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CN111534330A - Paraffin Pellet Generator - Google Patents

Paraffin Pellet Generator Download PDF

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Publication number
CN111534330A
CN111534330A CN202010424428.4A CN202010424428A CN111534330A CN 111534330 A CN111534330 A CN 111534330A CN 202010424428 A CN202010424428 A CN 202010424428A CN 111534330 A CN111534330 A CN 111534330A
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China
Prior art keywords
paraffin
heat
resistant
pipe
tank
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CN202010424428.4A
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Inventor
杨晓军
刘智刚
于天浩
胡英琦
常嘉文
靳晓宇
陈羽
刘文博
柳笑寒
周昊旻
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Civil Aviation University of China
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Civil Aviation University of China
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Priority to CN202010424428.4A priority Critical patent/CN111534330A/en
Publication of CN111534330A publication Critical patent/CN111534330A/en
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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G73/00Recovery or refining of mineral waxes, e.g. montan wax
    • C10G73/40Physical treatment of waxes or modified waxes, e.g. granulation, dispersion, emulsion, irradiation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2/00Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
    • B01J2/02Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops
    • B01J2/04Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops in a gaseous medium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J6/00Heat treatments such as Calcining; Fusing ; Pyrolysis
    • B01J6/005Fusing

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Dispersion Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Filling Or Discharging Of Gas Storage Vessels (AREA)

Abstract

A paraffin particle generator. The device comprises a compressor gas storage tank, a filter, an explosion-proof heat-resistant pipe, a heat exchanger, a lower gas spray head, a hard glass tank, a paraffin nozzle, an upper gas spray head, a heat-resistant backflow pipe, a gear pump, a liquid inlet pipe and a paraffin heating tank; the paraffin particle generator provided by the invention has the following beneficial effects: can continuously produce atomized paraffin particles, and has simple structure, low manufacturing cost and convenient use. In addition, the experimenter can visually observe the melting and solidification processes of the paraffin particles through the hard glass tank and the paraffin heating tank, and the method is very convenient and practical.

Description

石蜡颗粒发生器Paraffin Pellet Generator

技术领域technical field

本发明属于实验装置技术领域,特别是涉及一种主要用于科学研究中熔融态石蜡颗粒产生的发生器。The invention belongs to the technical field of experimental devices, in particular to a generator mainly used for generating molten paraffin particles in scientific research.

背景技术Background technique

石蜡作为熔点较低且黏性较高的工质,可以在较低温度的环境下雾化为石蜡颗粒,从而模拟灰尘颗粒在高温环境下的熔融和凝固过程。目前已有的石蜡颗粒发生器产生的石蜡颗粒无法展现颗粒物的熔融和凝固过程,且都是在常温下使用的仪器。因此,将石蜡加热为熔融态,并生成石蜡颗粒是目前所需解决的难题。As a working medium with low melting point and high viscosity, paraffin wax can be atomized into paraffin wax particles in a low temperature environment, thereby simulating the melting and solidification process of dust particles in a high temperature environment. The paraffin particles produced by the existing paraffin particle generators cannot show the melting and solidification process of the particles, and they are all instruments used at room temperature. Therefore, heating paraffin into a molten state and generating paraffin particles is a difficult problem to be solved at present.

发明内容SUMMARY OF THE INVENTION

为了解决上述问题,本发明的目的在于提供了一种石蜡颗粒发生器。In order to solve the above problems, the purpose of the present invention is to provide a paraffin particle generator.

为了达到上述目的,本发明提供的石蜡颗粒发生器包括压缩机储气罐、过滤器、防爆耐热管、换热器、下部气体喷头、硬质玻璃罐、石蜡喷嘴、上部气体喷头、耐热回流管、齿轮泵、进液管和石蜡加热罐;其中石蜡加热罐用于盛放和加热固态石蜡,并使石蜡保持在一定的温度;进液管的一端浸在石蜡加热罐内的石蜡中,另一端位于硬质玻璃罐的上方且与耐热回流管的一端相连,耐热回流管的另一端位于石蜡加热罐内;石蜡喷嘴安装在硬质玻璃罐的顶部且与进液管相连通;齿轮泵连接在进液管上;防爆耐热管的一端连接在压缩机储气罐的出气口,另一端分成两条支路,其中一条支路的末端连接在进液管上靠近石蜡喷嘴的位置且与上部气体喷头相连接,另一条支路的末端位于硬质玻璃罐内的下部且与下部气体喷头相连接;过滤器和换热器安装在防爆耐热管上;硬质玻璃罐的下端设有与实验段相连通的石蜡颗粒出口。In order to achieve the above purpose, the paraffin particle generator provided by the present invention includes a compressor gas storage tank, a filter, an explosion-proof and heat-resistant pipe, a heat exchanger, a lower gas nozzle, a hard glass tank, a paraffin nozzle, an upper gas nozzle, a heat-resistant Return pipe, gear pump, liquid inlet pipe and paraffin heating tank; the paraffin heating tank is used to hold and heat solid paraffin and keep the paraffin at a certain temperature; one end of the liquid inlet pipe is immersed in the paraffin in the paraffin heating tank , the other end is located above the rigid glass tank and is connected to one end of the heat-resistant return pipe, and the other end of the heat-resistant return pipe is located in the paraffin heating tank; the paraffin nozzle is installed on the top of the rigid glass tank and communicated with the liquid inlet pipe ;The gear pump is connected to the liquid inlet pipe; one end of the explosion-proof and heat-resistant pipe is connected to the air outlet of the compressor air storage tank, and the other end is divided into two branches, and the end of one branch is connected to the liquid inlet pipe near the paraffin nozzle The end of the other branch is located in the lower part of the rigid glass tank and connected to the lower gas nozzle; the filter and heat exchanger are installed on the explosion-proof heat-resistant pipe; the rigid glass tank The lower end is provided with a paraffin particle outlet that communicates with the experimental section.

所述的防爆耐热管上安装有压力表和总阀门开关;两条支路上分别安装有分阀门开关和流量计。A pressure gauge and a main valve switch are installed on the explosion-proof and heat-resistant pipe; a branch valve switch and a flow meter are respectively installed on the two branches.

所述的石蜡颗粒发生器还包括加热带和温控器,其中加热带包覆在防爆耐热管、进液管、耐热回流管和齿轮泵的外部,且加热带和温控器的测温探头电连接。The paraffin particle generator also includes a heating belt and a temperature controller, wherein the heating belt is wrapped on the outside of the explosion-proof heat-resistant pipe, the liquid inlet pipe, the heat-resistant return pipe and the gear pump, and the heating belt and the temperature controller are measured. The temperature probe is electrically connected.

所述的耐热回流管上安装在自动泄压阀。An automatic pressure relief valve is installed on the heat-resistant return pipe.

所述的石蜡喷嘴和下部气体喷头的喷射方向相反。The spraying directions of the paraffin nozzle and the lower gas spraying head are opposite.

所述的硬质玻璃罐的侧壁外部包覆有保温棉,下部外侧设有底座,上端口处设有密封盖,密封盖上安装有密封盖把手。The outer side wall of the rigid glass jar is covered with thermal insulation cotton, the outer side of the lower part is provided with a base, the upper port is provided with a sealing cover, and a sealing cover handle is installed on the sealing cover.

所述的石蜡加热罐的侧壁外部包覆有保温棉。The outside of the side wall of the paraffin heating tank is covered with thermal insulation cotton.

本发明提供的石蜡颗粒发生器具有如下有益效果:The paraffin particle generator provided by the present invention has the following beneficial effects:

可持续地产生雾化的石蜡颗粒,且结构简单,造价低廉,使用方便。另外,实验人员可通过硬质玻璃罐和石蜡加热罐直观地观察到石蜡颗粒的熔融和凝固过程,非常方便、实用。The atomized paraffin wax particles can be produced sustainably, the structure is simple, the cost is low, and the use is convenient. In addition, the experimenter can visually observe the melting and solidification process of the paraffin particles through the rigid glass tank and the paraffin heating tank, which is very convenient and practical.

附图说明Description of drawings

图1为本发明提供的石蜡颗粒发生器结构示意图。FIG. 1 is a schematic structural diagram of a paraffin particle generator provided by the present invention.

具体实施方式Detailed ways

下面结合附图和具体实施例对本发明进行详细说明。The present invention will be described in detail below with reference to the accompanying drawings and specific embodiments.

如图1所示,本发明提供的石蜡颗粒发生器包括压缩机储气罐1、过滤器4、防爆耐热管5、换热器6、下部气体喷头12、硬质玻璃罐16、石蜡喷嘴17、上部气体喷头20、耐热回流管21、齿轮泵23、进液管25和石蜡加热罐27;其中石蜡加热罐27用于盛放和加热固态石蜡11,并使石蜡11保持在一定的温度;进液管25的一端浸在石蜡加热罐27内的石蜡11中,另一端位于硬质玻璃罐16的上方且与耐热回流管21的一端相连,耐热回流管21的另一端位于石蜡加热罐27内;石蜡喷嘴17安装在硬质玻璃罐16的顶部且与进液管25相连通;齿轮泵23连接在进液管25上;防爆耐热管5的一端连接在压缩机储气罐1的出气口,另一端分成两条支路,其中一条支路的末端连接在进液管25上靠近石蜡喷嘴17的位置且与上部气体喷头20相连接,另一条支路的末端位于硬质玻璃罐16内的下部且与下部气体喷头12相连接;过滤器4和换热器6安装在防爆耐热管5上;硬质玻璃罐16的下端设有与实验段相连通的石蜡颗粒出口13。As shown in FIG. 1, the paraffin particle generator provided by the present invention includes a compressor gas storage tank 1, a filter 4, an explosion-proof and heat-resistant tube 5, a heat exchanger 6, a lower gas nozzle 12, a hard glass tank 16, and a paraffin nozzle. 17. The upper gas nozzle 20, the heat-resistant return pipe 21, the gear pump 23, the liquid inlet pipe 25 and the paraffin heating tank 27; wherein the paraffin heating tank 27 is used to hold and heat the solid paraffin 11 and keep the paraffin 11 at a certain level. Temperature; one end of the liquid inlet pipe 25 is immersed in the paraffin 11 in the paraffin heating tank 27, the other end is located above the rigid glass tank 16 and is connected to one end of the heat-resistant return pipe 21, and the other end of the heat-resistant return pipe 21 is located at Inside the paraffin heating tank 27; the paraffin nozzle 17 is installed on the top of the rigid glass tank 16 and communicated with the liquid inlet pipe 25; the gear pump 23 is connected to the liquid inlet pipe 25; one end of the explosion-proof heat-resistant pipe 5 is connected to the compressor storage tank. The gas outlet of the gas tank 1 is divided into two branches at the other end, and the end of one branch is connected to the liquid inlet pipe 25 near the paraffin nozzle 17 and is connected to the upper gas nozzle 20, and the end of the other branch is located at the position. The lower part in the rigid glass jar 16 is connected with the lower gas nozzle 12; the filter 4 and the heat exchanger 6 are installed on the explosion-proof and heat-resistant pipe 5; the lower end of the rigid glass jar 16 is provided with paraffin that communicates with the experimental section Particle outlet 13.

所述的防爆耐热管5上安装有压力表2和总阀门开关3;两条支路上分别安装有分阀门开关8和流量计10。A pressure gauge 2 and a main valve switch 3 are installed on the explosion-proof and heat-resistant pipe 5; a branch valve switch 8 and a flow meter 10 are installed on the two branches respectively.

所述的石蜡颗粒发生器还包括加热带7和温控器22,其中加热带7包覆在防爆耐热管5、进液管25、耐热回流管21和齿轮泵23的外部,且加热带7和温控器22的测温探头电连接。The paraffin particle generator also includes a heating belt 7 and a temperature controller 22, wherein the heating belt 7 is wrapped on the outside of the explosion-proof and heat-resistant pipe 5, the liquid inlet pipe 25, the heat-resistant return pipe 21 and the gear pump 23, and is heated. The temperature probe with 7 and thermostat 22 is electrically connected.

所述的耐热回流管21上安装在自动泄压阀24。The heat-resistant return pipe 21 is installed on the automatic pressure relief valve 24 .

所述的石蜡喷嘴17和下部气体喷头12的喷射方向相反。The spraying directions of the paraffin nozzle 17 and the lower gas spraying head 12 are opposite.

所述的硬质玻璃罐16的侧壁外部包覆有保温棉9,下部外侧设有底座14,上端口处设有密封盖18,密封盖18上安装有密封盖把手19。The outer side wall of the rigid glass jar 16 is covered with thermal insulation cotton 9 , the lower outer side is provided with a base 14 , the upper port is provided with a sealing cover 18 , and a sealing cover handle 19 is installed on the sealing cover 18 .

所述的石蜡加热罐27的侧壁外部包覆有保温棉9。The outside of the side wall of the paraffin heating tank 27 is covered with thermal insulation cotton 9 .

现将本发明提供的石蜡颗粒发生器的工作原理阐述如下:Now the working principle of the paraffin particle generator provided by the invention is described as follows:

第一步、由实验人员打开石蜡加热罐27上的开关,使其内的固态石蜡11熔化成液态石蜡11;In the first step, the experimenter turns on the switch on the paraffin heating tank 27 to melt the solid paraffin 11 into the liquid paraffin 11;

第二步、打开加热带7和温控器22,使齿轮泵23中的石蜡残留物熔化,同时也对防爆耐热管5、进液管25和耐热回流管21进行加热;The second step, open the heating belt 7 and the thermostat 22, melt the paraffin residue in the gear pump 23, and also heat the explosion-proof heat-resistant pipe 5, the liquid inlet pipe 25 and the heat-resistant return pipe 21;

第三步、打开压缩机储气罐1使压缩空气流入防爆耐热管5,然后根据压力表2调整总阀门开关3的开度,直至流经防爆耐热管5内的压缩空气达到适宜的压力;The third step is to open the compressor air storage tank 1 so that the compressed air flows into the explosion-proof and heat-resistant pipe 5, and then adjust the opening of the main valve switch 3 according to the pressure gauge 2 until the compressed air flowing through the explosion-proof and heat-resistant pipe 5 reaches a suitable pressure;

第四步、打开换热器6,这时压缩空气将依次流入过滤器4和换热器6,利用过滤器4滤除压缩空气中的杂质,同时利用换热器6对进入其内部的压缩空气进行加热,之后流入防爆耐热管5的两条支路,根据流量计10调整分阀门开关8的开度,直至压缩空气达到适宜的流量,最后热压缩空气将分别从上部气体喷头20和下部气体喷头12向外喷出;The fourth step is to open the heat exchanger 6. At this time, the compressed air will flow into the filter 4 and the heat exchanger 6 in turn. The filter 4 is used to filter out the impurities in the compressed air, and the heat exchanger 6 is used to compress the compressed air. The air is heated, and then flows into the two branches of the explosion-proof and heat-resistant pipe 5, and the opening of the sub-valve switch 8 is adjusted according to the flow meter 10 until the compressed air reaches a suitable flow rate. Finally, the hot compressed air will flow from the upper gas nozzle 20 and The lower gas nozzle 12 is ejected outward;

第五步、打开自动泄压阀24,以保证耐热回流管21中的液态石蜡11压力稳定;The fifth step, open the automatic pressure relief valve 24 to ensure that the pressure of the liquid paraffin 11 in the heat-resistant return pipe 21 is stable;

第六步、打开齿轮泵23,开始向进液管25中泵入液态石蜡11,液态石蜡11在上部气体喷头20处将与上部气体喷头20喷出的热压缩空气预混后变成石蜡颗粒并从石蜡喷嘴17向下喷出,喷出后的石蜡颗粒将与由下部气体喷头12向上喷出的热压缩空气相向碰撞,产生雾化的石蜡颗粒,根据伯努利原理,雾化的石蜡颗粒将通过石蜡颗粒出口13进入到研究用的试验段中;而过量的液态石蜡11将通过耐热回流管21流回石蜡加热罐27内。The sixth step, turn on the gear pump 23, start to pump the liquid paraffin 11 into the liquid inlet pipe 25, and the liquid paraffin 11 will be premixed with the hot compressed air ejected from the upper gas nozzle 20 and become paraffin particles at the upper gas nozzle 20. And sprayed downward from the paraffin nozzle 17, the sprayed paraffin particles will collide with the hot compressed air sprayed upward from the lower gas nozzle 12 to generate atomized paraffin particles. According to Bernoulli's principle, the atomized paraffin The particles will enter into the experimental section for research through the paraffin particle outlet 13;

Claims (7)

1. A paraffin particle generator, characterized in that: the paraffin particle generator comprises a compressor air storage tank (1), a filter (4), an explosion-proof heat-resistant pipe (5), a heat exchanger (6), a lower gas spray head (12), a hard glass tank (16), a paraffin nozzle (17), an upper gas spray head (20), a heat-resistant return pipe (21), a gear pump (23), a liquid inlet pipe (25) and a paraffin heating tank (27); the paraffin heating tank (27) is used for containing and heating the solid paraffin (11) and keeping the paraffin (11) at a certain temperature; one end of the liquid inlet pipe (25) is immersed in the paraffin (11) in the paraffin heating tank (27), the other end of the liquid inlet pipe is positioned above the hard glass tank (16) and is connected with one end of the heat-resistant return pipe (21), and the other end of the heat-resistant return pipe (21) is positioned in the paraffin heating tank (27); the paraffin nozzle (17) is arranged at the top of the hard glass tank (16) and is communicated with the liquid inlet pipe (25); the gear pump (23) is connected to the liquid inlet pipe (25); one end of the explosion-proof heat-resistant pipe (5) is connected with an air outlet of the compressor air storage tank (1), the other end of the explosion-proof heat-resistant pipe is divided into two branches, the tail end of one branch is connected with the position, close to the paraffin nozzle (17), on the liquid inlet pipe (25) and is connected with the upper gas nozzle (20), and the tail end of the other branch is located at the lower part in the hard glass tank (16) and is connected with the lower gas nozzle (12); the filter (4) and the heat exchanger (6) are arranged on the explosion-proof heat-resistant pipe (5); the lower end of the hard glass tank (16) is provided with a paraffin particle outlet (13) communicated with the experimental section.
2. The paraffin particle generator of claim 1, wherein: the explosion-proof heat-resistant pipe (5) is provided with a pressure gauge (2) and a main valve switch (3); the two branches are respectively provided with a branch valve switch (8) and a flowmeter (10).
3. The paraffin particle generator of claim 1, wherein: the paraffin particle generator further comprises a heating belt (7) and a temperature controller (22), wherein the heating belt (7) is coated outside the explosion-proof heat-resistant pipe (5), the liquid inlet pipe (25), the heat-resistant backflow pipe (21) and the gear pump (23), and the heating belt (7) is electrically connected with a temperature measuring probe of the temperature controller (22).
4. The paraffin particle generator of claim 1, wherein: the heat-resistant return pipe (21) is provided with an automatic pressure relief valve (24).
5. The paraffin particle generator of claim 1, wherein: the paraffin nozzle (17) and the lower gas nozzle (12) have opposite spraying directions.
6. The paraffin particle generator of claim 1, wherein: the side wall of the hard glass tank (16) is coated with heat insulation cotton (9), the outer side of the lower part of the hard glass tank is provided with a base (14), the upper port of the hard glass tank is provided with a sealing cover (18), and a sealing cover handle (19) is arranged on the sealing cover (18).
7. The paraffin particle generator of claim 1, wherein: the side wall of the paraffin heating tank (27) is coated with heat insulation cotton (9).
CN202010424428.4A 2020-05-19 2020-05-19 Paraffin Pellet Generator Pending CN111534330A (en)

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GB841562A (en) * 1955-05-27 1960-07-20 Edeleanu Gmbh Process and apparatus for separating paraffin wax from wax-containing hydrocarbon oils
DE1927389A1 (en) * 1969-05-29 1970-12-03 Hoechst Ag Free-flowing wax powder production
US5417153A (en) * 1993-08-09 1995-05-23 International Flavors & Fragrances Inc. Fluidizing spray chilling system for producing encapsulated materials
CN107744891A (en) * 2017-10-12 2018-03-02 中国民航大学 A kind of paraffin sprayer unit

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB841562A (en) * 1955-05-27 1960-07-20 Edeleanu Gmbh Process and apparatus for separating paraffin wax from wax-containing hydrocarbon oils
DE1927389A1 (en) * 1969-05-29 1970-12-03 Hoechst Ag Free-flowing wax powder production
US5417153A (en) * 1993-08-09 1995-05-23 International Flavors & Fragrances Inc. Fluidizing spray chilling system for producing encapsulated materials
CN107744891A (en) * 2017-10-12 2018-03-02 中国民航大学 A kind of paraffin sprayer unit

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