CN110123674A - A kind of smoothing toner and preparation method thereof containing oil and fat of sacha inchi microcapsules - Google Patents

Abstract

The present invention provides a kind of smoothing toner and preparation method thereof containing oil and fat of sacha inchi microcapsules.The smoothing toner containing oil and fat of sacha inchi microcapsules, in parts by weight, its raw material includes: 100-160 parts of distilled water, 3-5 parts of 1,3-BDOs, 4-6 parts of polyethylene glycol -32,2-4 parts of methyl gluceths -20,3-14 parts of moisturizer, 0.1-6 parts of antioxidants, 0.5-3 portions of preservatives and 2-8 parts of oil and fat of sacha inchi microcapsules.Using the present invention containing a few days after oil and fat of sacha inchi microcapsules smoothing toner after, can have apparent soft and moist skin, have and highlight skin, enhance the effect of skin elasticity, smoothing toner obtained by the present invention is nontoxic, and no sensitization, non-stimulated, use is safe.

Description

A kind of softening lotion containing sachaeto fruit oil microcapsules and preparation method thereof

technical field

The invention belongs to the field of cosmetics and relates to a lotion, in particular to a softening lotion containing saiteng fruit oil microcapsules and a preparation method for the softening lotion containing saiteng fruit oil microcapsules.

Background technique

Toner refers to a milder lotion with a pH close to 7. It has the effect of softening keratin, that is, removing aging keratin so as to make the skin moist and soft, improving dullness and lack of luster and elasticity of the skin. It also has the effect of preventing the formation of melanin, moisturizing the skin, balancing the acidity and alkalinity of the skin, and maintaining the skin in good condition. Suitable for dry and combination skin.

Cane fruit oil is a kind of vegetable oil extracted from the seeds of the genus Oleifera in South America. It has a high content of unsaturated fatty acids, and it also contains vitamin E, polyphenols, sterols and other lipids as active ingredients. , has the effects of whitening, moisturizing, freckle removal, anti-oxidation, anti-aging, etc., as a cosmetic raw material added to cosmetics, it will definitely have great benefits for the skin.

Microcapsule technology is a new type of technology that solidifies some gaseous or liquid substances into a solid state by a certain method. Generally speaking, microcapsules are composed of two parts: the outer shell, that is, the wall material, and the inner core material. Most microcapsules are spherical, and their wall materials are mainly prepared from natural polymer compounds or some inorganic substances through a series of physical and chemical reactions through certain equipment. The particle size of most microcapsules is extremely small, and microcapsules play a big role in life. Therefore, it is more convenient to use, and the cost is also lower. The formed microcapsules can protect the core material from contact with oxygen, thereby oxidative deterioration, or deterioration due to external environmental factors, which affects the shelf life.

According to the skin of oriental women, white, ruddy and shiny has always been the fashion that women admire and pursue, and then functional skin toners such as whitening, moisturizing or anti-oxidation are emerging in the market. In the past few decades, people mostly used physical masking technology such as "whitening powder" to achieve the effect of surface modification, which is highly targeted, but a change in skin condition is often accompanied by some other skin problems, such as dry skin, It is easy to cause dull and dull skin, premature skin aging, pigmentation and other problems.

Contents of the invention

The object of the present invention is to provide a softening lotion containing sachaeji oil microcapsules and a preparation method thereof, so as to solve the technical problems of sachaeba fruit oil instability, volatilization and limited application range.

In order to achieve the above object, the present invention provides a kind of skin softening water containing sachaeji fruit oil microcapsules, which is characterized in that, in parts by weight, its raw materials include: 100-160 parts of distilled water, 3-5 parts of 1,3- Butylene Glycol, 4-6 Parts Polyethylene Glycol-32, 2-4 Parts Methyl Gluceth-20, 3-14 Parts Humectants, 0.1-6 Parts Antioxidants, 0.5-3 Parts Preservatives and 2-8 servings of cane oil microcapsules.

Preferably, the moisturizer consists of sodium hyaluronate, propylene glycol and glycerin. More preferably, the mass ratio of sodium hyaluronate, propylene glycol and glycerin is 0.5-1.5:0.5-1.5:1, most preferably 1:1:1.

Preferably, the antioxidant consists of tocopherol and di-tert-butylcresol. More preferably, the mass ratio of tocopherol to di-tert-butylcresol is 0.5-1.5:1, most preferably 1:1.

Preferably, the preservative consists of sodium benzoate and parabens. More preferably, the mass ratio of tocopherol to di-tert-butylcresol is 0.5-1.5:1, most preferably 1:1.

Preferably, the raw material of the softening water containing sachaeji fruit oil microcapsules also contains 0.05-0.15 part of essence.

Preferably, the essence is a general daily chemical essence.

Preferably, the raw materials of the skin softening water containing sachaeji fruit oil microcapsules also include pigments and the like.

Preferably, the particle diameter of said sachaetra fruit oil microcapsules is 40nm-60nm.

Preferably, in parts by weight, the raw materials for the preparation of said cane oil microcapsules include: 2-15 parts of cane oil, 0.5-1 part of emulsifier, 0.2-5 parts of co-emulsifier, 0.5-5 parts of preservative 1 part and 100-160 parts of water.

More preferably, the emulsifier is composed of Span-80 and Tween-80, and the mass ratio of Span-80 and Tween-80 is 1:1-3.

More preferably, the co-emulsifier is any one of cetyl alcohol and 1,3-butanediol.

Preferably, the preparation method of described sachaeto fruit oil microcapsules comprises:

Step 1: Put 2-15 parts of cane oil, 0.5-1 part of emulsifier and 0.2-5 parts of co-emulsifier in a container, and process it homogeneously at a rate of 300-900 r/min to obtain a stable oil phase system;

Step 2: Dissolving 0.5-1 part of preservative in 100-160 parts of water to obtain the water phase;

Step 3: Add the obtained water phase to the obtained oil phase system at a temperature range of 65-85°C, and control the addition rate to 0.5-1.5mL/min to form an emulsified system;

Step 4: Add 10-15 parts of calcium chloride solution with a concentration of 3.0mol/l-4.5mol/l dropwise into the emulsification system, and control the temperature of the water bath to 65-80°C for emulsification for 0.8-1h;

Step 5: Add 10-15 parts of sodium carbonate solution with a concentration of 0.9mol/l-1.4mol/l dropwise to the emulsification system obtained in step 4. After the addition is completed, let it stand for 6-24h, filter it with suction, and dry it Dry to obtain sachaetra fruit oil microcapsule powder.

The present invention also provides the preparation method of the above-mentioned softening lotion containing sachaeji fruit oil microcapsules, which is characterized in that, comprising:

Step 1: Weigh 100-160 parts of distilled water, 3-5 parts of 1,3-butanediol, 4-6 parts of polyethylene glycol-32, 2-4 parts of methyl gluceth-20,3- 14 parts of moisturizing agents, 0.1-6 parts of antioxidants, 0.5-3 parts of preservatives and 2-8 parts of cane fruit oil microcapsules; the described moisturizing agent is sodium hyaluronate, propylene glycol and glycerin mixture, and the described anti-aging The oxidant is a mixture of tocopherol and di-tert-butylcresol; the preservative is a mixture of sodium benzoate and paraben;

Step 2: Dissolve 3-14 parts of moisturizer in 80-130 parts of distilled water, and mix evenly for 15-25 minutes under continuous stirring at 300-400 rpm;

Step 3: Add 0.1-6 parts of antioxidant to the remaining distilled water, heat to 40-60°C, and stir continuously at 400-600rpm for 10-40min;

Step 4: Add the mixture obtained in step 3 to the mixture obtained in step 2, mix evenly under continuous stirring at 500-700rpm, then add 0.5-3 parts of preservatives and mix with glacial acetic acid with a concentration of 4-6% by mass Adjust the pH of the solution to 5.5-6.5, and cool down to 15-30°C;

Step 5: Add 2-8 parts of cane fruit oil microcapsules, 3-5 parts of 1,3-butanediol, 4-6 parts of polyethylene glycol-32, 2-4 parts to the mixture obtained in step 4 Methyl gluceth-20, under continuous stirring at 450-650rpm, mix evenly until the microcapsules of cane oil microcapsules are evenly dispersed, then adjust the pH to 5- 6. Let it stand for 1-4 hours to get skin softening water.

The savine fruit oil microcapsule in skin softening water of the present invention comprises two parts, a core material and a wall material, wherein the savine fruit oil is used as the core material, and calcium carbonate is used as the wall material. The mass ratio of the core material to the wall material is 1-1.5:1.

After cleansing the skin, drop the soft skin lotion containing the cane fruit oil microcapsules of the present invention on the face, and gently pat it into the skin, preferably 2-3 times a day.

Compared with prior art, the beneficial effect of the present invention is:

In the present invention, the microcapsule of cane oil is used as a raw material of cosmetics in skin softening water, which has a series of effects on skin care, such as whitening and removing freckles, anti-aging, etc., and has good effects of moisturizing and nourishing the skin. A few days after using the softening lotion of the present invention containing microcapsules of cane fruit oil, the skin can be obviously soft and moisturized, and has the effect of brightening the skin and enhancing skin elasticity. The softening lotion prepared by the present invention is non-toxic and non-toxic Sensitive, non-irritating, safe to use.

In the present invention, because the raw material of the oil phase is sachaetra fruit oil, which has a relatively high content of unsaturated fatty acids, it has better effects of whitening, moisturizing, sun protection, and freckle removal when applied to cosmetics. Because it contains a variety of lipids as active ingredients, it has the functions of anti-aging, anti-oxidation, anti-inflammatory, increasing skin repair ability, enhancing skin barrier function, and controlling skin moisture loss, so that the skin can maintain a high degree of moisture.

The softening lotion containing cane oil microcapsules obtained by the present invention has excellent stability due to the use of microcapsule technology, controls the release rate of vegetable oil, and endows vegetable oil with higher use value and wider application A series of effects different from pure vegetable oil.

The softening lotion containing savine fruit oil microcapsules of the present invention is prepared by using savine fruit oil microcapsules and other raw materials to prepare the softening lotion. It is also good for keeping the skin moisturized and satisfies the deeper pursuit of modern people for the skin. It is to develop skin softening water suitable for different skin types according to the type of skin. Therefore, developing a skin softening water with moisturizing, moisturizing and anti-aging properties has a very wide application prospect and market prospect.

The particle size of the microcapsule of the present invention is very small, and the microcapsule of nanometer level can be easily absorbed by the skin, and is applied in cosmetics, so that the active ingredients can penetrate into the skin and improve the anti-aging ability of the skin.

Description of drawings

Fig. 1 is the particle size distribution figure of embodiment 2 gained cayenne fruit oil microcapsule softening lotion.

Detailed ways

Below in conjunction with specific embodiment, further illustrate the present invention. It should be understood that these examples are only used to illustrate the present invention and are not intended to limit the scope of the present invention. In addition, it should be understood that after reading the teachings of the present invention, those skilled in the art can make various changes or modifications to the present invention, and these equivalent forms also fall within the scope defined by the appended claims of the present application.

All raw materials used in the following examples are commercially available products.

The specifications of various raw materials or reagents used in the present invention and the information of the manufacturer are as follows:

1,3-Butanediol, analytically pure, Sinopharm Chemical Reagent Co., Ltd.;

Polyethylene glycol-32; analytically pure, Sinopharm Chemical Reagent Co., Ltd.;

Methyl gluceth-20, analytically pure, Sinopharm Chemical Reagent Co., Ltd.;

Glycerin, analytically pure, Sinopharm Chemical Reagent Co., Ltd.;

Tocopherol, Shanghai Jiachen Chemical Co., Ltd.;

Parabens, Shanghai Jiachen Chemical Co., Ltd.;

Rose essence, daily essence, Shanghai Exetin Fragrance Co., Ltd.;

Meiteng Fruit Oil, Yunnan Puer Lianzhong Biological Resources Development Co., Ltd.;

Tween-80, analytically pure, Sinopharm Chemical Reagent Co., Ltd.;

Span-80, analytically pure, Sinopharm Chemical Reagent Co., Ltd.;

Sodium benzoate, analytically pure, Sinopharm Chemical Reagent Co., Ltd.;

Sodium hyaluronate, Shanghai Hengsheng Chemical Co., Ltd.;

Di-tert-butylcresol, Shanghai Jiachen Chemical Co., Ltd.;

NaOH, analytically pure, Sinopharm Chemical Reagent Co., Ltd.;

Glacial acetic acid, analytically pure, Sinopharm Chemical Reagent Co., Ltd.;

The model of instrument equipment used in the present invention and the information of manufacturer are as follows:

Electronic balance, PL403, Mettler-Toledo Instruments Co., Ltd.:

Digital high-speed electric emulsifier, T-25 type, Germany IKA Co., Ltd.;

Constant temperature magnetic stirrer, 524G, Shanghai Meiyingpu Instrument Manufacturing Co., Ltd.;

Water bath oscillator, SHZ-B, Shanghai Boxun Industrial Co., Ltd.;

Laser particle size analyzer, Nano-ZS, Malvern Instruments (China) Co., Ltd.;

Skin Moisture Meter, AS-509, Guangzhou Ansen Electronic Technology Co., Ltd.

Example 1

A skin softening lotion containing sachaetra oil microcapsules, in parts by weight, its raw materials include: 100 parts of distilled water; 3 parts of 1,3-butanediol; 3 parts of propylene glycol; 3 parts of sodium hyaluronate; 4 parts 1 part polyethylene glycol-32; 2 parts methyl gluceth-20; 2 parts sachaetra oil microcapsules; 3 parts glycerin: 0.1 part tocopherol; 0.1 part di-tert-butylcresol; 0.50 part p-hydroxybenzene Formic esters; 0.5 parts sodium benzoate; 0.05 parts rose essence.

In parts by weight, the raw materials for preparing the sachaetra oil microcapsules include: 2 parts of sachaeto fruit oil, 0.6 part of emulsifier, 3 parts of co-emulsifier, 0.5 part of preservative and 100 parts of water. The emulsifier is a compound of Span-80 and Tween-80, and the ratio of Span-80:Tween-80 is 1:1. The co-emulsifier is 1,3-butanediol, and the preservative is paraben.

The preparation method of described cane fruit oil microcapsules is:

Step 1: Put 2 parts of sachaetra oil, 0.6 part of emulsifier and 3 parts of co-emulsifier in a container, and process it homogeneously at a rate of 600 r/min to obtain a stable oil phase system;

Step 2: Dissolving 0.5 part of preservative in 100 parts of water to obtain the water phase;

Step 3: Add the obtained water phase to the obtained oil phase system at a temperature range of 75°C, and control the addition rate to 1mL/min to form an emulsified system;

Step 4: Add 10 parts of calcium chloride solution with a concentration of 3.0 mol/l dropwise into the emulsification system, and control the temperature of the water bath to 80°C for emulsification for 1 hour;

Step 5: Add 10 parts of sodium carbonate solution with a concentration of 0.9mol/l dropwise to the emulsification system obtained in step 4, and control the rate of addition to 0.8ml/min. The obtained filter cake is repeatedly washed with distilled water, and dried at a controlled temperature of 60° C. to obtain white sachaycanthia oil microcapsule powder with a particle diameter of 40nm-60nm. Said cane fruit oil microcapsules use calcium carbonate as the wall material and cane fruit oil as the core material according to the mass ratio, wherein the core material: wall material is 1:1.

The preparation method of the above-mentioned skin softening water containing sachaeto fruit oil microcapsules is:

Step 1: Weigh 100 parts of distilled water; 3 parts of 1,3-butanediol; 3 parts of propylene glycol; 3 parts of sodium hyaluronate; 4 parts of polyethylene glycol-32; 20; 2 parts sachaeja oil microcapsules; 3 parts glycerin: 0.1 part tocopherol; 0.1 part di-tert-butylcresol; 0.50 part paraben; 0.5 part sodium benzoate; 0.05 part rose essence; Sodium, propylene glycol and glycerin are mixed in proportion to obtain 9 parts of sodium hyaluronate, propylene glycol and glycerin mixture as a humectant, and tocopherol and di-tert-butylcresol are mixed in proportion to obtain 0.2 parts of a mixture of tocopherol and di-tert-butylcresol as Antioxidant, mix sodium benzoate and paraben in proportion to get 1 part of a mixture of sodium benzoate and paraben as a preservative;

Step 2: Dissolve 9 parts of moisturizer in 80 parts of distilled water, and mix evenly for 15 minutes under continuous stirring at 400 rpm;

Step 3: Add 0.2 parts of antioxidant to the remaining distilled water, heat to 50°C, and stir continuously at 400rpm for 10min;

Step 4: Add the mixture obtained in step 3 to the mixture obtained in step 2, mix evenly under continuous stirring at 500pm, then add 1 part of preservative and mix, adjust the pH to 6 with 5% glacial acetic acid solution by mass percentage, Cool down to 25°C;

Step 5: To the mixture obtained in step 4, add 2 parts sachaetra oil microcapsules, 3 parts 1,3-butanediol, 4 parts polyethylene glycol-32, 2 parts methyl gluceth- 20, 0.05 parts of rose essence, mixed evenly under continuous stirring at 450rpm, this process continued for 2h, until the microcapsules of cane oil microcapsules were evenly dispersed, then adjusted the pH to 5.5 with NaOH solution with a concentration of 8% by mass percentage, and let it stand 3h, that is, softening water.

Example 2

A skin softening lotion containing sachaeto fruit oil microcapsules, in parts by weight, its raw materials include: 130 parts of distilled water; 4 parts of 1,3-butanediol; 4 parts of propylene glycol; 4 parts of sodium hyaluronate; 5 parts 3 parts of polyethylene glycol-32; 3 parts of methyl gluceth-20; 4 parts of sachaeja oil microcapsules; 3 parts of glycerin: 0.2 parts of tocopherol; 0.2 parts of di-tert-butylcresol; Formate; 0.8 parts sodium benzoate; 0.08 parts rose essence.

In parts by weight, the raw materials for preparing the sachaetra oil microcapsules include: 4 parts of sachaeto fruit oil, 0.8 parts of emulsifier, 4 parts of co-emulsifier, 0.75 part of preservative and 130 parts of water. The emulsifier is a compound of Span-80 and Tween-80, and the ratio of Span-80:Tween-80 is 1:1. The co-emulsifier is 1,3-butanediol, and the preservative is paraben.

The preparation method of described cane fruit oil microcapsules is:

Step 1: 4 parts of sachaetra oil, 0.8 part of emulsifier and 4 parts of co-emulsifier are placed in a container, and a stable oil phase system is obtained by homogeneous treatment at a rate of 600 r/min;

Step 2: Dissolving 0.75 parts of preservative in 130 parts of water to obtain the water phase;

Step 3: Add the obtained water phase to the obtained oil phase system at a temperature range of 75°C, and control the addition rate to 1mL/min to form an emulsified system;

Step 4: Add 12.5 parts of calcium chloride solution with a concentration of 3.75 mol/l dropwise into the emulsification system, and control the temperature of the water bath to 80°C for emulsification for 1 hour;

Step 5: Add 12.5 parts of sodium carbonate solution with a concentration of 1.18mol/l dropwise to the emulsification system obtained in step 4, and control the rate of addition to 0.8ml/min. The obtained filter cake was repeatedly washed with distilled water, and dried at a controlled temperature of 60° C. to obtain white sachaycanthia oil microcapsule powder, as shown in FIG. 1 , with a particle size of 40nm-60nm. Said cane fruit oil microcapsules use calcium carbonate as the wall material and cane fruit oil as the core material according to the mass ratio, wherein the core material: wall material is 1.2:1.

The preparation method of the above-mentioned skin softening water containing sachaeto fruit oil microcapsules is:

Step 1: Weigh 130 parts of distilled water; 4 parts of 1,3-butanediol; 4 parts of propylene glycol; 4 parts of sodium hyaluronate; 5 parts of polyethylene glycol-32; 20; 4 parts sachaeja oil microcapsules; 3 parts glycerin: 0.2 part tocopherol; 0.2 part di-tert-butyl cresol; 0.8 part paraben; 0.8 part sodium benzoate; 0.08 part rose essence;

Mix sodium hyaluronate, propylene glycol and glycerin in proportion to obtain 11 parts of a mixture of sodium hyaluronate, propylene glycol and glycerin as a moisturizer;

Tocopherol and di-tert-butylcresol are mixed in proportion to obtain 0.4 parts of tocopherol and di-tert-butylcresol mixture as an antioxidant;

Sodium benzoate and paraben are mixed in proportion to obtain 1.6 parts of a mixture of sodium benzoate and paraben as a preservative;

Step 2: Dissolve 11 parts of moisturizer in 100 parts of distilled water, and mix evenly for 15 minutes under continuous stirring at 400 rpm;

Step 3: Add 0.4 parts of antioxidant to the remaining distilled water, heat to 50°C, and stir continuously at 400rpm for 10min;

Step 4: Add the mixture obtained in step 3 to the mixture obtained in step 2, mix evenly under continuous stirring at 500pm, then add 1.6 parts of preservatives and mix, and adjust the pH to 6 with glacial acetic acid solution with a concentration of 5% by mass, Cool down to 25°C;

Step 5: To the mixture obtained in step 4, add 4 parts of sachaeto fruit oil microcapsules, 4 parts of 1,3-butanediol, 5 parts of polyethylene glycol-32, 3 parts of methyl gluceth- 20, 0.08 parts of rose essence, mixed evenly under continuous stirring at 450rpm, this process continued for 2h, until the microcapsules of cane fruit oil were uniformly dispersed, then adjusted the pH to 5.5 with NaOH solution with a mass percentage concentration of 8%, and let it stand 3h, that is, softening water.

Example 3

A skin softening lotion containing sachaeto fruit oil microcapsules, in parts by weight, its raw materials include: 160 parts of distilled water; 5 parts of 1,3-butanediol; 5 parts of propylene glycol; 5 parts of sodium hyaluronate; 6 parts 1 part Polyethylene Glycol-32; 4 parts Methyl Gluceth-20; 8 parts Sachaja Oil Microcapsules; 4 parts Glycerin: 0.3 parts Tocopherol; 0.3 parts Di-tert-Butylcresol; Formate; 1 part sodium benzoate; 0.1 part rose essence.

In parts by weight, the raw materials for the preparation of the sachaeji oil microcapsules include: 8 parts of sachaetra oil, 1 part of emulsifier, 5 parts of co-emulsifier, 1 part of preservative and 160 parts of water. The emulsifier is a compound of Span-80 and Tween-80, and the ratio of Span-80:Tween-80 is 1:1. The co-emulsifier is 1,3-butanediol, and the preservative is paraben.

The preparation method of described cane fruit oil microcapsules is:

Step 1: Put 8 parts of sachaetra oil, 1 part of emulsifier and 5 parts of co-emulsifier in a container, and process it homogeneously at a rate of 600 r/min to obtain a stable oil phase system;

Step 2: Dissolving 1 part of preservative in 160 parts of water to obtain the water phase;

Step 3: Add the obtained water phase to the obtained oil phase system at a temperature range of 75°C, and control the addition rate to 1mL/min to form an emulsified system;

Step 4: Add 15 parts of calcium chloride solution with a concentration of 4.5mol/l dropwise into the emulsification system, and control the temperature of the water bath to 80°C for emulsification for 1 hour;

Step 5: 15 parts of sodium carbonate solutions with a concentration of 1.41mol/l are added dropwise to the emulsification system obtained in step 4, and the rate of addition is controlled to 0.8ml/min. The obtained filter cake is repeatedly washed with distilled water, and dried at a controlled temperature of 60° C. to obtain white sachaycanthia oil microcapsule powder with a particle diameter of 40nm-60nm. Said cane fruit oil microcapsules use calcium carbonate as the wall material and cane fruit oil as the core material according to the mass ratio, wherein the core material: wall material is 1.5:1.

The preparation method of the above-mentioned skin softening water containing sachaeto fruit oil microcapsules is:

Step 1: Weigh 160 parts of distilled water; 5 parts of 1,3-butanediol; 5 parts of propylene glycol; 5 parts of sodium hyaluronate; 6 parts of polyethylene glycol-32; 20; 8 parts sachaeja oil microcapsules; 4 parts glycerin: 0.3 part tocopherol; 0.3 part di-tert-butylcresol; 1 part paraben; 1 part sodium benzoate; 0.1 part rose essence;

Mix sodium hyaluronate, propylene glycol and glycerin in proportion to obtain 14 parts of a mixture of sodium hyaluronate, propylene glycol and glycerin as a moisturizer;

Tocopherol and di-tert-butylcresol are mixed in proportion to obtain 0.6 parts of tocopherol and di-tert-butylcresol mixture as an antioxidant;

Sodium benzoate and paraben are mixed in proportion to obtain 2 parts of a mixture of sodium benzoate and paraben as a preservative;

Step 2: Dissolve 14 parts of moisturizer in 130 parts of distilled water, and mix evenly for 15 minutes under continuous stirring at 400 rpm;

Step 3: Add 0.6 parts of antioxidant to the remaining distilled water, heat to 50°C, and stir continuously at 400rpm for 10min;

Step 4: Add the mixture obtained in step 3 to the mixture obtained in step 2, mix evenly under continuous stirring at 500pm, then add 2 parts of preservatives and mix, and adjust the pH to 6 with 5% glacial acetic acid solution by mass percentage, Cool down to 25°C;

Step 5: To the mixture obtained in step 4, add 8 parts of cane oil microcapsules, 5 parts of 1,3-butanediol, 6 parts of polyethylene glycol-32, 4 parts of methyl gluceth- 20, 0.1 part of rose essence, mixed evenly under continuous stirring at 450rpm, this process continued for 2h, until the microcapsules of cane oil microcapsules were evenly dispersed, then adjusted the pH to 5.5 with NaOH solution with a concentration of 8% by mass percentage, and allowed to stand 3h, that is, softening water.

The above-mentioned cane fruit oil microcapsule softening lotion is elegant and white, suitable for skin care and maintenance, has the functions of whitening, moisturizing, anti-wrinkle, etc., is easy to absorb, has high safety performance, and is suitable for various skin types.

The moisturizing effect of the cane fruit oil microcapsule skin softening water of implementation case 1-3 is tested.

Test method: Select 60 people aged 20-50, half male and half male, healthy, regular life, no skin disease, randomly divided into 3 groups, 20 people in each group. The test environment temperature is 25°C and the relative humidity is 60% to measure the moisture content of the right face.

Draw a 2 square centimeter square experimental area on the right face as the skin test area. After cleansing the skin, the subjects wiped off the moisture on the skin surface, took 1g of cane fruit oil microcapsule softening water and applied it to the facial skin. Use a skin moisture meter to measure the moisture content of the skin on the right face 2 hours after applying the cane fruit oil microcapsule toner, and record the results. The specific results are shown in the table below.

The test results of the moisturizing effect of the cane fruit oil microcapsule softening water:

Skin moisture content, % Example 1 42.5 Example 2 43.3 Example 3 45.2

What has been described above is only one embodiment of the present invention. For those of ordinary skill in the art, without departing from the structure of the present invention, some deformations and transformations can also be made, which all belong to the scope of the present invention. protected range.

Claims (10)

1. a kind of smoothing toner containing oil and fat of sacha inchi microcapsules, which is characterized in that in parts by weight, raw material includes: 100-160 Part distilled water, 3-5 parts of 1,3-BDOs, 4-6 parts of polyethylene glycol -32,2-4 part methyl gluceth -20,3-14 part moisturizings Agent, 0.1-6 parts of antioxidants, 0.5-3 portions of preservatives and 2-8 parts of oil and fat of sacha inchi microcapsules.

2. the smoothing toner as described in claim 1 containing oil and fat of sacha inchi microcapsules, which is characterized in that the moisturizer is by saturating Bright matter acid sodium, propylene glycol and glycerol composition.

3. the smoothing toner as described in claim 1 containing oil and fat of sacha inchi microcapsules, which is characterized in that the antioxidant by Tocopherol and di-tert-butyl cresol composition.

4. the smoothing toner as described in claim 1 containing oil and fat of sacha inchi microcapsules, which is characterized in that the preservative is by benzene Sodium formate and p-hydroxybenzoate composition.

5. the smoothing toner as described in claim 1 containing oil and fat of sacha inchi microcapsules, which is characterized in that described contains U.S. rattan fruit The raw material of the smoothing toner of oil microcapsule also includes 0.05-0.15 parts of essence.

6. the smoothing toner as described in claim 1 containing oil and fat of sacha inchi microcapsules, which is characterized in that the oil and fat of sacha inchi is micro- The partial size of capsule is 40nm-60nm.

7. the smoothing toner as described in claim 1 containing oil and fat of sacha inchi microcapsules, which is characterized in that in parts by weight, described The raw materials for preparing of oil and fat of sacha inchi microcapsules include: 2-15 parts of oil and fat of sacha inchi, 0.5-1 parts of emulsifier, 0.2-5 parts of assistant for emulsifying agent, 0.5-1 parts and water 100-160 parts of preservative.

8. the smoothing toner as described in claim 1 containing oil and fat of sacha inchi microcapsules, which is characterized in that the emulsifier by The mass ratio of Span-80 and Tween-80 composition, the Span-80 and Tween-80 are 1:1-3；The assistant for emulsifying agent is Hexadecanol, 1,3-BDO any one.

9. the smoothing toner as described in claim 1 containing oil and fat of sacha inchi microcapsules, which is characterized in that the oil and fat of sacha inchi is micro- The preparation method of capsule includes:

Step 1: 2-15 parts of oil and fat of sacha inchi, 0.5-1 parts of emulsifiers and 0.2-5 parts of assistant for emulsifying agents being placed in container, with 300- 900r/min rate homogenization obtains stable oil-based system；

Step 2: 0.5-1 portions of preservatives being dissolved in 100-160 parts of water, water phase is obtained；

Step 3: being 65-85 DEG C in temperature range, resulting water phase is added in resulting oil-based system, speed is added in control For 0.5-1.5mL/min, emulsification system is formed；

Step 4: the calcium chloride solution that 10-15 parts of concentration are 3.0mol/l-4.5mol/l being added drop-wise in emulsification system, water is controlled Bath temperature is 65-80 DEG C of emulsification 0.8-1h；

Step 5: the sodium carbonate liquor that 10-15 parts of concentration are 0.9mol/l-1.4mol/l is added drop-wise to the resulting emulsified body of step 4 In system, after completion of dropwise addition, 6-24h is stood, by filtering, drying obtains oil and fat of sacha inchi microscapsule powder.

10. the preparation method of the smoothing toner containing oil and fat of sacha inchi microcapsules described in claim 1 characterized by comprising

Step 1: weighing 100-160 parts of distilled water, 3-5 parts of 1,3-BDOs, 4-6 parts of polyethylene glycol -32,2-4 part methyls Alcohol polyethers -20,3-14 part moisturizer, 0.1-6 parts of antioxidants, 0.5-3 portions of preservatives and 2-8 parts of oil and fat of sacha inchi microcapsules；Institute The moisturizer stated is Sodium Hyaluronate, propylene glycol and glycerol mixture, and the antioxidant is tocopherol and di-t-butyl first Phenol mixture；The preservative is the mixture of sodium benzoate and p-hydroxybenzoate；

Step 2: 3-14 parts of moisturizer are dissolved in 80-130 parts of distilled water, it is uniformly mixed under the continuously stirring of 300-400rpm Close 15-25min；

Step 3: 0.1-6 parts of antioxidants being added in remaining distilled water, 40-60 DEG C are heated to, 400-600rpm's Continuously stir 10-40min；

Step 4: the resulting mixture of step 3 being added in the resulting mixture of step 2, in the case where 500-700rpm is continuously stirred Uniformly mixing, is added 0.5-3 parts of preservative mixing later, adjusts pH with the glacial acetic acid solution that mass percent concentration is 4-6% To 5.5-6.5, it is cooled to 15-30 DEG C；

Step 5: 2-8 parts of oil and fat of sacha inchi microcapsules, 3-5 parts of 1,3-BDOs, 4-6 is added in resulting mixture in step 4 Part polyethylene glycol -32,2-4 part methyl gluceth -20, the uniform mixing under the continuously stirring of 450-650rpm, until beauty Until rattan fruit oil microcapsule is evenly dispersed, it is 5-6 that the NaOH solution for being then 6-10% with mass percent concentration, which adjusts pH, quiet 1-4h is set to get smoothing toner.