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CN111636146A - A kind of preparation method of non-woven fabric - Google Patents

A kind of preparation method of non-woven fabric Download PDF

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Publication number
CN111636146A
CN111636146A CN202010422472.1A CN202010422472A CN111636146A CN 111636146 A CN111636146 A CN 111636146A CN 202010422472 A CN202010422472 A CN 202010422472A CN 111636146 A CN111636146 A CN 111636146A
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China
Prior art keywords
spinning
raw material
parts
woven fabric
solution
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CN202010422472.1A
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Chinese (zh)
Inventor
朱英明
邱凯坤
孟思霖
蓝家平
杨振宝
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Jiangsu Clelo Material Technology Co ltd
Sichuan University
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Jiangsu Clelo Material Technology Co ltd
Sichuan University
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Priority to CN202010422472.1A priority Critical patent/CN111636146A/en
Publication of CN111636146A publication Critical patent/CN111636146A/en
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Classifications

    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/42Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
    • D04H1/4374Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece using different kinds of webs, e.g. by layering webs
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D1/00Treatment of filament-forming or like material
    • D01D1/10Filtering or de-aerating the spinning solution or melt
    • D01D1/106Filtering
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00General methods for the manufacture of artificial filaments or the like
    • D01F1/02Addition of substances to the spinning solution or to the melt
    • D01F1/10Other agents for modifying properties
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F8/00Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
    • D01F8/04Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
    • D01F8/06Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyolefin as constituent
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F8/00Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
    • D01F8/04Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
    • D01F8/08Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyacrylonitrile as constituent
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F8/00Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
    • D01F8/04Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
    • D01F8/10Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one other macromolecular compound obtained by reactions only involving carbon-to-carbon unsaturated bonds as constituent
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F8/00Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
    • D01F8/04Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
    • D01F8/14Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyester as constituent
    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/42Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
    • D04H1/4382Stretched reticular film fibres; Composite fibres; Mixed fibres; Ultrafine fibres; Fibres for artificial leather
    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H3/00Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length
    • D04H3/005Synthetic yarns or filaments
    • DTEXTILES; PAPER
    • D10INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10BINDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2401/00Physical properties
    • D10B2401/02Moisture-responsive characteristics
    • D10B2401/022Moisture-responsive characteristics hydrophylic

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Filtering Materials (AREA)
  • Nonwoven Fabrics (AREA)

Abstract

The invention discloses a preparation method of non-woven fabric, which comprises the following preparation steps: s1 preparing raw materials; s2 filtering; s3 spinning into a net; s4 carrying out solution jet spinning; s5 reinforcement and finishing; s6, drying; therefore, the non-woven fabric has fluffy feeling and thick feeling, the strength and the filtering capacity of the non-woven fabric are increased, the pressure drop is low, the melt-blown fabric can be replaced, and the production cost is reduced.

Description

一种无纺布的制备方法A kind of preparation method of non-woven fabric

技术领域technical field

本发明涉及无纺布生产技术领域,具体涉及一种无纺布的制备方法。The invention relates to the technical field of non-woven fabric production, in particular to a preparation method of a non-woven fabric.

背景技术Background technique

无纺布即非织造布,它是直接利用高聚物切片、短纤维或长丝将纤维通过气流或机械成网,然后经过溶液喷射纺丝、针刺或热乳加固,最后经过后整理形成的无编织的布料。纺粘无纺布:是将聚合物挤出、拉伸,形成连续长丝后,长丝铺设成网,纤网再经过自身粘合、热粘合、化学粘合或机械加固方法,使纤网变成无纺布;现有的纺粘无纺布的强力较低、过滤能力较差,压降高,因此,目前还无法替代熔喷布应用于空气、液体过滤材料、隔离材料、吸纳材料、口罩材料、保暖材料及擦拭布等领域。Non-woven fabrics are non-woven fabrics, which directly use polymer chips, short fibers or filaments to form fibers through air flow or machinery, and then are reinforced by solution jet spinning, needle punching or hot rolling, and finally formed after finishing. of non-woven fabrics. Spunbond non-woven fabric: After the polymer is extruded and stretched to form continuous filaments, the filaments are laid into a web, and the web is then self-bonded, thermally bonded, chemically bonded or mechanically reinforced to make the fibers The net becomes a non-woven fabric; the existing spunbond non-woven fabric has low strength, poor filtering ability, and high pressure drop. Therefore, it is currently unable to replace melt-blown cloth in air, liquid filter materials, isolation materials, absorption materials, etc. materials, mask materials, thermal insulation materials and wiping cloths and other fields.

发明内容SUMMARY OF THE INVENTION

为解决上述技术问题,本发明的目的在于提供一种无纺布的制备方法,不仅能够使无纺布具有蓬松感、厚实感,更增加无纺布的强力和过滤能力,其压降较低,可以替代熔喷布,降低了生产成本。In order to solve the above-mentioned technical problems, the purpose of the present invention is to provide a preparation method of a non-woven fabric, which can not only make the non-woven fabric have a fluffy and thick feeling, but also increase the strength and filtering ability of the non-woven fabric, and its pressure drop is relatively low. , which can replace the meltblown cloth and reduce the production cost.

为达到上述目的,本发明的技术方案如下:For achieving the above object, technical scheme of the present invention is as follows:

一种无纺布的制备方法,包括以下制备步骤:A preparation method of non-woven fabric, comprising the following preparation steps:

S1原料准备:将原料a混合后经过螺杆挤压机进行挤压熔融得到熔体a,原料b溶于溶剂后加入溶液喷射纺丝机的溶解釜内,经搅拌形成纺丝液b;S1 Raw material preparation: After mixing the raw material a, it is extruded and melted by a screw extruder to obtain a melt a, and the raw material b is dissolved in a solvent and then added to the dissolving kettle of the solution jet spinning machine, and a spinning solution b is formed by stirring;

S2过滤:将S1步骤中所得到的制备熔体a和纺丝液b分别经过滤器过滤去除杂质,然后分别进入纺丝组件;S2 Filtration: The prepared melt a and the spinning solution b obtained in the S1 step are filtered through a filter to remove impurities, respectively, and then enter the spinning assembly respectively;

S3纺丝成网:将S2步骤中过滤后的熔体a和纺丝液b分别采用计量泵定量送入纺丝组件,经纺丝机喷丝板喷出后,冷却固结成丝,丝束导入牵伸喷嘴经过气流牵引,在成网机上铺网得到纤维网A;S3 spinning into a web: the melt a and the spinning solution b filtered in the S2 step are respectively quantitatively fed into the spinning assembly by a metering pump, and after being ejected from the spinneret of the spinning machine, they are cooled and consolidated into filaments. The bundle is introduced into the drafting nozzle and drawn by the air stream, and the fiber web A is obtained by laying the web on the web forming machine;

S4溶液喷射纺丝:将S3步骤中纤维网A送入溶液喷射接受网,纺丝液b采用计量泵定量送入纺丝组件,经纺丝机喷丝板喷出后,丝束导入牵伸喷嘴经过气流牵引,在纤维网A上冷却固结成丝,在成网机上铺网得到纤维网B;S4 solution jet spinning: the fiber web A in step S3 is sent into the solution jet receiving net, the spinning solution b is quantitatively fed into the spinning assembly by a metering pump, and after being ejected from the spinneret of the spinning machine, the tow is introduced into the drafting The nozzle is drawn by the airflow, cooled and consolidated into filaments on the fiber web A, and laid on the web forming machine to obtain the fiber web B;

S5加固整理:将S4步骤中所得到的纤维网B重叠进入溶液喷射纺丝区进行加固,得到无纺布;S5 reinforcement and finishing: the fiber web B obtained in the step S4 is overlapped into the solution jet spinning area for reinforcement to obtain a non-woven fabric;

S6烘燥:将S5步骤中经溶液喷射纺丝后的无纺布输入到烘箱中进行烘燥。S6 drying: the non-woven fabric after the solution jet spinning in step S5 is input into an oven for drying.

本发明提供的提供一种无纺布的制备方法,不仅能够使无纺布具有蓬松感、厚实感,更增加无纺布的强力和过滤能力,其压降较低,可以替代熔喷布,降低了生产成本。The invention provides a preparation method of non-woven fabric, which can not only make the non-woven fabric have a fluffy and thick feeling, but also increase the strength and filtering ability of the non-woven fabric, and its pressure drop is low, which can replace the melt-blown fabric. Reduced production costs.

在上述技术方案的基础上,本发明还可以作如下改进:On the basis of the above-mentioned technical scheme, the present invention can also be improved as follows:

作为优选方案,所述原料a与所述原料b的组分不同或所述原料a与所述原料b的组分相同。As a preferred solution, the components of the raw material a and the raw material b are different or the components of the raw material a and the raw material b are the same.

作为优选方案,当所述原料a与所述原料b的组分不同时,所述原料a由以下重量份的原料组成:聚丙烯81-86.5份、丙烯基弹性体12.5-16份、柔软母粒0.5-1.5份和二氧化钛0.5-1.5份;所述原料b由以下重量份的原料组成:聚乳酸10-70份和聚丙烯腈20-80份。As a preferred solution, when the components of the raw material a and the raw material b are different, the raw material a is composed of the following raw materials by weight: 81-86.5 parts of polypropylene, 12.5-16 parts of propylene-based elastomer, soft mother 0.5-1.5 parts of particles and 0.5-1.5 parts of titanium dioxide; the raw material b is composed of the following raw materials by weight: 10-70 parts of polylactic acid and 20-80 parts of polyacrylonitrile.

作为优选方案,当所述原料a与所述原料b的组分相同时,所述原料a由以下重量份的原料组成:聚乳酸10-70份和聚丙烯腈20-80份;所述原料b由以下重量份的原料组成:聚乳酸10-70份和聚丙烯腈20-80份。As a preferred solution, when the components of the raw material a and the raw material b are the same, the raw material a is composed of the following raw materials in parts by weight: 10-70 parts of polylactic acid and 20-80 parts of polyacrylonitrile; the raw material b is composed of the following raw materials in parts by weight: 10-70 parts of polylactic acid and 20-80 parts of polyacrylonitrile.

作为优选方案,S3步骤和S4步骤中溶液喷射纺丝头的控制溶液喷射气流牵引风压力分别为2bar-70bar。As a preferred solution, in the step S3 and the step S4, the control solution jet air draught air pressure of the solution jet spinning head is 2bar-70bar, respectively.

作为优选方案,S5步骤中将完成溶液喷射纺丝得到的无纺布进行亲水处理。As a preferred solution, in step S5, the non-woven fabric obtained by completing the solution jet spinning is subjected to hydrophilic treatment.

作为优选方案,亲水剂和纯净水按重量比1比150混合搅拌获得亲水处理步骤中使用的亲水处理液。As a preferred solution, the hydrophilic treatment liquid used in the hydrophilic treatment step is obtained by mixing and stirring the hydrophilic agent and purified water in a weight ratio of 1 to 150.

作为优选方案,S6步骤中烘燥采用在第一道烘箱中对无纺布进行预烘燥,预烘燥后无纺布进入第二道烘箱中进行烘燥。As a preferred solution, in the drying step S6, the non-woven fabric is pre-dried in the first oven, and the non-woven fabric enters the second oven for drying after pre-drying.

作为优选方案,在一道烘箱中进行预烘燥的温度为

Figure BDA0002496558720000031
在第二道烘箱中进行烘燥的温度为
Figure BDA0002496558720000032
As a preferred solution, the temperature for pre-drying in an oven is
Figure BDA0002496558720000031
The drying temperature in the second oven is
Figure BDA0002496558720000032

作为优选方案,S2步骤过滤器过滤采用预过滤和精过滤的二级过滤方式,预过滤的粒径小于80um,精过滤的粒径小于30um。As a preferred solution, the S2 step filter filtration adopts the secondary filtration method of pre-filtration and fine filtration, the particle size of pre-filtration is less than 80um, and the particle size of fine filtration is less than 30um.

具体实施方式Detailed ways

下面将对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有作出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。The technical solutions in the embodiments of the present invention will be described clearly and completely below. Obviously, the described embodiments are only a part of the embodiments of the present invention, rather than all the embodiments. Based on the embodiments of the present invention, all other embodiments obtained by those of ordinary skill in the art without creative efforts shall fall within the protection scope of the present invention.

除非特别指明,以下实施例中所用的试剂均可从正规渠道商购获得。Unless otherwise specified, the reagents used in the following examples can be obtained commercially from regular channels.

为了达到本发明的目的,本发明提供的一种无纺布的制备方法,包括以下步骤:In order to achieve the purpose of the present invention, a kind of preparation method of non-woven fabric provided by the present invention comprises the following steps:

S1原料准备:将原料a混合后喂入料斗中,混合后原料a经过双螺杆挤压机进行挤压熔融得到熔体a,原料a由以下重量份的原料组成:聚丙烯81份、丙烯基弹性体12.5份、柔软母粒0.5份、二氧化钛0.5份;原料b溶于溶剂后加入溶液喷射纺丝机的溶解釜内,经搅拌形成纺丝液b;;原料b由以下重量份的原料组成:聚乳酸10份和聚丙烯腈20份;S1 Raw material preparation: Mix the raw material a and feed it into the hopper. After mixing, the raw material a is extruded and melted by a twin-screw extruder to obtain melt a. The raw material a is composed of the following raw materials by weight: 81 parts of polypropylene, propylene-based 12.5 parts of elastomers, 0.5 parts of soft masterbatch, and 0.5 parts of titanium dioxide; the raw material b is dissolved in the solvent and then added to the dissolving kettle of the solution jet spinning machine, and the spinning solution b is formed by stirring; the raw material b is composed of the following parts by weight of raw materials : 10 parts of polylactic acid and 20 parts of polyacrylonitrile;

S2熔融过滤:将S1步骤中所得到的熔体a、纺丝液b分别经过滤器过滤在线去除杂质,然后进入纺丝组件,过滤器在线过滤去除杂质采用预过滤和精过滤的二级过滤方式,预过滤的精度小于80um,精过滤的精度小于30um;S2 Melt Filtration: The melt a and spinning solution b obtained in step S1 are filtered through filters to remove impurities online respectively, and then enter the spinning assembly. The filters are filtered online to remove impurities using a secondary filtration method of pre-filtration and fine filtration. , the precision of pre-filtering is less than 80um, and the precision of fine-filtering is less than 30um;

S3纺丝成网:将S2步骤中过滤后的熔体a采用计量泵定量送入纺丝组件,经纺丝机喷丝板喷出后,冷却固结成丝,丝束导入牵伸喷嘴经过气流牵引,溶液喷射牵引风压力为50bar,在成网机上铺网分别得到纤维网A;S3 spinning into a web: the melt a filtered in step S2 is quantitatively fed into the spinning assembly by a metering pump, and after being ejected from the spinneret of the spinning machine, it is cooled and consolidated into filaments, and the tow is introduced into the drafting nozzle through the Airflow traction, solution jet traction wind pressure is 50bar, and fiber webs A are obtained by laying webs on the web forming machine;

S4溶液喷射纺丝:将S3步骤中纤维网A送入溶液喷射接受网,纺丝液b采用计量泵定量送入纺丝组件,经纺丝机喷丝板喷出后,丝束导入牵伸喷嘴经过气流牵引,溶液喷射牵引风压力为50bar,在纤维网A上冷却固结成丝,在成网机上铺网得到纤维网B;S4 solution jet spinning: the fiber web A in step S3 is sent into the solution jet receiving net, the spinning solution b is quantitatively fed into the spinning assembly by a metering pump, and after being ejected from the spinneret of the spinning machine, the tow is introduced into the drafting The nozzle is drawn by air flow, and the solution is sprayed with a pulling air pressure of 50 bar, cooled and consolidated into filaments on the fiber web A, and laid on the web forming machine to obtain the fiber web B;

S5加固整理:将S4步骤中所得到的纤维网B重叠进入溶液喷射纺丝区进行加固,得到无纺布,将无纺布表层进行亲水处理,亲水处理的处理液为亲水剂和纯净水按重量比1比150混合搅拌成液态状,加温至53℃。S5 reinforcement finishing: the fiber web B obtained in the step S4 is overlapped into the solution jet spinning area for reinforcement to obtain a non-woven fabric, and the surface layer of the non-woven fabric is subjected to hydrophilic treatment, and the treatment liquid for the hydrophilic treatment is a hydrophilic agent and a Pure water is mixed and stirred into a liquid state according to the weight ratio of 1:150, and heated to 53°C.

S6烘燥:将S5步骤中经亲水处理后的无纺布通过带液滚传输至烘箱中进行至少两次烘燥,首先在第一道烘箱中对无纺布进行预烘燥,在第一道烘箱中预烘燥温度为105℃;预烘燥后无纺布进入第二道烘箱中进行烘燥,第二道烘箱烘燥温度为110℃,经卷绕机切边、成卷,包装出厂。S6 drying: the non-woven fabric after the hydrophilic treatment in step S5 is transported to the oven for at least two times by rolling with liquid. First, the non-woven fabric is pre-dried in the first oven, and the The pre-drying temperature in the first oven is 105°C; after the pre-drying, the non-woven fabric enters the second oven for drying, and the drying temperature of the second oven is 110°C. Factory packing.

本实施例采用先纺粘铺网再溶液喷射纺丝进行无纺布1的生产,能够使无纺布1具有蓬松感、厚实感,增加无纺布1的强力、过滤能力,可以替代熔喷布降低生产成本,本实施例中对无纺布1的表层进行亲水处理,能够有效的提高无纺布1的亲水性。In this embodiment, the non-woven fabric 1 is produced by first spunbonding and then solution jet spinning, which can make the non-woven fabric 1 have a fluffy and thick feeling, increase the strength and filtering ability of the non-woven fabric 1, and can replace the melt-blown The cloth reduces the production cost. In this embodiment, the surface layer of the non-woven fabric 1 is subjected to hydrophilic treatment, which can effectively improve the hydrophilicity of the non-woven fabric 1 .

本发明提供的一种无纺布的制备方法,包括以下步骤:The preparation method of a kind of non-woven fabric provided by the invention comprises the following steps:

S1原料准备:将原料a混合后喂入料斗中,混合后原料a经过双螺杆挤压机进行挤压熔融得到熔体a,原料a由以下重量份的原料组成:聚丙烯86.5份、丙烯基弹性体16份、柔软母粒1.5份和二氧化钛1.5份;原料b溶于溶剂后加入溶液喷射纺丝机的溶解釜内,经搅拌形成纺丝液b;;原料b由以下重量份的原料组成:聚乳酸70份和聚丙烯腈80份;S1 Raw material preparation: Mix the raw material a and feed it into the hopper. After mixing, the raw material a is extruded and melted by a twin-screw extruder to obtain melt a. The raw material a is composed of the following raw materials by weight: 86.5 parts of polypropylene, propylene-based 16 parts of elastomer, 1.5 parts of soft masterbatch and 1.5 parts of titanium dioxide; raw material b is dissolved in a solvent and added to the dissolving kettle of the solution jet spinning machine, and a spinning solution b is formed by stirring; raw material b is composed of the following parts by weight of raw materials : 70 parts of polylactic acid and 80 parts of polyacrylonitrile;

S2熔融过滤:将S1步骤中所得到的熔体a、纺丝液b分别经过滤器在线去除杂质,然后进入纺丝组件,过滤器在线去除杂质采用预过滤和精过滤的二级过滤方式,预过滤的精度小于80um,精过滤的精度小于30um;S2 melt filtration: the melt a and spinning solution b obtained in step S1 are respectively removed from impurities online through the filter, and then enter the spinning assembly. The precision of filtration is less than 80um, and the precision of fine filtration is less than 30um;

S3纺丝成网:将S2步骤中过滤后的熔体a采用计量泵定量送入纺丝组件,经纺丝机喷丝板喷出后,冷却固结成丝,丝束导入牵伸喷嘴经过气流牵引,溶液喷射牵引风压力为70bar,在成网机上铺网分别得到纤维网A;S3 spinning into a web: the melt a filtered in step S2 is quantitatively fed into the spinning assembly by a metering pump, and after being ejected from the spinneret of the spinning machine, it is cooled and consolidated into filaments, and the tow is introduced into the drafting nozzle through the Airflow traction, solution jet traction wind pressure is 70bar, and fiber webs A are obtained by laying webs on the web forming machine;

S4溶液喷射纺丝:将S3步骤中纤维网A送入溶液喷射接受网,纺丝液b采用计量泵定量送入纺丝组件,经纺丝机喷丝板喷出后,丝束导入牵伸喷嘴经过气流牵引,溶液喷射牵引风压力为70bar,在纤维网A上冷却固结成丝,在成网机上铺网得到纤维网B;S4 solution jet spinning: the fiber web A in step S3 is sent into the solution jet receiving net, the spinning solution b is quantitatively fed into the spinning assembly by a metering pump, and after being ejected from the spinneret of the spinning machine, the tow is introduced into the drafting The nozzle is drawn by air flow, and the solution is sprayed with a pulling air pressure of 70 bar, cooled and consolidated into filaments on the fiber web A, and laid on the web forming machine to obtain the fiber web B;

S5加固整理:将S4步骤中所得到的纤维网B重叠进入溶液喷射纺丝区进行加固,得到无纺布,将无纺布表层进行亲水处理,亲水处理的处理液为亲水剂和纯净水按重量比1比150混合搅拌成液态状,加温至53℃;S5 reinforcement finishing: the fiber web B obtained in the step S4 is overlapped into the solution jet spinning area for reinforcement to obtain a non-woven fabric, and the surface layer of the non-woven fabric is subjected to hydrophilic treatment, and the treatment liquid for the hydrophilic treatment is a hydrophilic agent and a Pure water is mixed and stirred into a liquid state according to the weight ratio of 1:150, and heated to 53°C;

S6烘燥:将S5步骤中经亲水处理后的无纺布通过带液滚传输至烘箱中进行至少两次烘燥,首先在第一道烘箱中对无纺布进行预烘燥,在第一道烘箱中预烘燥温度为125℃;预烘燥后无纺布进入第二道烘箱中进行烘燥,第二道烘箱烘燥温度为130℃,经卷绕机切边、成卷,包装出厂。S6 drying: the non-woven fabric after the hydrophilic treatment in step S5 is transported to the oven for at least two times by rolling with liquid. First, the non-woven fabric is pre-dried in the first oven, and the The pre-drying temperature in the first oven is 125°C; after pre-drying, the non-woven fabric enters the second oven for drying, and the drying temperature of the second oven is 130°C. Factory packing.

本实施例采用先纺粘铺网再溶液喷射纺丝进行无纺布2的生产,能够使无纺布2具有蓬松感、厚实感,增加无纺布2的强力、过滤能力,可以替代熔喷布降低生产成本,本实施例中对无纺布2的表层做亲水处理,能够有效的提高无纺布2的亲水性。In this embodiment, the non-woven fabric 2 is produced by first spunbonding and then solution jet spinning, which can make the non-woven fabric 2 have a fluffy and thick feeling, increase the strength and filtering ability of the non-woven fabric 2, and can replace the melt-blown In this embodiment, the surface layer of the non-woven fabric 2 is subjected to hydrophilic treatment, which can effectively improve the hydrophilicity of the non-woven fabric 2 .

本发明提供的一种无纺布的制备方法,包括以下步骤:The preparation method of a kind of non-woven fabric provided by the invention comprises the following steps:

S1原料准备:将原料a混合后喂入料斗中,混合后原料a经过双螺杆挤压机进行挤压熔融得到熔体a,原料a由以下重量份的原料组成:聚丙烯83.75份、丙烯基弹性体14.25份、柔软母粒1.0份和二氧化钛1.0份;原料b溶于溶剂后加入溶液喷射纺丝机的溶解釜内,经搅拌形成纺丝液b;;原料b由以下重量份的原料组成:聚乳酸40份和聚丙烯腈50份;S1 Raw material preparation: Mix the raw material a and feed it into the hopper. After mixing, the raw material a is extruded and melted by a twin-screw extruder to obtain melt a. The raw material a is composed of the following raw materials by weight: 83.75 parts of polypropylene, propylene-based 14.25 parts of elastomer, 1.0 part of soft masterbatch and 1.0 part of titanium dioxide; raw material b is dissolved in a solvent and added to the dissolving kettle of the solution jet spinning machine, and a spinning solution b is formed by stirring; raw material b is composed of the following parts by weight of raw materials : 40 parts of polylactic acid and 50 parts of polyacrylonitrile;

S2熔融过滤:将S1步骤中所得到的熔体a、纺丝液b分别经过滤器在线过滤去除杂质,然后进入纺丝组件,过滤器在线过滤去除杂质采用预过滤和精过滤的二级过滤方式,预过滤的精度小于80um,精过滤的精度小于30um;S2 Melt filtration: the melt a and spinning solution b obtained in step S1 are respectively filtered online to remove impurities through the filter, and then enter the spinning assembly. , the precision of pre-filtering is less than 80um, and the precision of fine-filtering is less than 30um;

S3纺丝成网:将S2步骤中过滤后的熔体a采用计量泵定量送入纺丝组件,经纺丝机喷丝板喷出后,冷却固结成丝,丝束导入牵伸喷嘴经过气流牵引,溶液喷射牵引风压力为2bar,在成网机上铺网分别得到纤维网A;S3 spinning into a web: the melt a filtered in step S2 is quantitatively fed into the spinning assembly by a metering pump, and after being ejected from the spinneret of the spinning machine, it is cooled and consolidated into filaments, and the tow is introduced into the drafting nozzle through the Airflow traction, solution jet traction wind pressure is 2bar, and fiber webs A are obtained by laying webs on the web forming machine;

S4溶液喷射纺丝:将S3步骤中纤维网A送入溶液喷射接受网,纺丝液b采用计量泵定量送入纺丝组件,经纺丝机喷丝板喷出后,丝束导入牵伸喷嘴经过气流牵引,溶液喷射牵引风压力为2bar,在纤维网A上冷却固结成丝,在成网机上铺网得到纤维网B;S4 solution jet spinning: the fiber web A in step S3 is sent into the solution jet receiving net, the spinning solution b is quantitatively fed into the spinning assembly by a metering pump, and after being ejected from the spinneret of the spinning machine, the tow is introduced into the drafting The nozzle is drawn by air flow, and the solution is sprayed with a pulling air pressure of 2 bar, which is cooled and consolidated into filaments on the fiber web A, and the fiber web B is obtained by laying the web on the web forming machine;

S5加固整理:将S4步骤中所得到的纤维网B重叠进入溶液喷射纺丝区进行加固,得到无纺布,将无纺布表层进行亲水处理,亲水处理的处理液为亲水剂和纯净水按重量比1比150混合搅拌成液态状,加温至53℃;S5 reinforcement finishing: the fiber web B obtained in the step S4 is overlapped into the solution jet spinning area for reinforcement to obtain a non-woven fabric, and the surface layer of the non-woven fabric is subjected to hydrophilic treatment, and the treatment liquid for the hydrophilic treatment is a hydrophilic agent and a Pure water is mixed and stirred into a liquid state according to the weight ratio of 1:150, and heated to 53°C;

S6烘燥:将S5步骤中经亲水处理后的无纺布通过带液滚传输至烘箱中进行至少两次烘燥,首先在第一道烘箱中对无纺布进行预烘燥,在第一道烘箱中预烘燥温度为112℃;预烘燥后无纺布进入第二道烘箱中进行烘燥,第二道烘箱烘燥温度为142℃,经卷绕机切边、成卷,包装出厂。S6 drying: the non-woven fabric after the hydrophilic treatment in step S5 is transported to the oven for at least two times by rolling with liquid. First, the non-woven fabric is pre-dried in the first oven, and the The pre-drying temperature in the first oven is 112°C; after pre-drying, the non-woven fabric enters the second oven for drying, and the second oven drying temperature is 142°C, and is trimmed and rolled by the winder. Factory packing.

本实施例采用先纺粘铺网再溶液喷射纺丝进行无纺布3的生产,能够使无纺布3具有蓬松感、厚实感,增加无纺布的强力、过滤能力,可以替代熔喷布降低生产成本,对无纺布的表层做亲水处理,能够有效的提高无纺布的亲水性。In this embodiment, the non-woven fabric 3 is produced by first spunbonding and then solution jet spinning, which can make the non-woven fabric 3 have a fluffy and thick feeling, increase the strength and filtering ability of the non-woven fabric, and can replace the melt-blown fabric. To reduce the production cost, the hydrophilic treatment of the surface layer of the non-woven fabric can effectively improve the hydrophilicity of the non-woven fabric.

本发明提供的一种无纺布的制备方法,包括以下步骤:The preparation method of a kind of non-woven fabric provided by the invention comprises the following steps:

S1原料准备:将原料a混合后喂入料斗中,混合后原料a经过双螺杆挤压机进行挤压熔融得到熔体a,原料a由以下重量份的原料组成:聚乳酸10份和聚丙烯腈20份;原料b溶于溶剂后加入溶液喷射纺丝机的溶解釜内,经搅拌形成纺丝液b;;原料b由以下重量份的原料组成:聚乳酸10份和聚丙烯腈20份;S1 Raw material preparation: Mix the raw material a and feed it into the hopper. After mixing, the raw material a is extruded and melted by a twin-screw extruder to obtain a melt a. The raw material a is composed of the following raw materials by weight: 10 parts of polylactic acid and polypropylene 20 parts of nitrile; after the raw material b is dissolved in the solvent, it is added to the dissolving kettle of the solution jet spinning machine, and the spinning solution b is formed by stirring; the raw material b is composed of the following raw materials by weight: 10 parts of polylactic acid and 20 parts of polyacrylonitrile ;

S2熔融过滤:将S1步骤中所得到的熔体a、纺丝液b分别经过滤器在线过滤去除杂质,然后进入纺丝组件,过滤器在线过滤去除杂质采用预过滤和精过滤的二级过滤方式,预过滤的精度小于80um,精过滤的精度小于30um;S2 Melt filtration: the melt a and spinning solution b obtained in step S1 are respectively filtered online to remove impurities through the filter, and then enter the spinning assembly. , the precision of pre-filtering is less than 80um, and the precision of fine-filtering is less than 30um;

S3纺丝成网:将S2步骤中过滤后的熔体a采用计量泵定量送入纺丝组件,经纺丝机喷丝板喷出后,冷却固结成丝,丝束导入牵伸喷嘴经过气流牵引,在成网机上铺网分别得到纤维网A;S3 spinning into a web: the melt a filtered in step S2 is quantitatively fed into the spinning assembly by a metering pump, and after being ejected from the spinneret of the spinning machine, it is cooled and consolidated into filaments, and the tow is introduced into the drafting nozzle through the Air-drafting, laying the web on the web forming machine to obtain the fiber web A;

S4溶液喷射纺丝:将S3步骤中纤维网A送入溶液喷射接受网,纺丝液b采用计量泵定量送入纺丝组件,经纺丝机喷丝板喷出后,丝束导入牵伸喷嘴经过气流牵引,溶液喷射牵引风压力为50bar,在纤维网A上冷却固结成丝,在成网机上铺网得到纤维网B;S4 solution jet spinning: the fiber web A in step S3 is sent into the solution jet receiving net, the spinning solution b is quantitatively fed into the spinning assembly by a metering pump, and after being ejected from the spinneret of the spinning machine, the tow is introduced into the drafting The nozzle is drawn by air flow, and the solution is sprayed with a pulling air pressure of 50 bar, cooled and consolidated into filaments on the fiber web A, and laid on the web forming machine to obtain the fiber web B;

S5加固整理:将S4步骤中所得到的纤维网B重叠进入溶液喷射纺丝区进行加固,得到无纺布,将无纺布表层进行亲水处理,亲水处理的处理液为亲水剂和纯净水按重量比1比150混合搅拌成液态状,加温至53℃;S5 reinforcement finishing: the fiber web B obtained in the step S4 is overlapped into the solution jet spinning area for reinforcement to obtain a non-woven fabric, and the surface layer of the non-woven fabric is subjected to hydrophilic treatment, and the treatment liquid for the hydrophilic treatment is a hydrophilic agent and a Pure water is mixed and stirred into a liquid state according to the weight ratio of 1:150, and heated to 53°C;

S6烘燥:将S5步骤中经亲水处理后的无纺布通过带液滚传输至烘箱中进行至少两次烘燥,首先在第一道烘箱中对无纺布进行预烘燥,在第一道烘箱中预烘燥温度为105℃;预烘燥后无纺布进入第二道烘箱中进行烘燥,第二道烘箱烘燥温度为110℃,经卷绕机切边、成卷,包装出厂。S6 drying: the non-woven fabric after the hydrophilic treatment in step S5 is transported to the oven for at least two times by rolling with liquid. First, the non-woven fabric is pre-dried in the first oven, and the The pre-drying temperature in the first oven is 105°C; after the pre-drying, the non-woven fabric enters the second oven for drying, and the drying temperature of the second oven is 110°C. Factory packing.

本实施例采用先纺粘铺网再溶液喷射纺丝进行无纺布4的生产,能够使无纺布4具有蓬松感、厚实感,增加无纺布4的强力、过滤能力,可以替代熔喷布降低生产成本,本实施例中对无纺布4的表层做亲水处理,能够有效的提高无纺布的亲水性。In this embodiment, the non-woven fabric 4 is produced by first spunbonding and then solution jet spinning, which can make the non-woven fabric 4 have a fluffy and thick feeling, increase the strength and filtering ability of the non-woven fabric 4, and can replace the melt-blown In this embodiment, the surface layer of the non-woven fabric 4 is subjected to hydrophilic treatment, which can effectively improve the hydrophilicity of the non-woven fabric.

本发明提供的一种无纺布的制备方法,包括以下步骤:The preparation method of a kind of non-woven fabric provided by the invention comprises the following steps:

S1原料准备:将原料a混合后喂入料斗中,混合后原料a经过双螺杆挤压机进行挤压熔融得到熔体a,原料a由以下重量份的原料组成:聚乳酸70份和聚丙烯腈80份;原料b溶于溶剂后加入溶液喷射纺丝机的溶解釜内,经搅拌形成纺丝液b;;原料b由以下重量份的原料组成:聚乳酸70份和聚丙烯腈80份;S1 Raw material preparation: Mix the raw material a and feed it into the hopper. After mixing, the raw material a is extruded and melted by a twin-screw extruder to obtain melt a. The raw material a is composed of the following raw materials by weight: 70 parts of polylactic acid and polypropylene 80 parts of nitrile; the raw material b is dissolved in the solvent and added to the dissolving kettle of the solution jet spinning machine, and the spinning solution b is formed by stirring; the raw material b is composed of the following raw materials by weight: 70 parts of polylactic acid and 80 parts of polyacrylonitrile ;

S2熔融过滤:将S1步骤中所得到的熔体a、纺丝液b分别经过滤器在线过滤去除杂质,然后进入纺丝组件,过滤器在线过滤去除杂质采用预过滤和精过滤的二级过滤方式,预过滤的精度小于80um,精过滤的精度小于30um;S2 Melt filtration: the melt a and spinning solution b obtained in step S1 are respectively filtered online to remove impurities through the filter, and then enter the spinning assembly. , the precision of pre-filtering is less than 80um, and the precision of fine-filtering is less than 30um;

S3纺丝成网:将S2步骤中过滤后的熔体a采用计量泵定量送入纺丝组件,经纺丝机喷丝板喷出后,冷却固结成丝,丝束导入牵伸喷嘴经过气流牵引,在成网机上铺网分别得到纤维网A;S3 spinning into a web: the melt a filtered in step S2 is quantitatively fed into the spinning assembly by a metering pump, and after being ejected from the spinneret of the spinning machine, it is cooled and consolidated into filaments, and the tow is introduced into the drafting nozzle through the Air-drafting, laying the web on the web forming machine to obtain the fiber web A;

S4溶液喷射纺丝:将S3步骤中纤维网A送入溶液喷射接受网,纺丝液b采用计量泵定量送入纺丝组件,经纺丝机喷丝板喷出后,丝束导入牵伸喷嘴经过气流牵引,溶液喷射牵引风压力为50bar,在纤维网A上冷却固结成丝,在成网机上铺网得到纤维网B;S4 solution jet spinning: the fiber web A in step S3 is sent into the solution jet receiving net, the spinning solution b is quantitatively fed into the spinning assembly by a metering pump, and after being ejected from the spinneret of the spinning machine, the tow is introduced into the drafting The nozzle is drawn by air flow, and the solution is sprayed with a pulling air pressure of 50 bar, cooled and consolidated into filaments on the fiber web A, and laid on the web forming machine to obtain the fiber web B;

S5加固整理:将S4步骤中所得到的纤维网B重叠进入溶液喷射纺丝区进行加固,得到无纺布,将无纺布表层进行亲水处理,亲水处理的处理液为亲水剂和纯净水按重量比1比150混合搅拌成液态状,加温至53℃。S5 reinforcement finishing: the fiber web B obtained in the step S4 is overlapped into the solution jet spinning area for reinforcement to obtain a non-woven fabric, and the surface layer of the non-woven fabric is subjected to hydrophilic treatment, and the treatment liquid for the hydrophilic treatment is a hydrophilic agent and a Pure water is mixed and stirred into a liquid state according to the weight ratio of 1:150, and heated to 53°C.

S6烘燥:将S5步骤中经亲水处理后的无纺布通过带液滚传输至烘箱中进行至少两次烘燥,首先在第一道烘箱中对无纺布进行预烘燥,在第一道烘箱中预烘燥温度为105℃;预烘燥后无纺布进入第二道烘箱中进行烘燥,第二道烘箱烘燥温度为110℃,经卷绕机切边、成卷,包装出厂。S6 drying: the non-woven fabric after the hydrophilic treatment in step S5 is transported to the oven for at least two times by rolling with liquid. First, the non-woven fabric is pre-dried in the first oven, and the The pre-drying temperature in the first oven is 105°C; after the pre-drying, the non-woven fabric enters the second oven for drying, and the drying temperature of the second oven is 110°C. Factory packing.

本实施例采用先纺粘铺网再溶液喷射纺丝进行无纺布5的生产,能够使无纺布5具有蓬松感、厚实感,增加无纺布的强力、过滤能力,可以替代熔喷布降低生产成本,本实施例中对无纺布5的表层做亲水处理,能够有效的提高无纺布的亲水性。In this embodiment, the non-woven fabric 5 is produced by first spunbonding and then solution jet spinning, which can make the non-woven fabric 5 have a fluffy and thick feeling, increase the strength and filtering ability of the non-woven fabric, and can replace the melt-blown fabric. To reduce the production cost, in this embodiment, the surface layer of the non-woven fabric 5 is subjected to hydrophilic treatment, which can effectively improve the hydrophilicity of the non-woven fabric.

本发明提供的一种无纺布的制备方法,包括以下步骤:The preparation method of a kind of non-woven fabric provided by the invention comprises the following steps:

S1原料准备:将原料a混合后喂入料斗中,混合后原料a经过双螺杆挤压机进行挤压熔融得到熔体a,原料a由以下重量份的原料组成:聚乳酸40份和聚丙烯腈50份;原料b溶于溶剂后加入溶液喷射纺丝机的溶解釜内,经搅拌形成纺丝液b;原料b由以下重量份的原料组成:聚乳酸40份和聚丙烯腈50份;S1 Raw material preparation: Mix the raw material a and feed it into the hopper. After mixing, the raw material a is extruded and melted by a twin-screw extruder to obtain the melt a. The raw material a is composed of the following raw materials by weight: 40 parts of polylactic acid and polypropylene 50 parts of nitrile; after the raw material b is dissolved in the solvent, it is added to the dissolving kettle of the solution jet spinning machine, and the spinning solution b is formed by stirring; the raw material b is composed of the following raw materials by weight: 40 parts of polylactic acid and 50 parts of polyacrylonitrile;

S2熔融过滤:将S1步骤中所得到的熔体a、纺丝液b分别经过滤器在线过滤去除杂质,然后进入纺丝组件,过滤器在线过滤去除杂质采用预过滤和精过滤的二级过滤方式,预过滤的精度小于80um,精过滤的精度小于30um;S2 Melt filtration: the melt a and spinning solution b obtained in step S1 are respectively filtered online to remove impurities through the filter, and then enter the spinning assembly. , the precision of pre-filtering is less than 80um, and the precision of fine-filtering is less than 30um;

S3纺丝成网:将S2步骤中过滤后的熔体a采用计量泵定量送入纺丝组件,经纺丝机喷丝板喷出后,冷却固结成丝,丝束导入牵伸喷嘴经过气流牵引,在成网机上铺网分别得到纤维网A;S3 spinning into a web: the melt a filtered in step S2 is quantitatively fed into the spinning assembly by a metering pump, and after being ejected from the spinneret of the spinning machine, it is cooled and consolidated into filaments, and the tow is introduced into the drafting nozzle through the Air-drafting, laying the web on the web forming machine to obtain the fiber web A;

S4溶液喷射纺丝:将S3步骤中纤维网A送入溶液喷射接受网,纺丝液b采用计量泵定量送入纺丝组件,经纺丝机喷丝板喷出后,丝束导入牵伸喷嘴经过气流牵引,溶液喷射牵引风压力为50bar,在纤维网A上冷却固结成丝,在成网机上铺网得到纤维网B;S4 solution jet spinning: the fiber web A in step S3 is sent into the solution jet receiving net, the spinning solution b is quantitatively fed into the spinning assembly by a metering pump, and after being ejected from the spinneret of the spinning machine, the tow is introduced into the drafting The nozzle is drawn by air flow, and the solution is sprayed with a pulling air pressure of 50 bar, cooled and consolidated into filaments on the fiber web A, and laid on the web forming machine to obtain the fiber web B;

S5加固整理:将S4步骤中所得到的纤维网B重叠进入溶液喷射纺丝区进行加固,得到无纺布,将无纺布表层进行亲水处理,亲水处理的处理液为亲水剂和纯净水按重量比1比150混合搅拌成液态状,加温至53℃。S5 reinforcement finishing: the fiber web B obtained in the step S4 is overlapped into the solution jet spinning area for reinforcement to obtain a non-woven fabric, and the surface layer of the non-woven fabric is subjected to hydrophilic treatment, and the treatment liquid for the hydrophilic treatment is a hydrophilic agent and a Pure water is mixed and stirred into a liquid state according to the weight ratio of 1:150, and heated to 53°C.

S6烘燥:将S5步骤中经亲水处理后的无纺布通过带液滚传输至烘箱中进行至少两次烘燥,首先在第一道烘箱中对无纺布进行预烘燥,在第一道烘箱中预烘燥温度为105℃;预烘燥后无纺布进入第二道烘箱中进行烘燥,第二道烘箱烘燥温度为110℃,经卷绕机切边、成卷,包装出厂。S6 drying: the non-woven fabric after the hydrophilic treatment in step S5 is transported to the oven for at least two times by rolling with liquid. First, the non-woven fabric is pre-dried in the first oven, and the The pre-drying temperature in the first oven is 105°C; after the pre-drying, the non-woven fabric enters the second oven for drying, and the drying temperature of the second oven is 110°C. Factory packing.

本实施例采用先纺粘铺网再溶液喷射纺丝进行无纺布6的生产,能够使无纺布6具有蓬松感、厚实感,增加无纺布的强力、过滤能力,可以替代熔喷布降低生产成本,本实施例对无纺布6的表层做亲水处理,能够有效的提高无纺布的亲水性。In this embodiment, the non-woven fabric 6 is produced by first spunbonding and then solution jet spinning, which can make the non-woven fabric 6 have a fluffy and thick feeling, increase the strength and filtering ability of the non-woven fabric, and can replace the melt-blown fabric. To reduce the production cost, in this embodiment, the surface layer of the non-woven fabric 6 is subjected to hydrophilic treatment, which can effectively improve the hydrophilicity of the non-woven fabric.

效果测试:Effect test:

将上述实施例中所制成的无纺布以及空气过滤器的性能进行了测试(分别见表1和表2),并将测试结果与现有产品进行了对比,结果如下:The performance of the non-woven fabric made in the above-described embodiment and the air filter were tested (respectively in Table 1 and Table 2), and the test result was compared with the existing product, the results are as follows:

表1:透气度、孔径、耐破度、挺度、抑菌性的比较Table 1: Comparison of Air Permeability, Pore Size, Burst Resistance, Stiffness, and Antibacterial Properties

Figure BDA0002496558720000101
Figure BDA0002496558720000101

表2本发明提供的无纺布制作过滤器的过滤效率(以克重180-220克/平米为例)Table 2 The filtration efficiency of the non-woven fabric provided by the invention to make the filter (take the gram weight 180-220 g/square meter as an example)

Figure BDA0002496558720000102
Figure BDA0002496558720000102

2.测试标准2. Test standard

上述测试的各项内容所采用的标准如下:The criteria used for each of the above tests are as follows:

厚度测定采用GB/T3820-1997标准;透气性测定采用GB/T5453-1997标准;孔径测定采用GB/T2679.14-1996标准;耐破度测定采用GB/T454-1989标准;挺度测定采用GB/T2679.3-1996标准;抑菌性测定采用卫生部《消毒技术规范》(2002版)2.1.8.7震荡烧瓶试验;The thickness measurement adopts GB/T3820-1997 standard; the air permeability measurement adopts GB/T5453-1997 standard; the pore diameter measurement adopts GB/T2679.14-1996 standard; the burst resistance measurement adopts GB/T454-1989 standard; the stiffness measurement adopts GB/T454-1989 standard /T2679.3-1996 standard; the antibacterial activity was determined by the 2.1.8.7 shaking flask test of the "Technical Specification for Disinfection" (2002 Edition) of the Ministry of Health;

无纺布过滤器分级效率的测定在符合GB/14295-2008《空气过滤器》的试验台进行测试,采用CLJ-03A型激光尘埃粒子计数器,TSI-8108大粒径气溶胶发生器,采样流量为2.83L/min。The classification efficiency of the non-woven filter was tested on a test bench conforming to GB/14295-2008 "Air Filter", using CLJ-03A laser dust particle counter, TSI-8108 large particle size aerosol generator, sampling flow rate is 2.83L/min.

3.测试结果分析3. Analysis of test results

表1结果显示:在透气度、孔径、耐破度、挺度、抑菌性等方面,本发明提供的一种无纺布的制备方法制备得到的无纺布1-6的效果明显优于市场上的PET针刺无纺布滤材和滤纸。表明本发明提供的无纺布过滤材料效果明显优于现有产品。The results in Table 1 show: in terms of air permeability, pore size, burst resistance, stiffness, antibacterial properties, etc., the effect of the non-woven fabrics 1-6 prepared by the preparation method of a non-woven fabric provided by the present invention is obviously better than PET needle punched non-woven filter media and filter paper on the market. It is shown that the effect of the non-woven filter material provided by the present invention is obviously better than that of the existing products.

表2结果显示:由无纺布制备的过滤器满足GB12218-89中的高中效和亚高效过滤器的分级标准。The results in Table 2 show that the filters prepared from non-woven fabrics meet the classification standards for high-efficiency and sub-high-efficiency filters in GB12218-89.

4.结论4 Conclusion

本发明提供的提供一种无纺布的制备方法,不仅能够使无纺布1-6具有蓬松感、厚实感,更增加无纺布1-6的强力和过滤能力,其压降较低,可以替代熔喷布,降低了生产成本,本发明对无纺布1-6表层做亲水处理,能够有效的提高无纺布1-6的亲水性。The present invention provides a method for preparing a non-woven fabric, which can not only make the non-woven fabric 1-6 have a fluffy and thick feeling, but also increase the strength and filtration capacity of the non-woven fabric 1-6, and its pressure drop is low, It can replace the melt-blown cloth and reduce the production cost. The present invention performs hydrophilic treatment on the surface layer of the non-woven fabric 1-6, which can effectively improve the hydrophilicity of the non-woven fabric 1-6.

以上所述的仅是本发明的优选实施方式,应当指出,对于本领域的普通技术人员来说,在不脱离本发明创造构思的前提下,还可以做出若干变形和改进,这些都属于本发明的保护范围。The above are only the preferred embodiments of the present invention. It should be pointed out that for those of ordinary skill in the art, some modifications and improvements can be made without departing from the inventive concept of the present invention, which belong to the present invention. The scope of protection of the invention.

Claims (10)

1. The preparation method of the non-woven fabric is characterized by comprising the following preparation steps:
preparing S1 raw material: mixing the raw materials a, extruding and melting the mixture by a screw extruder to obtain a melt a, dissolving the raw materials b in a solvent, adding the dissolved raw materials b into a dissolving kettle of a solution jet spinning machine, and stirring to form a spinning solution b;
s2 filtering: filtering the prepared melt a and the spinning solution b obtained in the step S1 through filters respectively to remove impurities, and then feeding the melt a and the spinning solution b into a spinning assembly respectively;
s3 spinning into net: quantitatively feeding the melt a and the spinning solution b filtered in the step S2 into a spinning assembly by using metering pumps respectively, spraying the melt a and the spinning solution b by using a spinneret plate of a spinning machine, cooling and solidifying the melt a and the spinning solution b into filaments, guiding the filaments into a drawing nozzle, drawing the filaments by using air flow, and lapping on a lapping machine to obtain a fiber web A;
s4 solution jet spinning: feeding the fiber web A obtained in the step S3 into a solution jet receiving net, quantitatively feeding the spinning solution B into a spinning assembly by using a metering pump, after the spinning solution B is jetted out by a spinneret plate of a spinning machine, guiding tows into a drawing nozzle, drawing the tows by using air flow, cooling and solidifying the tows on the fiber web A into filaments, and laying a net on a net forming machine to obtain a fiber web B;
s5 reinforcement and finishing: overlapping the fiber web B obtained in the step S4 into a solution jet spinning area for reinforcement to obtain a non-woven fabric;
s6 drying: and (4) inputting the non-woven fabric subjected to the solution jet spinning in the step S5 into an oven for drying.
2. The method of claim 1, wherein the raw material a and the raw material b have different compositions or the raw material a and the raw material b have the same composition.
3. The method for preparing the non-woven fabric according to any one of claims 1 to 2, wherein when the components of the raw material a and the raw material b are different, the raw material a consists of the following raw materials in parts by weight: 81-86.5 parts of polypropylene, 12.5-16 parts of propenyl elastomer, 0.5-1.5 parts of soft master batch and 0.5-1.5 parts of titanium dioxide; the raw material b comprises the following raw materials in parts by weight: 10-70 parts of polylactic acid and 20-80 parts of polyacrylonitrile.
4. The method for preparing the non-woven fabric according to any one of claims 1 to 2, wherein when the components of the raw material a and the raw material b are the same, the raw material a consists of the following raw materials in parts by weight: 10-70 parts of polylactic acid and 20-80 parts of polyacrylonitrile; the raw material b comprises the following raw materials in parts by weight: 10-70 parts of polylactic acid and 20-80 parts of polyacrylonitrile.
5. The method of preparing a nonwoven fabric according to claim 1, wherein the drawing wind pressure of the solution jet control air stream of the solution jet spinning head in the steps of S3 and S4 is 2bar to 70bar, respectively.
6. The method of manufacturing a nonwoven fabric according to claim 1, wherein the nonwoven fabric obtained by the solution jet spinning in the step S5 is subjected to a hydrophilic treatment.
7. The method for producing a nonwoven fabric according to claim 6, wherein the hydrophilic treatment liquid used in the hydrophilic treatment step is obtained by mixing and stirring a hydrophilic agent and purified water at a weight ratio of 1 to 150.
8. The method of claim 1, wherein the step of drying in step S6 comprises pre-drying the nonwoven fabric in a first oven, and the pre-dried nonwoven fabric is dried in a second oven.
9. The method of claim 8, wherein the pre-drying is carried out in a single oven at a temperature of
Figure FDA0002496558710000021
The temperature for drying in the second drying oven is
Figure FDA0002496558710000022
10. The method of claim 1, wherein the step S2 is performed by two-stage filtration including pre-filtration and fine filtration, the pre-filtration has a particle size of less than 80um, and the fine filtration has a particle size of less than 30 um.
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