CN108359550A - A kind of draft soap Recipe - Google Patents
A kind of draft soap Recipe Download PDFInfo
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- CN108359550A CN108359550A CN201810199151.2A CN201810199151A CN108359550A CN 108359550 A CN108359550 A CN 108359550A CN 201810199151 A CN201810199151 A CN 201810199151A CN 108359550 A CN108359550 A CN 108359550A
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- 239000000344 soap Substances 0.000 title claims abstract description 95
- 239000000341 volatile oil Substances 0.000 claims abstract description 42
- 239000000463 material Substances 0.000 claims abstract description 39
- 238000003756 stirring Methods 0.000 claims abstract description 31
- 239000003921 oil Substances 0.000 claims abstract description 30
- 238000007873 sieving Methods 0.000 claims abstract description 13
- 238000000874 microwave-assisted extraction Methods 0.000 claims abstract description 9
- 244000067601 Chamaesyce thymifolia Species 0.000 claims abstract description 8
- 241000207199 Citrus Species 0.000 claims abstract description 8
- 244000294611 Punica granatum Species 0.000 claims abstract description 8
- 235000014360 Punica granatum Nutrition 0.000 claims abstract description 8
- 235000020971 citrus fruits Nutrition 0.000 claims abstract description 8
- 244000068988 Glycine max Species 0.000 claims abstract description 7
- 235000010469 Glycine max Nutrition 0.000 claims abstract description 7
- 229920002907 Guar gum Polymers 0.000 claims abstract description 7
- 244000179970 Monarda didyma Species 0.000 claims abstract description 7
- 235000010672 Monarda didyma Nutrition 0.000 claims abstract description 7
- 235000004347 Perilla Nutrition 0.000 claims abstract description 7
- 244000124853 Perilla frutescens Species 0.000 claims abstract description 7
- 240000005319 Sedum acre Species 0.000 claims abstract description 7
- 235000014327 Sedum acre Nutrition 0.000 claims abstract description 7
- 150000004676 glycans Chemical class 0.000 claims abstract description 7
- 239000000665 guar gum Substances 0.000 claims abstract description 7
- 229960002154 guar gum Drugs 0.000 claims abstract description 7
- 235000010417 guar gum Nutrition 0.000 claims abstract description 7
- 229920001282 polysaccharide Polymers 0.000 claims abstract description 7
- 239000005017 polysaccharide Substances 0.000 claims abstract description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 7
- 238000000034 method Methods 0.000 claims abstract description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Inorganic materials [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 50
- 235000019198 oils Nutrition 0.000 claims description 28
- 235000008216 herbs Nutrition 0.000 claims description 27
- 239000003094 microcapsule Substances 0.000 claims description 25
- 239000004909 Moisturizer Substances 0.000 claims description 18
- 230000001333 moisturizer Effects 0.000 claims description 18
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 15
- 230000008014 freezing Effects 0.000 claims description 15
- 238000007710 freezing Methods 0.000 claims description 15
- 238000000605 extraction Methods 0.000 claims description 13
- 238000002156 mixing Methods 0.000 claims description 12
- 238000002360 preparation method Methods 0.000 claims description 12
- 238000005303 weighing Methods 0.000 claims description 12
- 238000002844 melting Methods 0.000 claims description 7
- 230000008018 melting Effects 0.000 claims description 7
- 238000004806 packaging method and process Methods 0.000 claims description 7
- KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 claims description 6
- 240000002262 Litsea cubeba Species 0.000 claims description 6
- 235000012854 Litsea cubeba Nutrition 0.000 claims description 6
- 235000008331 Pinus X rigitaeda Nutrition 0.000 claims description 6
- 235000011613 Pinus brutia Nutrition 0.000 claims description 6
- 241000018646 Pinus brutia Species 0.000 claims description 6
- 235000004789 Rosa xanthina Nutrition 0.000 claims description 6
- 241000109329 Rosa xanthina Species 0.000 claims description 6
- 235000018936 Vitellaria paradoxa Nutrition 0.000 claims description 6
- 241001135917 Vitellaria paradoxa Species 0.000 claims description 6
- 235000013871 bee wax Nutrition 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 6
- 235000021018 plums Nutrition 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 6
- 238000010257 thawing Methods 0.000 claims description 6
- 239000002775 capsule Substances 0.000 claims description 5
- 239000003240 coconut oil Substances 0.000 claims description 5
- 235000019864 coconut oil Nutrition 0.000 claims description 5
- 229920002643 polyglutamic acid Polymers 0.000 claims description 5
- 238000001694 spray drying Methods 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims 1
- 239000012166 beeswax Substances 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 7
- WCXDHFDTOYPNIE-UHFFFAOYSA-N acetamiprid Chemical compound N#CN=C(C)N(C)CC1=CC=C(Cl)N=C1 WCXDHFDTOYPNIE-UHFFFAOYSA-N 0.000 abstract description 2
- 230000003712 anti-aging effect Effects 0.000 abstract description 2
- 239000000284 extract Substances 0.000 abstract description 2
- 230000003020 moisturizing effect Effects 0.000 abstract description 2
- 230000002087 whitening effect Effects 0.000 abstract description 2
- 241000220317 Rosa Species 0.000 abstract 1
- 239000000203 mixture Substances 0.000 description 6
- 238000009472 formulation Methods 0.000 description 4
- 239000003292 glue Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 3
- 239000003205 fragrance Substances 0.000 description 3
- 229920002674 hyaluronan Polymers 0.000 description 3
- 229960003160 hyaluronic acid Drugs 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- OSDLLIBGSJNGJE-UHFFFAOYSA-N 4-chloro-3,5-dimethylphenol Chemical compound CC1=CC(O)=CC(C)=C1Cl OSDLLIBGSJNGJE-UHFFFAOYSA-N 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 2
- 239000005864 Sulphur Substances 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 230000000855 fungicidal effect Effects 0.000 description 2
- 239000000417 fungicide Substances 0.000 description 2
- 208000015181 infectious disease Diseases 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 235000019489 Almond oil Nutrition 0.000 description 1
- 241000205585 Aquilegia canadensis Species 0.000 description 1
- 235000009024 Ceanothus sanguineus Nutrition 0.000 description 1
- 241000218646 Cedrus deodara Species 0.000 description 1
- 240000003538 Chamaemelum nobile Species 0.000 description 1
- 235000007866 Chamaemelum nobile Nutrition 0.000 description 1
- ZHLKXBJTJHRTTE-UHFFFAOYSA-N Chlorobenside Chemical compound C1=CC(Cl)=CC=C1CSC1=CC=C(Cl)C=C1 ZHLKXBJTJHRTTE-UHFFFAOYSA-N 0.000 description 1
- 244000060011 Cocos nucifera Species 0.000 description 1
- 235000013162 Cocos nucifera Nutrition 0.000 description 1
- 240000007311 Commiphora myrrha Species 0.000 description 1
- 235000006965 Commiphora myrrha Nutrition 0.000 description 1
- 208000035473 Communicable disease Diseases 0.000 description 1
- 241000208152 Geranium Species 0.000 description 1
- 244000032014 Java citronella Species 0.000 description 1
- 240000003553 Leptospermum scoparium Species 0.000 description 1
- 235000015459 Lycium barbarum Nutrition 0.000 description 1
- 235000007232 Matricaria chamomilla Nutrition 0.000 description 1
- 241000378544 Melaleuca quinquenervia Species 0.000 description 1
- 235000007265 Myrrhis odorata Nutrition 0.000 description 1
- 240000002505 Pogostemon cablin Species 0.000 description 1
- 235000011751 Pogostemon cablin Nutrition 0.000 description 1
- 208000003251 Pruritus Diseases 0.000 description 1
- 240000004808 Saccharomyces cerevisiae Species 0.000 description 1
- 240000002657 Thymus vulgaris Species 0.000 description 1
- 235000007303 Thymus vulgaris Nutrition 0.000 description 1
- XEFQLINVKFYRCS-UHFFFAOYSA-N Triclosan Chemical compound OC1=CC(Cl)=CC=C1OC1=CC=C(Cl)C=C1Cl XEFQLINVKFYRCS-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000008168 almond oil Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000013065 commercial product Substances 0.000 description 1
- 239000000287 crude extract Substances 0.000 description 1
- 238000005202 decontamination Methods 0.000 description 1
- 230000003588 decontaminative effect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000013538 functional additive Substances 0.000 description 1
- 230000001408 fungistatic effect Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000003906 humectant Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 239000002085 irritant Substances 0.000 description 1
- 231100000021 irritant Toxicity 0.000 description 1
- BEJNERDRQOWKJM-UHFFFAOYSA-N kojic acid Chemical compound OCC1=CC(=O)C(O)=CO1 BEJNERDRQOWKJM-UHFFFAOYSA-N 0.000 description 1
- 229960004705 kojic acid Drugs 0.000 description 1
- WZNJWVWKTVETCG-UHFFFAOYSA-N kojic acid Natural products OC(=O)C(N)CN1C=CC(=O)C(O)=C1 WZNJWVWKTVETCG-UHFFFAOYSA-N 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 239000002068 microbial inoculum Substances 0.000 description 1
- 210000000214 mouth Anatomy 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 210000003800 pharynx Anatomy 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 239000001585 thymus vulgaris Substances 0.000 description 1
- ICUTUKXCWQYESQ-UHFFFAOYSA-N triclocarban Chemical compound C1=CC(Cl)=CC=C1NC(=O)NC1=CC=C(Cl)C(Cl)=C1 ICUTUKXCWQYESQ-UHFFFAOYSA-N 0.000 description 1
- 229960001325 triclocarban Drugs 0.000 description 1
- 229960003500 triclosan Drugs 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000010497 wheat germ oil Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/06—Inorganic compounds
- C11D9/18—Water-insoluble compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/225—Polymers
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/44—Perfumes; Colouring materials; Brightening agents ; Bleaching agents
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
- Cosmetics (AREA)
Abstract
The present invention proposes a kind of draft soap Recipe, includes the following steps：Choose pomegranate seed, fragrant citrus pericarp, Euphorbia thymifolia, purpleflower stonecrop herb, bergamot, purple perilla, rose and Song Hongmei；It dries, crushes, sieving is added in Microwave Extraction Apparatus and extracts, and collects oil phase；Soluble soybean polysaccharide and guar gum are weighed respectively, wall material is obtained after being stirred, wall material is added to the water, wall material solution is obtained after stirring and dissolving, oil phase is added into wall material solution, is spray-dried after homogeneous, the technique of the application can keep the performance of essential oil for a long time, to whitening, moisturizing, it is anti-aging have good effect, and the faint scent to assail the nostrils can be given out.
Description
Technical field
The invention belongs to wash shield product scope, and in particular to a kind of draft soap Recipe.
Background technology
Perfumed soap is a kind of common daily necessities, and current market sales of tradition perfumed soap all uses chemical substance to synthesize
It makes, as the improvement of people's living standards, the especially outburst of the extensive infectious disease caused by bacterium infection, more exacerbates people
Demand to antibacterial type perfumed soap.Common fungicide has sulphur in perfumed soap, and such as triclosan etc. of microbial inoculum containing chlorbenside has research
The bacteria resistance function of current common commercially available perfumed soap is compared, finds to indicate the perfumed soap with degerming component in commercial product
(sulphur, triclocarban, parachlorometaxylenol etc.) all has different degrees of fungistatic effect, is significantly higher than conventional toilet soaps (no
Containing degerming component).The one side that these chemical type fungicide also have its unfavorable, such as parachlorometaxylenol, to oral cavity, throat and
Stomach is irritant and corrosivity.In order to overcome the problems, such as these, it is attempted to substitute chemical synthesis with natural plant extracts
The use of product, as functional additive in perfumed soap and natural fragrance.
A kind of essential oil soap of bactericidal function of CN201210516639.6 disclosure of the invention, it is by Sweet Almond Oil and small
Wheat germ oil is put into a container and stirs evenly, be then added tea tree ethereal oil, Pogostemon cablin essential, niaouli essential oil,
Cus-cus essential oil, myrrh essential oil and deodar essential oil, and stir evenly；Again by cold process soap soap base, it is heated to cold after melting completely
But, when soap base temperature is cooled to 50 DEG C or so, deployed essential oil solution is added, and stir evenly, finally pours into system
In the mold of soap, taken out after being cooled to room temperature.
A kind of soap containing plants essential oil of CN200710177304.5 disclosure of the invention, it mainly by Geranium Essential,
Soap matrix system is added after mixing according to a certain percentage in chamomile essential oil, honeysuckle essential oil, oil of Cymbopogon winterianus, thyme essence etc.
At.Body is moistened in clearing heat and detoxicating, the sterilizing and itch-relieving of soap energy of the invention, Clean Living.
It is to be applied directly to the crude extract of plant perfumed soap is made in soap base to prepare natural herb toilet soap in the prior art all, in advance
Processing is simple, and made perfumed soap fragrance is bad, and essential oil bioactivity is low, and power loss of tests is fast.So the present invention develops one kind and can hold
Kubo holds the fancy soap formula and technique of vegetation essential oil bioactivity.
Invention content
The technical problems to be solved by the invention：It is by the thick of plant for natural herb toilet soap is prepared in the prior art all
Extract is applied directly to that perfumed soap is made in soap base, and pretreatment is simple, and made perfumed soap fragrance is bad, and essential oil activity is low, and power loss of tests is fast
The problem of, provide a kind of draft soap Recipe.
In order to solve the above technical problems, the technical solution adopted by the present invention is：
A kind of draft soap Recipe, it is characterised in that：It counts in parts by weight：Including 15~25 parts of micro- glue of essential oils of herbs
Capsule, 50~70 portions of soap lyes, 2~5 parts of moisturizer, 3~5 parts of diatomite and 5~7 parts of vinasse；
The preparation method of the essential oils of herbs microcapsules is:
(1) it counts in parts by weight, chooses 10~15 parts of pomegranate seeds, 5~10 parts of fragrant citrus pericarps, 20~25 parts of Euphorbia thymifolias, 3 respectively
~5 parts of purpleflower stonecrop herbs, 2~8 portions of bergamots, 5~10 parts of purple perillas, 6~12 portions of roses and 8~15 parts of red plums of pine；
(2) it mixes, dries after weighing above-mentioned raw materials by weight, crush, microwave is added in the material after sieving by sieving
In abstraction instrument, 30~40min of Microwave Extraction under 300~400W power, after extraction at a temperature of 3~5 DEG C stand 30~
50min collects oil phase；
(3) in mass ratio 3:1, soluble soybean polysaccharide and guar gum are weighed respectively, wall material are obtained after being stirred, by wall
Material is added to the water, and wall material solution is obtained after stirring and dissolving, oil phase is added into wall material solution, is spray-dried after homogeneous, obtains draft essence
Oil microcapsule.
The mass fraction of the wall material solution be 10~15%, oil phase addition be wall material solution quality 10~
20%.
The spray drying condition 180~220 DEG C of inlet air temperature in order to control, 700~900L/h of compressed air require, into
Expect 2.5~3.0mL/min of speed.
The preparation method of the soap lye is：It counts in parts by weight, chooses 10~15 parts of shea butters, 3~5 portions of coconut palms respectively
Seed oil, 5~7 portions of litsea citrate oils and 6~10 parts of beeswaxs, are heated to melting after being stirred, and delay into the compound lard after thawing
It is slow that 5~10% mass fraction of oil quality, 20% sodium hydroxide solution is added, it is added mixed with 400~600r/min rotating speeds simultaneously
It closes, stirring is at thick, you can obtains soap lye.
The moisturizer is one or more in hyaluronic acid, gamma-polyglutamic acid, Aloe Vera Gel, sorbierite.
A kind of draft soap Recipe, specific process step are：
(1) it is put into mixing machine after first weighing soap lye, moisturizer, diatomite and vinasse according to the ratio, 55~65
5~10min is stirred at a temperature of DEG C, and draft extraction microcapsules are divided equally into 3~5 addition blenders, continue to stir after being all added
Mix 10~15min；
(2) it discharges and pours into mold while hot after stirring, moved into freezing chamber after being cooled to room temperature, at -20 DEG C~-15 DEG C
At a temperature of freeze 8~10h, room temperature is transferred to after freezing, dry in the air soap 10~15 days at room temperature, stripping and slicing, packaging after the soap that dries in the air, you can
Draft soap.
Compared with other methods, advantageous effects are the present invention：
(1) present invention carries out Microwave Extraction from the substances such as pomegranate seed, fragrant citrus pericarp, Euphorbia thymifolia and obtains essential oil, without using molten
Agent, not only environmentally friendly, it is short to shorten extraction time, improves product yield, and it is purer to obtain essential oils of herbs, essential oil activity
It is high；
(2) present invention by Microwave Extraction to essential oil be prepared into microcapsules, microcapsule wall material is water-soluble substances, can be effective
Essential oil is encapsulated, to keep the performance of essential oil for a long time, improves the stability and activity of essential oil；
(3) diatomite and vinasse are added in the present invention in draft soap formula, and wherein diatomite not only has absorption pore dirty
Dirt, and essential oils of herbs microcapsules can be supported in its porous structure, it is that essential oils of herbs microcapsules uniformly divide in soap
Cloth, and to whitening, moisturizing, anti-aging have good effect rich in a large amount of yeast, kojic acid in vinasse；
(4) it is using essential oils of herbs microcapsules and soap lye as main component that draft soap, which is prepared, in the present invention, and auxiliary addition is protected
Humectant, diatomite and vinasse discharge after heating mixing and pour into mold, and dry in the air soap after freezing, stripping and slicing, packaging, you can draft soap is obtained,
The effect of draft formula components safety does not stimulate mildly, and the draft soap being prepared can persistently play essential oils of herbs microcapsules,
Specific excellent skin care decontamination, and the faint scent to assail the nostrils can be given out.
Specific implementation mode
Step 1：The preparation of essential oils of herbs microcapsules
(1) it counts in parts by weight, chooses 10~15 parts of pomegranate seeds, 5~10 parts of fragrant citrus pericarps, 20~25 parts of Euphorbia thymifolias, 3 respectively
~5 parts of purpleflower stonecrop herbs, 2~8 portions of bergamots, 5~10 parts of purple perillas, 6~12 portions of roses and 8~15 parts of red plums of pine；
(2) it mixes, dries after weighing above-mentioned raw materials by weight, crush, microwave is added in the material after sieving by sieving
In abstraction instrument, 30~40min of Microwave Extraction under 300~400W power, after extraction at a temperature of 3~5 DEG C stand 30~
50min collects oil phase；
(3) in mass ratio 3:1, soluble soybean polysaccharide and guar gum are weighed respectively, wall material are obtained after being stirred, by wall
Material is added to the water, and mass fraction is 10~15% wall material solutions after stirring and dissolving, is added oil phase into wall material solution, after homogeneous
It sprays under conditions of 180~220 DEG C, 700~900L/h of compressed air require, 2.5~3.0mL/min of charging rate of inlet air temperature
It is dry, obtain essential oils of herbs microcapsules.
Step 2：The preparation of soap lye
It counts in parts by weight, chooses 10~15 parts of shea butters, 3~5 portions of coconut oil, 5~7 portions of litsea citrate oils and 6 respectively
~10 parts of beeswaxs, are heated to melting after being stirred, and 5~10% matter of oil quality is slowly added into the compound lard after thawing
20% sodium hydroxide solution of score is measured, is added and is mixed simultaneously with 400~600r/min rotating speeds, stirring is at thick, you can
To soap lye.
Step 3：Draft soap formulation ratio
It counts in parts by weight：Including 15~25 parts of essential oils of herbs microcapsules, 50~70 portions of soap lyes, 2~5 parts of moisturizer, 3~
5 parts of diatomite and 5~7 parts of vinasse；
The moisturizer is one or more in hyaluronic acid, gamma-polyglutamic acid, Aloe Vera Gel, sorbierite.
Step 4：Draft soap processing step
(1) it is put into mixing machine after first weighing soap lye, moisturizer, diatomite and vinasse according to the ratio, 55~65
5~10min is stirred at a temperature of DEG C, and draft extraction microcapsules are divided equally into 3~5 addition blenders, continue to stir after being all added
Mix 10~15min；
(2) it discharges and pours into mold while hot after stirring, moved into freezing chamber after being cooled to room temperature, at -20 DEG C~-15 DEG C
At a temperature of freeze 8~10h, room temperature is transferred to after freezing, dry in the air soap 10~15 days at room temperature, stripping and slicing, packaging after the soap that dries in the air, you can
Draft soap.
Example 1
Step 1：The preparation of essential oils of herbs microcapsules
(1) count in parts by weight, respectively choose 10 parts of pomegranate seeds, 5 parts of fragrant citrus pericarps, 20 parts of Euphorbia thymifolias, 3 parts of purpleflower stonecrop herbs, 2 parts
Bergamot, 5 parts of purple perillas, 6 portions of roses and 8 parts of red plums of pine；
(2) it mixes, dries after weighing above-mentioned raw materials by weight, crush, microwave is added in the material after sieving by sieving
In abstraction instrument, the Microwave Extraction 30min under 300W power stands 30min at a temperature of 3 DEG C after extraction, collect oil phase；
(3) in mass ratio 3:1, soluble soybean polysaccharide and guar gum are weighed respectively, wall material are obtained after being stirred, by wall
Material is added to the water, and mass fraction is 10% wall material solution after stirring and dissolving, and oil phase is added into wall material solution, is being entered the wind after homogeneous
It is spray-dried under conditions of 180 DEG C, compressed air require 700L/h, charging rate 2.5mL/min of temperature, obtains the micro- glue of essential oils of herbs
Capsule.
Step 2：The preparation of soap lye
It counts in parts by weight, chooses 10 parts of shea butters, 3 portions of coconut oil, 5 portions of litsea citrate oils and 6 parts of beeswaxs, stirring respectively
It is heated to melting after mixing, 5% mass fraction of oil quality, 20% sodium hydroxide is slowly added into the compound lard after thawing
Solution is added and is mixed simultaneously with 400r/min rotating speeds, and stirring is at thick, you can obtains soap lye.
Step 3：Draft soap formulation ratio
It counts in parts by weight：Including 15 parts of essential oils of herbs microcapsules, 50 portions of soap lyes, 2 parts of moisturizer, 3 parts of diatomite and 5 parts
Vinasse；
Moisturizer is hyaluronic acid and gamma-polyglutamic acid in mass ratio 1:1 mixes.
Step 4：Draft soap processing step
(1) it is put into mixing machine after first weighing soap lye, moisturizer, diatomite and vinasse according to the ratio, in 55 DEG C of temperature
Degree is lower to stir 5min, and draft extraction microcapsules are added three times blender, continue to be stirred 10min after being all added；
(2) it discharges and pours into mold while hot after stirring, moved into freezing chamber after being cooled to room temperature, in -20 DEG C of DEG C of temperature
Lower freezing 8h, is transferred to room temperature after freezing, dry in the air soap 10 days at room temperature, stripping and slicing, packaging after the soap that dries in the air, you can draft soap.
Example 2
Step 1：The preparation of essential oils of herbs microcapsules
(1) count in parts by weight, respectively choose 13 parts of pomegranate seeds, 7 parts of fragrant citrus pericarps, 23 parts of Euphorbia thymifolias, 4 parts of purpleflower stonecrop herbs, 6 parts
Bergamot, 7 parts of purple perillas, 10 portions of roses and 10 parts of red plums of pine；
(2) it mixes, dries after weighing above-mentioned raw materials by weight, crush, microwave is added in the material after sieving by sieving
In abstraction instrument, the Microwave Extraction 35min under 350W power stands 40min at a temperature of 4 DEG C after extraction, collect oil phase；
(3) in mass ratio 3:1, soluble soybean polysaccharide and guar gum are weighed respectively, wall material are obtained after being stirred, by wall
Material is added to the water, and mass fraction is 13% wall material solution after stirring and dissolving, and oil phase is added into wall material solution, is being entered the wind after homogeneous
It is spray-dried under conditions of 200 DEG C, compressed air require 800L/h, charging rate 2.7mL/min of temperature, obtains the micro- glue of essential oils of herbs
Capsule.
Step 2：The preparation of soap lye
It counts in parts by weight, chooses 13 parts of shea butters, 4 portions of coconut oil, 6 portions of litsea citrate oils and 8 parts of beeswaxs, stirring respectively
It is heated to melting after mixing, 5~10% mass fraction of oil quality, 20% hydrogen-oxygen is slowly added into the compound lard after thawing
Change sodium solution, be added and mixed simultaneously with 400~600r/min rotating speeds, stirring is at thick, you can obtains soap lye.
Step 3：Draft soap formulation ratio
It counts in parts by weight：Including 20 parts of essential oils of herbs microcapsules, 60 portions of soap lyes, 3 parts of moisturizer, 4 parts of diatomite and 6 parts
Vinasse；
The moisturizer is gamma-polyglutamic acid and Aloe Vera Gel in mass ratio 1:1 mixes.
Step 4：Draft soap processing step
(1) it is put into mixing machine after first weighing soap lye, moisturizer, diatomite and vinasse according to the ratio, in 60 DEG C of temperature
Degree is lower to stir 7min, and draft extraction microcapsules are divided equally 4 addition blenders, continue to be stirred 13min after being all added；
(2) it discharges and pours into mold while hot after stirring, moved into freezing chamber after being cooled to room temperature, at a temperature of -18 DEG C
Freeze 9h, room temperature be transferred to after freezing, dry in the air soap 12 days at room temperature, stripping and slicing, packaging after the soap that dries in the air, you can draft soap.
Example 3
Step 1：The preparation of essential oils of herbs microcapsules
(1) it counts in parts by weight, chooses 15 parts of pomegranate seeds, 10 parts of fragrant citrus pericarps, 25 parts of Euphorbia thymifolias, 5 parts of purpleflower stonecrop herbs, 8 respectively
Part bergamot, 10 parts of purple perillas, 12 portions of roses and 8~15 parts of red plums of pine；
(2) it mixes, dries after weighing above-mentioned raw materials by weight, crush, microwave is added in the material after sieving by sieving
In abstraction instrument, the Microwave Extraction 40min under 400W power stands 50min at a temperature of 5 DEG C after extraction, collect oil phase；
(3) in mass ratio 3:1, soluble soybean polysaccharide and guar gum are weighed respectively, wall material are obtained after being stirred, by wall
Material is added to the water, and mass fraction is 15% wall material solution after stirring and dissolving, and oil phase is added into wall material solution, is being entered the wind after homogeneous
It is spray-dried under conditions of 220 DEG C, compressed air require 900L/h, charging rate 3.0mL/min of temperature, obtains the micro- glue of essential oils of herbs
Capsule.
Step 2：The preparation of soap lye
It counts in parts by weight, chooses 15 parts of shea butters, 5 portions of coconut oil, 7 portions of litsea citrate oils and 10 parts of beeswaxs respectively, stir
It is heated to melting after mixing mixing, 10% mass fraction of oil quality, 20% hydroxide is slowly added into the compound lard after thawing
Sodium solution is added and is mixed simultaneously with 600r/min rotating speeds, and stirring is at thick, you can obtains soap lye.
Step 3：Draft soap formulation ratio
It counts in parts by weight：Including 25 parts of essential oils of herbs microcapsules, 70 portions of soap lyes, 5 parts of moisturizer, 5 parts of diatomite and 7 parts
Vinasse；
The moisturizer is Aloe Vera Gel and sorbierite in mass ratio 1:1 mixes.
Step 4：Draft soap processing step
(1) it is put into mixing machine after first weighing soap lye, moisturizer, diatomite and vinasse according to the ratio, in 65 DEG C of temperature
Degree is lower to stir 10min, and draft extraction microcapsules are divided equally 5 addition blenders, continue to be stirred 15min after being all added；
(2) it discharges and pours into mold while hot after stirring, moved into freezing chamber after being cooled to room temperature, at a temperature of -15 DEG C
Freeze 10h, room temperature be transferred to after freezing, dry in the air soap 15 days at room temperature, stripping and slicing, packaging after the soap that dries in the air, you can draft soap.
Claims (6)
1. a kind of draft soap Recipe, it is characterised in that：It counts in parts by weight：Including 15~25 parts of essential oils of herbs microcapsules,
50~70 portions of soap lyes, 2~5 parts of moisturizer, 3~5 parts of diatomite and 5~7 parts of vinasse；
The preparation method of the essential oils of herbs microcapsules is:
(1) it counts in parts by weight, chooses 10~15 parts of pomegranate seeds, 5~10 parts of fragrant citrus pericarps, 20~25 parts of Euphorbia thymifolias, 3~5 respectively
Part purpleflower stonecrop herb, 2~8 portions of bergamots, 5~10 parts of purple perillas, 6~12 portions of roses and 8~15 parts of red plums of pine；
(2) it mixes, dries after weighing above-mentioned raw materials by weight, crush, microwave abstracting is added in the material after sieving by sieving
In instrument, 30~40min of Microwave Extraction under 300~400W power stands 30~50min at a temperature of 3~5 DEG C after extraction, receive
Collect oil phase；
(3) in mass ratio 3:1, weigh soluble soybean polysaccharide and guar gum respectively, after being stirred wall material, by wall material plus
Enter in water, wall material solution is obtained after stirring and dissolving, oil phase is added into wall material solution, is spray-dried after homogeneous, it is micro- to obtain essential oils of herbs
Capsule.
2. a kind of draft soap Recipe according to claim 1, it is characterised in that：The quality of the wall material solution point
Number is 10~15%, and oil phase addition is the 10~20% of wall material solution quality.
3. a kind of draft soap Recipe according to claim 1, it is characterised in that：The spray drying condition is control
180~220 DEG C, 700~900L/h of compressed air require, 2.5~3.0mL/min of charging rate of inlet air temperature processed.
4. a kind of draft soap Recipe according to claim 1, it is characterised in that：The preparation method of the soap lye
For：It counts in parts by weight, respectively 10~15 parts of shea butters of selection, 3~5 portions of coconut oil, 5~7 portions of litsea citrate oils and 6~10 parts
Beeswax is heated to melting after being stirred, and 5~10% mass fraction of oil quality is slowly added into the compound lard after thawing
20% sodium hydroxide solution is added and is mixed simultaneously with 400~600r/min rotating speeds, and stirring is at thick, you can obtains soap lye.
5. a kind of draft soap Recipe according to claim 1, it is characterised in that：The moisturizer is hyalomitome
It is one or more in acid, gamma-polyglutamic acid, Aloe Vera Gel, sorbierite.
6. according to a kind of draft soap Recipe of claim 1~6 any one of them, it is characterised in that：Specific process step
For：
(1) it is put into mixing machine after first weighing soap lye, moisturizer, diatomite and vinasse according to the ratio, in 55~65 DEG C of temperature
Degree is lower to stir 5~10min, and draft extraction microcapsules are divided equally 3~5 addition blenders, continue to be stirred after being all added
10~15min；
(2) it discharges and pours into mold while hot after stirring, moved into freezing chamber after being cooled to room temperature, in -20 DEG C~-15 DEG C temperature
8~10h of lower freezing, is transferred to room temperature after freezing, dry in the air soap 10~15 days at room temperature, stripping and slicing, packaging after the soap that dries in the air, you can draft
Soap.
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| CN201810199151.2A CN108359550A (en) | 2018-03-12 | 2018-03-12 | A kind of draft soap Recipe |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810199151.2A CN108359550A (en) | 2018-03-12 | 2018-03-12 | A kind of draft soap Recipe |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111454797A (en) * | 2020-04-21 | 2020-07-28 | 居永明 | Grape seed oil red wine handmade soap and preparation method thereof |
| CN112625814A (en) * | 2020-12-17 | 2021-04-09 | 广州立白企业集团有限公司 | Soap composition containing microcapsule essence and production method thereof |
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