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CN108524393A - A kind of ginger shampoo and preparation method thereof - Google Patents

A kind of ginger shampoo and preparation method thereof Download PDF

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CN108524393A
CN108524393A CN201810595695.0A CN201810595695A CN108524393A CN 108524393 A CN108524393 A CN 108524393A CN 201810595695 A CN201810595695 A CN 201810595695A CN 108524393 A CN108524393 A CN 108524393A
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ginger
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shampoo
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CN108524393B (en
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胡孝勇
黄小梅
侯要华
刘智慧
彭永梅
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Chongqing Super Star Technology Co ltd
Guangzhou Birou Biotechnology Co ltd
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Guangxi Yao Dan Biotechnology Co Ltd
Guangxi University of Science and Technology
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42Amides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/006Antidandruff preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95

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Abstract

The present invention relates to a kind of ginger shampoo and preparation method thereof, the raw material of the ginger shampoo is ginger, gleditsia sinensis, the tuber of multiflower knotweed, aloe, thickener, foaming agent, antipruritic, nutritional ingredient, moisturizer, preservative, pearling agent, citric acid, edible oil, flavouring agent, conditioner, pure water.The preferred ginger of preparation process of the present invention, gleditsia sinensis fleece-flower root, aloe preparation method:It is combined with pulverizer and colloid mill, ginger, gleditsia sinensis etc. can not only dissolved out to the greatest extent, but also can make what it stablized to be present in system, preferably play its effectiveness, while also more energy efficient;Preparation process is repeatedly combined with homogenizer, makes its system dispersion micronized, while keeping system more stable.Therefore this product cleaning effect is good, hair soft after hair washing is easy to comb, and hair-growing effects are good, while can raise scalp, restore scalp ecological environment balance, inhibit head itch, dandruff the problems such as.

Description

一种生姜洗发水及其制备方法A kind of ginger shampoo and preparation method thereof

技术领域technical field

本发明属于洗发用品技术领域,涉及一种生姜洗发水及其制备方法。The invention belongs to the technical field of shampoo products, and relates to a ginger shampoo and a preparation method thereof.

背景技术Background technique

洗发水是指一种具有去头屑、焗油等功能的护发产品,洗发水中含有多种成分,这些成份的综合作用能起到清洁头皮和头发的功能。现代社会人们生活节奏越来越快,带来了作息不规律、精神压力大、经常性失眠等诸多问题。头发健康问题,特别是头屑多、头皮发痒是一道长期困扰人们难以解决的问题。因此,只具有洁发功能的传统洗发水已经不能满足人们的需求。含有生姜的洗发水,更够刺激头皮血管,促进血液循环,刺激毛囊打开,促进毛发再生,同时可以抗维生素E的缺乏,且温和不刺激,在控制头皮油脂分泌也起到一定的作用,而且这种洗发水对人体健康无副作用。同时利用皂角可以治疗粉刺、杀菌的的功效,利用芦荟的保湿功效,能够滋润头发。现有技术中有采用生姜作为原料的洗发水,存在以下问题:不能够使生姜中的姜辣素及其他有效物最大限度的溶出,不能均匀稳定的存在于体系中,容易沉降,生姜的功效不能得到充分利用,生发效果不明显以及清洁抑菌效果不理想。Shampoo refers to a hair care product with the functions of anti-dandruff and oil treatment. Shampoo contains various ingredients. The combined effect of these ingredients can clean the scalp and hair. In modern society, people's life rhythm is getting faster and faster, which has brought many problems such as irregular work and rest, high mental stress, and frequent insomnia. Hair health problems, especially dandruff and itchy scalp are a long-term problem that has plagued people and is difficult to solve. Therefore, the traditional shampoo that only has the hair-cleaning function can no longer satisfy people's needs. Shampoo containing ginger can stimulate blood vessels in the scalp, promote blood circulation, stimulate hair follicles to open, and promote hair regeneration. At the same time, it can resist the lack of vitamin E, and is mild and non-irritating. It also plays a certain role in controlling the secretion of scalp oil, and This shampoo has no side effects on human health. At the same time, using saponins can treat acne and sterilize the effect, and using the moisturizing effect of aloe vera can moisturize the hair. In the prior art, there is a shampoo using ginger as a raw material, which has the following problems: the gingerol and other effective substances in the ginger cannot be dissolved to the maximum extent, they cannot be uniformly and stably present in the system, and they are easy to settle. Can not be fully utilized, the hair growth effect is not obvious and the cleaning and antibacterial effect is not ideal.

公开号为CN106924116A的中国发明专利文件公开了一种茶麸洗发水,该专利将茶麸粉碎成2000目以上的微粉,然后浸泡12-24h,使茶麸中的有效成分溶出,再加入低聚果糖、透明质酸、山茶油,该专利中未清楚说明如何将茶麸粉碎成2000目以上的微粉,实际操作过程中本领域的人员很难将茶麸粉碎成2000目以上;另外,若仅是将茶麸粉碎成微粉,后续的制备过程没有其他使茶麸微粉均匀稳定的存在于体系中的制备步骤,其制备得到的成品还是存在茶麸不能均匀稳定的存在于体系中,容易沉降,茶麸的功效不能得到充分利用,清洁抑菌效果不理想的缺点。且该专利中未提到采用生姜作为原料制作洗发水。The Chinese invention patent document with the publication number CN106924116A discloses a tea bran shampoo. In this patent, the tea bran is crushed into a fine powder of more than 2000 mesh, and then soaked for 12-24 hours to dissolve the active ingredients in the tea bran, and then add oligomer Fructose, hyaluronic acid, camellia oil, the patent does not clearly explain how to crush the tea bran into a fine powder of more than 2000 mesh, it is difficult for those skilled in the art to crush the tea bran into a fine powder of more than 2000 mesh; The tea bran is pulverized into fine powder, and there are no other preparation steps in the subsequent preparation process to make the tea bran fine powder exist in the system uniformly and stably. The finished product still has tea bran that cannot exist uniformly and stably in the system, and is easy to settle. The efficacy of tea bran cannot be fully utilized, and the cleaning and antibacterial effect is not ideal. And do not mention adopting ginger to make shampoo as raw material in this patent.

发明内容Contents of the invention

本发明要解决的技术问题是:提供一种产品清洁、抑菌效果好的生姜洗发水及其制备方法,可以使生姜、皂角、首乌、芦荟更细,更稳定的存在于体系中,使其能更好的发挥其效果,解决了在制备洗发水过程中生姜不易稳定的存在于体系中的问题。The technical problem to be solved in the present invention is: provide a kind of ginger shampoo with good product cleaning and antibacterial effect and preparation method thereof, can make ginger, saponin, Radix Polygonum multiflorum and aloe finer and exist in the system more stably, It can better exert its effect, and solves the problem that ginger is not easy to stabilize in the system during the preparation of shampoo.

解决上述技术问题的技术方案是:一种生姜洗发水,其特征在于:该洗发水主要由下述重量份数的原料制备而成:各原料的总份数为100份,其中生姜5-25份、皂角0-5份、首乌0-5份、芦荟0-5份、增稠剂0.5-12份、发泡剂3-18份、止痒剂0.01-0.6份、营养成分0.1-0.5份、保湿剂0.01-0.05份、防腐剂0.01-1.1份、珠光剂0.3-3份、柠檬酸0.1-0.8份、食用油0.01-0.5份、香味剂0.01-0.3份、调理剂0.1-4份、纯水余量。The technical solution for solving the above-mentioned technical problems is: a ginger shampoo, characterized in that: the shampoo is mainly prepared from the following raw materials in parts by weight: the total parts of each raw material is 100 parts, wherein 5-25 parts of ginger 0-5 parts of saponins, 0-5 parts of Shouwu, 0-5 parts of aloe, 0.5-12 parts of thickener, 3-18 parts of foaming agent, 0.01-0.6 parts of antipruritic agent, 0.1-0.1- 0.5 parts, moisturizing agent 0.01-0.05 parts, preservatives 0.01-1.1 parts, pearlescent agent 0.3-3 parts, citric acid 0.1-0.8 parts, edible oil 0.01-0.5 parts, flavoring agent 0.01-0.3 parts, conditioner 0.1-4 parts parts, the balance of pure water.

芦荟具有杀菌、抗炎作用和湿润美容作用,同时还具有免疫作用、再生作用、解毒作用、抗衰老作用、镇痛和镇静作用以及防晒作用等。Aloe vera has bactericidal, anti-inflammatory and moisturizing beauty effects, and also has immune, regeneration, detoxification, anti-aging, analgesic and sedative effects, and sunscreen effects.

所述止痒剂是己脒定二(羟乙基磺酸盐)和甘宝素;对引起头屑的真菌有很好的抑制效果。The antipruritic agent is hexamidine bis(isethionate) and campanol; it has a good inhibitory effect on fungi that cause dandruff.

所述增稠剂是椰油酰胺丙基甜菜碱(CAB-35)、椰油酰胺DEA、椰油酰胺MEA和丙烯酸(酯)类共聚物。The thickener is cocamide propyl betaine (CAB-35), cocamide DEA, cocamide MEA and acrylic acid (ester) copolymer.

所述发泡剂是月桂醇聚醚硫酸酯钠和月桂醇硫酸脂铵;具有优异的去污,乳化和柔顺调理头发的功效。The foaming agent is sodium laureth sulfate and ammonium lauryl sulfate; it has excellent effects of decontamination, emulsification and smooth conditioning of hair.

所述营养成分是低聚果糖和D-泛醇;低聚果糖:可以抑制皮肤表面有害菌的生长,并且能有效减缓色素沉淀,淡化并消除色斑,对皮肤有良好的作用;D-泛醇:持久的保湿功能,防止头发开叉,受损,可以增加头发的密度,提高发质的光泽。The nutritional ingredients are fructooligosaccharides and D-panthenol; fructooligosaccharides: can inhibit the growth of harmful bacteria on the skin surface, and can effectively slow down pigmentation, dilute and eliminate stains, and have a good effect on the skin; D-panthenol Alcohol: Long-lasting moisturizing function, prevent hair split ends, damage, increase hair density, and improve hair luster.

所述保湿剂是玻尿酸;滋润皮肤、头发,增加头发的光泽。The humectant is hyaluronic acid; moisturizes the skin, hair, and increases the luster of the hair.

所述防腐剂是苯氧乙醇和卡松。The preservatives are phenoxyethanol and Cathone.

所述珠光剂是乙二醇二硬质酸钠。Described pearlescent agent is sodium ethylene glycol distearate.

所述食用油是茶籽油。The edible oil is tea seed oil.

所述香味剂是香精。The flavoring agent is essence.

所述调理剂是聚季铵盐和瓜尔胶羟丙基三甲基氯化铵。The conditioners are polyquaternium and guar hydroxypropyltrimonium chloride.

本发明的进一步技术方案是:一种生姜洗发水,该洗发水主要由下述重量份数的原料制备而成:各原料的总份数为100份,其中生姜10份,皂角0.1份,首乌0.1份,芦荟0.1份,椰油酰胺丙基甜菜碱(CAB-35)7份,椰油酰胺DEA 1份,椰油酰胺MEA 1份,丙烯酸(酯)类共聚物3份,月桂醇聚醚硫酸酯钠9份,月桂醇硫酸酯铵3份,己脒定二(羟乙基磺酸盐)0.1份,甘宝素0.5份,低聚果糖0.2份,D-泛醇0.1份,玻尿酸0.01份,苯氧乙醇1份,卡松0.1份,乙二醇二硬脂酸酯1.2份,柠檬酸0.4份,茶籽油0.2份,香精0.2份,聚季铵盐-47 1.5份,聚季铵盐-10 0.8份,瓜尔胶羟丙基三甲基氯化铵1份,纯水余量。The further technical scheme of the present invention is: a kind of ginger shampoo, this shampoo is mainly prepared from the raw material of following parts by weight: the total parts of each raw material is 100 parts, wherein 10 parts of ginger, 0.1 part of saponins, 0.1 part of Shouwu, 0.1 part of aloe vera, 7 parts of cocamidopropyl betaine (CAB-35), 1 part of cocamide DEA, 1 part of cocamide MEA, 3 parts of acrylic (ester) copolymer, lauryl alcohol 9 parts of sodium polyether sulfate, 3 parts of ammonium lauryl sulfate, 0.1 part of hexamidine di(isethionate), 0.5 part of campanola, 0.2 part of fructooligosaccharide, 0.1 part of D-panthenol, 0.01 part of hyaluronic acid 1 part of phenoxyethanol, 0.1 part of Cathone, 1.2 parts of ethylene glycol distearate, 0.4 parts of citric acid, 0.2 parts of tea seed oil, 0.2 parts of essence, 1.5 parts of polyquaternium-47, polyquaternium 0.8 parts of ammonium salt-10, 1 part of guar gum hydroxypropyltrimethylammonium chloride, and the balance of pure water.

本发明的另一技术方案是:一种上述生姜洗发水的制备方法,包括以下步骤:Another technical scheme of the present invention is: a kind of preparation method of above-mentioned ginger shampoo, comprises the following steps:

⑴用粉碎机将干燥后的生姜或生姜与皂角、生姜、芦荟中的一种、两种、三种原料粉碎,粉碎成100~200目的粉末;(1) Use a pulverizer to pulverize the dried ginger or ginger and one, two or three raw materials of saponins, ginger and aloe, and pulverize them into powders of 100 to 200 meshes;

⑵在乳化锅中加入13~18份纯水,再加入前一步骤制到的物质和茶籽油,加热至95~105℃,在95~105℃熬制0.8~1.2h,冷却静置10~13h;⑵Add 13-18 parts of pure water to the emulsification pot, then add the substance prepared in the previous step and tea seed oil, heat to 95-105°C, boil at 95-105°C for 0.8-1.2h, cool and stand for 10 ~13h;

⑶重新加温到78~83℃,第一步向乳化锅中加入丙烯酸(酯)类共聚物, 均质15~20min,第二步向乳化锅中加入均质过的月桂醇聚醚硫酸酯钠水溶液,加入后均质10~30min;第三步向乳化锅中加入月桂醇硫酸酯铵水溶液和椰油酰胺丙基甜菜碱(CAB-35)水溶液;加料时温度维持在78~83℃;(3) Reheat to 78-83°C, add acrylic acid (ester) copolymer to the emulsification pot in the first step, homogenize for 15-20 minutes, and add homogenized lauryl polyether sulfate into the emulsification pot in the second step Sodium aqueous solution, homogenized for 10-30 minutes after adding; the third step is to add ammonium lauryl sulfate aqueous solution and cocamidopropyl betaine (CAB-35) aqueous solution to the emulsification pot; the temperature is maintained at 78-83 ° C during feeding;

⑷温度维持在78~83℃向乳化锅中加入椰油酰胺DEA、椰油酰胺MEA、甘宝素、己脒定二(羟乙基磺酸盐)和玻尿酸;(4) Maintain the temperature at 78-83°C and add cocamide DEA, cocamide MEA, campanola, hexamidine bis(isethionate) and hyaluronic acid into the emulsification pot;

⑸温度维持在78~83℃随后向乳化锅中加入聚季铵盐-47水溶液、低聚果糖水溶液、D-泛醇水溶液和瓜尔胶羟丙基三甲基氯化铵水溶液,然后向乳化锅中加入聚季铵盐-10水溶液;⑸Maintain the temperature at 78~83℃, then add polyquaternium-47 aqueous solution, fructooligosaccharide aqueous solution, D-panthenol aqueous solution and guar gum hydroxypropyl trimethyl ammonium chloride aqueous solution to the emulsification pot, and then add to the emulsification pot Add polyquaternium-10 aqueous solution to the pot;

⑹温度维持在78~83℃向乳化锅中加入已均质好的乙二醇二硬脂酸酯水溶液,搅拌均质25~35min;⑹The temperature is maintained at 78-83°C. Add the homogenized ethylene glycol distearate aqueous solution into the emulsification pot, and stir for 25-35 minutes;

⑺温度维持在78~83℃向乳化锅中添加2-3份纯水,搅拌均质1.5~2.5h后可以开始降温;⑺The temperature is maintained at 78-83°C, add 2-3 parts of pure water to the emulsification pot, stir and homogenize for 1.5-2.5 hours, then start to cool down;

⑻降温至38~43℃向乳化锅中加入柠檬酸水溶液、苯氧乙醇、卡松和香精,最后补充剩余的水分后搅拌均质1.5~2.5h;(8) Cool down to 38-43°C and add citric acid aqueous solution, phenoxyethanol, Cathone and essence to the emulsification pot, and finally add the remaining water and stir for homogenization for 1.5-2.5 hours;

制备过程还包括有过胶体磨步骤,使步骤⑴粉碎的原料成较稳定的胶体状态,所述的过胶体磨步骤或是设置在步骤⑴与步骤⑵之间,或是设置在步骤⑵与步骤⑶之间,或是设置在步骤⑻之后。The preparation process also includes a step of colloid milling, so that the raw materials pulverized in step (1) are in a relatively stable colloidal state, and the step of colloid milling is either set between step (1) and step (2), or between step (2) and step ⑶, or after step ⑻.

所述月桂醇聚醚硫酸酯钠水溶液、月桂醇硫酸酯铵水溶液、聚季铵盐-47水溶液、瓜尔胶羟丙基三甲基氯化铵水溶液、聚季铵盐-10水溶液和乙二醇二硬脂酸酯水溶液的制备过程是:向溶质中加水使溶质刚好溶解后均质制得;所述低聚果糖水溶液、D-泛醇水溶液和柠檬酸水溶液的制备过程是:向溶质中加水使溶质刚好溶解后制得。Described sodium laureth sulfate aqueous solution, ammonium lauryl sulfate aqueous solution, polyquaternium-47 aqueous solution, guar gum hydroxypropyl trimethyl ammonium chloride aqueous solution, polyquaternium-10 aqueous solution and ethylene glycol The preparation process of the alcohol distearate aqueous solution is: add water to the solute so that the solute just dissolves and then homogeneously obtain; the preparation process of the described fructooligosaccharide aqueous solution, D-panthenol aqueous solution and citric acid aqueous solution is: Add water to make the solute just dissolved in the system.

由于采用上述技术方案,本发明的有益效果为:可以使生姜、皂角、首乌、芦荟更细,更稳定的存在于体系中,使其能更好的发挥其效果。本产品清洁效果好,洗头后头发柔软,易于梳理,生发效果好,同时能够调养头皮,恢复头皮生态环境平衡,抑制头痒、头屑等问题。本发明的优点具体分述如下:Due to the adoption of the above technical scheme, the beneficial effects of the present invention are: the ginger, saponin, Radix Polygoni Multiflori and aloe can be finer and more stable in the system, so that they can better exert their effects. This product has a good cleaning effect. After shampooing, the hair is soft, easy to comb, and has a good hair growth effect. At the same time, it can take care of the scalp, restore the balance of the ecological environment of the scalp, and inhibit itching, dandruff and other problems. Advantage of the present invention is specifically described as follows:

1、本发明优选生姜、皂角、首乌和芦荟的制备方法:用粉碎机和胶体磨联用,不仅可以使生姜、皂角等最大程度的溶出,而且可使其稳定的存在于体系中,更好的发挥其效用,同时还更节能。在制备洗发水过程中,多次与均质机联用,使其体系分散物微粒化,同时使体系更稳定。1. The preferred preparation method of ginger, saponins, Radix Polygoni Multiflori and aloe vera in the present invention: combine the use of pulverizer and colloid mill, not only can make ginger, saponins, etc. dissolve to the greatest extent, but also make them exist stably in the system , better play its role, but also more energy-saving. In the process of preparing shampoo, it is used in conjunction with a homogenizer many times to make the dispersion of the system micronized, and at the same time make the system more stable.

2、本发明原料采用己脒定二(羟乙基磺酸盐)和生姜以及其他原料进行复配,能够产生很好的清洁、抑菌效果。同时生姜中的姜辣素可以刺激头皮血管,促进血液循环,刺激毛囊打开,促进毛发再生,也可以抗维生素E的缺乏。2. The raw materials of the present invention are compounded with hexamidine bis(isethionate) and ginger and other raw materials, which can produce good cleaning and antibacterial effects. At the same time, gingerol in ginger can stimulate blood vessels in the scalp, promote blood circulation, stimulate hair follicles to open, promote hair regeneration, and can also resist vitamin E deficiency.

3、本发明中芦荟具有一定的杀菌、保湿和消除粉刺的功效,同时可以使头发柔软而有光泽、轻松舒缓。3. The aloe vera of the present invention has a certain effect of sterilization, moisturizing and eliminating acne, and can make hair soft and shiny, easy and soothing at the same time.

4、本发明中还添加了低聚果糖和D-泛醇作为营养成分,可以有效抑制皮肤表面有害菌的生长和持久的保湿功效。4. In the present invention, fructooligosaccharide and D-panthenol are also added as nutrients, which can effectively inhibit the growth of harmful bacteria on the skin surface and have a lasting moisturizing effect.

具体实施方式Detailed ways

实施例1Example 1

一种生姜洗发水,各组份重量份数为(纯水和物料共100份):生姜10份,皂角0.1份,首乌0.1份,芦荟0.1份,椰油酰胺丙基甜菜碱(CAB-35)7份,椰油酰胺DEA 1份,椰油酰胺MEA 1份,丙烯酸(酯)类共聚物3份,月桂醇聚醚硫酸酯钠9份,月桂醇硫酸酯铵3份,己脒定二(羟乙基磺酸盐)0.1份,甘宝素0.5份,低聚果糖0.2份,D-泛醇0.1份,玻尿酸0.01份,苯氧乙醇1份,卡松0.1份,乙二醇二硬脂酸酯1.2份,柠檬酸0.4份,茶籽油0.2份,香精0.2份,聚季铵盐-47 1.5份,聚季铵盐-10 0.8份,瓜尔胶羟丙基三甲基氯化铵1份,纯水余量(相当于58.39份)。A ginger shampoo, the parts by weight of each component are (100 parts in total of pure water and materials): 10 parts of ginger, 0.1 part of saponins, 0.1 part of Shouwu, 0.1 part of aloe, cocamidopropyl betaine (CAB -35) 7 parts, 1 part cocamide DEA, 1 part cocamide MEA, 3 parts acrylic (ester) copolymer, 9 parts sodium laureth sulfate, 3 parts ammonium lauryl sulfate, hexamidine 0.1 part of Dingdi (isethionate), 0.5 part of Campanola, 0.2 part of fructooligosaccharide, 0.1 part of D-panthenol, 0.01 part of hyaluronic acid, 1 part of phenoxyethanol, 0.1 part of Cathone, ethylene glycol dihard Fatty acid ester 1.2 parts, citric acid 0.4 parts, tea seed oil 0.2 parts, essence 0.2 parts, polyquaternium-47 1.5 parts, polyquaternium-10 0.8 parts, guar gum hydroxypropyl trimethyl chloride 1 part of ammonium, the balance of pure water (equivalent to 58.39 parts).

实施例2Example 2

一种生姜洗发水,各组份重量份数为(纯水和物料共100份):生姜5份,椰油酰胺丙基甜菜碱(CAB-35)5份,椰油酰胺DEA 0.5份,椰油酰胺MEA 0.5份,丙烯酸(酯)类共聚物1.5份,月桂醇聚醚硫酸酯钠5份,月桂醇硫酸酯铵2份,己脒定二(羟乙基磺酸盐)0.1份,甘宝素0.5份,低聚果糖0.1份,D-泛醇0.1份,玻尿酸0.01份,苯氧乙醇1份,卡松0.1份,乙二醇二硬脂酸酯0.4份,柠檬酸0.2份,茶籽油0.1份,香精0.1份,聚季铵盐-47 1份,聚季铵盐-10 0.5份,瓜尔胶羟丙基三甲基氯化铵0.5份,纯水余量(相当于75.79份)。 A ginger shampoo, the parts by weight of each component are (100 parts of pure water and materials): 5 parts of ginger, 5 parts of cocamidopropyl betaine (CAB-35), 0.5 part of cocamide DEA, coconut oil amide DEA 0.5 parts of oleamide MEA, 1.5 parts of acrylic acid (ester) copolymer, 5 parts of sodium laureth sulfate, 2 parts of ammonium lauryl sulfate, 0.1 part of hexamidine bis(isethionate), campanol 0.5 parts, 0.1 parts of fructooligosaccharides, 0.1 parts of D-panthenol, 0.01 parts of hyaluronic acid, 1 part of phenoxyethanol, 0.1 parts of Cathone, 0.4 parts of ethylene glycol distearate, 0.2 parts of citric acid, tea seed oil 0.1 part, 0.1 part of essence, 1 part of polyquaternium-47, 0.5 part of polyquaternium-10, 0.5 part of guar gum hydroxypropyl trimethyl ammonium chloride, the balance of pure water (equivalent to 75.79 parts) .

实施例3Example 3

一种生姜洗发水,各组份重量份数为(纯水和物料共100份):生姜25份,皂角5份,首乌5份,芦荟5份,椰油酰胺丙基甜菜碱(CAB-35)5份,椰油酰胺DEA 2份,椰油酰胺MEA 2份,丙烯酸(酯)类共聚物3份,月桂醇聚醚硫酸酯钠10份,月桂醇硫酸酯铵5份,己脒定二(羟乙基磺酸盐)0.1份,甘宝素0.5份,低聚果糖0.2份,D-泛醇0.1份,玻尿酸0.01份,苯氧乙醇1份,卡松0.1份,乙二醇二硬脂酸酯0.8份,柠檬酸0.4份,茶籽油0.2份,香精0.3份,聚季铵盐-47 1份,聚季铵盐-10 1份,瓜尔胶羟丙基三甲基氯化铵1份,纯水余量(相当于26.29份)。A ginger shampoo, the parts by weight of each component are (100 parts in total of pure water and materials): 25 parts of ginger, 5 parts of saponins, 5 parts of Radix Polygoni Multiflori, 5 parts of aloe vera, cocamidopropyl betaine (CAB -35) 5 parts, 2 parts of cocamide DEA, 2 parts of cocamide MEA, 3 parts of acrylic (ester) copolymer, 10 parts of sodium laureth sulfate, 5 parts of ammonium lauryl sulfate, hexamidine 0.1 part of Dingdi (isethionate), 0.5 part of Campanola, 0.2 part of fructooligosaccharide, 0.1 part of D-panthenol, 0.01 part of hyaluronic acid, 1 part of phenoxyethanol, 0.1 part of Cathone, ethylene glycol dihard Fatty acid ester 0.8 part, citric acid 0.4 part, tea seed oil 0.2 part, essence 0.3 part, polyquaternium-47 1 part, polyquaternium-10 1 part, guar gum hydroxypropyl trimethyl chloride 1 part of ammonium, the balance of pure water (equivalent to 26.29 parts).

实施例4Example 4

一种实施例1-实施例3所述生姜洗发水的制备方法,采用粉碎机与胶体磨联用,使生姜、皂角、首乌、芦荟成较稳定的胶体状态,使其不沉降,能稳定的存在于体系中,发挥其效用,同时在制备洗发水的过程中多次使用移动均质机使其体系分散物微粒化。A kind of preparation method of the ginger shampoo described in embodiment 1-embodiment 3 adopts pulverizer to be combined with colloid mill to make ginger, saponin, Radix Polygoni Multiflori, and aloe into a relatively stable colloidal state, so that it does not settle and can It exists stably in the system and exerts its effect. At the same time, in the process of preparing shampoo, the mobile homogenizer is used many times to make the dispersion of the system micronized.

包括以下具体步骤:。Including the following specific steps:.

⑴用粉碎机将干燥后的生姜、皂角、首乌、芦荟原料粉碎,粉碎成150目的粉末。(1) Grind the dried ginger, saponins, Radix Polygoni Multiflori and aloe vera raw materials into 150-mesh powder with a pulverizer.

⑵粉碎后的生姜、皂角、首乌、芦荟原料调湿后,边搅拌过胶体磨(胶体磨在常温常压下使用),使其成较稳定的胶体状态。⑵ After the crushed ginger, saponins, Radix Polygoni Multiflori, and aloe vera raw materials are adjusted in humidity, they are stirred through a colloid mill (colloid mills are used at normal temperature and pressure) to make them into a relatively stable colloidal state.

⑶在乳化锅中加入15份纯水(其余的在后面各步加入),再加入过完胶体磨的生姜、皂角、首乌、芦荟等物质和茶籽油,加热至100℃,在100℃熬制1h后关掉蒸汽,在乳化锅中静置12h。(3) Add 15 parts of pure water into the emulsification pot (the rest will be added in the following steps), then add the colloid-milled ginger, saponin, Radix Polygoni Multiflori, aloe and other substances and tea seed oil, heat to 100°C, After boiling at ℃ for 1 hour, turn off the steam, and let it stand in the emulsification pot for 12 hours.

⑷加热使温度为80℃(在加料过程中要保持温度基本稳定),第一步加入丙烯酸(酯)类共聚物(SF-1、液态),均质15~20min,第二步加入均质过的月桂醇聚醚硫酸酯钠水溶液(月桂醇聚醚硫酸酯钠为半固体,加入水使其刚好溶解均质后加入乳化锅),加入后均质30min;第三步加入月桂醇硫酸酯铵水溶液(月桂醇硫酸酯铵为半固体,加入水使其刚好溶解均质后加入乳化锅)、椰油酰胺丙基甜菜碱(CAB-35)(液体)。⑷Heat to keep the temperature at 80°C (keep the temperature basically stable during the feeding process), add acrylic acid (ester) copolymer (SF-1, liquid) in the first step, homogenize for 15-20 minutes, and add homogeneous The aqueous solution of sodium laureth sulfate (sodium laureth sulfate is semi-solid, add water to make it just dissolve and homogenize, then add to the emulsification pot), homogenize for 30 minutes after adding; the third step is to add lauryl sulfate Ammonium aqueous solution (ammonium lauryl sulfate is semi-solid, add water to make it just dissolve and homogenize, then add to the emulsification pot), cocamidopropyl betaine (CAB-35) (liquid).

⑸加入椰油酰胺DEA和椰油酰胺MEA(液态),加入甘宝素(直接用筛子添加),己脒定二(羟乙基磺酸盐)和玻尿酸(固态,直接加入)。⑸ Add Cocamide DEA and Cocamide MEA (liquid), add Campanile (add directly with a sieve), hexamidine di (isethionate) and hyaluronic acid (solid, add directly).

⑹随后加入聚季铵盐-47均质15~20min,(聚季铵盐-47为液态,加入纯水使其刚好溶解均质后加入乳化锅),低聚果糖水溶液(低聚果糖为固态,即加入适量纯水使其刚好溶解后加入乳化锅),D-泛醇水溶液(D-泛醇为液态,可加入适量纯水使其刚好溶解后加入乳化锅),瓜尔胶羟丙基三甲基氯化铵水溶液(瓜尔胶羟丙基三甲基氯化铵为固态,即加入纯水使其刚好溶解均质后加入乳化锅),然后加入聚季铵盐-10水溶液(聚季铵盐-10为固态,加入使其刚好溶解均质后加入乳化锅,该物质容易溶胀,所以在允许的情况下可以尽量多加纯水)。⑹Then add polyquaternium-47 and homogenize for 15-20 minutes, (polyquaternium-47 is in liquid state, add pure water to make it just dissolve and homogeneously add to the emulsification pot), aqueous solution of fructo-oligosaccharide (fructo-oligosaccharide is solid , that is, add an appropriate amount of pure water to make it just dissolve and then add to the emulsification pot), D-panthenol aqueous solution (D-panthenol is in a liquid state, you can add an appropriate amount of pure water to make it just dissolve and then add to the emulsification pot), guar gum hydroxypropyl Trimethyl ammonium chloride aqueous solution (guar gum hydroxypropyl trimethyl ammonium chloride is solid, that is, add pure water to make it just dissolve and homogenize and add to the emulsification pot), then add polyquaternium-10 aqueous solution (polyquaternium Quaternary ammonium salt-10 is solid, add it to make it just dissolved and homogeneous, then add it to the emulsification pot, the substance is easy to swell, so you can add as much pure water as possible).

⑺最后加入已均质好的乙二醇二硬脂酸酯水溶液(珠光片,乙二醇二硬脂酸酯为固态,先加入纯水使其刚好溶解均质珠光片将其颗粒粉碎)加入乳化锅中搅拌均质30min。⑺Finally, add the homogeneous aqueous solution of ethylene glycol distearate (pearl flakes, ethylene glycol distearate is solid, first add pure water to make it just dissolve the homogeneous pearl flakes and crush the particles) Stir and homogenize in the emulsification pot for 30 minutes.

⑻在80℃所有的原料加完之后,在此温度下添加约2-3份纯水,搅拌均质2h后可以开始降温(在自然状态下大概每小时下降3℃,跟外界温度有关)。⑻ After adding all the raw materials at 80°C, add about 2-3 parts of pure water at this temperature, stir and homogenize for 2 hours, and then start to cool down (in a natural state, it will drop by about 3°C per hour, which is related to the external temperature).

⑼在40℃加入柠檬酸水溶液(柠檬酸固态,需要少量水使其刚好溶解),苯氧乙醇(液态),卡松(液态),香精(液态),原料全部加入,并补充剩余的水分后搅拌均质2h,得到成品。⑼Add citric acid aqueous solution at 40°C (citric acid is solid, needs a small amount of water to make it just dissolve), phenoxyethanol (liquid), Cathone (liquid), essence (liquid), add all the raw materials, and add the remaining water Stir homogeneously for 2h to obtain the finished product.

实施例5Example 5

一种实施例1-实施例3所述生姜洗发水的制备方法,包括以下具体步骤:A preparation method of ginger shampoo described in embodiment 1-embodiment 3, comprises the following concrete steps:

⑴用粉碎机将干燥后的生姜、皂角、首乌、芦荟原料粉碎,粉碎成150目的粉末。(1) Grind the dried ginger, saponins, Radix Polygoni Multiflori and aloe vera raw materials into 150-mesh powder with a pulverizer.

⑵在乳化锅中加入15份纯水(其余的在后面各步加入),再加入粉碎的生姜、皂角、首乌、芦荟等物质和茶籽油,加热至100℃,在100℃熬制1h后关掉蒸汽,在乳化锅中静置10h。⑵Add 15 parts of pure water to the emulsification pot (the rest will be added in the following steps), then add crushed ginger, saponin, Radix Polygoni Multiflori, aloe vera and other substances and tea seed oil, heat to 100°C, and boil at 100°C After 1h, turn off the steam, and let it stand in the emulsification pot for 10h.

⑶将步骤⑵制得的物料过胶体磨(胶体磨在常温常压下使用),使其成较稳定的胶体状态。(3) Pass the material obtained in step (2) through a colloid mill (the colloid mill is used at normal temperature and pressure) to make it into a relatively stable colloidal state.

⑷加热使温度为80℃(在加料过程中要保持温度基本稳定),第一步加入丙烯酸(酯)类共聚物(SF-1、液态),均质15~20min,第二步加入均质过的月桂醇聚醚硫酸酯钠水溶液(月桂醇聚醚硫酸酯钠为半固体,加入水使其刚好溶解均质后加入乳化锅),加入后均质30min;第三步加入月桂醇硫酸酯铵水溶液(月桂醇硫酸酯铵为半固体,加入水使其刚好溶解均质后加入乳化锅)、椰油酰胺丙基甜菜碱(液体)。⑷Heat to keep the temperature at 80°C (keep the temperature basically stable during the feeding process), add acrylic acid (ester) copolymer (SF-1, liquid) in the first step, homogenize for 15-20 minutes, and add homogeneous The aqueous solution of sodium laureth sulfate (sodium laureth sulfate is semi-solid, add water to make it just dissolve and homogenize, then add to the emulsification pot), homogenize for 30 minutes after adding; the third step is to add lauryl sulfate Ammonium aqueous solution (ammonium lauryl sulfate is semi-solid, add water to make it just dissolve and homogenize, then add to the emulsification pot), cocamidopropyl betaine (liquid).

⑸加入椰油酰胺DEA和椰油酰胺MEA(液态),加入甘宝素(直接用筛子添加),己脒定二(羟乙基磺酸盐)和玻尿酸(固态,直接加入)。⑸ Add Cocamide DEA and Cocamide MEA (liquid), add Campanile (add directly with a sieve), hexamidine di (isethionate) and hyaluronic acid (solid, add directly).

⑹随后加入聚季铵盐-47均质15~20min,(聚季铵盐-47为液态,加入纯水使其刚好溶解均质后加入乳化锅),低聚果糖水溶液(低聚果糖为固态,即加入适量纯水使其刚好溶解后加入乳化锅),D-泛醇水溶液(D-泛醇为液态,可加入适量纯水使其刚好溶解后加入乳化锅),瓜尔胶羟丙基三甲基氯化铵水溶液(瓜尔胶羟丙基三甲基氯化铵为固态,即加入纯水使其刚好溶解均质后加入乳化锅),然后加入聚季铵盐-10水溶液(聚季铵盐-10为固态,加入使其刚好溶解均质后加入乳化锅,该物质容易溶胀,所以在允许的情况下可以尽量多加纯水)。⑹Then add polyquaternium-47 and homogenize for 15-20 minutes, (polyquaternium-47 is in liquid state, add pure water to make it just dissolve and homogeneously add to the emulsification pot), aqueous solution of fructo-oligosaccharide (fructo-oligosaccharide is solid , that is, add an appropriate amount of pure water to make it just dissolve and then add to the emulsification pot), D-panthenol aqueous solution (D-panthenol is in a liquid state, you can add an appropriate amount of pure water to make it just dissolve and then add to the emulsification pot), guar gum hydroxypropyl Trimethyl ammonium chloride aqueous solution (guar gum hydroxypropyl trimethyl ammonium chloride is solid, that is, add pure water to make it just dissolve and homogenize and add to the emulsification pot), then add polyquaternium-10 aqueous solution (polyquaternium Quaternary ammonium salt-10 is solid, add it to make it just dissolved and homogeneous, then add it to the emulsification pot, the substance is easy to swell, so you can add as much pure water as possible).

⑺最后加入已均质好的乙二醇二硬脂酸酯水溶液(珠光片,乙二醇二硬脂酸酯为固态,先加入纯水使其刚好溶解均质珠光片将其颗粒粉碎)加入乳化锅中搅拌均质30min。⑺Finally, add the homogeneous aqueous solution of ethylene glycol distearate (pearl flakes, ethylene glycol distearate is solid, first add pure water to make it just dissolve the homogeneous pearl flakes and crush the particles) Stir and homogenize in the emulsification pot for 30 minutes.

⑻在80℃所有的原料加完之后,在此温度下添加约2-3份纯水,搅拌均质2h后可以开始降温(在自然状态下大概每小时下降3℃,跟外界温度有关)。⑻ After adding all the raw materials at 80°C, add about 2-3 parts of pure water at this temperature, stir and homogenize for 2 hours, and then start to cool down (in a natural state, it will drop by about 3°C per hour, which is related to the external temperature).

⑼在40℃加入柠檬酸水溶液(柠檬酸固态,需要少量水使其刚好溶解),苯氧乙醇(液态),卡松(液态),香精(液态),原料全部加入,并补充剩余的水分后搅拌均质2h,得到成品。⑼Add citric acid aqueous solution at 40°C (citric acid is solid, needs a small amount of water to make it just dissolve), phenoxyethanol (liquid), Cathone (liquid), essence (liquid), add all the raw materials, and add the remaining water Stir homogeneously for 2h to obtain the finished product.

实施例6Example 6

一种实施例1-实施例3所述生姜洗发水的制备方法,包括以下具体步骤:A preparation method of ginger shampoo described in embodiment 1-embodiment 3, comprises the following concrete steps:

⑴用粉碎机将干燥后的生姜、皂角、首乌、芦荟原料粉碎,粉碎成150目的粉末。(1) Grind the dried ginger, saponins, Radix Polygoni Multiflori and aloe vera raw materials into 150-mesh powder with a pulverizer.

⑵在乳化锅中加入15份纯水(其余的在后面各步加入),再加入粉碎的生姜、皂角、首乌、芦荟等物质和茶籽油,加热至100℃,在100℃熬制1h后关掉蒸汽,在乳化锅中静置12h。⑵Add 15 parts of pure water to the emulsification pot (the rest will be added in the following steps), then add crushed ginger, saponin, Radix Polygoni Multiflori, aloe vera and other substances and tea seed oil, heat to 100°C, and boil at 100°C After 1h, turn off the steam and let it stand in the emulsification pot for 12h.

⑶加热使温度为80℃(在加料过程中要保持温度基本稳定),第一步加入丙烯酸(酯)类共聚物(SF-1、液态),均质15~20min,第二步加入均质过的月桂醇聚醚硫酸酯钠水溶液(月桂醇聚醚硫酸酯钠为半固体,加入水使其刚好溶解均质后加入乳化锅),加入后均质30min;第三步加入月桂醇硫酸酯铵水溶液(月桂醇硫酸酯铵为半固体,加入水使其刚好溶解均质后加入乳化锅)、椰油酰胺丙基甜菜碱(液体)。(3) Heating to keep the temperature at 80°C (keep the temperature basically stable during the feeding process), add acrylic acid (ester) copolymer (SF-1, liquid) in the first step, homogenize for 15-20 minutes, and add homogeneous The aqueous solution of sodium laureth sulfate (sodium laureth sulfate is semi-solid, add water to make it just dissolve and homogenize, then add to the emulsification pot), homogenize for 30 minutes after adding; the third step is to add lauryl sulfate Ammonium aqueous solution (ammonium lauryl sulfate is semi-solid, add water to make it just dissolve and homogenize, then add to the emulsification pot), cocamidopropyl betaine (liquid).

⑷加入椰油酰胺DEA和椰油酰胺MEA(液态),加入甘宝素(直接用筛子添加),己脒定二(羟乙基磺酸盐)和玻尿酸(固态,直接加入)。⑷ Add Cocamide DEA and Cocamide MEA (liquid), add Campanile (add directly with a sieve), hexamidine di (isethionate) and hyaluronic acid (solid, add directly).

⑸随后加入聚季铵盐-47均质15~20min,(聚季铵盐-47为液态,加入纯水使其刚好溶解均质后加入乳化锅),低聚果糖水溶液(低聚果糖为固态,即加入适量纯水使其刚好溶解后加入乳化锅),D-泛醇水溶液(D-泛醇为液态,可加入适量纯水使其刚好溶解后加入乳化锅),瓜尔胶羟丙基三甲基氯化铵水溶液(瓜尔胶羟丙基三甲基氯化铵为固态,即加入纯水使其刚好溶解均质后加入乳化锅),然后加入聚季铵盐-10水溶液(聚季铵盐-10为固态,加入使其刚好溶解均质后加入乳化锅,该物质容易溶胀,所以在允许的情况下可以尽量多加纯水)。(5) Then add polyquaternium-47 and homogenize for 15 to 20 minutes, (polyquaternium-47 is in liquid state, add pure water to make it just dissolve and homogeneously add to the emulsification pot), aqueous solution of fructo-oligosaccharide (fructo-oligosaccharide is solid , that is, add an appropriate amount of pure water to make it just dissolve and then add to the emulsification pot), D-panthenol aqueous solution (D-panthenol is in a liquid state, you can add an appropriate amount of pure water to make it just dissolve and then add to the emulsification pot), guar gum hydroxypropyl Trimethyl ammonium chloride aqueous solution (guar gum hydroxypropyl trimethyl ammonium chloride is solid, that is, add pure water to make it just dissolve and homogenize and add to the emulsification pot), then add polyquaternium-10 aqueous solution (polyquaternium Quaternary ammonium salt-10 is solid, add it to make it just dissolved and homogeneous, then add it to the emulsification pot, the substance is easy to swell, so you can add as much pure water as possible).

⑹最后加入已均质好的乙二醇二硬脂酸酯水溶液(珠光片,乙二醇二硬脂酸酯为固态,先加入纯水使其刚好溶解均质珠光片将其颗粒粉碎)加入乳化锅中搅拌均质30min。⑹Finally, add the homogenized ethylene glycol distearate aqueous solution (pearl flakes, ethylene glycol distearate is solid, first add pure water to make it just dissolve the homogeneous pearl flakes and crush the particles) Stir and homogenize in the emulsification pot for 30 minutes.

⑺在80℃所有的原料加完之后,在此温度下添加约2-3份纯水,搅拌均质2h后可以开始降温(在自然状态下大概每小时下降3℃,跟外界温度有关)。⑺ After adding all the raw materials at 80°C, add about 2-3 parts of pure water at this temperature, stir for homogenization for 2 hours, and then start to cool down (in a natural state, it will drop by about 3°C per hour, which is related to the external temperature).

⑻在40℃加入柠檬酸水溶液(柠檬酸固态,需要少量水使其刚好溶解),苯氧乙醇(液态),卡松(液态),香精(液态),原料全部加入,并补充剩余的水分后搅拌均质2h。⑻Add citric acid aqueous solution at 40°C (citric acid is solid and needs a small amount of water to make it just dissolve), phenoxyethanol (liquid), kason (liquid), essence (liquid), add all the raw materials, and add the remaining water Stir homogeneously for 2h.

⑼将步骤(8)所得到产品过胶体磨(胶体磨在常温常压下使用),过完胶体磨后得成品再进行罐装。⑼ Pass the product obtained in step (8) through a colloid mill (the colloid mill is used at normal temperature and pressure), and then the finished product can be packed after the colloid mill.

本发明效果优越的对比试验The comparative test of the superior effect of the present invention

1、耗电量对比。1. Power consumption comparison.

本发明采用粉碎机和胶体磨联用与采用超微粉碎、冷冻超微粉碎技术将物料粉碎至相同细度(800目),耗电量对比结果见表1。The present invention adopts pulverizer and colloid mill to pulverize materials to the same fineness (800 meshes) with superfine pulverization and freezing superfine pulverization technology, and the comparison results of power consumption are shown in Table 1.

表1 耗电量对比一览表Table 1 Comparison list of power consumption

注:对比例1,采用超微粉碎技术;对比例2,采用冷冻超微粉碎技术。Note: Comparative example 1 adopts superfine pulverization technology; Comparative example 2 adopts freezing superfine pulverization technology.

由表1可知,本发明采用粉碎机和胶体磨联用比采用超微粉碎、冷冻超微粉碎更节能,更利于实际应用推广。It can be known from Table 1 that the combination of pulverizer and colloid mill in the present invention is more energy-saving than ultrafine pulverization and freezing superfine pulverization, and is more conducive to practical application and popularization.

2、洗发水梳理性、柔软性、保湿性的性能对比。2. Performance comparison of shampoo combability, softness and moisture retention.

对比例:市售某品牌的生姜洗发水。Comparative example: a commercially available ginger shampoo of a certain brand.

按本发明方法所制得实施例1-3的洗发水和对比例产品进行性能检测,具体的检测方法如下:对自愿受试者进行使用,每组10个人测量一个月的头发生长长度,取其平均值。根据GB11432对其梳理性、柔软性、保湿性进行测试,各项性能设为6个等级具体如下:6:极好;5:好;4:较好;3:一般;2:较差;1:差。具体检测结果见表2。The shampoo of embodiment 1-3 made by the method of the present invention and comparative example product carry out performance detection, and concrete detection method is as follows: volunteer experimenter is used, every group of 10 people measures the hair growth length of a month, takes its average. According to GB11432, its combability, softness and moisture retention are tested, and the performance is set into 6 grades as follows: 6: excellent; 5: good; 4: good; 3: general; 2: poor; 1 :Difference. The specific test results are shown in Table 2.

表2 洗发水梳理性、柔软性、保湿性的性能检测结果一览表Table 2 List of performance test results of shampoo combability, softness and moisture retention

由表2可知,本发明洗发水的梳理性、柔软性和保湿效果都比较好,本发明生姜的生发效果好。As can be seen from Table 2, the combability, softness and moisturizing effect of the shampoo of the present invention are all better, and the hair growth effect of ginger of the present invention is good.

3、使用胶体磨和没使用胶体磨的物料稳定性对比。3. The material stability comparison between using colloid mill and not using colloid mill.

实验组是将物料(生姜、皂角、首乌、芦荟等)先经过粉碎机再过胶体磨,对照组是采用与本发明相同的物料,只是未采用胶体磨,而是采用其他手段将物料粉碎至与实验组相同的细度,原料稳定性实验结果对比见表3。In the experimental group, the materials (ginger, saponin, Radix Polygoni Multiflori, aloe, etc.) first pass through the pulverizer and then through the colloid mill. Grinding to the same fineness as the experimental group, the comparison of raw material stability test results is shown in Table 3.

表3 物料稳定性对比一览表Table 3 Comparison list of material stability

由表3可知,过完胶体磨之后,其体系的稳定性明显提高,有利于体系的稳定存在。It can be seen from Table 3 that after the colloid mill is completed, the stability of the system is significantly improved, which is conducive to the stable existence of the system.

4、使用均质机制备的洗发水稳定性对比。4. Comparison of the stability of shampoos prepared using a homogenizer.

实验组是按照本发明制备方法所制得实施例1-3的洗发水,与公开号为CN106924116A的中国发明专利制备的一种茶麸洗发水作为对比例进行对比,洗发水稳定性对比实验结果见表4。The experimental group is the shampoo of Example 1-3 prepared according to the preparation method of the present invention, compared with a kind of tea bran shampoo prepared by the Chinese invention patent with the publication number CN106924116A as a comparative example, and the results of the shampoo stability comparison experiment See Table 4.

表4 洗发水稳定性结果检测一览表Table 4 Test list of shampoo stability results

注:表4中,分别是记录常温(25℃)条件下放置1周后检测得到的结果,耐热(48℃)条件下放置2周后检测得到的结果,耐寒(-5~-18℃)条件下放置3周后检测得到的结果。测试条件“耐热-耐寒循环,常温”,时间1个月,是指耐热条件下放置10天,耐寒条件下放置10天,常温条件下放置10天后检测得到的结果;时间2个月,是指耐热条件下放置20天,耐寒条件下放置20天,常温条件下放置20天后检测得到的结果;时间3个月,是指耐热条件下放置30天,耐寒条件下放置30天,常温条件下放置30天后检测得到的结果。Note: In Table 4, the results obtained after being placed under normal temperature (25°C) for 1 week, the results obtained after being placed under heat-resistant (48°C) for 2 weeks, and the results obtained under cold-resistant (-5~-18°C) ) under the conditions of 3 weeks after the detection of the results obtained. The test condition "heat-resistant-cold-resistant cycle, normal temperature", the time is 1 month, refers to the results obtained after being placed under heat-resistant conditions for 10 days, under cold-resistant conditions for 10 days, and at normal temperature for 10 days; the time is 2 months, It refers to the results obtained after being placed under heat-resistant conditions for 20 days, under cold-resistant conditions for 20 days, and under normal temperature conditions for 20 days; the time period is 3 months, which means that it is placed under heat-resistant conditions for 30 days, and under cold-resistant conditions for 30 days. The results obtained after being placed at room temperature for 30 days.

由表4可知,本发明使用可移动均质机后,所得到产品的更稳定。As can be seen from Table 4, after the present invention uses movable homogenizer, the obtained product is more stable.

5、洗发水抑菌效果对比。5. Comparison of antibacterial effect of shampoo.

按照《化妆品微生物检测标准方法细菌总数测定》的方法,检测按本发明的方法所制得实施例1-3的洗发水产品的菌落总数,得到的结果见表5。According to the method of "Cosmetic Microorganism Detection Standard Method for Determination of Total Bacteria", the total number of colonies of the shampoo products of Examples 1-3 prepared by the method of the present invention was detected, and the results obtained are shown in Table 5.

表5洗发水菌落计数结果一览表Table 5 List of Shampoo Colony Count Results

注:1、实施序号0为未添加己眯定二(羟乙基磺酸盐)的菌落总数。2、CFU:菌落形成单位。Note: 1. Implementation number 0 is the total number of colonies without adding hexamidin bis(isethionate). 2. CFU: colony forming unit.

由表6可知,实施例1、2、3中所得的产品均达到国家规定标准(菌落总数≤1000CFU/g)。It can be seen from Table 6 that the products obtained in Examples 1, 2, and 3 all meet the national standard (total number of colonies≤1000CFU/g).

6、根据GB/T29679-2013测试本发明洗发水的理化指标,结果见表6。6. According to GB/T29679-2013, the physical and chemical indicators of the shampoo of the present invention were tested, and the results are shown in Table 6.

表6 洗发水指标(GB/T19679-2013)一览表Table 6 List of shampoo indicators (GB/T19679-2013)

Claims (5)

1. a kind of ginger shampoo, it is characterised in that:The shampoo is mainly prepared by the raw material of following portions by weight:Each original The total number of material be 100 parts, wherein ginger 5-25 parts, 0-5 parts of gleditsia sinensis, 0-5 parts of the tuber of multiflower knotweed, 0-5 parts of aloe, thickener 0.5-12 Part, 3-18 parts of foaming agent, 0.01-0.6 parts of antipruritic, 0.1-0.5 parts of nutritional ingredient, 0.01-0.05 parts of moisturizer, preservative 0.01-1.1 parts, 0.3-3 parts of pearling agent, 0.1-0.8 parts of citric acid, 0.01-0.5 parts of edible oil, 0.01-0.3 parts of flavouring agent, adjust Manage 0.1-4 parts of agent, pure water surplus;
The antipruritic is hexamidine two (isethionate) and climbazole.
2. a kind of ginger shampoo according to claim 1, it is characterised in that:The thickener is cocamidopropyl propyl amide sweet tea Dish alkali (CAB-35), coconut oleoyl amine DEA, coconut oleoyl amine MEA and acrylic acid(Ester)Analog copolymer;
The foaming agent is laureth sodium sulfovinate and laruyl alcohol sulfuric acid ester ammonium;
The nutritional ingredient is oligofructose and D-pantothenyl aleohol;
The moisturizer is sodium hyaluronate;
The preservative is Phenoxyethanol and Kathon CG;
The pearling agent is two stearic acid sodium of ethylene glycol;
The edible oil is tea-seed oil;
The flavouring agent is essence;
The conditioner is polyquaternium and guar hydroxypropyltrimonium ammonium chloride.
3. a kind of ginger shampoo according to claim 2, it is characterised in that:The shampoo is mainly by following portions by weight Raw material be prepared:The total number of each raw material is 100 parts, wherein 10 parts of ginger, 0.1 part of gleditsia sinensis, 0.1 part of the tuber of multiflower knotweed, aloe 0.1 Part, Cocoamidopropyl betaine(CAB-35)7 parts, 1 part of 1 part of coconut oleoyl amine DEA, coconut oleoyl amine MEA, acrylic acid(Ester)Class 3 parts of copolymer, 9 parts of laureth sodium sulfovinate, 3 parts of bay alcohol sulfuric ester ammonium, hexamidine two(Isethionate)0.1 Part, 0.5 part of climbazole, 0.2 part of oligofructose, 0.1 part of D-pantothenyl aleohol, 0.01 part of sodium hyaluronate, 1 part of Phenoxyethanol, 0.1 part of Kathon CG, 1.2 parts of glycol distearate, 0.4 part of citric acid, 0.2 part of tea-seed oil, 0.2 part of essence, 1.5 parts of polyquaternium -47 gather 0.8 part of quaternary ammonium salt -10,1 part of guar hydroxypropyltrimonium ammonium chloride, pure water surplus.
4. a kind of preparation method of the ginger shampoo as described in Claims 2 or 3, it is characterised in that:Include the following steps:
(1) the ginger after drying or one kind in ginger and gleditsia sinensis, ginger, aloe, two kinds, three kinds of raw materials are crushed with pulverizer, It is ground into 100~200 mesh powders;
(2) 13~18 parts of pure water are added in emulsifying pot, the substance and tea-seed oil that the previous step system that adds arrives, it is heated to 95~ 105 DEG C, 0.8~1.2h, 10~13h of cooling and standings are boiled at 95~105 DEG C;
(3) 78~83 DEG C are warmed to again, and acrylic acid is added into emulsification pot in the first step(Ester)Analog copolymer, homogeneous 15~ The laureth sodium sulfovinate aqueous solution crossed of homogeneous is added into emulsification pot in 20min, second step, and homogeneous 10 after addition~ 30min;Third is walked is added bay alcohol sulfuric ester aqueous ammonium and Cocoamidopropyl betaine into emulsification pot(CAB-35)Water Solution;Temperature maintains 78~83 DEG C when charging;
(4) temperature maintains 78~83 DEG C and coconut oleoyl amine DEA, coconut oleoyl amine MEA, climbazole, hexamidine two is added into emulsification pot (Isethionate)And sodium hyaluronate;
(5) temperature maintains 78~83 DEG C then to -47 aqueous solution of addition polyquaternium, oligofructose aqueous solution, D- in emulsification pot Then it is water-soluble Polyquaternium-10 to be added into emulsification pot in panthenol aqueous solution and guar hydroxypropyltrimonium aqueous ammonium chloride solution Liquid;
(6) temperature maintains 78~83 DEG C and the good glycol distearate aqueous solution of homogeneous is added into emulsification pot, and stirring is equal 25~35min of matter;
(7) temperature maintains 78~83 DEG C and adds 2-3 parts of pure water into emulsification pot, can start to drop after 1.5~2.5h of stirring homogeneous Temperature;
(8) it is cooled to 38~43 DEG C and aqueous citric acid solution, Phenoxyethanol, Kathon CG and essence is added into emulsification pot, finally supplement is surplus 1.5~2.5h of homogeneous is stirred after remaining moisture;
Preparation process further includes having colloid mill step, makes (1) raw material that step crushes at relatively stable colloidal state, described Cross colloid mill step or be provided in step (1) with step (2) between, or be provided in step (2) with step (3) between, or set Set step (8) after.
5. the preparation method of ginger shampoo as claimed in claim 4, it is characterised in that:The laureth sodium sulfovinate water Solution, -47 aqueous solution of polyquaternium, guar hydroxypropyltrimonium aqueous ammonium chloride solution, gathers bay alcohol sulfuric ester aqueous ammonium The preparation process of -10 aqueous solution of quaternary ammonium salt and glycol distearate aqueous solution is:Into solute plus water keeps solute just molten It homogenizes after solution;The preparation process of the oligofructose aqueous solution, D-pantothenyl aleohol aqueous solution and aqueous citric acid solution is:To solute In plus water so that solute just dissolve after it is obtained.
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CN109730956A (en) * 2019-03-13 2019-05-10 广州二广生物科技有限公司 Ginger shampoo and preparation method thereof
CN110693786A (en) * 2019-11-15 2020-01-17 蒙建玲 Traditional Chinese medicine hair conditioner and preparation method thereof
CN111658598A (en) * 2020-05-28 2020-09-15 江苏微康生物科技有限公司 Composition for improving scalp ecology and preparation method thereof
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CN113089151A (en) * 2021-04-07 2021-07-09 罗莱生活科技股份有限公司 Three-dimensional antibacterial yarn containing cotton fibers, preparation method of three-dimensional antibacterial yarn and towel product

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CN109730956A (en) * 2019-03-13 2019-05-10 广州二广生物科技有限公司 Ginger shampoo and preparation method thereof
CN109730956B (en) * 2019-03-13 2021-12-07 广州二广生物科技有限公司 Ginger shampoo and preparation method thereof
CN110693786A (en) * 2019-11-15 2020-01-17 蒙建玲 Traditional Chinese medicine hair conditioner and preparation method thereof
CN111658598A (en) * 2020-05-28 2020-09-15 江苏微康生物科技有限公司 Composition for improving scalp ecology and preparation method thereof
CN111956587A (en) * 2020-09-16 2020-11-20 陈媛婷 Black-hair and bright-hair shampoo and preparation method thereof
CN113089151A (en) * 2021-04-07 2021-07-09 罗莱生活科技股份有限公司 Three-dimensional antibacterial yarn containing cotton fibers, preparation method of three-dimensional antibacterial yarn and towel product
CN113089151B (en) * 2021-04-07 2022-06-17 罗莱生活科技股份有限公司 Three-dimensional antibacterial yarn containing cotton fibers, preparation method of three-dimensional antibacterial yarn and towel product

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