is 100%.
2. A method for preparing the blue and white marbled glaze according to claim 1, characterized in that the method comprises the steps of:
preparing blue surface glaze slurry and white base glaze slurry;
applying white ground coat on the blank body by adopting white ground coat slip, and then coating blue overglaze on the white ground coat by adopting blue overglaze slip to form blue-white alternate stripes on the glaze surface;
putting the glazed green body into a kiln to be sintered at 1270 ℃; wherein,
the preparation process of the blue surface glaze slip and the white bottom glaze slip comprises the following steps:
preparing the materials according to the mass percent of each component;
wet ball milling is carried out for 20 hours according to the mass ratio of glaze to ball to water being 1 to 1.8 to 0.6, the ball milled glaze is sieved by a 250-mesh sieve, and the glaze slurry with Baume concentration of 50-52 is prepared for standby after the sieve residue is 0.1%.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113308695A (en) * | 2021-05-26 | 2021-08-27 | 永康市江南搪瓷制品有限公司 | Enamel pot production process with high-gloss enamel glass enamel layer |
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