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CN106587371A - Water quality purifying agent and preparation method thereof - Google Patents

Water quality purifying agent and preparation method thereof Download PDF

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Publication number
CN106587371A
CN106587371A CN201611134855.9A CN201611134855A CN106587371A CN 106587371 A CN106587371 A CN 106587371A CN 201611134855 A CN201611134855 A CN 201611134855A CN 106587371 A CN106587371 A CN 106587371A
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bacillus
agent
water
ivermectin
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许尤厚
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Qinzhou University
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F3/00Biological treatment of water, waste water, or sewage
    • C02F3/34Biological treatment of water, waste water, or sewage characterised by the microorganisms used
    • C02F3/341Consortia of bacteria
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/20Nature of the water, waste water, sewage or sludge to be treated from animal husbandry

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  • Life Sciences & Earth Sciences (AREA)
  • Microbiology (AREA)
  • Biodiversity & Conservation Biology (AREA)
  • Hydrology & Water Resources (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)
  • Detergent Compositions (AREA)
  • Micro-Organisms Or Cultivation Processes Thereof (AREA)

Abstract

本发明公开了一种水质净化剂及其制备方法,由以下质量份数配方成分组成:去离子水40‑60份、枯草芽孢杆菌8‑10份、乳化剂2‑4份、蜡状芽孢杆菌6‑8份、弯曲芽孢杆菌7‑9份、豆粕粉10‑20份、海水30‑50份、伊维菌素3‑5份、碳酸镁5‑7份、碳酸氢钠6‑8份、氨基磺酸7‑9份、过硫酸氢钾复合盐3‑5份、防霉剂1‑2份,本发明对水体环境耐受性强,漂浮性、悬浮性以及沉浮可控性好,有利于海水养殖水体三维立体的净化效果,避免水体酸化和臭底,有效抑制病原微生物,提高海参养殖的产量和质量。The invention discloses a water purifying agent and a preparation method thereof, which is composed of the following formula components in parts by mass: 40-60 parts of deionized water, 8-10 parts of Bacillus subtilis, 2-4 parts of emulsifier, and Bacillus cereus 6‑8 parts, 7‑9 parts of Bacillus curvedus, 10‑20 parts of soybean meal powder, 30‑50 parts of seawater, 3‑5 parts of ivermectin, 5‑7 parts of magnesium carbonate, 6‑8 parts of sodium bicarbonate, 7-9 parts of sulfamic acid, 3-5 parts of potassium hydrogen persulfate compound salt, and 1-2 parts of antifungal agent. It is beneficial to the three-dimensional purification effect of the sea cucumber water body, avoids acidification and odor of the water body, effectively inhibits pathogenic microorganisms, and improves the yield and quality of sea cucumber culture.

Description

一种水质净化剂及其制备方法A kind of water purification agent and preparation method thereof

技术领域technical field

本发明涉及海产品养殖技术领域,具体而言涉及一种水质净化剂及其制备方法。The invention relates to the technical field of marine product cultivation, in particular to a water purifier and a preparation method thereof.

背景技术Background technique

海水是海参等海珍品赖以生存的基本环境条件,俗话说:“三分养鱼,七分养水”。水质的好坏直接影响到海参的生长状况和养殖户的经济效益。随着经济和科学的发展,人们对海参的需求日益增加,在天然捕捞不能满足市场需求的情况下,海参养殖业已由传统的粗放型经营、资源依赖型养殖方式转化为现在的集约化和工厂化的养殖方式,刺参养殖已成为中国水产养殖业的支柱产业之一。然而,随着刺参集约化和规模化养殖迅速的发展,出现了一些严重问题,制约了其产业的发展,比如残存饵料以及排泄物和动物死体在水体中沉积,分解生成很多的有害物质,恶化了水质,病原菌大量繁殖,致使海参产生强烈的应激反应,出现了摇头不食、口肿、身体收缩僵直、排脏、体表溃疡等现象,最后体壁大面积腐烂而死。为了对抗海参病疫,长期和大量滥用抗生素以及化学合成药物,不仅导致了海参对病原微生物的易感性以及细菌病原微生物等的耐药性,还会使抗生素检测超标,并造成整个生态环境的污染,严重影响了节约减排、食品安全和阻碍了无公害刺参养殖业的可持续发展。Seawater is the basic environmental condition for the survival of sea cucumbers and other sea treasures. As the saying goes: "Three points for fish, seven points for water". The quality of water quality directly affects the growth status of sea cucumbers and the economic benefits of farmers. With the development of economy and science, people's demand for sea cucumbers is increasing day by day. Under the circumstances that natural fishing cannot meet the market demand, the sea cucumber farming industry has transformed from the traditional extensive management and resource-dependent farming methods to the current intensive and factory farming methods. With the modernization of farming methods, sea cucumber farming has become one of the pillar industries of China's aquaculture industry. However, with the rapid development of intensive and large-scale cultivation of sea cucumber, some serious problems have appeared, which have restricted the development of its industry, such as the deposition of residual bait, excrement and animal dead bodies in the water body, decomposing and generating a lot of harmful substances, The water quality deteriorated, and pathogenic bacteria multiplied in large numbers, causing sea cucumbers to have a strong stress response, shaking their heads without eating, mouth swelling, body contraction and stiffness, viscera discharge, body surface ulcers, etc. Finally, a large area of the body wall rotted and died. In order to combat sea cucumber disease, the long-term and large-scale abuse of antibiotics and chemically synthesized drugs not only leads to the susceptibility of sea cucumbers to pathogenic microorganisms and the drug resistance of bacterial pathogenic microorganisms, but also causes the detection of antibiotics to exceed the standard and pollutes the entire ecological environment. It has seriously affected the conservation and emission reduction, food safety and hindered the sustainable development of the pollution-free sea cucumber breeding industry.

发明内容Contents of the invention

本发明提供了一种水质净化剂及其制备方法,本发明对水体环境耐受性强,漂浮性、悬浮性以及沉浮可控性好,有利于海水养殖水体三维立体的净化效果,避免水体酸化和臭底,有效抑制病原微生物,提高海参养殖的产量和质量。The invention provides a water quality purifying agent and a preparation method thereof. The invention has strong tolerance to the water body environment, good buoyancy, suspension and ups and downs controllability, is beneficial to the three-dimensional purification effect of the mariculture water body, and avoids acidification of the water body And smelly bottom, effectively inhibit pathogenic microorganisms, improve the yield and quality of sea cucumber culture.

为实现上述目的,本发明提供如下技术方案:To achieve the above object, the present invention provides the following technical solutions:

一种水质净化剂及其制备方法,由以下质量份数配方成分组成:去离子水40-60份、枯草芽孢杆菌8-10份、乳化剂2-4份、蜡状芽孢杆菌6-8份、弯曲芽孢杆菌7-9份、豆粕粉10-20份、海水30-50份、伊维菌素3-5份、碳酸镁5-7份、碳酸氢钠6-8份、氨基磺酸7-9份、过硫酸氢钾复合盐3-5份、防霉剂1-2份。A water purifier and a preparation method thereof, comprising the following ingredients in parts by mass: 40-60 parts of deionized water, 8-10 parts of Bacillus subtilis, 2-4 parts of emulsifier, and 6-8 parts of Bacillus cereus , 7-9 parts of Bacillus flexus, 10-20 parts of soybean meal powder, 30-50 parts of seawater, 3-5 parts of ivermectin, 5-7 parts of magnesium carbonate, 6-8 parts of sodium bicarbonate, 7 parts of sulfamic acid -9 parts, potassium hydrogen persulfate compound salt 3-5 parts, antifungal agent 1-2 parts.

进一步:由以下质量份数配方成分组成:去离子水40份、枯草芽孢杆菌8份、乳化剂2份、蜡状芽孢杆菌6份、弯曲芽孢杆菌7份、豆粕粉10份、海水30份、伊维菌素3份、碳酸镁5份、碳酸氢钠6份、氨基磺酸7份、过硫酸氢钾复合盐3份、防霉剂1份。Further: It consists of the following formula components in parts by mass: 40 parts of deionized water, 8 parts of Bacillus subtilis, 2 parts of emulsifier, 6 parts of Bacillus cereus, 7 parts of Bacillus flexus, 10 parts of soybean meal powder, 30 parts of seawater, 3 parts of ivermectin, 5 parts of magnesium carbonate, 6 parts of sodium bicarbonate, 7 parts of sulfamic acid, 3 parts of potassium persulfate compound salt, 1 part of antifungal agent.

进一步:由以下质量份数配方成分组成:去离子水50份、枯草芽孢杆菌9份、乳化剂3份、蜡状芽孢杆菌7份、弯曲芽孢杆菌8份、豆粕粉15份、海水40份、伊维菌素4份、碳酸镁6份、碳酸氢钠7份、氨基磺酸8份、过硫酸氢钾复合盐4份、防霉剂1.5份。Further: It consists of the following formula components in parts by mass: 50 parts of deionized water, 9 parts of Bacillus subtilis, 3 parts of emulsifier, 7 parts of Bacillus cereus, 8 parts of Bacillus flexus, 15 parts of soybean meal powder, 40 parts of seawater, 4 parts of ivermectin, 6 parts of magnesium carbonate, 7 parts of sodium bicarbonate, 8 parts of sulfamic acid, 4 parts of potassium persulfate compound salt, 1.5 parts of antifungal agent.

进一步:由以下质量份数配方成分组成:去离子水60份、枯草芽孢杆菌10份、乳化剂4份、蜡状芽孢杆菌8份、弯曲芽孢杆菌9份、豆粕粉20份、海水50份、伊维菌素5份、碳酸镁7份、碳酸氢钠8份、氨基磺酸9份、过硫酸氢钾复合盐5份、防霉剂2份。Further: It consists of the following formula components in parts by mass: 60 parts of deionized water, 10 parts of Bacillus subtilis, 4 parts of emulsifier, 8 parts of Bacillus cereus, 9 parts of Bacillus flexus, 20 parts of soybean meal powder, 50 parts of seawater, 5 parts of ivermectin, 7 parts of magnesium carbonate, 8 parts of sodium bicarbonate, 9 parts of sulfamic acid, 5 parts of potassium persulfate compound salt, 2 parts of antifungal agent.

进一步:本发明制备方法具有如下步骤:Further: the preparation method of the present invention has the following steps:

步骤一、将上述菌类分别加培养基,pH7.0~7.5,33~37℃震荡培养12~16h,再以1:1:1的体积比混合,制备成益生菌原液;Step 1. Add culture medium to the above-mentioned fungi respectively, pH 7.0-7.5, shake culture at 33-37°C for 12-16 hours, and then mix at a volume ratio of 1:1:1 to prepare a probiotic stock solution;

步骤二、将海水与去离子水进行混合加入除防霉剂和乳化剂的剩余原料进行混合;Step 2, seawater and deionized water are mixed, and the remaining raw materials for removing mildew and emulsifying agent are added for mixing;

步骤三、将步骤一所得与步骤二所得进行混合搅拌,在搅拌过程中加入防霉剂和乳化剂;Step 3, mixing and stirring the obtained step 1 and the obtained step 2, and adding antifungal agent and emulsifier during the stirring process;

步骤四、将步骤三进行过滤后装包冷藏既得成品。Step 4, after filtering step 3, pack and refrigerate to obtain the finished product.

本发明的有益效果是:The beneficial effects of the present invention are:

1、本发明对水体环境耐受性强,漂浮性、悬浮性以及沉浮可控性好;1. The present invention has strong tolerance to water environment, good buoyancy, suspension and controllability of ups and downs;

2、有利于海水养殖水体三维立体的净化效果,避免水体酸化和臭底;2. It is beneficial to the three-dimensional purification effect of the mariculture water body, avoiding the acidification of the water body and the smelly bottom;

3、有效抑制病原微生物,提高海参养殖的产量和质量。3. Effectively inhibit pathogenic microorganisms and improve the yield and quality of sea cucumber culture.

具体实施方式detailed description

下面将结合本发明实施例,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。The technical solutions in the embodiments of the present invention will be clearly and completely described below in conjunction with the embodiments of the present invention. Apparently, the described embodiments are only some of the embodiments of the present invention, not all of them. Based on the embodiments of the present invention, all other embodiments obtained by persons of ordinary skill in the art without making creative efforts belong to the protection scope of the present invention.

实施例一:Embodiment one:

一种水质净化剂由以下质量份数配方成分组成:去离子水40-60份、枯草芽孢杆菌8-10份、乳化剂2-4份、蜡状芽孢杆菌6-8份、弯曲芽孢杆菌7-9份、豆粕粉10-20份、海水30-50份、伊维菌素3-5份、碳酸镁5-7份、碳酸氢钠6-8份、氨基磺酸7-9份、过硫酸氢钾复合盐3-5份、防霉剂1-2份。A water purifier is composed of the following formula components in parts by mass: 40-60 parts of deionized water, 8-10 parts of Bacillus subtilis, 2-4 parts of emulsifier, 6-8 parts of Bacillus cereus, 7 parts of Bacillus flexus -9 parts, 10-20 parts of soybean meal powder, 30-50 parts of seawater, 3-5 parts of ivermectin, 5-7 parts of magnesium carbonate, 6-8 parts of sodium bicarbonate, 7-9 parts of sulfamic acid, over 3-5 parts of potassium bisulfate compound salt, 1-2 parts of fungicide.

实施例二:Embodiment two:

一种水质净化剂由以下质量份数配方成分组成:去离子水40份、枯草芽孢杆菌8份、乳化剂2份、蜡状芽孢杆菌6份、弯曲芽孢杆菌7份、豆粕粉10份、海水30份、伊维菌素3份、碳酸镁5份、碳酸氢钠6份、氨基磺酸7份、过硫酸氢钾复合盐3份、防霉剂1份。A water purifier is composed of the following formula components in parts by mass: 40 parts of deionized water, 8 parts of Bacillus subtilis, 2 parts of emulsifier, 6 parts of Bacillus cereus, 7 parts of Bacillus flexus, 10 parts of soybean meal powder, sea water 30 parts, 3 parts of ivermectin, 5 parts of magnesium carbonate, 6 parts of sodium bicarbonate, 7 parts of sulfamic acid, 3 parts of potassium persulfate compound salt, 1 part of antifungal agent.

实施例三:Embodiment three:

一种水质净化剂由以下质量份数配方成分组成:去离子水50份、枯草芽孢杆菌9份、乳化剂3份、蜡状芽孢杆菌7份、弯曲芽孢杆菌8份、豆粕粉15份、海水40份、伊维菌素4份、碳酸镁6份、碳酸氢钠7份、氨基磺酸8份、过硫酸氢钾复合盐4份、防霉剂1.5份。A water purifier consists of the following ingredients in parts by mass: 50 parts of deionized water, 9 parts of Bacillus subtilis, 3 parts of emulsifier, 7 parts of Bacillus cereus, 8 parts of Bacillus flexus, 15 parts of soybean meal powder, seawater 40 parts, 4 parts of ivermectin, 6 parts of magnesium carbonate, 7 parts of sodium bicarbonate, 8 parts of sulfamic acid, 4 parts of potassium persulfate compound salt, 1.5 parts of antifungal agent.

实施例四:Embodiment four:

一种水质净化剂由以下质量份数配方成分组成:去离子水60份、枯草芽孢杆菌10份、乳化剂4份、蜡状芽孢杆菌8份、弯曲芽孢杆菌9份、豆粕粉20份、海水50份、伊维菌素5份、碳酸镁7份、碳酸氢钠8份、氨基磺酸9份、过硫酸氢钾复合盐5份、防霉剂2份。A water purifier is composed of the following formula components in parts by mass: 60 parts of deionized water, 10 parts of Bacillus subtilis, 4 parts of emulsifier, 8 parts of Bacillus cereus, 9 parts of Bacillus flexus, 20 parts of soybean meal powder, sea water 50 parts, 5 parts of ivermectin, 7 parts of magnesium carbonate, 8 parts of sodium bicarbonate, 9 parts of sulfamic acid, 5 parts of potassium persulfate compound salt, 2 parts of antifungal agent.

实施例五:Embodiment five:

一种水质净化剂的制备方法制备方法包括如下步骤:A kind of preparation method of water purification agent The preparation method comprises the following steps:

步骤一、将上述菌类分别加培养基,pH7.0~7.5,33~37℃震荡培养12~16h,再以1:1:1的体积比混合,制备成益生菌原液;Step 1. Add culture medium to the above-mentioned fungi respectively, pH 7.0-7.5, shake culture at 33-37°C for 12-16 hours, and then mix at a volume ratio of 1:1:1 to prepare a probiotic stock solution;

步骤二、将海水与去离子水进行混合加入除防霉剂和乳化剂的剩余原料进行混合;Step 2, seawater and deionized water are mixed, and the remaining raw materials for removing mildew and emulsifying agent are added for mixing;

步骤三、将步骤一所得与步骤二所得进行混合搅拌,在搅拌过程中加入防霉剂和乳化剂;Step 3, mixing and stirring the obtained step 1 and the obtained step 2, and adding antifungal agent and emulsifier during the stirring process;

步骤四、将步骤三进行过滤后装包冷藏既得成品。Step 4, after filtering step 3, pack and refrigerate to obtain the finished product.

此外,应当理解,虽然本说明书按照实施方式加以描述,但并非每个实施方式仅包含一个独立的技术方案,说明书的这种叙述方式仅仅是为清楚起见,本领域技术人员应当将说明书作为一个整体,各实施例中的技术方案也可以经适当组合,形成本领域技术人员可以理解的其他实施方式。In addition, it should be understood that although this specification is described according to implementation modes, not each implementation mode only contains an independent technical solution, and this description in the specification is only for clarity, and those skilled in the art should take the specification as a whole , the technical solutions in the various embodiments can also be properly combined to form other implementations that can be understood by those skilled in the art.

Claims (5)

1. a kind of water quality cleansing agent, it is characterised in that:It is made up of following mass fraction formula components:
Deionized water 40-60 parts, bacillus subtilises 8-10 parts, emulsifying agent 2-4 parts, Bacillus cercuses 6-8 parts, bending spore Bacillus 7-9 parts, bean cake powder 10-20 parts, sea water 30-50 parts, ivermectin 3-5 parts, magnesium carbonate 5-7 parts, sodium bicarbonate 6-8 parts, Sulfamic acid 7-9 parts, ammonium persulfate-sodium bisulfate 3-5 parts, antifungus agent 1-2 parts.
2. a kind of water quality cleansing agent according to claim 1, it is characterised in that:By following mass fraction formula components group Into:
40 parts of deionized water, 8 parts of bacillus subtilises, 2 parts of emulsifying agent, 6 parts of Bacillus cercuses, 7 parts of Bacillus flexus, bean 10 parts of dregs of rice powder, 30 parts of sea water, 3 parts of ivermectin, 5 parts of magnesium carbonate, 6 parts of sodium bicarbonate, 7 parts of sulfamic acid, potassium hydrogen persulfate are multiple Close 3 parts of salt, 1 part of antifungus agent.
3. a kind of water quality cleansing agent according to claim 1, it is characterised in that:By following mass fraction formula components group Into:
50 parts of deionized water, 9 parts of bacillus subtilises, 3 parts of emulsifying agent, 7 parts of Bacillus cercuses, 8 parts of Bacillus flexus, bean 15 parts of dregs of rice powder, 40 parts of sea water, 4 parts of ivermectin, 6 parts of magnesium carbonate, 7 parts of sodium bicarbonate, 8 parts of sulfamic acid, potassium hydrogen persulfate are multiple Close 4 parts of salt, 1.5 parts of antifungus agent.
4. a kind of water quality cleansing agent according to claim 1, it is characterised in that:By following mass fraction formula components group Into:
60 parts of deionized water, 10 parts of bacillus subtilises, 4 parts of emulsifying agent, 8 parts of Bacillus cercuses, 9 parts of Bacillus flexus, 20 parts of bean cake powder, 50 parts of sea water, 5 parts of ivermectin, 7 parts of magnesium carbonate, 8 parts of sodium bicarbonate, 9 parts of sulfamic acid, potassium hydrogen persulfate 5 parts of complex salt, 2 parts of antifungus agent.
5. a kind of a kind of preparation method of water quality cleansing agent according to claim 1, it is characterised in that:Including following step Suddenly:
Step one, above-mentioned mushroom is added respectively culture medium, pH7.0~7.5,33~37 DEG C of 12~16h of concussion and cultivate, then with 1:1: 1 volume ratio mixing, is prepared into probiotic bacteria stock solution;
Step 2, sea water and deionized water are carried out mixing add except the surplus stock of antifungus agent and emulsifying agent is mixed;
Step 3, step one gained be mixed with step 2 gained, the addition antifungus agent and emulsifying in whipping process Agent;
Step 4, step 3 is filtered after fill bag cold preservation both finished product.
CN201611134855.9A 2016-12-11 2016-12-11 Water quality purifying agent and preparation method thereof Pending CN106587371A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117736938A (en) * 2024-02-07 2024-03-22 南京万瑞环境科技有限公司 A kind of microbial composite flora and its application

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