CN108277114A - A kind of production method of the handmade soap containing tangerine oil - Google Patents
A kind of production method of the handmade soap containing tangerine oil Download PDFInfo
- Publication number
- CN108277114A CN108277114A CN201810274819.5A CN201810274819A CN108277114A CN 108277114 A CN108277114 A CN 108277114A CN 201810274819 A CN201810274819 A CN 201810274819A CN 108277114 A CN108277114 A CN 108277114A
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- Prior art keywords
- oil
- citrus
- tangerine oil
- hydrosol
- soap
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- 239000000344 soap Substances 0.000 title claims abstract description 81
- 241000675108 Citrus tangerina Species 0.000 title claims abstract description 60
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 11
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 84
- 239000003921 oil Substances 0.000 claims abstract description 64
- 235000019198 oils Nutrition 0.000 claims abstract description 64
- 241000207199 Citrus Species 0.000 claims abstract description 40
- 235000020971 citrus fruits Nutrition 0.000 claims abstract description 40
- 238000003756 stirring Methods 0.000 claims abstract description 34
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 25
- 238000010438 heat treatment Methods 0.000 claims abstract description 13
- 235000019482 Palm oil Nutrition 0.000 claims abstract description 11
- 235000019483 Peanut oil Nutrition 0.000 claims abstract description 11
- 239000003240 coconut oil Substances 0.000 claims abstract description 11
- 235000019864 coconut oil Nutrition 0.000 claims abstract description 11
- 239000002540 palm oil Substances 0.000 claims abstract description 11
- 239000000312 peanut oil Substances 0.000 claims abstract description 11
- 239000007788 liquid Substances 0.000 claims abstract description 9
- 238000002156 mixing Methods 0.000 claims abstract description 8
- 238000009423 ventilation Methods 0.000 claims abstract description 8
- 238000005303 weighing Methods 0.000 claims abstract description 8
- 238000012360 testing method Methods 0.000 claims description 17
- 239000000341 volatile oil Substances 0.000 claims description 8
- 239000006260 foam Substances 0.000 claims description 7
- 239000007787 solid Substances 0.000 claims description 7
- 238000009835 boiling Methods 0.000 claims description 5
- 239000002994 raw material Substances 0.000 claims description 5
- 238000010992 reflux Methods 0.000 claims description 5
- 238000005057 refrigeration Methods 0.000 claims description 5
- 230000000694 effects Effects 0.000 abstract description 13
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 6
- 208000003251 Pruritus Diseases 0.000 abstract description 4
- 239000004615 ingredient Substances 0.000 abstract description 4
- 238000005406 washing Methods 0.000 abstract description 4
- 230000017531 blood circulation Effects 0.000 abstract description 3
- 238000004140 cleaning Methods 0.000 abstract description 3
- 239000003205 fragrance Substances 0.000 abstract description 3
- 238000001816 cooling Methods 0.000 abstract 1
- 239000000284 extract Substances 0.000 abstract 1
- 235000015097 nutrients Nutrition 0.000 abstract 1
- 239000013589 supplement Substances 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 9
- 235000003140 Panax quinquefolius Nutrition 0.000 description 6
- 240000005373 Panax quinquefolius Species 0.000 description 6
- 230000000638 stimulation Effects 0.000 description 6
- 230000003020 moisturizing effect Effects 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- 241001411320 Eriogonum inflatum Species 0.000 description 3
- 206010040880 Skin irritation Diseases 0.000 description 3
- 230000000845 anti-microbial effect Effects 0.000 description 3
- 239000008131 herbal destillate Substances 0.000 description 3
- 230000007794 irritation Effects 0.000 description 3
- 239000012528 membrane Substances 0.000 description 3
- 238000007789 sealing Methods 0.000 description 3
- 230000036556 skin irritation Effects 0.000 description 3
- 231100000475 skin irritation Toxicity 0.000 description 3
- 241000222122 Candida albicans Species 0.000 description 2
- 241000588724 Escherichia coli Species 0.000 description 2
- 229940095731 candida albicans Drugs 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 230000001408 fungistatic effect Effects 0.000 description 2
- 230000002496 gastric effect Effects 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- FFRBMBIXVSCUFS-UHFFFAOYSA-N 2,4-dinitro-1-naphthol Chemical compound C1=CC=C2C(O)=C([N+]([O-])=O)C=C([N+]([O-])=O)C2=C1 FFRBMBIXVSCUFS-UHFFFAOYSA-N 0.000 description 1
- 208000002874 Acne Vulgaris Diseases 0.000 description 1
- 241001478240 Coccus Species 0.000 description 1
- 241000255925 Diptera Species 0.000 description 1
- 206010013786 Dry skin Diseases 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- 244000178870 Lavandula angustifolia Species 0.000 description 1
- 235000010663 Lavandula angustifolia Nutrition 0.000 description 1
- 244000246386 Mentha pulegium Species 0.000 description 1
- 235000016257 Mentha pulegium Nutrition 0.000 description 1
- 235000004357 Mentha x piperita Nutrition 0.000 description 1
- AFCARXCZXQIEQB-UHFFFAOYSA-N N-[3-oxo-3-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)propyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CCNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 AFCARXCZXQIEQB-UHFFFAOYSA-N 0.000 description 1
- 241000191967 Staphylococcus aureus Species 0.000 description 1
- 206010047139 Vasoconstriction Diseases 0.000 description 1
- 235000009754 Vitis X bourquina Nutrition 0.000 description 1
- 235000012333 Vitis X labruscana Nutrition 0.000 description 1
- 240000006365 Vitis vinifera Species 0.000 description 1
- 235000014787 Vitis vinifera Nutrition 0.000 description 1
- 206010000496 acne Diseases 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000007815 allergy Effects 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000000767 anti-ulcer Effects 0.000 description 1
- 230000000840 anti-viral effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000010495 camellia oil Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 230000002279 cholagogic effect Effects 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000037336 dry skin Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000686 essence Substances 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000004088 foaming agent Substances 0.000 description 1
- 210000000245 forearm Anatomy 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 235000001050 hortel pimenta Nutrition 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 230000007803 itching Effects 0.000 description 1
- 239000001102 lavandula vera Substances 0.000 description 1
- 235000018219 lavender Nutrition 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 239000005445 natural material Substances 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 230000001151 other effect Effects 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 230000008855 peristalsis Effects 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 238000004445 quantitative analysis Methods 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 208000017520 skin disease Diseases 0.000 description 1
- 230000036559 skin health Effects 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 230000035900 sweating Effects 0.000 description 1
- 230000025033 vasoconstriction Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/005—Synthetic soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/44—Perfumes; Colouring materials; Brightening agents ; Bleaching agents
- C11D9/442—Perfumes
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
The present invention relates to articles for washing fields, disclose a kind of production method of the handmade soap containing tangerine oil, include the following steps：Prepare tangerine oil and citrus hydrosol；After weighing peanut oil, coconut oil, palm oil mixing, water proof is stirred while heating；NaOH is weighed to be dissolved in citrus hydrosol；Buck is slowly poured into miscella, and uniform stirring, and tangerine oil is added, is stirred for uniformly until liquid is at thick；Soap lye pours into mold；Cooling, demoulding, ventilation curing.The present invention extracts tangerine oil using orange peel, citrus hydrosol replaces pure water, make tangerine oil handmade soap, handmade soap ingredient obtained is all natural, performance is mild, non-stimulated to skin, has the distinctive peculiar fragrance of citrus itself, also it is that skin supplements pure natural nutrient, and has the effect of anti-bacterial, anti-itching, promote blood circulation while cleaning skin.
Description
Technical field
The invention belongs to daily articles for washing field, more particularly to the production method of a kind of handmade soap containing tangerine oil.
Background technology
Handmade soap with it is pure natural, do not add any chemicals, be easy in safe, high nutrition, environment degradation, moisturizing
The features such as nourishing ingredient abundant and unique moulding by people increasingly favor.With the rise of low-carbon environment-friendly trend, naturally
Essential oil Manual perfumed soap will become the new propensity to consume.
The development of handmade soap new product also constantly has been reported that, is improved particularly with the addition of certain ingredients with special efficacy
The effect of handmade soap, such as Lavender, which is added in handmade soap, can expel mosquito, help cytothesis, improve micro- follow
Ring increases skin gloss, elasticity；Peppermint essential oil, which is added in handmade soap, can promote perspiration, vasoconstriction；Tea oil plus
Enter into handmade soap to resist itching, antiviral, sterilization, can also promote sweating, purify grease, acne inflammation.
Volatile oil in orange peel has stimulation to alimentary canal, can increase gastric secretion, promotes gastrointestinal peristalsis, stomach invigorating
Wind-dispelling.Orange peel also has anti-inflammatory, antiulcer, antibacterial and cholagogic and other effects.There is not been reported for the preparation of tangerine oil handmade soap.
Invention content
It is an object of the invention in view of the shortcomings of the prior art, provide a kind of raw material it is natural, without adding any essence, green
Colour circle protects, the production method of the good tangerine oil handmade soap of moisturizing and nourishing effect.
In order to solve the above technical problems, the present invention adopts the following technical scheme that：
A kind of production method of the handmade soap containing tangerine oil, includes the following steps：
（1）It chooses fresh orange peel and prepares citrus hydrosol and tangerine oil as raw material, it is spare；
（2）After weighing 144 ~ 150 g of peanut oil, 60 ~ 90 g of coconut oil and palm oil 36 ~ 60 g mixing, water proof is heated to 50
DEG C, heating while, is stirred；
（3）36.06 ~ 45.5 g of NaOH are weighed, 95 ~ 118 mL steps are slowly dissolved in（1）In citrus hydrosol obtained, stirring is extremely
NaOH is completely dissolved, its temperature is waited for drop to 50 DEG C；
（4）By step（3）Buck obtained slowly pours into step（2）In miscella in, and uniform stirring；
（5）Take out 2 mL steps（1）Tangerine oil obtained, is added to step（4）In the mixed liquor stirred evenly, it is stirred for
Uniformly until liquid is at thick, even soap lye is obtained；
（6）By step（5）Obtained even soap lye pours into mold；It is cooled to solid state, is demoulded, obtains and pure natural contains tangerine oil
Handmade soap；
（7）By step（6）Obtained handmade soap is placed at shady and cool ventilation indoors 4-6 weeks, waits for that the base number of soap declines, test is by hand
The foam pH value that soap rubs can be used 8 or so.
The step（1）The detailed process for preparing citrus hydrosol and tangerine oil is：
A, fresh orange peel is selected, is put into clean beaker, clear water is cleaned, and is cut into small pieces, is smashed to pieces with scissors；
B, the orange peel after appropriate smash to pieces is taken, is set in flask, suitable quantity of water is added, connects volatile oil determination apparatus and reflux condensing tube；It sets
It is slowly heated to boil in electric jacket；And oil mass in slightly boiling to analyzer is kept not to be further added by, stop heating, place a moment, occurs
Apparent layering；The piston for opening analyzer lower end, removes layer and obtains citrus hydrosol, upper layer is taken to obtain tangerine oil, spare；
C, it contains and takes citrus hydrosol and tangerine oil, seal, place it in 4 DEG C of refrigerators, refrigeration is spare.
The beneficial effects of the present invention are：The handmade soap of the present invention adds tangerine oil active constituent in the production process,
Citrus hydrosol replaces pure water, can retain the nutritional ingredient in natural material, will not stimulate skin, moisturizing effect in use
Fruit is good, has the distinctive peculiar fragrance of citrus itself, the work(for having anti-bacterial, anti-itching while cleaning skin, promoting blood circulation
Effect.
Specific implementation mode
Below in conjunction with specific embodiment, the present invention will be further described, but the present invention is not limited only to these embodiments.
Embodiment 1
Composition of raw materials：144 g of peanut oil, 60 g of coconut oil, palm oil 36 g, NaOH 36.06 g, tangerine oil 2ml, citrus
95 ml of hydrosol.
Preparation method：
1, citrus hydrosol and tangerine oil are prepared：
A, fresh orange peel is selected, is put into clean beaker, clear water is cleaned, and is cut into small pieces, is smashed to pieces with scissors；
B, the orange peel after appropriate smash to pieces is taken, is set in flask, suitable quantity of water is added, connects volatile oil determination apparatus and reflux condensing tube；It sets
It is slowly heated to boil in electric jacket；And oil mass in slightly boiling to analyzer is kept not to be further added by, stop heating, place a moment, occurs
Apparent layering；The piston for opening analyzer lower end, removes layer and obtains citrus hydrosol, upper layer is taken to obtain tangerine oil, spare；
C, citrus hydrosol, sealed membrane sealing, conical flask with cover Sheng is taken to take tangerine oil and stoppered with bottle stopper with clean beaker Sheng；
4 DEG C of refrigerators are placed in, refrigeration is spare.
2, tangerine oil handmade soap is prepared：
（1）After weighing 144 g of peanut oil, 60 g of coconut oil, palm oil 36 g mixing, water proof is heated to 50 DEG C, while heating
Stirring；
（2）36.06 g of NaOH are weighed, are slowly dissolved in 95 mL citrus hydrosols, stirring is completely dissolved to NaOH, waits for its temperature
Drop to 50 DEG C；
（3）By step（2）Buck obtained slowly pours into step（1）In miscella in, be used in combination stirring rod same direction uniform
Stirring；
（4）2ml tangerine oils are measured, step is added to（3）In the mixed liquor stirred evenly, continue to stir evenly until liquid
At thick, even soap lye is obtained；
（5）By step（4）Obtained even soap lye pours into mold；It is cooled to solid state, is demoulded, it is manual to obtain pure natural tangerine oil
Soap；
（6）By step（5）Handmade soap obtained is placed at shady and cool ventilation indoors 4-6 weeks, waits for that the base number of soap declines, test is by hand
The foam pH value that soap rubs can be used 8 or so.
Embodiment 2
Formula：150 g of peanut oil, 90 g of coconut oil, palm oil 60 g, NaOH 45.5 g, tangerine oil 2ml, citrus hydrosol
118 ml
Preparation method：
1, citrus hydrosol and tangerine oil are prepared：
A, fresh orange peel is selected, is put into clean beaker, clear water is cleaned, and is cut into small pieces, is smashed to pieces with scissors；
B, the orange peel after appropriate smash to pieces is taken, is set in flask, suitable quantity of water is added, connects volatile oil determination apparatus and reflux condensing tube；It sets
It is slowly heated to boil in electric jacket；And oil mass in slightly boiling to analyzer is kept not to be further added by, stop heating, place a moment, occurs
Apparent layering；The piston for opening analyzer lower end, removes layer and obtains citrus hydrosol, upper layer is taken to obtain tangerine oil, spare；
C, citrus hydrosol, sealed membrane sealing, conical flask with cover Sheng is taken to take tangerine oil and stoppered with bottle stopper with clean beaker Sheng；
4 DEG C of refrigerators are placed in, refrigeration is spare.
2, tangerine oil handmade soap is prepared：
（1）After weighing 150 g of peanut oil, 90 g of coconut oil, palm oil 60 g mixing, water proof is heated to 50 DEG C, while heating
It is used in combination stirring rod same direction to stir；
（2）NaOH 45.5g are weighed, are slowly dissolved in 118 mL citrus hydrosols, stirring is completely dissolved to NaOH, waits for its temperature
Drop to 50 DEG C；
（3）By step（2）Buck obtained slowly pours into step（1）In miscella in, be used in combination stirring rod same direction uniform
Stirring；
（4）2ml tangerine oils are measured, step is added to（3）In the mixed liquor stirred evenly, continue to stir evenly until liquid
At thick, even soap lye is obtained；
（5）By step（4）Obtained even soap lye pours into mold；It is cooled to solid state, is demoulded, it is manual to obtain pure natural tangerine oil
Soap；
（6）By step（5）Handmade soap obtained is placed at shady and cool ventilation indoors 4-6 weeks, waits for that the base number of soap declines, test is by hand
The foam pH value that soap rubs can be used 8 or so.
Embodiment 3
Composition of raw materials：147 g of peanut oil, 75 g of coconut oil, palm oil 48 g, NaOH 40.78 g, tangerine oil 2ml, citrus
106.5 ml of hydrosol.
Preparation method：
1, citrus hydrosol and tangerine oil are prepared：
A, fresh orange peel is selected, is put into clean beaker, clear water is cleaned, and is cut into small pieces, is smashed to pieces with scissors；
B, the orange peel after appropriate smash to pieces is taken, is set in flask, suitable quantity of water is added, connects volatile oil determination apparatus and reflux condensing tube；It sets
It is slowly heated to boil in electric jacket；And oil mass in slightly boiling to analyzer is kept not to be further added by, stop heating, place a moment, occurs
Apparent layering；The piston for opening analyzer lower end, removes layer and obtains citrus hydrosol, upper layer is taken to obtain tangerine oil, spare；
C, citrus hydrosol, sealed membrane sealing, conical flask with cover Sheng is taken to take tangerine oil and stoppered with bottle stopper with clean beaker Sheng；
4 DEG C of refrigerators are placed in, refrigeration is spare.
2, tangerine oil handmade soap is prepared：
（1）After weighing 147 g of peanut oil, 75 g of coconut oil, palm oil 48 g mixing, water proof is heated to 50 DEG C, while heating
It is used in combination stirring rod same direction to stir；
（2）40.78 g of NaOH are weighed, are slowly dissolved in 106.5 mL citrus hydrosols, stirring is completely dissolved to NaOH, waits for it
Temperature drops to 50 DEG C；
（3）By step（2）Buck obtained slowly pours into step（1）In miscella in, be used in combination stirring rod same direction uniform
Stirring；
（4）2ml tangerine oils are measured, step is added to（3）In the mixed liquor stirred evenly, continue to stir evenly until liquid
At thick, even soap lye is obtained；
（5）By step（4）Obtained even soap lye pours into mold；It is cooled to solid state, is demoulded, it is manual to obtain pure natural tangerine oil
Soap；
（6）By step（5）Handmade soap obtained is placed at shady and cool ventilation indoors 4-6 weeks, waits for that the base number of soap declines, test is by hand
The foam pH value that soap rubs can be used 8 or so.
Comparative example 1
（1）After weighing 147 g of peanut oil, 75 g of coconut oil, palm oil 48 g mixing, water proof is heated to 50 DEG C, while heating
It is used in combination stirring rod same direction to stir；
（2）40.78 g of NaOH are weighed, are slowly dissolved in 106.5 mL water, stirring is completely dissolved to NaOH, its temperature is waited for drop
To 50 DEG C；
（3）By step（2）Buck obtained slowly pours into step（1）In miscella in, be used in combination stirring rod same direction uniform
Stirring；
（4）2ml tangerine oils are measured, step is added to（3）In the mixed liquor stirred evenly, continue to stir evenly until liquid
At thick, even soap lye is obtained；
（5）By step（4）Obtained even soap lye pours into mold；It is cooled to solid state, demoulds, obtains handmade soap；
（6）By step（5）Handmade soap obtained is placed at shady and cool ventilation indoors 4-6 weeks, waits for that the base number of soap declines, test is by hand
The foam pH value that soap rubs can be used 8 or so.
Comparative example 2
（1）After weighing 147 g of peanut oil, 75 g of coconut oil, palm oil 48 g mixing, water proof is heated to 50 DEG C, while heating
It is used in combination stirring rod same direction to stir；
（2）40.78 g of NaOH are weighed, are slowly dissolved in 108.5 mL water, stirring is completely dissolved to NaOH, its temperature is waited for drop
To 50 DEG C；
（3）By step（2）Buck obtained slowly pours into step（1）In miscella in, be used in combination stirring rod same direction uniform
Stirring, until liquid at thick, obtains even soap lye；
（4）By step（3）Obtained even soap lye pours into mold；It is cooled to solid state, demoulds, obtains handmade soap；
（5）By step（4）Handmade soap obtained is placed at shady and cool ventilation indoors 4-6 weeks, waits for that the base number of soap declines, test is by hand
The foam pH value that soap rubs can be used 8 or so.
Performance test
1, irritation is tested
Skin irritation test is carried out to handmade soap made from embodiment 1 ~ 3 and comparative example 1-2 respectively, specially：Experiment soap
A concentration of 5wt% of liquid when dosage is 0.3ml, is classified by HET VAM measurements determination dermoreactions（Opposite values is classified）, by force
Strong stimulation ＞ 2.0% stimulates 1.2-2.0%, as a result medium stimulation 0.8-1.2%, minimal irritation 0.0-0.8% see the table below 1.
The skin irritation test of 1 tangerine oil handmade soap of the present invention of table
As shown in Table 1, comparative example 2 is without addition tangerine oil and citrus hydrosol, obtained by stimulation of the handmade soap to skin
Property belongs to minimal irritation, but has been approached medium field stimulation；Comparative example 1 is reduced due to being added to tangerine oil to skin
Irritation；Due to being added to tangerine oil and citrus hydrosol in embodiment 1 ~ 3, stimulation of the handmade soap to skin is significantly reduced
Property, the mildness of handmade soap can be effectively improved by showing tangerine oil and citrus hydrosol.
2, anti-microbial property test
According to QB/T 2738《The anti-fungistatic effect evaluation method of daily chemical products》Suspension quantitative method to handmade soap produced by the present invention into
Row anti-microbial property test, wherein test concentrations 1:100, action time 20min, test strain is staphylococcus aureus
ATCC6538, Escherichia coli 8099 and Candida albicans, as a result see the table below 2.
The anti-microbial property test result of 2 tangerine oil handmade soap of the present invention of table
As shown in Table 2, due to being added to tangerine oil and citrus hydrosol in embodiment 1 ~ 3 so that handmade soap is to golden yellow grape
Coccus, Escherichia coli, Candida albicans bacteriostasis rate reach 99% or more；And the antibacterial effect of handmade soap made from comparative example 1 ~ 2
Fruit has different degrees of reduction, especially most apparent with the reduction of the fungistatic effect of comparative example 2, shows tangerine oil and citrus hydrosol
With the use of antibacterial, fungistatic effect can be significantly improved.
3, moistening effect is tested
The trial volunteer for choosing 50 skin healths, without skin disease allergies, in volunteer's right hand inner forearm 5cm2's
Position draws test zone, and the water content and the skin after washing 2h for testing the preceding skin of washing respectively with moisture tester contain
Water calculates the increased percentage of water content, as a result see the table below 3.
The moistening effect test result of 3 tangerine oil handmade soap of the present invention of table
As shown in Table 3, tangerine oil handmade soap made from the embodiment of the present invention 1 ~ 3 is pure due to being added to tangerine oil and citrus
Dew has good moisture retention to skin, dry skin tight feeling is effectively relieved, keeps skin smooth tender.And comparative example 1 ~ 2
There is handmade soap made from different degrees of decrease, especially comparative example 2 to the moistening effect of skin in handmade soap obtained
Moistening effect decrease is the most apparent, shows that moistening effect, especially citrus hydrosol pair can be improved in tangerine oil and citrus hydrosol
The moistening effect for improving handmade soap has remarkable effect.
The handmade soap of the implementation case is free of pigment essence, foaming agent and surfactant, will not stimulate skin in use
Skin, moisturizing effect is good, has the distinctive peculiar fragrance of citrus itself, has anti-bacterial, anti-itching while cleaning skin, promotees
Into the effect of blood circulation.
The foregoing is merely presently preferred embodiments of the present invention, all equivalent changes done according to scope of the present invention patent with
Modification should all belong to the covering scope of the present invention.
Claims (2)
1. a kind of production method of handmade soap containing tangerine oil, it is characterised in that：Include the following steps：
（1）It chooses fresh orange peel and prepares citrus hydrosol and tangerine oil as raw material, it is spare；
（2）After weighing 144 ~ 150 g of peanut oil, 60 ~ 90 g of coconut oil and palm oil 36 ~ 60 g mixing, water proof is heated to 50
DEG C, heating while, stirs；
（3）36.06 ~ 45.5 g of NaOH are weighed, 95 ~ 118 mL steps are slowly dissolved in（1）In citrus hydrosol obtained, stirring is extremely
NaOH is completely dissolved, its temperature is waited for drop to 50 DEG C；
（4）By step（3）Buck obtained slowly pours into step（2）In miscella in, and uniform stirring；
（5）Take out 2 mL steps（1）Tangerine oil obtained, is added to step（4）In the mixed liquor stirred evenly, it is stirred for
Uniformly until liquid is at thick, even soap lye is obtained；
（6）By step（5）Obtained even soap lye pours into mold；It is cooled to solid state, is demoulded, obtains and pure natural contains tangerine oil
Handmade soap；
（7）By step（6）Obtained handmade soap is placed at shady and cool ventilation indoors 4-6 weeks, waits for that the base number of soap declines, test is by hand
The foam pH value that soap rubs can be used 8.
2. a kind of production method of handmade soap containing tangerine oil according to claim 1, it is characterised in that：The step
（1）The detailed process for preparing citrus hydrosol and tangerine oil is：
A, fresh orange peel is selected, is put into clean beaker, clear water is cleaned, and is cut into small pieces, is smashed to pieces with scissors；
B, the orange peel after smashing to pieces is taken, is set in flask, water is added, connects volatile oil determination apparatus and reflux condensing tube；It sets in electric jacket
It is slowly heated to boil；And oil mass in slightly boiling to analyzer is kept not to be further added by, stop heating, place a moment, occurs apparent point
Layer；The piston for opening analyzer lower end, removes layer and obtains citrus hydrosol, upper layer is taken to obtain tangerine oil, spare；
C, it contains and takes citrus hydrosol and tangerine oil, seal, place it in 4 DEG C of refrigerators, refrigeration is spare.
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